An acrylic acid washing device for acrylic acid production

By using technical means such as driving motors, vibrators and hydraulic rods in the acrylic washing device, uniform distribution of quartz sand and automatic loading and unloading are achieved, the problem of uneven distribution of filter media is solved, and the filtration effect and sealing are improved.

CN118718675BActive Publication Date: 2024-12-17ZIBO XINGLU CHEM CO LTD
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Patent Information

Application Number
CN202411191244.2
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-08-28
Publication Date
2024-12-17
Estimated Expiration
2044-08-28

AI Technical Summary

Technical Problem

When the existing acrylic washing device puts the filter media, the medium is prone to concentrate near the filler port, resulting in local accumulation and uneven distribution of the filter media, affecting the filtration effect.

Method used

An acrylic washing device including washing components and sealing components was designed. The driving motor drives the push claw rake to evenly distribute the quartz sand, the vibrator realizes automatic loading, the electric push rod realizes automatic loading, and improves sealing through the hydraulic rod. , ensure uniform distribution and sealing of the filter media.

Benefits of technology

The uniform loading and unloading of quartz sand is achieved, the filtration effect is improved, manual operation is reduced, the loading efficiency is improved, and the sealing of the scrubber is enhanced to prevent acrylic gas leakage.

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Abstract

The invention discloses an acrylic acid washing device for acrylic acid production, and relates to the technical field of acrylic acid processing, including a washing component and a sealing component. When the invention is used, a driving motor is started to drive a rotating rod and a plurality of flattening claw rakes to rotate, and the quartz sand filter medium put in at multiple positions is moved to make it evenly distributed inside the conical filter frame, and at the same time, the push plate is rotated to flatten the topmost quartz sand to make it evenly distributed, so as to achieve the effect of uniform feeding, prevent the filter medium from being locally accumulated, and help improve the filtering effect. After being cooled, the acrylic acid gas enters the scrubber through the air inlet pipe and flows upward, and the high-pressure liquid pump is started in advance, and the washing absorption liquid is transported to the infusion pipe through the connecting pipe, and then enters the sprayer for atomization and spraying, and forms a countercurrent contact with the acrylic acid gas to form acrylic acid liquid, and then passes through the filter medium to separate impurities.
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Description

Technical Field

[0001] The invention relates to the technical field of acrylic acid processing, in particular to an acrylic acid washing device used for acrylic acid production. Background Art

[0002] Acrylic acid is an important organic compound and the simplest unsaturated carboxylic acid. It is mainly used to produce polymers, coatings, adhesives, dyes and many other chemicals. Currently, it constitutes a unique acrylic acid industry in the modern chemical industry. It is an important derivative of propylene like polypropylene, acrylonitrile and propylene oxide. Acrylic acid has excellent polymerization and esterification capabilities, providing an extremely important intermediate for the synthesis and preparation of various fine chemicals.

[0003] In the prior art, for example, Chinese patent publication number: CN213221579U discloses an acrylic acid washing device in acrylic acid production, comprising: a washing tank, a controller, a cooling assembly, an air inlet pipe, a spray assembly, a spray pipe, a liquid discharge pipe and an exhaust pipe. The controller is used to control the operation of the washing device; the cooling assembly is respectively connected to the acrylic acid production equipment and the washing tank, and is used to cool the high-temperature acrylic acid gas; the air inlet pipe is used to transport the cooled acrylic acid gas into the washing tank; the spray assembly is used to spray the washing absorption liquid into the washing tank; the spray pipe, the first end of which is connected to the spray assembly, and the second end of which is connected to the material box containing the washing absorption liquid; the liquid discharge pipe is used to discharge the washed acrylic acid liquid out of the washing tank; the exhaust pipe is used to discharge the waste gas generated in the washing tank.

[0004] In the prior art, in the process of converting acrylic acid gas into acrylic acid liquid through a washing device after cooling treatment, in order to improve the quality of the acrylic acid liquid, a filter plate is provided in the washing device, and a quartz sand filter medium is added to the filter plate through a filling port on the washing device. However, in the process of adding the quartz sand, the quartz sand tends to concentrate near the filling port and fall, causing the filter medium to concentrate in a certain area and cause local accumulation, thereby causing uneven distribution of the filter medium inside the washing device, which easily causes part of the quartz sand filter medium to be oversaturated, while other parts are not fully used, affecting the overall filtering effect.

[0005] Therefore, we propose an acrylic acid washing device for acrylic acid production to solve the problems raised in the above background technology. Summary of the invention

[0006] The object of the present invention is to provide an acrylic acid washing device for acrylic acid production, so as to solve the problem that in the acrylic acid washing device proposed in the above background technology, during the process of adding filter media, the filter media is easy to fall near the filling port, resulting in local accumulation, resulting in uneven distribution of the filter media inside the washing device, and it is easy for some filter media to be over-saturated while other parts are not fully used, affecting the overall filtering effect.

[0007] To achieve the above object, the present invention provides the following technical solution: an acrylic acid washing device for acrylic acid production, comprising a washing component and a sealing component, wherein the washing component is used to wash acrylic acid gas, the sealing component is used to provide a sealing effect, a uniform component is arranged inside the washing component, and a loading and unloading component is arranged on the outer surface of the washing component, the uniform component is used to flatten the quartz sand filter medium put in, and the loading and unloading component is used to realize automatic input and automatic discharge of the quartz sand filter medium;

[0008] The washing assembly comprises a washer, a bottom cover of which is installed at the bottom by bolts, and a plurality of feeding ports are provided on the outer surface of the washer;

[0009] The uniform component includes a conical filter frame, a protective cover is fixedly installed on the bottom of the conical filter frame, a driving motor is fixedly installed on the bottom surface inside the protective cover, a rotating rod is fixedly installed on the output end of the driving motor, a movable sleeve on the outer surface of the rotating rod is provided with a pointed sleeve, a plurality of leveling claw rakes are fixedly installed on the outer surface of the rotating rod, a material unloading claw rake is fixedly installed on the outer surface of the rotating rod near the pointed sleeve, and a pushing plate is fixedly installed on the outer surface of the rotating rod near the top.

[0010] Preferably, the outer surface of the conical filter frame is fixedly mounted on the inner wall of the scrubber near the feeding port near the top, the bottom of the pointed sleeve is fixedly mounted on the bottom surface inside the conical filter frame, the inner wall of the pointed sleeve is in contact with the outer surface of the rotating rod near the top, and the top end of the rotating rod moves through the interior of the conical filter frame.

[0011] Preferably, the sealing assembly includes a connecting plate, a hydraulic rod is fixedly installed on the bottom of the connecting plate, a bellows is arranged on the outer surface of the hydraulic rod, a moving block is fixedly installed on the bottom end of the hydraulic rod, a plurality of fixed rods are fixedly installed on the outer surface of the moving block, an annular sealing plate is fixedly installed on one end of the plurality of fixed rods, a sealing ring is fixedly connected to the outer surface of the annular sealing plate, the outer surface of the sealing ring is in contact with the inner wall of the washer, the outer surfaces of both sides of the connecting plate are fixedly installed on the inner wall of the washer, the top of the bellows is fixedly installed on the bottom of the connecting plate, and the bottom of the bellows is fixedly installed on the top of the moving block.

[0012] Preferably, the loading and unloading assembly includes a loading rack, a PLC controller is arranged on the top of the loading rack, a vibration groove is opened inside the loading rack, a plurality of loading boxes are movably embedded inside the vibration groove, the tops of the plurality of loading boxes are fixedly connected with elastic pads, a plurality of loading pipes are arranged on the top of the loading rack, the bottom ends of the plurality of loading pipes are fixedly passed through the loading rack to the inside of the vibration groove, the bottom ends of the plurality of loading pipes are movably passed through the plurality of elastic pads to the inside of the plurality of loading boxes, and the bottoms of the plurality of loading boxes are fixedly connected with four vibration springs.

[0013] Preferably, one ends of the plurality of vibration springs are fixedly mounted on the bottom surface inside the vibration groove, two vibration rods are fixedly mounted on the bottom of the plurality of feeding boxes, the bottom ends of the plurality of vibration rods are movably extended to the bottom of the feeding rack, vibration plates are installed on the bottom ends of the plurality of vibration rods by bolts, a vibrator is arranged near the center of the top of the vibration plate, the inner wall of the feeding rack is provided with a plurality of movable holes, the top and bottom surfaces inside the plurality of movable holes are fixedly connected with elastic strips, and feeding pipes are movably embedded inside the plurality of movable holes.

[0014] Preferably, one ends of the multiple feeding pipes are fixedly connected to the outer surfaces of the multiple feeding boxes, and the other ends of the multiple feeding pipes are movably embedded in the inside of the feeding ports. A threaded hole is provided at the bottom of the bottom cover, and a sealing hole is provided at the bottom of the bottom cover near the threaded hole. A feeding pipe is fixedly connected to the bottom of the conical filter frame near the protective cover.

[0015] Preferably, the outer surface of the feed pipe is fixedly connected to a discharge pipe, the outer surface of the discharge pipe is fixedly connected to a sealing sleeve, the outer surface of the sealing sleeve is in contact with the inner wall of the sealing hole, the bottom threaded sleeve of the feed pipe is provided with a threaded cover, the outer surface of the threaded cover is threadedly connected to the inner wall of the threaded hole, and a fixing block is fixedly installed on the bottom surface of the threaded cover.

[0016] Preferably, an electric push rod is fixedly installed on the top of the fixed block, and an inclined guide block is fixedly installed on the top of the electric push rod. The outer surface of the inclined guide block is movably embedded in the inside of the discharge pipe. The outer surface of the fixed block and the outer surface of the electric push rod are both located inside the discharge pipe. A plurality of supporting legs are fixedly installed on the outer surface of the loading rack, and the outer surface of the washer is fixedly installed inside the loading rack.

[0017] Preferably, a top cover is installed on the top of the scrubber by bolts, an exhaust pipe is fixedly connected to the top of the top cover, a sprayer is fixedly installed inside the scrubber, an input end of the sprayer is fixedly penetrated to the outer surface of the scrubber, a high-pressure liquid pump is arranged on the outer surface of the scrubber, and an air intake pipe is arranged on the outer surface of the scrubber.

[0018] Preferably, the output end of the high-pressure liquid pump is connected to an infusion tube via a flange, one end of the infusion tube is connected to the input end of the sprayer via a flange, a sealing ring is fixedly connected to the top of the bottom cover near the edge, the outer surface of the sealing ring fits with the inner wall of the scrubber near the bottom, and a drain pipe is fixedly connected to the bottom of the bottom cover.

[0019] Compared with the prior art, the present invention has the following beneficial effects:

[0020] 1. When the present invention is used, the driving motor is started to drive the rotating rod and a plurality of leveling claws to rotate, and the quartz sand filter medium inserted at multiple points is moved to make it evenly distributed inside the conical filter frame. At the same time, the push plate is rotated to level the quartz sand on the top to make it evenly distributed, thereby achieving the effect of uniform feeding and preventing the filter medium from being locally accumulated, which is beneficial to improving the filtering effect. After being cooled, the acrylic acid gas enters the scrubber through the air inlet pipe and flows upward. The high-pressure liquid pump is started in advance, and the washing absorption liquid is transported to the infusion pipe through the connecting pipe, and then enters the sprayer for atomization and spraying, forming a countercurrent contact with the acrylic acid gas rising from the bottom to form acrylic acid liquid. Then the acrylic acid liquid passes through the filter medium to separate the internal impurities.

[0021] 2. When the present invention is used, the vibrator is started to drive the vibration plate and the vibration rod to vibrate. Under the elastic support of the vibration spring, the feeding box is driven to vibrate up and down, and the top of the feeding box is protected by the elastic pad. At the same time, the feeding pipe is driven to vibrate inside the movable hole and the feeding port. The feeding pipe is protected by the elastic strip, so that the filter medium inside the feeding box enters the feeding port through the feeding pipe, then enters the scrubber, and finally falls into the conical filter frame, thereby achieving the effect of automatic feeding, without the need for manual filling bit by bit, reducing workload and time, and improving feeding efficiency. By equidistantly arranging multiple feeding ports and feeding boxes, the entry position of the quartz sand filter medium can be dispersed, which is conducive to the quartz sand being evenly scattered into the conical filter frame from different directions, thereby assisting in improving the feeding uniformity.

[0022] 3. When the present invention is used, the electric push rod is started to pull the inclined guide block to move downward, so that an inclined channel is formed between the discharge pipe and the inside of the discharge pipe. At this time, the filter medium enters the discharge pipe and slides along the inclined surface of the inclined guide block to the inside of the discharge pipe, thereby discharging the filter medium, thereby achieving the effect of automatic discharge. The driving motor is started again to make the rotating rod drive the discharge claw rake to rotate together, which is conducive to pushing the filter medium on the bottom surface of the inner bottom of the conical filter frame to the discharge pipe for discharge. The threaded cover is unscrewed, the fixed block and the electric push rod are pulled out of the discharge pipe, and the inclined guide block is further taken out of the discharge pipe, so as to facilitate the grinding of the inclined surface of the inclined guide block to make its inclined surface smoother, which is conducive to discharging the filter medium into the discharge pipe and preventing the inclined surface of the inclined guide block from being worn and affecting the smoothness.

[0023] 4. When the present invention is used, the hydraulic rod is started to push the moving block and the fixed rod downward, and the annular sealing plate is further pushed downward, so that the sealing ring moves downward along the inner wall of the scrubber. When the bottom of the annular sealing plate contacts the top of the conical filter frame, the sealing ring just seals the multiple feeding ports, thereby improving the sealing performance of the scrubber and preventing part of the acrylic acid gas from accidentally leaking out from the feeding port when the scrubbing assembly is working. BRIEF DESCRIPTION OF THE DRAWINGS

[0024] Figure 1 It is a front perspective view of an acrylic acid washing device for acrylic acid production of the present invention;

[0025] Figure 2 It is a structural sectional expanded stereoscopic diagram of an acrylic acid washing device for acrylic acid production of the present invention;

[0026] Figure 3 It is a structural cross-sectional expanded stereoscopic diagram of a washing component in an acrylic acid washing device for acrylic acid production according to the present invention;

[0027] Figure 4 It is a structural sectional expanded stereoscopic diagram of a sealing component in an acrylic acid washing device for acrylic acid production according to the present invention;

[0028] Figure 5 It is a structural cross-sectional expanded stereoscopic diagram of a uniform component in an acrylic acid washing device for acrylic acid production according to the present invention;

[0029] Figure 6 It is a structural cross-sectional expanded stereoscopic diagram of a discharge pipe in an acrylic acid washing device for acrylic acid production according to the present invention;

[0030] Figure 7 It is a perspective view of the structure of the upper and lower material components in an acrylic acid washing device for acrylic acid production according to the present invention;

[0031] Figure 8 It is a structural sectional expanded stereoscopic diagram of a loading rack in an acrylic acid washing device for acrylic acid production according to the present invention;

[0032] Fig. 9 It is a structural cross-sectional expanded stereoscopic diagram of a loading box in an acrylic acid washing device for acrylic acid production according to the present invention;

[0033] Fig.10 The present invention is a structural sectional and expanded stereoscopic diagram of a feeding pipe in an acrylic acid washing device used for acrylic acid production.

[0034] In the figure:

[0035] 1. Washing assembly; 101. Washer; 102. Top cover; 103. Exhaust pipe; 104. High-pressure liquid pump; 105. Infusion pipe; 106. Bottom cover; 107. Inlet pipe; 108. Sprayer; 109. Discharge pipe; 110. Feeding port; 111. Sealing hole; 112. Threaded hole; 113. Sealing ring; 2. Loading and unloading assembly; 201. Loading rack; 202. Support leg; 203. Vibrating plate; 204. Vibrating machine; 205. Loading box; 206. Loading pipe; 207. Vibrating rod; 208. Elastic pad; 209. Vibrating spring; 210. Feeding pipe; 211. Elastic strip; 212. Movable hole ; 213, feed pipe; 214, discharge pipe; 215, sealing sleeve; 216, threaded cover; 217, inclined guide block; 218, electric push rod; 219, fixed block; 220, vibration trough; 3, uniform component; 301, conical filter frame; 302, protective cover; 303, drive motor; 304, pointed sleeve; 305, rotating rod; 306, push plate; 307, push claw rake; 308, feed claw rake; 4, sealing component; 401, connecting plate; 402, bellows; 403, annular sealing plate; 404, sealing ring; 405, hydraulic rod; 406, moving block; 407, fixed rod; 5, PLC controller. DETAILED DESCRIPTION

[0036] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the implementation regulations described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0037] Example 1: Please refer to Figure 1-Figure 10As shown, the present invention provides a technical solution: an acrylic acid washing device for acrylic acid production, comprising a washing component 1 and a sealing component 4, wherein the washing component 1 is used to wash acrylic acid gas, the sealing component 4 is used to provide a sealing effect, a uniform component 3 is arranged inside the washing component 1, and a loading and unloading component 2 is arranged on the outer surface of the washing component 1, the uniform component 3 is used to flatten the quartz sand filter medium put in, and the loading and unloading component 2 is used to realize automatic input and automatic discharge of the quartz sand filter medium; the washing component 1 comprises a scrubber 101, and the bottom of the scrubber 101 is installed with a bottom screw through bolts. The cover 106, the outer surface of the scrubber 101 is provided with a plurality of feeding ports 110; the uniform component 3 includes a conical filter frame 301, a protective cover 302 is fixedly installed at the bottom of the conical filter frame 301, a driving motor 303 is fixedly installed on the bottom surface of the inner part of the protective cover 302, a rotating rod 305 is fixedly installed at the output end of the driving motor 303, a pointed cover 304 is movably provided on the outer surface of the rotating rod 305, a plurality of leveling claw rakes 307 are fixedly installed on the outer surface of the rotating rod 305, a material unloading claw rake 308 is fixedly installed on the outer surface of the rotating rod 305 near the pointed cover 304, and the outer surface of the rotating rod 305 A push plate 306 is fixedly installed near the top, the outer surface of the conical filter frame 301 is fixedly installed near the top on the inner wall of the scrubber 101 near the feeding port 110, the bottom of the pointed sleeve 304 is fixedly installed on the bottom surface inside the conical filter frame 301, the inner wall of the pointed sleeve 304 is in contact with the outer surface of the rotating rod 305 near the top, the top of the rotating rod 305 is movable and penetrates into the inside of the conical filter frame 301, the top of the scrubber 101 is fixedly installed with a top cover 102 by bolts, the top of the top cover 102 is fixedly connected with an exhaust pipe 103, and the inside of the scrubber 101 is fixedly installed with a sprayer 108, the input end of the sprayer 108 is fixedly connected to the outer surface of the scrubber 101, the outer surface of the scrubber 101 is provided with a high-pressure liquid pump 104, the outer surface of the scrubber 101 is provided with an air inlet pipe 107, the output end of the high-pressure liquid pump 104 is connected with a liquid infusion pipe 105 through a flange, one end of the liquid infusion pipe 105 is connected with the input end of the sprayer 108 through a flange, a sealing ring 113 is fixedly connected to the top of the bottom cover 106 near the edge, the outer surface of the sealing ring 113 is in contact with the inner wall of the scrubber 101 near the bottom, and a drain pipe 109 is fixedly connected to the bottom of the bottom cover 106.

[0038] In this embodiment, when in use, the high-pressure liquid pump 104, the vibrator 204, the electric push rod 218, the drive motor 303, the hydraulic rod 405 and the PLC controller 5 are electrically connected. When the quartz sand filter medium is put into the scrubber 101 at multiple points through the upper and lower material assembly 2, the drive motor 303 is started, and the rotation of the output end of the drive motor 303 drives the rotating rod 305 to rotate, and further drives the multiple leveling claw rakes 307 to rotate. The multiple leveling claw rakes 307 rotate, and the quartz sand filter medium put into the conical filter frame 301 at multiple points is further moved to make it evenly distributed inside the conical filter frame 301. When the upper and lower material assembly 2 is used, the drive motor 303 is started, and the rotating rod 305 is driven to rotate by the rotation of the output end of the drive motor 303, and the multiple leveling claw rakes 307 are driven to rotate. After the material assembly 2 completes the loading, the quartz sand in the conical filter frame 301 is at the bottom of the push plate 306. The quartz sand is evenly moved by a plurality of push claw rakes 307. At the same time, the push plate 306 pushes the quartz sand on the top to make the top quartz sand evenly distributed, thereby achieving the effect of uniform loading and preventing the filter medium from being locally accumulated, which is beneficial to improving the filtering effect. The tip of the pointed sleeve 304 contacts the outer surface of the rotating rod 305. Under the action of the pointed sleeve 304, smaller filter media are prevented from falling onto the drive motor 303 through the gap between the rotating rod 305 and the conical filter frame 301, affecting The normal operation of the driving motor 303 is solved, and the problem that the filter medium is easily concentrated near the filling port and falls during the process of putting the filter medium in the acrylic acid washing device, resulting in local accumulation, resulting in uneven distribution of the filter medium inside the washing device, and it is easy for some filter media to be over-saturated while other parts are not fully used, affecting the overall filtering effect. After cooling, the acrylic acid gas enters the scrubber 101 through the air inlet pipe 107 and flows upward, starting the high-pressure liquid pump 104 in advance. The input end of the high-pressure liquid pump 104 is connected to the washing absorption liquid storage tank through a connecting pipe. Under the action of the high-pressure liquid pump 104 The washing absorption liquid is transported to the infusion pipe 105 and then enters the sprayer 108. The sprayer 108 is composed of a shunt pipe, a ring pipe and a nozzle. The washing absorption liquid is sprayed downward in an atomized manner to form a countercurrent contact with the acrylic acid gas rising from the bottom. In this process, the acrylic acid gas is absorbed by the absorbent and becomes acrylic acid liquid. Then the acrylic acid liquid is filtered through a quartz sand filter medium to separate the internal impurities. The filtered acrylic acid liquid falls onto the bottom cover 106 and is discharged through the drain pipe 109. The sealing between the scrubber 101 and the bottom cover 106 is increased by the sealing ring 113 to prevent liquid leakage.

[0039] Embodiment 2: Figure 1-Figure 2 and Figure 4-Figure 10As shown, a uniform component 3 is arranged inside the washing component 1, and a loading and unloading component 2 is arranged on the outer surface of the washing component 1. The uniform component 3 is used to flatten the quartz sand filter medium put in, and the loading and unloading component 2 is used to realize automatic input and automatic discharge of the quartz sand filter medium. The loading and unloading component 2 includes a loading rack 201, and a PLC controller 5 is arranged on the top of the loading rack 201. A vibration groove 220 is opened inside the loading rack 201, and a plurality of loading boxes 205 are movably embedded inside the vibration groove 220. The tops of the plurality of loading boxes 205 are fixedly connected with elastic pads 208. A plurality of loading pipes 206 are arranged on the top of the loading rack 201, and the bottom ends of the plurality of loading pipes 206 are fixedly penetrated from the loading rack 201 to the vibration groove 220. 20, the bottom ends of the multiple feeding tubes 206 are respectively movable through the multiple elastic pads 208 to the inside of the multiple feeding boxes 205, the bottoms of the multiple feeding boxes 205 are fixedly connected with four vibration springs 209, one end of the multiple vibration springs 209 is fixedly installed on the bottom surface of the vibration groove 220, the bottoms of the multiple feeding boxes 205 are fixedly installed with two vibration rods 207, the bottom ends of the multiple vibration rods 207 are movable through the bottom of the feeding rack 201, the bottom ends of the multiple vibration rods 207 are bolted with vibration plates 203, the top of the vibration plate 203 is near the center. A vibrator 204 is set, and the inner wall of the feeding rack 201 is provided with a plurality of movable holes 212. The top and bottom surfaces are fixedly connected with elastic strips 211, and the interiors of the multiple movable holes 212 are movably embedded with feeding pipes 210, one ends of the multiple feeding pipes 210 are respectively fixedly connected to the outer surfaces of the multiple loading boxes 205, and the other ends of the multiple feeding pipes 210 are respectively movably embedded in the interiors of the feeding ports 110, a threaded hole 112 is provided at the bottom of the bottom cover 106, and a sealing hole 111 is provided at the bottom of the bottom cover 106 near the threaded hole 112, and a lowering pipe 213 is fixedly connected to the bottom of the conical filter frame 301 near the protective cover 302, and a discharge pipe 214 is fixedly connected to the outer surface of the discharge pipe 214, and a sealing sleeve 215 is fixedly connected to the outer surface of the discharge pipe 214, and the outer surface of the sealing sleeve 215 is fixedly connected to the outer surface of the sealing sleeve 215. The inner wall of the sealing hole 111 is in contact with each other, and a threaded cover 216 is provided on the bottom threaded sleeve of the discharge pipe 213. The outer surface of the threaded cover 216 is threadedly connected to the inner wall of the threaded hole 112. A fixed block 219 is fixedly installed on the bottom surface of the threaded cover 216, and an electric push rod 218 is fixedly installed on the top of the fixed block 219. An inclined guide block 217 is fixedly installed on the top of the electric push rod 218. The outer surface of the inclined guide block 217 is movably embedded in the interior of the discharge pipe 213. The outer surface of the fixed block 219 and the outer surface of the electric push rod 218 are both located in the interior of the discharge pipe 213. A plurality of supporting legs 202 are fixedly installed on the outer surface of the loading rack 201, and the outer surface of the scrubber 101 is fixedly installed inside the loading rack 201.

[0040] In this embodiment, when in use, five feeding ports 110, feeding pipes 206, feeding boxes 205 and feeding pipes 210 are provided, which are distributed along the circumference of the scrubber 101. The feeding pipe 210 is embedded in the movable hole 212 and does not contact the two elastic strips 211. The tops of the feeding boxes 205 and the elastic pads 208 are provided with relatively large circular holes. The bottom end of the feeding pipe 206 is embedded in the circular hole and does not contact the feeding boxes 205 and the elastic pads 208. The staff pours the same amount of quartz sand filter medium into the five feeding boxes 205 through the five feeding pipes 206 in advance, starts the vibrator 204, drives the vibration plate 203 to vibrate, and drives the multiple vibration rods 207 to vibrate. Under the elastic support of the vibration springs 209, the five feeding boxes 2 05 vibrates up and down inside the vibration trough 220, and the top of the loading box 205 is protected by the elastic pad 208 to prevent the top of the loading box 205 from accidentally colliding with the top surface inside the vibration trough 220 and causing wear, and at the same time drives the five feeding pipes 210 to vibrate inside the movable hole 212 and the feeding port 110. Under the protection of the elastic strip 211, the feeding pipe 210 is prevented from accidentally colliding with the top and bottom surfaces inside the movable hole 212. Under the vibration of the loading box 205, the quartz sand filter medium inside the loading box 205 enters the feeding port 110 through the feeding pipe 210, and enters the inside of the scrubber 101 along the inclined surface inside the feeding port 110, and finally falls into the inside of the conical filter frame 301, thereby achieving the effect of automatic feeding, without the need for Manually filling little by little can reduce workload and time and improve feeding efficiency. By equidistantly setting multiple feeding ports 110 and feeding boxes 205, the entry position of the quartz sand filter medium can be dispersed, which is conducive to the uniform scattering of quartz sand into the conical filter frame 301 from different directions, and assists in improving the uniformity of feeding. When the filter medium needs to be replaced, the electric push rod 218 is started to pull the inclined guide block 217 to move downward in the discharge pipe 213. When the electric push rod 218 is automatically closed, the inclined guide block 217 just moves to the intersection of the discharge pipe 214 and the discharge pipe 213. At this time, the lowest point of the inclined surface of the inclined guide block 217 is flush with the lowest point of the feed port of the discharge pipe 214. Under the action of the inclined guide block 217, the discharge pipe 213 and the discharge pipe 214 are connected. 214 forms an inclined channel, at this time, the filter medium in the conical filter frame 301 enters the discharge pipe 213, and slides along the inclined surface of the inclined guide block 217 to the inside of the discharge pipe 214, so as to discharge the filter medium, thereby achieving the effect of automatic discharge, and through the cooperation of the sealing sleeve 215 and the sealing hole 111, the sealing performance between the discharge pipe 214 and the sealing hole 111 is improved to prevent accidental leakage of acrylic acid liquid. During the discharge process, the driving motor 303 is started again, so that the rotating rod 305 drives the discharge claw rake 308 to rotate together, which is conducive to pushing the filter medium on the bottom surface of the inner side of the conical filter frame 301 to the discharge pipe 213 for discharge, thereby reducing the residue of the filter medium in the conical filter frame 301, and by rotating the threaded cover 216,Unscrew it from the inside of the threaded hole 112 and the outer surface of the discharge pipe 213, then pull the threaded cover 216 outward, extract the fixing block 219 and the electric push rod 218 from the discharge pipe 213, and further remove the inclined guide block 217 from the discharge pipe 213, so as to facilitate the grinding of the inclined surface of the inclined guide block 217 to make it smoother, which is conducive to discharging the filter medium into the discharge pipe 214 and prevent the inclined surface of the inclined guide block 217 from being worn and affecting the smoothness.

[0041] Embodiment 3: Figure 1-Figure 5 As shown, the washing component 1 includes a washer 101, a bottom cover 106 is installed at the bottom of the washer 101 by bolts, a plurality of feeding ports 110 are opened on the outer surface of the washer 101, and a sealing component 4 includes a connecting plate 401, a hydraulic rod 405 is fixedly installed at the bottom of the connecting plate 401, a bellows 402 is arranged on the outer surface of the hydraulic rod 405, a moving block 406 is fixedly installed at the bottom end of the hydraulic rod 405, a plurality of fixed rods 407 are fixedly installed on the outer surface of the moving block 406, an annular sealing plate 403 is fixedly installed at one end of the plurality of fixed rods 407, a sealing ring 404 is fixedly connected to the outer surface of the annular sealing plate 403, an outer surface of the sealing ring 404 is in contact with the inner wall of the washer 101, outer surfaces of both sides of the connecting plate 401 are fixedly installed on the inner wall of the washer 101, the top of the bellows 402 is fixedly installed on the bottom of the connecting plate 401, and the bottom of the bellows 402 is fixedly installed on the top of the moving block 406.

[0042] In this embodiment, when in use, after the quartz sand medium is evenly loaded through the loading and unloading assembly 2 and the uniform assembly 3, the hydraulic rod 405 is started to push the moving block 406 and the fixed rod 407 to move downward, and further push the annular sealing plate 403 to move downward along the inner wall of the scrubber 101, so that the sealing ring 404 moves downward along the inner wall of the scrubber 101. When the bottom of the annular sealing plate 403 contacts the top of the conical filter frame 301, the sealing ring 404 just seals the multiple feeding ports 110, thereby improving the sealing performance of the scrubber 101 and preventing part of the acrylic acid gas from accidentally leaking out from the feeding port 110 when the scrubbing assembly 1 is working.

[0043] The effect and working principle of the whole mechanism are as follows: the high-pressure liquid pump 104, the vibrator 204, the electric push rod 218, the drive motor 303, the hydraulic rod 405 and the PLC controller 5 are electrically connected, the vibrator 204 is started, the vibration plate 203 and the vibration rod 207 are driven to vibrate, and under the elastic support of the vibration spring 209, the five feeding boxes 205 are driven to vibrate up and down inside the vibration groove 220, and the top of the feeding box 205 is protected by the elastic pad 208, and at the same time, the five feeding pipes 210 are driven to vibrate inside the movable hole 212 and the feeding port 110, so that the quartz sand filter medium inside the feeding box 205 enters the feeding port 110 through the feeding pipe 210, and enters the scrubber along the inclined surface inside the feeding port 110 101, and finally falls into the conical filter frame 301, and the driving motor 303 is started to drive the rotating rod 305 and multiple leveling claws and rakes 307 to rotate. Through the rotation of multiple leveling claws and rakes 307, the quartz sand filter medium put into the conical filter frame 301 at multiple points is further moved to make it evenly distributed inside the conical filter frame 301. After the loading is completed, the quartz sand in the conical filter frame 301 is located at the bottom of the pushing plate 306. The quartz sand is evenly moved by multiple leveling claws and rakes 307, and the pushing plate 306 flattens the quartz sand on the top, so that the top quartz sand is evenly distributed, so as to achieve the effect of uniform loading, and the hydraulic rod 405 is started to push the moving block 406 and the fixed rod 407 to move downward, further pushing the annular The sealing plate 403 moves downward along the inner wall of the scrubber 101, so that the sealing ring 404 moves downward along the inner wall of the scrubber 101. When the bottom of the annular sealing plate 403 contacts the top of the conical filter frame 301, the sealing ring 404 just seals the multiple feeding ports 110. The acrylic acid gas enters the scrubber 101 through the air inlet pipe 107 after cooling and flows upward. The high-pressure liquid pump 104 is started in advance. The input end of the high-pressure liquid pump 104 is connected to the washing absorption liquid storage tank through a connecting pipe. Under the action of the high-pressure liquid pump 104, the washing absorption liquid is transported to the infusion pipe 105, and then enters the sprayer 108. The washing absorption liquid is sprayed downward in an atomized manner to form a gas with the acrylic acid gas rising from the bottom. Countercurrent contact, during this process, acrylic acid gas is absorbed by the absorbent to become acrylic acid liquid, and then the acrylic acid liquid is filtered through the quartz sand filter medium to separate the internal impurities. The filtered acrylic acid liquid falls on the bottom cover 106 and is discharged through the drain pipe 109. When the filter medium needs to be replaced, the electric push rod 218 is started to pull the inclined guide block 217 to move downward, so that an inclined channel is formed between the feed pipe 213 and the inside of the discharge pipe 214. At this time, the filter medium in the conical filter frame 301 enters the feed pipe 213 and slides along the inclined surface of the inclined guide block 217 to the inside of the discharge pipe 214, thereby discharging the filter medium, and starting the drive motor 303 again, so that the rotating rod 305 drives the feed claw rake 308 to rotate together,It is convenient to push the filter medium on the bottom surface of the conical filter frame 301 to the feed pipe 213 for feeding, rotate the threaded cover 216, unscrew it from the inside of the threaded hole 112 and the outer surface of the feed pipe 213, then pull out the fixing block 219 and the electric push rod 218 from the feed pipe 213, and further remove the inclined guide block 217 from the feed pipe 213, so as to facilitate grinding the inclined surface of the inclined guide block 217 to make its inclined surface smoother.

[0044] Among them, the high-pressure liquid pump 104, the vibrator 204, the electric push rod 218, the drive motor 303, the hydraulic rod 405 and the PLC controller 5 are all existing technologies, and their components and operating principles are all public technologies, which will not be explained in detail here.

[0045] Although the present invention has been described in detail with reference to the aforementioned embodiments, it is still possible for those skilled in the art to modify the technical solutions described in the aforementioned embodiments, or to make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. An acrylic acid washing device for acrylic acid production, comprising a washing component (1) and a sealing component (4), wherein the washing component (1) is used to wash acrylic acid gas, and the sealing component (4) is used to provide a sealing function, characterized in that: A leveling component (3) is arranged inside the washing component (1), and a loading and unloading component (2) is arranged on the outer surface of the washing component (1), wherein the leveling component (3) is used to flatten the quartz sand filter medium that is put in, and the loading and unloading component (2) is used to realize automatic input and automatic discharge of the quartz sand filter medium; The washing assembly (1) comprises a washer (101), a bottom cover (106) being mounted on the bottom of the washer (101) by means of bolts, and a plurality of feeding ports (110) being provided on the outer surface of the washer (101); The uniformizing component (3) comprises a conical filter frame (301), a protective cover (302) is fixedly mounted on the bottom of the conical filter frame (301), a driving motor (303) is fixedly mounted on the bottom surface inside the protective cover (302), a rotating rod (305) is fixedly mounted on the output end of the driving motor (303), a pointed sleeve (304) is movably sleeved on the outer surface of the rotating rod (305), a plurality of leveling claw rakes (307) are fixedly mounted on the outer surface of the rotating rod (305), a material unloading claw rake (308) is fixedly mounted on the outer surface of the rotating rod (305) near the pointed sleeve (304), and a pushing plate (306) is fixedly mounted on the outer surface of the rotating rod (305) near the top; The outer surface of the conical filter frame (301) is fixedly mounted near the top on the inner wall of the scrubber (101) near the feeding port (110); the bottom of the pointed sleeve (304) is fixedly mounted on the bottom surface inside the conical filter frame (301); the inner wall of the pointed sleeve (304) is in contact with the outer surface of the rotating rod (305) near the top; and the top end of the rotating rod (305) is movable and penetrates into the interior of the conical filter frame (301); The sealing assembly (4) comprises a connecting plate (401), a hydraulic rod (405) is fixedly mounted on the bottom of the connecting plate (401), a bellows (402) is arranged on the outer surface of the hydraulic rod (405), a moving block (406) is fixedly mounted on the bottom end of the hydraulic rod (405), a plurality of fixed rods (407) are fixedly mounted on the outer surface of the moving block (406), an annular sealing plate (403) is fixedly mounted on one end of the plurality of fixed rods (407), a sealing ring (404) is fixedly connected to the outer surface of the annular sealing plate (403), the outer surface of the sealing ring (404) is in contact with the inner wall of the washer (101), the outer surfaces of both sides of the connecting plate (401) are fixedly mounted on the inner wall of the washer (101), the top of the bellows (402) is fixedly mounted on the bottom of the connecting plate (401), and the bottom of the bellows (402) is fixedly mounted on the top of the moving block (406); The loading and unloading assembly (2) comprises a loading rack (201), a PLC controller (5) is arranged on the top of the loading rack (201), a vibration groove (220) is opened inside the loading rack (201), a plurality of loading boxes (205) are movably embedded inside the vibration groove (220), the tops of the plurality of loading boxes (205) are fixedly connected with elastic pads (208), a plurality of loading pipes (206) are arranged on the top of the loading rack (201), the bottom ends of the plurality of loading pipes (206) are fixedly passed through the loading rack (201) to the inside of the vibration groove (220), the bottom ends of the plurality of loading pipes (206) are movably passed through the plurality of elastic pads (208) to the inside of the plurality of loading boxes (205), and the bottoms of the plurality of loading boxes (205) are fixedly connected with four vibration springs (209); One end of the plurality of vibration springs (209) is fixedly mounted on the bottom surface of the vibration groove (220), two vibration rods (207) are fixedly mounted on the bottom of the plurality of feeding boxes (205), the bottom ends of the plurality of vibration rods (207) are movably connected to the bottom of the feeding rack (201), a vibration plate (203) is mounted on the bottom ends of the plurality of vibration rods (207) by bolts, a vibrator (204) is arranged near the center of the top of the vibration plate (203), the inner wall of the feeding rack (201) is provided with a plurality of movable holes (212), the top and bottom surfaces of the plurality of movable holes (212) are fixedly connected with elastic strips (211), and a feeding pipe (210) is movably embedded in the interior of the plurality of movable holes (212); One ends of the plurality of feeding pipes (210) are respectively fixedly connected to the outer surfaces of the plurality of loading boxes (205), and the other ends of the plurality of feeding pipes (210) are respectively movably embedded in the inside of the feeding port (110); a threaded hole (112) is provided at the bottom of the bottom cover (106); a sealing hole (111) is provided at the bottom of the bottom cover (106) near the threaded hole (112); and a feeding pipe (213) is fixedly connected to the bottom of the conical filter frame (301) near the protective cover (302); The outer surface of the feed pipe (213) is fixedly connected to a discharge pipe (214), and the outer surface of the discharge pipe (214) is fixedly connected to a sealing sleeve (215), and the outer surface of the sealing sleeve (215) is in contact with the inner wall of the sealing hole (111). The bottom end of the feed pipe (213) is threadedly sleeved with a threaded cover (216), and the outer surface of the threaded cover (216) is threadedly connected to the inner wall of the threaded hole (112), and a fixing block (219) is fixedly installed on the bottom surface of the threaded cover (216); An electric push rod (218) is fixedly mounted on the top of the fixed block (219), an inclined guide block (217) is fixedly mounted on the top of the electric push rod (218), the outer surface of the inclined guide block (217) is movably embedded in the interior of the discharge pipe (213), the outer surface of the fixed block (219) and the outer surface of the electric push rod (218) are both located inside the discharge pipe (213), a plurality of supporting legs (202) are fixedly mounted on the outer surface of the loading rack (201), and the outer surface of the washer (101) is fixedly mounted inside the loading rack (201); The rotation of the output end of the driving motor (303) drives the rotating rod (305) to rotate, which further drives the plurality of push claw rakes (307) to rotate. The plurality of push claw rakes (307) rotate, and the quartz sand filter medium introduced at multiple points in the conical filter frame (301) is further moved so as to be evenly distributed inside the conical filter frame (301). When the loading and unloading assembly (2) completes the loading, the height of the quartz sand in the conical filter frame (301) is located at the bottom of the push plate (306). The plurality of push claw rakes (307) evenly move the quartz sand, and the quartz sand is evenly moved. The push plate (306) pushes the quartz sand on the top to make it evenly distributed, thereby achieving the effect of even feeding, preventing the filter medium from being locally accumulated, and facilitating improving the filtering effect. The tip of the pointed sleeve (304) contacts the outer surface of the rotating rod (305). Under the action of the pointed sleeve (304), the smaller filter medium is prevented from falling onto the drive motor (303) through the gap between the rotating rod (305) and the conical filter frame (301), thereby affecting the normal operation of the drive motor (303); The staff pours the same amount of quartz sand filter medium into the five feeding boxes (205) through the five feeding pipes (206) in advance, starts the vibrator (204), drives the vibration plate (203) to vibrate, and drives the multiple vibration rods (207) to vibrate. Under the elastic support of the vibration spring (209), the five feeding boxes (205) are driven to vibrate up and down inside the vibration trough (220). The top of the feeding box (205) is protected by the elastic pad (208) to prevent the top of the feeding box (205) from accidentally colliding with the top surface inside the vibration trough (220) to cause wear. At the same time, the five feeding pipes (210) are driven to vibrate inside the movable hole (212) and the feeding port (110). Under the protection of the elastic strip (211), the feeding pipes (210) are prevented from accidentally colliding with the top surface and the bottom surface inside the movable hole (212). Under the vibration of the feeding box (205), the quartz sand filter medium inside the feeding box (205) enters the feeding port (110) through the feeding pipes (210), and enters the inside of the scrubber (101) along the inclined surface inside the feeding port (110), and finally falls into the inside of the conical filter frame (301), thereby achieving The automatic feeding effect does not require manual filling bit by bit, thus reducing the workload and time and improving the feeding efficiency. By equidistantly arranging multiple feeding ports (110) and feeding boxes (205), the entry position of the quartz sand filter medium can be dispersed, which is conducive to the quartz sand being evenly scattered into the conical filter frame (301) from different directions, thereby helping to improve the feeding uniformity. When the filter medium needs to be replaced, the electric push rod (218) is started to pull the inclined guide block (217) to move downward in the feeding pipe (213). When the electric push rod (218) is automatically closed, the inclined guide block (217) is just It is best to move to the intersection of the discharge pipe (214) and the discharge pipe (213). At this time, the lowest point of the inclined surface of the inclined guide block (217) is flush with the lowest point of the feed inlet of the discharge pipe (214). Under the action of the inclined guide block (217), an inclined channel is formed between the discharge pipe (213) and the inside of the discharge pipe (214). At this time, the filter medium in the conical filter frame (301) enters the discharge pipe (213) and slides along the inclined surface of the inclined guide block (217) to the inside of the discharge pipe (214), thereby discharging the filter medium, thereby achieving the effect of automatic discharge; During the material discharge process, the driving motor (303) is started so that the rotating rod (305) drives the material discharge claw rake (308) to rotate together, which is conducive to pushing the filter medium on the inner bottom surface of the conical filter frame (301) to the discharge pipe (213) for material discharge, thereby reducing the residual filter medium in the conical filter frame (301). The threaded cover (216) is rotated to unscrew it from the inside of the threaded hole (112) and the outer surface of the discharge pipe (213), and then the threaded cover (216) is pulled outward to extract the fixed block (219) and the electric push rod (218) from the discharge pipe (213), and further remove the inclined guide block (217) from the discharge pipe (213), so as to facilitate grinding the inclined surface of the inclined guide block (217) to make its inclined surface smoother, which is conducive to discharging the filter medium into the discharge pipe (214) and prevent the inclined surface of the inclined guide block (217) from being worn and affecting the smoothness; The hydraulic rod (405) is started to push the moving block (406) and the fixed rod (407) downward, further pushing the annular sealing plate (403) downward along the inner wall of the scrubber (101), so that the sealing ring (404) moves downward along the inner wall of the scrubber (101). When the bottom of the annular sealing plate (403) contacts the top of the conical filter frame (301), the sealing ring (404) just seals the multiple feeding ports (110), thereby improving the sealing performance of the scrubber (101) and preventing part of the acrylic acid gas from accidentally leaking out from the feeding port (110) when the scrubbing assembly (1) is working.

2. The acrylic acid washing device for acrylic acid production according to claim 1, characterized in that: A top cover (102) is installed on the top of the scrubber (101) by means of bolts, an exhaust pipe (103) is fixedly connected to the top of the top cover (102), a sprayer (108) is fixedly installed inside the scrubber (101), an input end of the sprayer (108) is fixedly penetrated to the outer surface of the scrubber (101), a high-pressure liquid pump (104) is arranged on the outer surface of the scrubber (101), and an air intake pipe (107) is arranged on the outer surface of the scrubber (101).

3. The acrylic acid washing device for acrylic acid production according to claim 2, characterized in that: The output end of the high-pressure liquid pump (104) is connected to a liquid infusion tube (105) via a flange, one end of the liquid infusion tube (105) is connected to the input end of the sprayer (108) via a flange, a sealing ring (113) is fixedly connected to the top of the bottom cover (106) near the edge, the outer surface of the sealing ring (113) is in contact with the inner wall of the scrubber (101) near the bottom, and a liquid discharge tube (109) is fixedly connected to the bottom of the bottom cover (106).