A volumetric moisture meter with reusable electrolyte

The volumetric moisture meter with a reusable electrolyte system addresses inaccuracies due to water vapor and electrolyte concentration changes by using a sealing and mixing mechanism, ensuring accurate and efficient moisture content determination without frequent electrolyte replacement.

CN118858525BActive Publication Date: 2024-12-20HANGZHOU SENZE PHARM TECH CO LTD
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Patent Information

Application Number
CN202411311816.6
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-09-20
Publication Date
2024-12-20
Estimated Expiration
2044-09-20

AI Technical Summary

Technical Problem

Existing moisture meters are affected by external water vapor and electrolyte concentration changes during multiple measurements, leading to inaccurate results and the need for frequent electrolyte replacement.

Method used

A volumetric moisture meter with a reusable electrolyte system featuring a titration cup with a drying cylinder, a sealing mechanism to prevent water vapor entry, and a mixing mechanism for thorough solvent-electrolyte mixing using an energy storage gear and rotating gear ring to ensure accurate measurements without frequent electrolyte replacement.

Benefits of technology

The system prevents external water vapor from affecting measurements and ensures efficient mixing of solvents and electrolytes, maintaining measurement accuracy and reducing the need for electrolyte replacement.

✦ Generated by Eureka AI based on patent content.

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Abstract

The present invention relates to the field of moisture meters, and specifically to a reusable volumetric moisture meter for electrolytes, which solves the problem of external water vapor affecting the measured data. The present invention comprises a mainframe, a titration cup and an injection syringe, wherein the titration cup is mounted on the mainframe, and the mainframe performs moisture measurement on the solvent added into the titration cup. The titration cup is provided with a drying cylinder for absorbing the water vapor inside the titration cup. The present invention, through the provision of a lower barrel, can enable the lower pressing plate on the syringe to contact with the lower pressing ring during the process of the injection syringe injecting the reagent, and push the lower pressing ring to move downward, so that a plurality of clamping arc plates move toward the direction of the injection syringe and contact with the outer wall of the injection syringe, thereby limiting and clamping the injection syringe, preventing the injection syringe from being offset so that the sealing rubber sleeve is opened, thereby allowing external water vapor to enter the titration cup, and improving the detection accuracy of the moisture meter.
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Description

Technical Field

[0001] The invention relates to the technical field of moisture meter, in particular to a volumetric moisture meter with reusable electrolyte. Background Art

[0002] The principle of the electrolyte moisture meter is to use the reaction between Karl Fischer reagent and water. Specifically, when the Karl Fischer reagent in the electrolytic cell of the instrument reaches equilibrium, a water-containing sample is injected. Water participates in the redox reaction of iodine and sulfur dioxide. In the presence of pyridine and methanol, pyridine hydroiodide and pyridine methyl sulfate are generated. The consumed iodine is electrolyzed at the anode, thereby allowing the redox reaction to continue until all the water is consumed. According to Faraday's law of electrolysis, the iodine produced by electrolysis is directly proportional to the amount of electricity consumed during electrolysis, thereby determining the water content in the solvent.

[0003] In actual operation, when the solvent to be measured is sampled through a syringe and injected into the measuring instrument, if the syringe is offset too far, the sealed rubber sleeve will not be able to effectively isolate the external water vapor, which will affect the measurement results.

[0004] When the solvent is added, it takes a certain amount of time to fully mix with the electrolyte. Because multiple measurements will also cause the concentration of the electrolyte to change, which will affect the contact efficiency with the measured solvent, in order to increase the number of times the electrolyte is used, it is necessary to design a method to avoid frequent replacement of the electrolyte due to changes in the concentration of the electrolyte caused by multiple measurements.

[0005] Therefore, the present invention provides a volumetric moisture meter with reusable electrolyte to solve the above problems. Summary of the invention

[0006] In view of the above situation, in order to overcome the defects of the prior art, the present invention provides a volumetric moisture meter with reusable electrolyte to solve the above-mentioned problem that the external water vapor affects the measurement data.

[0007] In order to achieve the above object, the technical solution adopted by the present invention is:

[0008] A reusable volumetric moisture meter for electrolyte, comprising a host, a titration cup and an injection syringe, wherein the titration cup is mounted on the host, the host measures the moisture content of the solvent added into the titration cup, and the titration cup is provided with a drying cylinder for absorbing the water vapor inside the titration cup;

[0009] The top of the titration cup is provided with a top cover for sealing, and the bottom of the top cover is connected to a sealing mechanism for limiting the position of the injection syringe, the sealing mechanism includes an energy storage gear rotatably connected to the bottom of the top cover, and a lower barrel is connected to the middle position of the energy storage gear, and the injection syringe adds solvent into the titration cup through the lower barrel, and a sealing rubber sleeve is provided in the lower barrel;

[0010] A mixing mechanism is provided in the titration cup, and the mixing mechanism is used to fully mix the added solvent and the electrolyte. The mixing mechanism comprises a rotating gear ring rotatably connected to the top of the inner wall of the titration cup, wherein the energy storage gear and the rotating gear ring are adapted to each other.

[0011] Preferably, a liquid adding tube is connected to a side of the top cover close to the titration cup, and the liquid adding tube is connected to an external device through a connecting hose, and the external device is used to add a measurement reagent into the titration cup.

[0012] Preferably, an inner ring is provided at the bottom of the top cover, an outer ring is provided at the top of the titration cup, the top cover and the titration cup are connected via the inner ring and the outer ring, and the titration cup is sealed by inserting the inner ring and the outer ring.

[0013] Preferably, a driving ring is fixedly connected to the top of the top cover, an arc-shaped rotating opening is opened on the driving ring, a lower barrel is located on the inner side of the driving ring, a lower slide shaft is fixedly connected to the outer wall of the lower barrel, and when the lower barrel moves downward, the rotating opening drives the lower barrel to move downward and rotates at the same time;

[0014] Two limit blocks are fixedly connected to the inner side of the energy storage gear, and a sliding groove corresponding to the limit blocks is opened on the lower barrel. The limit blocks and the inner side wall of the sliding groove can slide relative to each other, and the lower barrel can slide relative to the energy storage gear in the vertical direction;

[0015] The lower material barrel penetrates the top cover, and a return spring is arranged between the outer side wall of the lower material barrel and the bottom of the top cover, and the return spring is used for returning the lower material barrel after being pressed down.

[0016] Preferably, the inner side wall of the lower barrel is provided with a downward moving groove, the inner side wall of the downward moving groove is slidably connected with a downward moving rod, the bottom end of the downward moving rod is fixedly connected with a downward pressing ring, and the outer side wall of the injection syringe is fixedly connected with a downward pressing sheet, and the downward pressing sheet pushes the downward pressing ring downward by contact and pressing during the downward moving process;

[0017] The interior of the lower barrel is connected to a clamping arc plate through a telescopic rod, and a guide block is provided on the top of the clamping arc plate to facilitate the downward movement of the injection syringe. A fixed spring is provided between the lower moving rod and the inner side wall of the lower moving groove. The lower moving rod is connected to the clamping arc plate through a transmission rod. During the downward movement of the lower moving rod, the transmission rod drives the clamping arc plate to be pushed toward the direction of the injection syringe.

[0018] Preferably, the lower end of the rotating gear ring is fixedly connected to two symmetrically arranged push rods, the inner side wall of the titration cup is fixedly connected to a first guide arc and a second guide arc, the first guide arc and the second guide arc are symmetrically arranged, and both the first guide arc and the second guide arc are arc-shaped, and a sliding opening is provided on the push rod, and the height of the sliding opening corresponds to the height of the first guide arc and the second guide arc in the vertical direction;

[0019] Sliding blocks corresponding to the first guide arc and the second guide arc are arranged in the sliding opening. The two sliding blocks move in the sliding opening through the first guide arc and the second guide arc respectively. The sliding blocks are provided with guide arc plates, which are arranged opposite to each other.

[0020] Preferably, the bottom end of the pushing rod is fixedly connected to a stirring block for pushing the electrolyte to flow, a stirring gear ring is fixedly connected between the two stirring blocks, the inner bottom of the titration cup is rotatably connected to a stirring shaft, and the outer side wall of the stirring shaft is fixedly connected to a stirring rod for stirring the electrolyte.

[0021] Preferably, the inner bottom of the titration cup is rotatably connected to a transmission gear, the transmission gear is meshed with the teeth on the inner side of the stirring gear ring, and the outer side wall of the stirring shaft is fixedly connected to a rotating gear, and the transmission gear is meshed with the rotating gear.

[0022] Preferably, a central control screen is provided on the front side of the host, and instrument keyboards for controlling the host are provided on both sides of the central control screen.

[0023] The beneficial effects of the present invention are:

[0024] 1. In this scheme, by setting up a lower barrel, during the process of injecting reagent into the injection syringe, the lower pressure sheet on the syringe will contact the lower pressure ring and push the lower pressure ring to move downward, so that multiple clamping arc plates move toward the direction of the injection syringe and contact the outer wall of the injection syringe, thereby limiting the clamping of the injection syringe to prevent the sealing rubber sleeve from being opened due to the deviation of the injection syringe, thereby allowing external water vapor to enter the titration cup, thereby improving the detection accuracy of the moisture meter.

[0025] 2. This solution uses an energy storage gear arranged on the outer wall of the lower barrel, which can store energy while the operator pushes the lower barrel into the titration cup through the injection syringe, and at the same time causes the lower barrel to rotate. Then, after the reagent is injected below the electrolyte surface through the injection syringe, the lower barrel will be reset during the process of the syringe and the lower barrel being separated, thereby stirring the electrolyte in the titration cup to achieve sufficient mixing between the test agent and the electrolyte, and there is no need to frequently replace the electrolyte due to incomplete mixing. BRIEF DESCRIPTION OF THE DRAWINGS

[0026] Figure 1It is a structural schematic diagram of the present invention.

[0027] Figure 2 It is a cross-sectional view of the titration cup of the present invention.

[0028] Figure 3 It is a schematic structural diagram of the driving ring and the discharge barrel of the present invention.

[0029] Figure 4 For the present invention Figure 3 Enlarged view of point A in the middle.

[0030] Figure 5 For the present invention Figure 3 Enlarged view of point B in the middle.

[0031] Figure 6 It is a cross-sectional view of the blanking barrel of the present invention.

[0032] Figure 7 It is a schematic structural diagram of the rotating gear ring of the present invention.

[0033] Figure 8 It is a schematic diagram of the positions of the first guide arc and the second guide arc of the present invention.

[0034] Fig. 9 This is a flow direction diagram of the electrolyte when adding materials in the present invention.

[0035] In the figure: 1. Main unit; 2. Titration cup; 3. Drying cylinder; 4. Connecting hose; 5. Central control screen; 6. Top cover; 7. Inner ring; 8. Outer ring; 9. Adding pipe; 10. Driving ring; 11. Unloading cylinder; 12. Energy storage gear; 13. Rotating mouth; 14. Lowering shaft; 15. Sliding groove; 16. Limiting block; 17. Sealing rubber sleeve; 18. Injection syringe; 19. Lower pressure plate; 20. Lower pressure ring; 21. Lower displacement groove; 22. Shift rod; 23. Fixed spring; 24. Clamping arc plate; 25. Telescopic rod; 26. Transmission rod; 27. Guide block; 28. Return spring; 29. ​​Rotating gear ring; 30. Push rod; 31. First guide arc path; 32. Second guide arc path; 33. Sliding mouth; 34. Sliding block; 35. Guide arc plate; 36. Stirring block; 37. Stirring gear ring; 38. Transmission gear; 39. Stirring shaft; 40. Stirring rod; 41. Rotating gear. DETAILED DESCRIPTION

[0036] The following will refer to the attached Figures 1 to 9 The embodiments of the present invention are described in detail. It should be understood by those skilled in the art that these embodiments are only used to explain the technical principles of the present invention and are not intended to limit the protection scope of the present invention.

[0037] A volumetric moisture meter with reusable electrolyte, as shown in the attached Figure 1 -Attached Fig. 9 The main unit 1 includes a host 1, a titration cup 2 and an injection syringe 18. The titration cup 2 is the place where the water sample is actually measured. The titration cup 2 is installed on the main unit 1. The main unit 1 measures the water content of the solvent added to the titration cup 2. The titration cup 2 is provided with a drying cylinder 3 for absorbing the water vapor inside the titration cup 2. The front side of the main unit 1 is provided with a central control screen 5. Both sides of the central control screen 5 are provided with instrument keyboards for controlling the main unit 1. The drying cylinder 3, the central control screen 5 and the instrument keyboard are all prior art and will not be described in detail.

[0038] The top of the titration cup 2 is provided with a top cover 6 for sealing, and a liquid adding tube 9 is connected to the side of the top cover 6 close to the titration cup 2. The liquid adding tube 9 is connected to an external device through a connecting hose 4, and the external device is used to add a measuring reagent into the titration cup 2. The main function of the external device is to prevent the user from directly contacting the KF reagent and to simplify the user's operation. It is an auxiliary device designed, including the functions of KF reagent inlet and outlet.

[0039] An inner ring 7 is provided at the bottom of the top cover 6, and an outer ring 8 is provided at the top of the titration cup 2. The top cover 6 and the titration cup 2 are connected via the inner ring 7 and the outer ring 8, and the titration cup 2 is sealed by inserting the inner ring 7 and the outer ring 8. When the titration cup 2 needs to be sealed, the top cover 6 is moved to the top of the titration cup 2, and then the inner ring 7 is aligned with the outer ring 8, and the top cover 6 is pressed downward so that the top cover 6 seals the titration cup 2. It should be noted that in the process of installing the top cover 6 on the titration cup 2, the energy storage gear 12 will mesh with the inner side of the rotating gear ring 29, which is convenient for the subsequent liquid inlet stirring process.

[0040] Example 1

[0041] This embodiment is designed to solve the problem that external water vapor may enter the titration cup 2 during the process of adding material to the injection syringe 18 .

[0042] The bottom of the top cover 6 is connected to a sealing mechanism for limiting the position of the injection syringe 18, and the sealing mechanism includes an energy storage gear 12 rotatably connected to the bottom of the top cover 6, and a lower barrel 11 is connected to the middle position of the energy storage gear 12. The injection syringe 18 adds solvent to the titration cup 2 through the lower barrel 11. A sealing rubber sleeve 17 is provided in the lower barrel 11, and a downward movement groove 21 is opened on the inner side wall of the lower barrel 11. A downward movement rod 22 is slidably connected to the inner side wall of the downward movement groove 21, and a downward pressure ring 20 is fixedly connected to the bottom end of the downward movement rod 22. A downward pressure plate 19 is fixedly connected to the outer side wall of the injection syringe 18, and the lower pressure plate 19 pushes the downward pressure ring 20 downward by contact and pressing during the downward movement process.

[0043] When testing the moisture content of the solvent to be measured, the user sucks the solvent into the injection syringe 18 through the injection syringe 18, and then extends the injection syringe 18 into the discharge barrel 11. The injection syringe 18 will push the central part of the sealing rubber sleeve 17 that maintains the seal, and the other parts of the sealing rubber sleeve 17 will be tightly attached to the injection syringe 18, thereby maintaining a sealed state (if the injection syringe 18 moves too far to one side, the sealing rubber sleeve 17 will not be able to stick to the side wall of the injection syringe 18). When the injection syringe 18 continues to move downward, the lower pressing plate 19 on the injection syringe 18 will contact the lower pressing ring 20 and push the lower pressing ring 20 downward.

[0044] The interior of the lower barrel 11 is connected to a clamping arc plate 24 via a telescopic rod 25. A guide block 27 is provided on the top of the clamping arc plate 24 to facilitate the downward movement of the injection syringe 18. A fixing spring 23 is provided between the lower moving rod 22 and the inner side wall of the lower moving groove 21. The lower moving rod 22 is connected to the clamping arc plate 24 via a transmission rod 26. During the downward movement of the lower moving rod 22, the clamping arc plate 24 is driven by the transmission rod 26 to be pushed toward the direction of the injection syringe 18.

[0045] As mentioned above, when the injection syringe 18 continues to move downward, the downward pressure ring 20 will be pushed downward synchronously through the downward pressure sheet 19 on its surface. The downward movement of the downward pressure ring 20 will cause the downward movement rod 22 to move downward synchronously. At this time, the downward movement rod 22 will push the clamping arc plate 24 to move toward the injection syringe 18 under the action of the transmission rod 26, thereby limiting the position of the injection syringe 18 to prevent it from shifting to one side when in the discharge barrel 11, ensuring the sealing performance of the sealing rubber sleeve 17 when in contact with the injection syringe 18, preventing external water vapor from entering the titration cup 2, and ensuring the accuracy of moisture measurement.

[0046] Example 2

[0047] This embodiment enables the lower barrel 11 to rotate while being pushed downward by the injection syringe 18, thereby realizing the effect of energy storage, making it convenient for the subsequent injection syringe 18 to stir the reagent and electrolyte after leaving the lower barrel 11, so that they can be fully mixed and the measurement efficiency is improved.

[0048] A driving ring 10 is fixedly connected to the top of the top cover 6, and an arc-shaped rotating port 13 is opened on the driving ring 10. The lower barrel 11 is located on the inner side of the driving ring 10, and a lower slide shaft 14 is fixedly connected to the outer wall of the lower barrel 11. When the lower barrel 11 moves downward, the rotating port 13 drives the lower barrel 11 to move downward and rotates at the same time;

[0049] Two limit blocks 16 are fixedly connected to the inner side of the energy storage gear 12. A sliding groove 15 corresponding to the limit blocks 16 is opened on the lower barrel 11. The limit blocks 16 and the inner side walls of the sliding groove 15 can slide relative to each other, and the lower barrel 11 can slide relative to the energy storage gear 12 in the vertical direction.

[0050] As described in Example 1, the injection syringe 18 enters the lower barrel 11 and contacts the pressing ring 20 to press the lower barrel 11 downward as a whole. Due to the relative sliding between the slide groove 15 and the limit block 16, the lower barrel 11 can move downward relative to the energy storage gear 12, and in the process of the lower barrel 11 moving downward, refer to the attached Figure 3 Under the guidance of the arc-shaped rotating opening 13 , the lower slide shaft 14 synchronously rotates the discharge barrel 11 , so that the energy storage gear 12 rotates with the rotation of the discharge barrel 11 .

[0051] The lower barrel 11 passes through the top cover 6, and a return spring 28 is provided between the outer wall of the lower barrel 11 and the bottom of the top cover 6. The return spring 28 is used to return the lower barrel 11 after being pressed down. In the process of the lower barrel 11 moving downward, the return spring 28 will be stretched, thereby accumulating energy, and when the injection syringe 18 is separated from the lower barrel 11, the lower barrel 11 will move upward and return to its original position.

[0052] Example 3

[0053] This embodiment is a supplementary explanation to Embodiment 2. When the lower barrel 11 moves downward and accumulates energy through the return spring 28, the electrolyte is stirred, and when the return spring 28 releases energy, the solvent and the electrolyte are further mixed, thereby improving the measurement efficiency of the measuring instrument.

[0054] A mixing mechanism is provided in the titration cup 2 for fully mixing the added solvent and the electrolyte. The mixing mechanism comprises a rotating gear ring 29 rotatably connected to the top of the inner wall of the titration cup 2 , wherein the energy storage gear 12 and the rotating gear ring 29 are adapted to each other.

[0055] The lower end of the rotating gear ring 29 is fixedly connected to two symmetrically arranged push rods 30, and the inner side wall of the titration cup 2 is fixedly connected to a first guide arc 31 and a second guide arc 32, the first guide arc 31 and the second guide arc 32 are symmetrically arranged, and the first guide arc 31 and the second guide arc 32 are both arc-shaped, and a sliding opening 33 is opened on the push rod 30, and the height of the sliding opening 33 corresponds to the height of the first guide arc 31 and the second guide arc 32 in the vertical direction;

[0056] A sliding block 34 corresponding to the first guide arc 31 and the second guide arc 32 is provided in the sliding opening 33. The two sliding blocks 34 move in the sliding opening 33 through the first guide arc 31 and the second guide arc 32 respectively. A guide arc plate 35 is provided on the sliding block 34, and the two guide arc plates 35 are arranged opposite to each other.

[0057] When the push rod 30 rotates, it drives the sliding block 34 to move along the first guide arc 31 or the second guide arc 32 . At this time, the sliding block 34 moves up or down in the sliding opening 33 .

[0058] When the injection syringe 18 extends into the lower barrel 11 and pushes the lower barrel 11 downward, the energy storage gear 12 rotates clockwise, driving the corresponding rotating gear ring 29 to rotate clockwise. When the rotating gear ring 29 rotates clockwise, Figure 8 The push rod 30 on the right side will move toward the upper direction of the second guide arc 32, and drive the right guide arc plate 35 to move upward under the action of the second guide arc 32 and the sliding block 34; and the push rod 30 on the right side will move toward the bottom end of the first guide arc 31, driving the corresponding guide arc plate 35 to move downward, so as to achieve the following Fig. 9 The arrow in the figure indicates the flow direction of the electrolyte, thereby accelerating the flow of the electrolyte and avoiding the situation where the concentration of the electrolyte at the injection solvent position is reduced due to repeated use and inaccurate detection. When the injection syringe 18 injects the reagent into the electrolyte, the needle should be below the liquid level to facilitate the mixing of the reagent and the electrolyte.

[0059] Similarly, when the injection syringe 18 is separated from the lower barrel 11, the return spring 28 will contract, so that the lower barrel 11 can move up, and at the same time, it rotates counterclockwise under the action of the rotating mouth 13, synchronously causing the energy storage gear 12 to rotate counterclockwise, driving the rotating gear ring 29 to rotate counterclockwise, thereby achieving the electrolyte and the added solvent such as the attached Fig. 9 The two substances flow in the opposite direction indicated by the arrow, which speeds up the mixing of the two and improves the measurement efficiency.

[0060] The inner bottom of the titration cup 2 is rotatably connected to a transmission gear 38, which meshes with the teeth on the inner side of the stirring gear ring 37, and the outer side wall of the stirring shaft 39 is fixedly connected to a rotating gear 41, which meshes with the transmission gear 38 and the rotating gear 41. The bottom end of the push rod 30 is fixedly connected to a stirring block 36 for pushing the electrolyte to flow, and a stirring gear ring 37 is fixedly connected between the two stirring blocks 36. The inner bottom of the titration cup 2 is rotatably connected to a stirring shaft 39, and the outer side wall of the stirring shaft 39 is fixedly connected to a stirring rod 40 for stirring the electrolyte.

[0061] When the push rod 30 rotates, the two stirring blocks 36 at the bottom can rotate, and the electrolyte is stirred horizontally during the flow of the electrolyte, thereby accelerating its stirring speed. The stirring blocks 36 will synchronously drive the stirring gear ring 37 to rotate, and the stirring gear ring 37 will rotate the stirring shaft 39 through the transmission action of the transmission gear 38 and the rotating gear 41. It should be noted that the rotation direction of the stirring shaft 39 is opposite to that of the stirring block 36, thereby increasing the degree of mixing after the reagent and the electrolyte come into contact, thereby increasing the measurement speed of the reagent.

[0062] It should be noted that in the description of the present invention, the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer" and the like indicating directions or positional relationships are based on the directions or positional relationships shown in the drawings, which are only for the convenience of description, and do not indicate or imply that the device or element must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as limiting the present invention. In addition, the terms "first", "second", and "third" are used for descriptive purposes only, and cannot be understood as indicating or implying relative importance.

[0063] In addition, it should be noted that in the description of the present invention, unless otherwise clearly specified and limited, the terms "installed", "connected", and "connected" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection, or it can be indirectly connected through an intermediate medium, or it can be the internal communication of two components. For those skilled in the art, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.

[0064] So far, the technical solutions of the present invention have been described in conjunction with the preferred embodiments shown in the accompanying drawings. However, it is easy for those skilled in the art to understand that the protection scope of the present invention is obviously not limited to these specific embodiments. Without departing from the principle of the present invention, those skilled in the art can make equivalent changes or substitutions to the relevant technical features, and the technical solutions after these changes or substitutions will fall within the protection scope of the present invention.

Claims

1. A reusable volumetric moisture meter for electrolyte, comprising a main unit (1), a titration cup (2) and an injection syringe (18), characterized in that: The titration cup (2) is mounted on a host (1), and the host (1) measures the water content of a solvent added into the titration cup (2). The titration cup (2) is provided with a drying cylinder (3) for absorbing water vapor inside the titration cup (2); The top of the titration cup (2) is provided with a top cover (6) for sealing, the bottom of the top cover (6) is connected to a sealing mechanism for limiting the position of the injection syringe (18), the sealing mechanism comprises an energy storage gear (12) rotatably connected to the bottom of the top cover (6), a lower barrel (11) is connected to the middle position of the energy storage gear (12), the injection syringe (18) adds solvent into the titration cup (2) through the lower barrel (11), and a sealing rubber sleeve (17) is provided in the lower barrel (11); The titration cup (2) is provided with a mixing mechanism, which is used to fully mix the added solvent and the electrolyte, and the mixing mechanism comprises a rotating gear ring (29) rotatably connected to the top of the inner wall of the titration cup (2), wherein the energy storage gear (12) and the rotating gear ring (29) are adapted to each other; The top of the top cover (6) is fixedly connected to a driving ring (10), and an arc-shaped rotating opening (13) is provided on the driving ring (10). The lower barrel (11) is located on the inner side of the driving ring (10), and a lower sliding shaft (14) is fixedly connected to the outer wall of the lower barrel (11). When the lower barrel (11) moves downward, the rotating opening (13) drives the lower barrel (11) to move downward and rotates at the same time; Two limit blocks (16) are fixedly connected to the inner side of the energy storage gear (12); a slide groove (15) corresponding to the limit blocks (16) is provided on the lower barrel (11); the limit blocks (16) and the inner side walls of the slide groove (15) are able to slide relative to each other; and the lower barrel (11) is able to slide relative to the energy storage gear (12) in a vertical direction; The lower material barrel (11) passes through the top cover (6), and a return spring (28) is provided between the outer wall of the lower material barrel (11) and the bottom of the top cover (6), and the return spring (28) is used to return the lower material barrel (11) after being pressed down; The inner wall of the lower material barrel (11) is provided with a downward moving groove (21), the inner wall of the downward moving groove (21) is slidably connected with a downward moving rod (22), the bottom end of the downward moving rod (22) is fixedly connected with a downward pressing ring (20), and the outer wall of the injection syringe (18) is fixedly connected with a downward pressing plate (19), and the downward pressing plate (19) pushes the downward pressing ring (20) downward by contact and pressing during the downward moving process; The interior of the lower barrel (11) is connected to a clamping arc plate (24) via a telescopic rod (25); a guide block (27) is provided on the top of the clamping arc plate (24) for facilitating the downward movement of the injection syringe (18); a fixing spring (23) is provided between the downward movement rod (22) and the inner side wall of the downward movement groove (21); the downward movement rod (22) is connected to the clamping arc plate (24) via a transmission rod (26); during the downward movement of the downward movement rod (22), the transmission rod (26) drives the clamping arc plate (24) to move in the direction of the injection syringe (18); The lower end of the rotating gear ring (29) is fixedly connected to two symmetrically arranged push rods (30); the inner side wall of the titration cup (2) is fixedly connected to a first guide arc (31) and a second guide arc (32); the first guide arc (31) and the second guide arc (32) are symmetrically arranged, and both the first guide arc (31) and the second guide arc (32) are arc-shaped; a sliding opening (33) is provided on the push rod (30); the height of the sliding opening (33) corresponds to the height of the first guide arc (31) and the second guide arc (32) in the vertical direction; A sliding block (34) corresponding to the first guide arc path (31) and the second guide arc path (32) is provided in the sliding opening (33); the two sliding blocks (34) move in the sliding opening (33) through the first guide arc path (31) and the second guide arc path (32) respectively; a guide arc plate (35) is provided on the sliding block (34); the two guide arc plates (35) are arranged opposite to each other; The bottom end of the pushing rod (30) is fixedly connected to a stirring block (36) for pushing the electrolyte to flow, a stirring gear ring (37) is fixedly connected between the two stirring blocks (36), the inner bottom of the titration cup (2) is rotatably connected to a stirring shaft (39), and the outer side wall of the stirring shaft (39) is fixedly connected to a stirring rod (40) for stirring the electrolyte; The inner bottom of the titration cup (2) is rotatably connected to a transmission gear (38), the transmission gear (38) and the teeth on the inner side of the stirring gear ring (37) are meshed with each other, and the outer side wall of the stirring shaft (39) is fixedly connected to a rotating gear (41), and the transmission gear (38) and the rotating gear (41) are meshed with each other.

2. A reusable volumetric moisture meter for electrolyte according to claim 1, characterized in that: A liquid adding tube (9) is connected to the side of the top cover (6) facing the titration cup (2), and the liquid adding tube (9) is connected to an external device through a connecting hose (4), and the external device is used to add a measuring reagent into the titration cup (2).

3. The reusable volumetric moisture meter for electrolyte according to claim 1, characterized in that: An inner connecting ring (7) is provided at the bottom of the top cover (6), and an outer connecting ring (8) is provided at the top of the titration cup (2); the top cover (6) and the titration cup (2) are connected via the inner connecting ring (7) and the outer connecting ring (8); the titration cup (2) is sealed by inserting the inner connecting ring (7) and the outer connecting ring (8).

4. According to the reusable volumetric moisture meter for electrolyte solution as claimed in claim 1, a central control screen (5) is provided on the front side of the main unit (1), and instrument keyboards for controlling the main unit (1) are provided on both sides of the central control screen (5).

Citation Information

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