Gel aging and drying equipment

By designing gel aging and drying equipment, using rotary heating and pitch adjustment of quartz glass tubes, the problem of long and large pollution in the aging process in the sol-gel method is solved, and efficient gel aging and production efficiency are achieved.

CN119103846AInactive Publication Date: 2024-12-10中建材衢州金格兰石英有限公司 +1
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Patent Information

Application Number
CN202411365216.8
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-09-29
Publication Date
2024-12-10
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

When gel products prepared by the existing sol-gel method are placed in an oven to aged after precipitation or aged in a solvent, it takes a long time, has a high pollution and low production efficiency.

Method used

A gel aging and drying equipment is designed, including quartz glass tubes, fixing mechanisms, heating mechanisms, rotating mechanisms and elevation adjustment mechanisms. Through the rotational heating and pitch angle adjustment of quartz glass tubes, uniform heating and rapid heating of the gel are achieved. aging.

Benefits of technology

It effectively reduces equipment pollution during gel aging, reduces drying cycle, improves production efficiency, and is suitable for products with high impurity requirements.

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Abstract

The invention discloses gel aging and drying equipment which comprises a base support, a quartz glass tube, a fixing mechanism, a heating mechanism, a rotating mechanism and an elevation angle adjusting mechanism, an assembling frame is rotationally installed at the top of the base support, glass tube supporting rings are arranged at the two ends of the quartz glass tube, and the fixing mechanism is arranged on the glass tube supporting rings; the quartz glass tube is fixed on the glass tube supporting ring through the fixing mechanism, the glass tube supporting ring is rotatably installed on the assembling frame through the positioning mechanism, the heating mechanism heats materials in the quartz glass tube, the rotating mechanism drives the quartz glass tube to rotate, and therefore the materials can be evenly heated and prevented from being bonded into blocks. The elevation angle adjusting mechanism adjusts the elevation angle of the quartz glass tube, feeding and discharging are convenient, the quartz glass tube is adopted, equipment pollution is reduced in the material drying process, the cleanliness is high, the drying period is short, and the production efficiency is high.
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Description

Technical Field

[0001] The invention relates to the technical field of drying, in particular to gel aging drying equipment. Background Art

[0002] Solid materials prepared by the sol-gel method have the characteristics of high specific surface area, high porosity, low density, and good thermal insulation performance. Therefore, they have unique and excellent properties in thermal, optical, electrical, acoustic and other aspects.

[0003] However, since the pore size of the gel is at the nanoscale and there are a large number of hydroxyl groups on the surface, capillary contraction is likely to occur, causing the gel network structure to gradually collapse and rupture, resulting in poor uniformity of the finished product. Therefore, it must undergo a gel aging process, which can fix the gel size structure, reduce surface activity, and improve stability. Currently, most porous silica, titanium dioxide and other products prepared by the sol-gel method need to be aged in an oven after precipitation is generated, or aged in a solvent. This method takes a long time, causes high pollution, and has low industrial production efficiency. To this end, we propose a drying device for gel aging. Summary of the invention

[0004] The purpose of the present invention is to provide a gel aging and drying device, so as to solve the technical problems of the existing sol-gel method preparation process in which the precipitate is placed in an oven for aging after being generated, or the aging in a solvent takes a long time, causes great pollution and has low production efficiency.

[0005] To achieve the above object, the present invention provides the following technical solutions:

[0006] A gel aging and drying device, comprising:

[0007] A base bracket, the top of which is rotatably mounted with an assembly frame;

[0008] A quartz glass tube, one end of which is sealed, and both ends of the quartz glass tube are provided with glass tube support rings;

[0009] A fixing mechanism, which is arranged on the glass tube supporting ring and fixes the quartz glass tube on the glass tube supporting ring;

[0010] The glass tube support ring is rotatably mounted on the assembly frame through a positioning mechanism, and the positioning mechanism is arranged on the assembly frame;

[0011] A heating mechanism, wherein the heating mechanism is sleeved on the outer wall of the quartz glass tube;

[0012] A rotating mechanism, which drives the quartz glass tube to rotate;

[0013] The elevation angle adjustment mechanism is arranged between the base support and the assembly frame, and the elevation angle adjustment mechanism adjusts the pitch angle of the quartz glass tube.

[0014] As a further solution of the present invention, a positioning mechanism is provided on the front mounting frame and the rear mounting frame at both ends of the assembly frame. The positioning mechanism includes three positioning wheels in a triangular shape. The positioning wheels are rotatably mounted on the assembly frame through a rotating shaft. An annular limiting groove is provided on the positioning wheel. The glass tube support ring is rollingly mounted on the annular limiting groove. The three positioning wheels are distributed in a triangular shape around the glass tube support ring to limit the glass tube support ring between the three positioning wheels.

[0015] As a further solution of the present invention, the fixing mechanism includes a chain, two chains are provided, both ends of the two chains are provided with locking components, the two chains are fixed to the quartz glass tube through the locking components, and the chains are provided with fastening components for fixing the chains to the glass tube support ring.

[0016] As a further solution of the present invention, the locking assembly includes a first mounting angle iron fixed on the chain plates at both ends of the chain, and a connecting plate is fixedly connected to the first mounting angle iron. The two connecting plates on the same side of the two chains are fixedly connected by bolts, and the upper end of the bolt passes through the two connecting plates in sequence and is threadedly fixed with a nut.

[0017] As a further solution of the present invention, the fastening assembly includes a second mounting angle iron fixed on the chain plate, the second mounting angle iron is fixed to one side of the glass tube support ring by a screw, a waist hole is opened on the second mounting angle iron, one end of the screw passes through the glass tube support ring and the waist hole and is threadedly fixed with a nut.

[0018] As a further solution of the present invention, a rotating mechanism is arranged at one end of the assembly frame close to the rear mounting frame, and the rotating mechanism includes a motor, which is fixedly mounted on the assembly frame. The rotating shafts of the two positioning wheels located on the rear mounting frame are fixedly connected with synchronous wheels, and a pulley is fixedly mounted on the rotating shaft of the motor. The pulley is connected to the two synchronous wheels through a synchronous belt, and the rotating synchronous wheel drives the glass tube support ring to rotate in coordination with the quartz glass tube.

[0019] As a further solution of the present invention, the heating mechanism includes an insulation sleeve, which is arranged on the outside of the quartz glass tube, and a gap is left between the inner wall of the insulation sleeve and the outer wall of the quartz glass tube. A ceramic sheet with a plurality of heating wires embedded therein is arranged in the insulation sleeve. A support rod is fixedly connected between the front mounting frame and the rear mounting frame, a limit ring is fixedly connected to the support rod, and the insulation sleeve is arranged in the limit ring.

[0020] As a further solution of the present invention, an anti-slip felt layer is arranged between the chain and the quartz glass tube.

[0021] As a preferred embodiment of the present invention, the elevation angle adjustment mechanism includes a cylinder, a lower hinge seat is fixedly connected to the base bracket, an upper hinge seat is fixedly connected to the bottom of the assembly frame close to the motor, the lower end of the cylinder is rotatably connected to the lower hinge seat, and the upper end of the cylinder's piston rod is rotatably connected to the upper hinge seat.

[0022] As a preferred solution of the present invention, the inner wall of the quartz glass tube is formed with a plurality of longitudinal baffles, and the plurality of longitudinal baffles are arranged alternately and staggered.

[0023] Compared with the prior art, the beneficial effects of the gel aging and drying equipment of the present invention are:

[0024] The present invention fixes the quartz glass tube by a fixing mechanism, and the quartz glass tube will not be loose or slip during use. The quartz glass tube is rotated by a rotating mechanism during operation, and the heating mechanism evenly heats the material inside the quartz glass tube, so that the equipment pollution of the gel product is reduced during the production process. The invention is suitable for products with high impurity requirements and effectively reduces the drying cycle.

[0025] The rotating mechanism and the longitudinal baffles on the inner wall of the quartz glass tube can heat the material evenly and prevent the material from sticking together. The elevation adjustment mechanism is convenient for adjusting the elevation angle of the quartz glass tube, which is convenient for feeding and unloading. BRIEF DESCRIPTION OF THE DRAWINGS

[0026] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings required for use in the embodiments are briefly introduced below. Obviously, the drawings described below are only examples of the embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.

[0027] Figure 1 It is a structural schematic diagram of an embodiment of the present invention;

[0028] Figure 2 It is a schematic diagram of a local structure of an embodiment of the present invention;

[0029] Figure 3 It is a structural schematic diagram of a fixing mechanism in an embodiment of the present invention;

[0030] Figure 4 Schematic diagram of the top view of the quartz glass tube in an embodiment of the present invention;

[0031] Figure 5 Schematic diagram of the cross-sectional structure of a quartz glass tube in an embodiment of the present invention;

[0032] Figure 6 It is a structural schematic diagram of the rotating mechanism in an embodiment of the present invention;

[0033] Figure 7It is a schematic side view of the structure of the positioning wheel and the glass tube support ring in an embodiment of the present invention.

[0034] Reference numerals:

[0035] 1. Base bracket;

[0036] 2. Assembly frame; 201. Front mounting frame; 202. Rear mounting frame; 203. Support rod; 204. Limiting ring;

[0037] 3. Insulation cover;

[0038] 4. Elevation angle adjustment mechanism; 401. Cylinder; 402. Lower articulated seat; 403. Upper articulated seat;

[0039] 5. Rotating mechanism; 501. Motor; 502. Synchronous belt;

[0040] 6. Quartz glass tube; 601. Longitudinal baffle;

[0041] 7. Glass tube support ring; 701. Chain; 702. First mounting angle iron; 703. Connecting plate; 704. Bolt; 705. Second mounting angle iron; 7051. Waist hole; 7052. Screw;

[0042] 8. Positioning wheel; 801. Synchronous wheel; 802. Annular limiting groove;

[0043] 9. Anti-slip felt layer. DETAILED DESCRIPTION

[0044] In order to make the purpose, technical solution and advantages of the embodiments of the present invention more clear, the embodiments of the present invention are further described in detail in conjunction with the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are only used to explain the present invention and are not used to limit the present invention.

[0045] In the description of the embodiments of the present invention, it should be understood that the terms "upper", "lower", "front", "back", "inside", "outside", etc. indicate directions or positional relationships based on the directions or positional relationships shown in the accompanying drawings, and are only for the convenience of describing the embodiments of the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific direction, be constructed and operated in a specific direction, and therefore should not be understood as a limitation on the embodiments of the present invention.

[0046] In the description of the embodiments of the present invention, it should be noted that, unless otherwise clearly specified and limited, the terms "installation", "connection" and "connection" should be understood in a broad sense. For example, it can be a fixed connection, an integral connection, or a detachable connection; it can be the internal connection of two components; it can be directly connected or indirectly connected through an intermediate medium. For ordinary technicians in this field, the specific meanings of the above terms in the embodiments of the present invention can be understood according to specific circumstances.

[0047] See also Figure 1-2 As shown, the present invention provides a gel aging and drying device, comprising a base support 1, a quartz glass tube 6, a fixing mechanism for fixing the quartz glass tube 6, a heating mechanism for heating the quartz glass tube 6, a rotating mechanism 5 for rotating the quartz glass tube 6, and an elevation adjustment mechanism 4 for adjusting the pitch angle of the quartz glass tube 6.

[0048] An assembly frame 2 is rotatably mounted on the top of the base bracket 1 .

[0049] Glass tube support rings 7 are provided at both ends of the quartz glass tube 6 ; a fixing mechanism fixes the quartz glass tube 6 on the glass tube support ring 7 ; the glass tube support ring 7 is rotatably mounted on the assembly frame 2 through a positioning mechanism, and the positioning mechanism is arranged on the assembly frame 2 .

[0050] One end of the quartz glass tube 6 is sealed, and the heating mechanism is sleeved on the outer wall of the glass tube 6 .

[0051] The rotating mechanism is arranged on the assembly frame 2 near the sealing end of the quartz glass tube 6, and the rotating mechanism 5 drives the quartz glass tube 6 to rotate. The elevation angle adjustment mechanism 4 is arranged between the base support 1 and the assembly frame 2.

[0052] See also Figure 5 As shown, the fixing mechanism in the embodiment of the present invention includes a chain 701, and two chains 701 are provided. Both ends of the two chains 701 are provided with locking components. The two chains 701 are fixed to the quartz glass tube 6 through the locking components, and the chain 701 is provided with a fastening component for fixing the chain 701 to the glass tube support ring 7.

[0053] Among them, the locking assembly includes a first mounting angle iron 702 fixed on the chain plates at both ends of the chain 701, and a connecting plate 703 is fixedly connected to the first mounting angle iron 702. The two connecting plates 703 on the same side of the two chains 701 are fixedly connected by bolts 704. The upper end of the bolt 704 passes through the two connecting plates 703 in sequence and is threadedly fixed with a nut.

[0054] The fastening assembly includes a second mounting angle iron 705 fixed on the chain plate of the chain 701. The second mounting angle iron 705 is fixed to one side of the glass tube support ring 7 by a screw 7052. A waist hole 7051 is opened on the second mounting angle iron 705. One end of the screw 7052 passes through the glass tube support ring 7 and the waist hole 7051 and is threadedly fixed with a nut.

[0055] By adopting the above technical solution, the quartz glass tube 6 can be fixed on the glass tube support ring 7. During installation, one end of the two chains 701 is first connected through the locking assembly, and then the two chains 701 are wrapped around the quartz glass tube 6. The other ends of the two chains 701 are connected through the locking assembly, and then the chains 701 can be fixed on the quartz glass tube 6. The second installation angle iron 705 is fixed to the glass tube support ring 7 by the screw 7052 to complete the connection between the glass tube support ring 7 and the quartz glass tube 6.

[0056] In order to prevent the chain 701 from scratching the quartz glass tube 6 and to increase the friction between the chain 701 and the quartz glass tube 6 and ensure the connection strength between the chain 701 and the quartz glass tube 6, an anti-slip felt layer 9 is provided between the chain 701 and the quartz glass tube 6 as a buffer material.

[0057] See also Figure 6 , 7 As shown, in the embodiment of the present invention, the front mounting frame 201 and the rear mounting frame 202 at both ends of the assembly frame 2 are provided with positioning mechanisms, and the positioning mechanisms include three positioning wheels 8 in triangular sections, the positioning wheels 8 are rotatably mounted on the assembly frame 2 through a rotating shaft, an annular limiting groove 802 is provided on the positioning wheels 8, and the glass tube support ring 7 is rollingly mounted on the annular limiting groove 802, and the three positioning wheels 8 are distributed in a triangular shape around the glass tube support ring 7, and the glass tube support ring 7 is limited between the three positioning wheels 8. The glass tube support ring 7 is rotatably set on the assembly frame 2, so that the quartz glass tube 6 can be rotated.

[0058] In the embodiment of the present invention, the rotating mechanism 5 is arranged at one end of the assembly frame 2 close to the rear mounting frame 202, and the rotating mechanism 5 includes a motor 501, which is fixedly mounted on the assembly frame 2. The rotating shafts of the two positioning wheels 8 located on the rear mounting frame 202 are fixedly connected with synchronous wheels 801, and a pulley is fixedly mounted on the rotating shaft of the motor 501. The pulley is connected to the two synchronous wheels 801 through a synchronous belt 502. The rotating synchronous wheel 801 drives the glass tube support ring 7 to rotate, thereby rotating the quartz glass tube 6 fixed on the glass tube support ring 7.

[0059] See also Figure 2As shown, in the embodiment of the present invention, the heating mechanism includes an insulation sleeve 3, which is sleeved on the outside of the quartz glass tube 6, and a gap is left between the inner wall of the insulation sleeve 3 and the outer wall of the quartz glass tube 6. A ceramic sheet embedded with a plurality of heating wires is arranged in the insulation sleeve 3. A support rod 203 is fixedly connected between the front mounting frame 201 and the rear mounting frame 202, and a limit ring 204 is fixedly connected to the support rod 203. The insulation sleeve 3 is sleeved in the limit ring 204, and the ceramic sheet embedded with a plurality of heating wires heats the quartz glass tube 6, thereby heating, aging and drying the material inside the quartz glass tube 6. The insulation sleeve 3 can keep warm to prevent the heat from being lost too quickly.

[0060] See also Figure 2 As shown, in the embodiment of the present invention, the elevation adjustment mechanism 4 includes a cylinder 401, a lower hinge seat 402 is fixedly connected to the base bracket 1, an upper hinge seat 403 is fixedly connected to the bottom of one end of the assembly frame 2 close to the motor 501, the lower end of the cylinder 401 is rotatably connected to the lower hinge seat 402, the upper end of the piston rod of the cylinder 401 is rotatably connected to the upper hinge seat 403, and the piston rod of the cylinder 401 telescopically supports the assembly frame 2, thereby adjusting the pitch angle of the quartz glass tube 6 to facilitate loading and unloading of the quartz glass tube 6.

[0061] See also Figure 3 , 4 As shown, the inner wall of the quartz glass tube 6 is formed with a plurality of longitudinal baffles 601, which are arranged alternately and staggered. The plurality of longitudinal baffles 601 can turn the material when the quartz glass tube 6 rotates to avoid agglomeration of the material, so that the material inside the quartz glass tube 6 is heated more evenly.

[0062] When the embodiment of the present invention is used, the material to be dried or aged is placed in the quartz glass tube 6, and the rotating mechanism 5 and the heating mechanism are started. When the material inside the quartz glass tube 6 is heated, the rotating shaft of the motor 501 drives the synchronous wheel 801 to rotate through the motor 501, and the rotating synchronous wheel 801 drives the positioning wheel 8 to rotate, so that the rotating positioning wheel 8 frictionally drives the glass tube support ring 7 to rotate, and then the quartz glass tube 6 rotates. The rotating quartz glass tube 6 cooperates with a plurality of longitudinal baffles 601 to turn the material to prevent the material from agglomerating, so that the material inside the quartz glass tube 6 is heated more evenly. When the aging or drying operation is completed, the piston rod of the cylinder 401 is extended, and the open end of the quartz glass tube 6 is tilted downward to facilitate material unloading.

[0063] The above shows and describes the basic principles of the present invention. The above are only preferred embodiments of the present invention and are not intended to limit the present invention. The above embodiments and descriptions in the specification are only intended to illustrate the principles of the present invention. Without departing from the scope of the present invention, any modifications, equivalent substitutions and improvements made within the spirit and scope of the present invention should be included in the protection scope of the present invention.

Claims

1. A gel aging and drying device, characterized in that include: A base support (1), wherein an assembly frame (2) is rotatably mounted on the top of the base support (1); A glass tube (6), one end of the glass tube (6) being sealed, and both ends of the glass tube (6) being provided with glass tube support rings (7); a fixing mechanism, the fixing mechanism being arranged on the glass tube supporting ring (7), the fixing mechanism fixing the glass tube (6) on the glass tube supporting ring (7); The glass tube support ring (7) is rotatably mounted on the assembly frame (2) via a positioning mechanism, and the positioning mechanism is arranged on the assembly frame (2); A heating mechanism, wherein the heating mechanism is sleeved on the outer wall of the quartz glass tube (6); A rotating mechanism (5), wherein the rotating mechanism (5) drives the quartz glass tube (6) to rotate; An elevation angle adjustment mechanism (4), the elevation angle adjustment mechanism (4) being arranged between the base support (1) and the assembly frame (2), and the elevation angle adjustment mechanism (4) adjusting the elevation angle of the quartz glass tube (6).

2. The gel aging and drying equipment according to claim 1, characterized in that: The positioning mechanism is provided on the front mounting frame (201) and the rear mounting frame (202) at both ends of the assembly frame (2), and comprises three positioning wheels (8) distributed in a triangular shape, the positioning wheels (8) being rotatably mounted on the assembly frame (2) via a rotating shaft, the positioning wheels (8) being provided with an annular limiting groove (802), the glass tube support ring (7) being rollingly mounted on the annular limiting groove (802), the three positioning wheels (8) being distributed in a triangular shape around the periphery of the glass tube support ring (7), and limiting the glass tube support ring (7) between the three positioning wheels (8).

3. The gel aging and drying equipment according to claim 2, characterized in that: The fixing mechanism comprises a chain (701), wherein two chains (701) are provided, and locking components are provided at both ends of the two chains (701), and the two chains (701) are fixed to the quartz glass tube (6) via the locking components, and the chains (701) are provided with fastening components for fixing the chains (701) to the glass tube support ring (7).

4. The gel aging and drying equipment according to claim 3, characterized in that: The locking assembly comprises a first mounting angle iron (702) fixed to the chain plates at both ends of the chain (701), a connecting plate (703) being fixedly connected to the first mounting angle iron (702), two connecting plates (703) located on the same side of the two chains (701) being fixedly connected via a bolt (704), and the upper end of the bolt (704) sequentially penetrates the two connecting plates (703) and is threadedly fixedly mounted with a nut.

5. The gel aging and drying equipment according to claim 4, characterized in that: The fastening assembly comprises a second mounting angle iron (705) fixed to a chain plate of the chain (701); the second mounting angle iron (705) is fixed to one side of the glass tube support ring (7) via the screw (7052); a waist hole (7051) is provided on the second mounting angle iron (7055); one end of the screw (7052) passes through the glass tube support ring (7) and the waist hole (7051) and is then threadedly fixed with a nut.

6. The gel aging and drying equipment according to claim 5, characterized in that: The rotating mechanism (5) is arranged at one end of the assembly frame (2) close to the rear mounting frame (202), and comprises a motor (501). The motor (501) is fixedly mounted on the assembly frame (2), and the rotating shafts of the two positioning wheels (8) located on the rear mounting frame (202) are fixedly connected with synchronous wheels (801). A pulley is fixedly mounted on the rotating shaft of the motor (501), and the pulley is transmission-connected to the two synchronous wheels (801) via a synchronous belt (502). The synchronous wheel (801) drives the glass tube support ring (7) to rotate in coordination with the quartz glass tube (6).

7. The gel aging and drying equipment according to claim 6, characterized in that: The heating mechanism comprises a heat-insulating sleeve (3), the heat-insulating sleeve (3) being sleeved on the outside of the quartz glass tube (6), a gap being left between the inner wall of the heat-insulating sleeve (3) and the outer wall of the quartz glass tube (6), and a ceramic sheet embedded with a plurality of heating wires being arranged in the heat-insulating sleeve (3); a support rod (203) being fixedly connected between the front mounting frame (201) and the rear mounting frame (202), a limit ring (204) being fixedly connected to the support rod (203), and the heat-insulating sleeve (3) being sleeved in the limit ring (204).

8. The gel aging and drying equipment according to claim 7, characterized in that: An anti-slip felt layer (9) is provided between the chain (701) and the quartz glass tube (6).

9. The gel aging and drying equipment according to claim 5, characterized in that: The elevation angle adjustment mechanism (4) comprises a cylinder (401), a lower hinge seat (402) is fixedly connected to the base bracket (1), an upper hinge seat (403) is fixedly connected to the bottom of one end of the assembly frame (2) close to the motor (501), the lower end of the cylinder (401) is rotatably connected to the lower hinge seat (402), and the upper end of the piston rod of the cylinder (401) is rotatably connected to the upper hinge seat (403).

10. The gel aging and drying equipment according to claim 1, characterized in that: The inner wall of the quartz glass tube (6) is formed with a plurality of longitudinal baffles (601), and the plurality of longitudinal baffles (601) are arranged in a staggered and alternating manner.

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