Production process capable of improving strength and heat-conducting property of graphite material
By using specific components and rotary structures in graphite impregnation technology, the problems of uneven distribution of impregnation liquid and safety risks are solved, the thermal conductivity and mechanical strength of graphite are improved, and a safer and more efficient impregnation process is achieved.
Patent Information
- Application Number
- CN202411258386.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-09
- Publication Date
- 2024-12-13
AI Technical Summary
In the existing graphite impregnation technology, the impregnation liquid is stirred by the circular limit frame, causing the preheating furnace to surge, the sun gear loses the limit, and the circular limit frame rotates, which drives the square block to rotate, resulting in inconvenient use of the device and safety risks. , affect the experience.
The impregnation liquid containing components such as MgCl2, Al(OH)3, H3PO4 is used to enhance the thermal conductivity of graphite, and a protective layer is formed by soaking, pressurizing, relieving and baking in a high-pressure storage tank, combining with the rotating structure and stirring structure to ensure uniform distribution of impregnation liquid, avoid precipitation and layering, and improve the mechanical strength and thermal conductivity of graphite.
It effectively improves the thermal conductivity and mechanical strength of graphite materials, ensures uniform distribution of impregnation liquid, avoids safety risks and user experience issues during the use of the device, and improves the overall performance of graphite products.
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Figure CN119118120A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of graphite production, and in particular to a production process capable of improving the strength and thermal conductivity of graphite materials. Background Art
[0002] In the graphite production process, the graphite material needs to be impregnated, and the impregnation furnace needs to be pressurized and heated, and then the preheated product is placed in the impregnation tank for impregnation. Most of the current graphite impregnation technologies maintain the uniformity of the impregnation liquid by stirring the impregnation liquid to prevent precipitation or stratification of components, thereby ensuring that the graphite is evenly exposed to the impregnation during the entire impregnation process.
[0003] In this regard, China's patent application number: CN202410676795.1 discloses a graphite electrode impregnation preheating furnace, including a furnace shell, a preheating furnace body is arranged inside the furnace shell, an annular heating plate is fixedly connected to the outer wall of the preheating furnace body, the annular heating plate is in contact with the furnace shell, an outer ring plate is fixedly connected to the top of the outer wall of the furnace shell, a fixed plate is fixedly connected to the bottom of the inner wall of the furnace shell, a rotating mechanism is arranged on the preheating furnace body, and a separation and combination mechanism is arranged on the furnace shell and the fixed plate; the invention can prevent cracks and damage to high-power graphite electrodes, improve the service life of high-power graphite electrodes, and make the impregnation liquid evenly distributed on the surface of the high-power graphite electrode, prevent the impregnation liquid from settling, improve the impregnation uniformity, and avoid damage or breakage of the high-power graphite electrode and damage to the preheating furnace body.
[0004] The device is provided with a detachable square block and a square slot, which can prevent the rotating mechanism from injuring people when placing materials. However, in actual use, the impregnation liquid is stirred by the circular limit frame and surges in the preheating furnace body. After the preheating furnace body rises, the sun gear loses its limit, so the circular limit frame is in an active state. Under the push of the impregnation liquid, the circular limit frame will rotate, and there is still a risk of injury from the rotating mechanism. In addition, the circular limit frame will drive the sun gear and the square block to rotate, causing the square block to shift relative to the square slot. When the preheating furnace body descends, the square block cannot be inserted into the square slot, resulting in the inability to connect the sun gear and the second drive shaft, which affects the user experience of the device.
[0005] Therefore, in order to solve the above problems, a production process is proposed to improve the strength and thermal conductivity of graphite materials. Summary of the invention
[0006] The object of the present invention is to provide a production process that can improve the strength and thermal conductivity of graphite materials, so as to solve the problem that the device in the prior art proposed in the above background technology can avoid the rotating mechanism from injuring people when placing materials by setting a detachable square block and a square groove. However, in actual use, the impregnation liquid will surge in the preheating furnace body due to the stirring of the circular limit frame. After the preheating furnace body is raised, the sun gear loses its limit, so the circular limit frame is in an active state. Under the push of the impregnation liquid, the circular limit frame will rotate, and there is still a risk of injury from the rotating mechanism. In addition, the circular limit frame will drive the sun gear and the square block to rotate, so that the square block is offset relative to the angle of the square groove. When the preheating furnace body descends, the square block cannot be inserted into the square groove, resulting in the inability to connect the sun gear and the second drive shaft, which will affect the user experience of the device.
[0007] To achieve the above object, the present invention provides the following technical solution: A graphite material capable of improving the strength of graphite equipment:
[0008] S1. Use an impregnation solution containing MgCl2, Al(OH)3, H3PO4 and other components. These substances react with graphite at high temperatures to form compounds with higher thermal conductivity, thereby enhancing the thermal conductivity of graphite. Similarly, impregnation solutions containing borax, sodium tripolyphosphate and TiO2 also show good improvement effects. The protective layer formed by these components on the graphite surface not only improves the high-temperature oxidation resistance, but also enhances the thermal conductivity to a certain extent. The processed ordinary graphite products are completely immersed in the impregnation solution in the high-pressure storage tank;
[0009] S2. Release the pressure in the high-pressure storage tank to normal pressure, take out the graphite product and immerse it in water;
[0010] S3. Take out the graphite product, wipe off the surface moisture, immerse it in the impregnation liquid storage tank again, and pressurize the impregnation liquid storage tank;
[0011] S4. Release the pressure of the impregnation liquid storage tank to normal pressure, take out the graphite product and let it stand at room temperature for 4 hours to solidify the impregnation liquid in the graphite product; then wipe the resin precipitated on the surface of the graphite product with an organic reagent;
[0012] S5. The impregnated graphite products were baked at 31-39°C, 71-79°C and 111-119°C for 6h, 6h and 12h, respectively, and the temperature was slowly raised to allow the impregnation liquid to completely solidify and fill the micropores;
[0013] S6. Then, the sepiolite powder is filled into the micropores of the graphite product, and the product is naturally dried and subjected to low temperature heat treatment (100-150°C), thereby increasing the mechanical strength of the graphite and improving its original thermal conductivity.
[0014] A production process capable of improving the strength and thermal conductivity of graphite materials, comprising: a cylinder, an electric telescopic rod is installed on the rear wall of the cylinder, a motor is fixedly connected to the extended end of the electric telescopic rod, and a top cover is fixedly connected to the output end of the motor;
[0015] The bottom surface of the top cover is rotatably connected with a rotating pad;
[0016] A rotating structure is installed on the inner side of the cylinder, and the rotating structure includes a fixed plate, which is fixedly installed on the inner bottom of the cylinder, a motor is installed on the bottom surface of the fixed plate, an output end of the fixed plate is fixedly connected to a positioning plate, a top surface of the positioning plate is fixedly connected to a plug rod, a top surface of the fixed plate is fixedly connected to a first spring, a top end of the first spring is fixedly connected to a gear ring plate, and the top surface of the gear ring plate is rotatably connected to an impregnation cylinder via a bearing.
[0017] Preferably, a stirring structure is installed on the inner side of the cylinder body, and the stirring structure includes a rotating block, which is rotatably installed on the inner bottom surface of the immersion cylinder, and the top surface of the rotating block is fixedly connected to a placement net cylinder, and a stirring blade is rotatably installed on the top surface of the rotating block, and a movable groove is opened on the bottom surface of the stirring blade, and a first rubber pad is provided on the inner side of the movable groove, and a gear shaft is fixedly connected to the bottom surface of the rotating block, and a lifting frame is slidably installed on the inner side of the movable groove, and a second rubber pad is provided on the top surface of the lifting frame, and a connecting rod is fixedly connected to the bottom surface of the lifting frame, and a second spring is fixedly connected to the outer side of the upper end of the connecting rod, and a positioning frame is fixedly installed on the upper end of the inner wall of the immersion cylinder.
[0018] Preferably, an alignment structure is installed on the inner side of the stirring structure, and the alignment structure includes a connecting shaft, the connecting shaft is fixedly connected to the bottom surface of the impregnation cylinder, a gear plate is fixedly connected to the outer wall of the connecting shaft, a slot is provided on the bottom surface of the connecting shaft, a third spring is fixedly connected to the inner top surface of the slot, a connecting arm is fixedly connected to the bottom end of the third spring, and a positioning rod is fixedly connected to the bottom of the outer wall of the connecting shaft.
[0019] Preferably, the bottom surface of the rotating pad is fitted with the top surface of the impregnation cylinder, the output end of the motor passes through the fixed plate, the positioning plate and the insertion rod are both located on the upper side of the fixed plate, the insertion rod is inserted into the slot, and the gear ring plate is slidably mounted on the inner wall of the cylinder.
[0020] Preferably, the rotating block is provided with four groups, four groups of stirring blades are installed on the rotating block, the placement net cylinder is located on the inner side of the four groups of stirring blades, the upper ends of the stirring blades are rotatably connected to the positioning frame, and the four groups of gear shafts are all engaged with the gear plate.
[0021] Preferably, the bottom end of the lifting frame is movably mounted on the inner side of the rotating block, the second rubber pad cooperates with the first rubber pad, the bottom end of the connecting rod is fixedly connected to the connecting arm, and one end of the second spring is fixedly connected to the inner wall of the rotating block.
[0022] Preferably, the connecting arm is in a cross shape, the connecting arm passes through the side wall of the connecting shaft, and the connecting arm is slidably installed on the inner side of the slot.
[0023] Preferably, the slot is matched with the insertion rod, and the bottom end of the positioning rod passes through the positioning plate.
[0024] Compared with the prior art, the beneficial effects of the present invention are as follows: the stirring blades of the present invention can remain fixedly connected to the rotating block when the impregnation cylinder descends, so that the stirring blades can be driven to rotate by the rotating block to stir the impregnation liquid inside the cylinder body, and when the impregnation cylinder is raised, the stirring blades can rotate on the rotating block, so that the action of the impregnation liquid on the stirring blades cannot be transmitted to the rotating block, so that the rotating block remains fixed, and the placed net cylinder is fixed in place, which is convenient for taking and placing materials in the placed net cylinder, thereby improving the safety of the use of the device.
[0025] A rotating structure, a stirring structure and a stirring structure are provided. The insertion rod is inserted into the slot. When the motor is started, the connecting shaft and the gear plate can be driven to rotate through the insertion rod. The gear plate is meshed with the gear shaft. The rotation of the gear plate can drive the rotating block to rotate through the gear shaft. The second rubber pad abuts against the bottom surface of the first rubber pad. The stirring blade can be fixed to the top surface of the rotating block through the lifting frame. Therefore, when the rotating block rotates, the impregnation liquid in the impregnation cylinder can be stirred by the stirring blade to avoid precipitation and stratification of the impregnation liquid, thereby ensuring the impregnation effect of the graphite. The rotation of the connecting shaft drives the impregnation cylinder to rotate, which can further stir the impregnation liquid.
[0026] When the electric telescopic rod is started to lift the top cover, the top cover releases the limit of the impregnation cylinder, and the impregnation cylinder is lifted in the cylinder body under the action of the first spring, the gear ring plate drives the impregnation cylinder to lift, and the impregnation cylinder drives the connecting shaft and the connecting rod to move, and the connecting shaft moves upward away from the insertion rod, the insertion rod is separated from the slot, and the connecting arm loses the abutment of the insertion rod, and the connecting arm descends in the slot under the action of the third spring, and the connecting arm drives the connecting rod to move inside the rotating block, and the connecting rod pulls the lifting frame, and the lifting frame squeezes the second spring, and the lifting frame moves in the movable groove, and the lifting frame drives the second rubber pad to descend, and the second rubber pad is away from the first rubber pad, and the friction relationship between the second rubber pad and the first rubber pad can be released, so the stirring blade can rotate on the rotating block, and at this time, when the impregnation liquid flowing in the impregnation cylinder acts on the stirring blade, it can drive the stirring blade to rotate, and at this time, the rotation of the stirring blade will not drive the rotating block to move, so the rotating block can remain fixed, and the placement net cylinder is fixed in place, which is convenient for taking and placing materials in the placement net cylinder, thereby improving the safety of the device;
[0027] At the same time, when the connecting shaft moves upward away from the insertion rod, it can drive the positioning rod to move. The positioning rod rises on the inner side of the positioning plate, so that the angles of the slot and the insertion rod are relatively fixed, thereby preventing the connecting shaft from rotating after the impregnation cylinder is raised, causing the angle of the slot to shift, and making it impossible for the slot and the insertion rod to be aligned when the impregnation cylinder is reset downward, thereby affecting the driving effect of the motor on the impregnation cylinder and the stirring blades. BRIEF DESCRIPTION OF THE DRAWINGS
[0028] Figure 1 It is a schematic front view of the structure of the present invention;
[0029] Figure 2 It is a schematic front cross-sectional view of the structure of the cylinder of the present invention;
[0030] Figure 3 It is a schematic front view of the structure of the rotating structure of the present invention;
[0031] Figure 4 It is a bottom view schematic diagram of the structure of the gear ring plate of the present invention;
[0032] Figure 5 It is a schematic top view of the structure of the positioning plate of the present invention;
[0033] Figure 6 It is a schematic front cross-sectional view of the structure of the impregnation cylinder of the present invention;
[0034] Figure 7 It is a schematic front view of the structure of the stirring structure of the present invention;
[0035] Figure 8 It is a front cross-sectional schematic diagram of the structure of the rotating block and the movable groove of the present invention;
[0036] Fig. 9 It is a schematic side cross-sectional view of the alignment structure of the present invention.
[0037] In the figure: 1. cylinder; 11. electric telescopic rod; 12. motor; 13. top cover; 14. rotating pad; 2. rotating structure; 21. fixed plate; 22. motor; 23. positioning plate; 24. plug rod; 25. first spring; 26. gear ring plate; 27. bearing; 28. impregnation cylinder; 3. stirring structure; 31. rotating block; 32. placing net cylinder; 33. stirring blade; 34. movable groove; 35. first rubber pad; 36. gear shaft; 37. lifting frame; 38. second rubber pad; 39. connecting rod; 310. second spring; 311. positioning frame; 4. alignment structure; 41. connecting shaft; 42. gear plate; 43. slot; 44. third spring; 45. connecting arm; 46. positioning rod. DETAILED DESCRIPTION
[0038] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0039] See also Figure 1-Figure 9 , an embodiment provided by the present invention:
[0040] The barrel 1, electric telescopic rod 11, motor 12, motor 22 and impregnation barrel 28 used in the present application are products that can be directly purchased on the market. Their principles and connection methods are existing technologies well known to those skilled in the art, so they will not be repeated here.
[0041] A graphite material that can improve the strength of graphite equipment:
[0042] S1. Use an impregnation solution containing MgCl2, Al(OH)3, H3PO4 and other components. These substances react with graphite at high temperatures to form compounds with higher thermal conductivity, thereby enhancing the thermal conductivity of graphite. Similarly, impregnation solutions containing borax, sodium tripolyphosphate and TiO2 also show good improvement effects. The protective layer formed by these components on the graphite surface not only improves the high-temperature oxidation resistance, but also enhances the thermal conductivity to a certain extent. The processed ordinary graphite products are completely immersed in the impregnation solution in the high-pressure storage tank;
[0043] S2. Release the pressure in the high-pressure storage tank to normal pressure, take out the graphite product and immerse it in water;
[0044] S3. Take out the graphite product, wipe off the surface moisture, immerse it in the impregnation liquid storage tank again, and pressurize the impregnation liquid storage tank;
[0045] S4. Release the pressure of the impregnation liquid storage tank to normal pressure, take out the graphite product and let it stand at room temperature for 4 hours to solidify the impregnation liquid in the graphite product; then wipe the resin precipitated on the surface of the graphite product with an organic reagent;
[0046] S5. The impregnated graphite products were baked at 31-39°C, 71-79°C and 111-119°C for 6h, 6h and 12h, respectively, and the temperature was slowly raised to allow the impregnation liquid to completely solidify and fill the micropores;
[0047] S6. Then, the sepiolite powder is filled into the micropores of the graphite product, and the product is naturally dried and subjected to low temperature heat treatment (100-150°C), thereby increasing the mechanical strength of the graphite and improving its original thermal conductivity.
[0048] A production process capable of improving the strength and thermal conductivity of graphite materials, comprising: a cylinder 1, an electric telescopic rod 11 is installed on the rear wall of the cylinder 1, a motor 12 is fixedly connected to the extended end of the electric telescopic rod 11, and a top cover 13 is fixedly connected to the output end of the motor 12;
[0049] The bottom surface of the top cover 13 is rotatably connected with a rotating pad 14;
[0050] A rotating structure 2 is installed on the inner side of the cylinder 1, and the rotating structure 2 includes a fixed plate 21, which is fixedly installed on the inner bottom of the cylinder 1, and a motor 22 is installed on the bottom surface of the fixed plate 21. A positioning plate 23 is fixedly connected to the output end of the fixed plate 21, and a plug rod 24 is fixedly connected to the top surface of the positioning plate 23. A first spring 25 is fixedly connected to the top surface of the fixed plate 21, and a gear ring plate 26 is fixedly connected to the top of the first spring 25. The top surface of the gear ring plate 26 is rotatably connected to an impregnation cylinder 28 through a bearing 27. The fixed plate 21 can drive the positioning plate 23 and the plug rod 24 to rotate, and the gear ring plate 26 can move up and down on the top surface of the fixed plate 21 through the first spring 25, and the impregnation cylinder 28 can rotate on the top surface of the gear ring plate 26 through the bearing 27.
[0051] Further, a stirring structure 3 is installed on the inner side of the cylinder 1, and the stirring structure 3 includes a rotating block 31, which is rotatably installed on the inner bottom surface of the impregnation cylinder 28, and a net cylinder 32 is fixedly connected to the top surface of the rotating block 31, and a stirring blade 33 is rotatably installed on the top surface of the rotating block 31. A movable groove 34 is provided on the bottom surface of the stirring blade 33, and a first rubber pad 35 is provided on the inner side of the movable groove 34. A gear shaft 36 is fixedly connected to the bottom surface of the rotating block 31, and a lifting frame 37 is slidably installed on the inner side of the movable groove 34. A second rubber pad 38 is provided on the top surface of the lifting frame 37, and a connecting rod 39 is fixedly connected to the bottom surface of the lifting frame 37. A second spring 310 is fixedly connected to the outer side of the upper end, and a positioning frame 311 is fixedly installed on the upper end of the inner wall of the impregnation cylinder 28. The stirring blade 33 can remain fixedly connected to the rotating block 31 when the impregnation cylinder 28 descends, so that the stirring blade 33 is driven to rotate by the rotating block 31 to stir the impregnation liquid inside the cylinder body 1, and when the impregnation cylinder 28 rises, the stirring blade 33 can rotate on the rotating block 31, so that the action of the impregnation liquid on the stirring blade 33 cannot be transmitted to the rotating block 31, so that the rotating block 31 remains fixed, and the placement net cylinder 32 is fixed in place, which is convenient for taking and placing materials in the placement net cylinder 32, thereby improving the safety of the device.
[0052] Furthermore, an alignment structure 4 is installed on the inner side of the stirring structure 3, and the alignment structure 4 includes a connecting shaft 41, which is fixedly connected to the bottom surface of the impregnation cylinder 28, and a gear plate 42 is fixedly connected to the outer wall of the connecting shaft 41. A slot 43 is provided on the bottom surface of the connecting shaft 41, and a third spring 44 is fixedly connected to the inner top surface of the slot 43, and a connecting arm 45 is fixedly connected to the bottom end of the third spring 44. A positioning rod 46 is fixedly connected to the bottom of the outer wall of the connecting shaft 41. The rotation of the insertion rod 24 can drive the stirring structure 3 to operate through the alignment structure 4, and the connecting arm 45 can be raised and lowered in the slot 43 through the third spring 44, and the connecting shaft 41 can drive the positioning rod 46 to move.
[0053] Furthermore, the bottom surface of the rotating pad 14 is fitted with the top surface of the impregnation cylinder 28, the output end of the motor 22 passes through the fixed plate 21, the positioning plate 23 and the insertion rod 24 are both located on the upper side of the fixed plate 21, the insertion rod 24 is inserted into the inside of the slot 43, and the gear ring plate 26 is slidably installed on the inner wall of the cylinder 1. The rotating pad 14 can rotate on the bottom surface of the top cover 13 when the impregnation cylinder 28 rotates, the insertion rod 24 can drive the connecting shaft 41 and the gear plate 42 to rotate through the slot 43, and the gear ring plate 26 can stably rise and fall in the cylinder 1.
[0054] Furthermore, the rotating block 31 is provided with four groups, and four groups of stirring blades 33 are installed on the rotating block 31. The mesh cylinder 32 is placed on the inner side of the four groups of stirring blades 33. The upper end of the stirring blade 33 is rotatably connected to the positioning frame 311. The four groups of gear shafts 36 are all engaged with the gear plate 42. The four groups of stirring blades 33 can stir the impregnation liquid near the rotating block 31 to avoid precipitation and stratification of the impregnation liquid, thereby ensuring the impregnation effect of the graphite. The rotation of the gear plate 42 can drive the rotation of the four groups of gear shafts 36.
[0055] Furthermore, the bottom end of the lifting frame 37 is movably mounted on the inner side of the rotating block 31, the second rubber pad 38 cooperates with the first rubber pad 35, the bottom end of the connecting rod 39 is fixedly connected to the connecting arm 45, one end of the second spring 310 is fixedly connected to the inner wall of the rotating block 31, and when the second rubber pad 38 is in contact with the first rubber pad 35, the stirring blade 33 can be fixed on the rotating block 31, and when the rotating block 31 rotates, the immersion liquid can be stirred by the stirring blade 33, and when the second rubber pad 38 is separated from the first rubber pad 35, the movement of the immersion liquid can push the stirring blade 33 to rotate, so that the rotating block 31 is fixed, and the movement of the connecting arm 45 can drive the lifting frame 37 to move through the connecting rod 39, and the second spring 310 provides power for the movement of the lifting frame 37 in the rotating block 31.
[0056] Furthermore, the connecting arm 45 is in a "cross" shape, and the connecting arm 45 passes through the side wall of the connecting shaft 41. The connecting arm 45 is slidably installed on the inner side of the slot 43. The movement of the connecting arm 45 on the inner side of the slot 43 can drive the movement of the four groups of connecting rods 39.
[0057] Furthermore, the slot 43 is adapted to the insertion rod 24, and the bottom end of the positioning rod 46 passes through the positioning plate 23. The slot 43 is aligned with the insertion rod 24 at an angle. When the impregnation cylinder 28 descends, the insertion rod 24 can be straightly inserted into the slot 43. The positioning rod 46 cooperates with the positioning plate 23 to limit the angle between the slot 43 and the insertion rod 24, thereby preventing the impregnation cylinder 28 from driving the connecting shaft 41 to rotate, causing the slot 43 and the insertion rod 24 to deviate, resulting in the inability to insert the insertion rod 24 into the slot 43.
[0058] Working principle: When in use, start the electric telescopic rod 11 to lift the top cover 13, start the motor 12 to drive the top cover 13 to rotate, move the top cover 13 to the outside of the cylinder 1, so as to place the material inside the net cylinder 32, and then control the electric telescopic rod 11 and the motor 12 to cover the top surface of the cylinder 1;
[0059] The plug rod 24 is inserted into the slot 43, and the motor 22 is started. The plug rod 24 can drive the connecting shaft 41 and the gear plate 42 to rotate. The gear plate 42 is meshed with the gear shaft 36. The rotation of the gear plate 42 can drive the rotating block 31 to rotate through the gear shaft 36. The second rubber pad 38 abuts against the bottom surface of the first rubber pad 35. The stirring blade 33 can be fixed to the top surface of the rotating block 31 through the lifting frame 37. Therefore, when the rotating block 31 rotates, the stirring blade 33 can stir the impregnation liquid in the impregnation cylinder 28 to avoid precipitation and stratification of the impregnation liquid, thereby ensuring the impregnation effect of the graphite. The rotation of the connecting shaft 41 drives the impregnation cylinder 28 to rotate, which can further stir the impregnation liquid.
[0060] The electric telescopic rod 11 is started to lift the top cover 13, and the top cover 13 releases the limit on the dipping cylinder 28. The dipping cylinder 28 rises in the cylinder body 1 under the action of the first spring 25, and the gear ring plate 26 drives the dipping cylinder 28 to rise. The dipping cylinder 28 drives the connecting shaft 41 and the connecting rod 39 to move, and the connecting shaft 41 moves upward away from the insertion rod 24, and the insertion rod 24 is separated from the slot 43, and the connecting arm 45 loses the abutment of the insertion rod 24. The connecting arm 45 descends in the slot 43 under the action of the third spring 44, and the connecting arm 45 drives the connecting rod 39 to move inside the rotating block 31, and the connecting rod 39 pulls the lifting frame 37, and the lifting frame 37 squeezes the second spring 31. 0, the lifting frame 37 moves in the movable groove 34, and the lifting frame 37 drives the second rubber pad 38 to descend, and the second rubber pad 38 moves away from the first rubber pad 35, so that the friction relationship between the second rubber pad 38 and the first rubber pad 35 can be released, so the stirring blade 33 can rotate on the rotating block 31. At this time, when the impregnation liquid flowing in the impregnation cylinder 28 acts on the stirring blade 33, it can drive the stirring blade 33 to rotate. At this time, the rotation of the stirring blade 33 will not drive the rotating block 31 to move, so the rotating block 31 can remain fixed, and the placement net cylinder 32 is fixed in place, which is convenient for taking and placing materials in the placement net cylinder 32, thereby improving the safety of the device;
[0061] At the same time, when the connecting shaft 41 moves upward away from the insertion rod 24, it can drive the positioning rod 46 to move. The positioning rod 46 rises on the inner side of the positioning plate 23, so that the angles of the slot 43 and the insertion rod 24 are relatively fixed, thereby preventing the connecting shaft 41 from rotating after the immersion cylinder 28 is raised, causing the angle of the slot 43 to shift, and making it impossible for the slot 43 and the insertion rod 24 to be aligned when the immersion cylinder 28 is reset downward, thereby affecting the driving effect of the motor 22 on the immersion cylinder 28 and the stirring blade 33.
[0062] The above description is only a preferred embodiment of the present invention and does not limit the present invention in any form. Any ordinary technician in the industry can smoothly implement the present invention as shown in the drawings and described above. However, any equivalent changes, modifications and evolutions made by technicians familiar with the profession without departing from the scope of the technical solution of the present invention using the technical content disclosed above are all equivalent embodiments of the present invention. At the same time, any equivalent changes, modifications and evolutions made to the above embodiments based on the essential technology of the present invention are still within the protection scope of the technical solution of the present invention.
Claims
1. A production process for improving the strength and thermal conductivity of graphite materials, characterized in that: S1. Use an impregnation solution containing MgCl2, Al(OH)3, H3PO4 and other components. These substances react with graphite at high temperatures to form compounds with higher thermal conductivity, thereby enhancing the thermal conductivity of graphite. Similarly, impregnation solutions containing borax, sodium tripolyphosphate and TiO2 also show good improvement effects. The protective layer formed by these components on the graphite surface not only improves the high-temperature oxidation resistance, but also enhances the thermal conductivity to a certain extent. The processed ordinary graphite products are completely immersed in the impregnation solution in the high-pressure storage tank; S2. Release the pressure in the high-pressure storage tank to normal pressure, take out the graphite product and immerse it in water; S3. Take out the graphite product, wipe off the surface moisture, immerse it in the impregnation liquid storage tank again, and pressurize the impregnation liquid storage tank; S4. Release the pressure of the impregnation liquid storage tank to normal pressure, take out the graphite product and let it stand at room temperature for 4 hours to solidify the impregnation liquid in the graphite product; then wipe the resin precipitated on the surface of the graphite product with an organic reagent; S5. The impregnated graphite products were baked at 31-39°C, 71-79°C and 111-119°C for 6h, 6h and 12h, respectively, and the temperature was slowly increased to completely solidify the impregnation liquid and fill the micropores; S6. Then, the sepiolite powder is filled into the micropores of the graphite product, and the product is naturally dried and subjected to low temperature heat treatment (100-150°C), thereby increasing the mechanical strength of the graphite and improving its original thermal conductivity.
2. A production process for improving the strength and thermal conductivity of graphite materials, comprising: A cylinder (1), wherein an electric telescopic rod (11) is mounted on the rear wall of the cylinder (1), the extended end of the electric telescopic rod (11) is fixedly connected to a motor (12), and the output end of the motor (12) is fixedly connected to a top cover (13); Features: The bottom surface of the top cover (13) is rotatably connected to a rotating pad (14); A rotating structure (2) is installed on the inner side of the cylinder (1), and the rotating structure (2) comprises a fixed plate (21), the fixed plate (21) is fixedly installed on the inner bottom of the cylinder (1), a motor (22) is installed on the bottom surface of the fixed plate (21), an output end of the fixed plate (21) is fixedly connected to a positioning plate (23), a top surface of the positioning plate (23) is fixedly connected to an insertion rod (24), a top surface of the fixed plate (21) is fixedly connected to a first spring (25), a top end of the first spring (25) is fixedly connected to a toothed ring plate (26), and a top surface of the toothed ring plate (26) is rotatably connected to an impregnation cylinder (28) via a bearing (27).
3. A production process for improving the strength and thermal conductivity of graphite materials according to claim 2, characterized in that: A stirring structure (3) is installed on the inner side of the cylinder (1), and the stirring structure (3) comprises a rotating block (31), the rotating block (31) is rotatably installed on the inner bottom surface of the impregnation cylinder (28), the top surface of the rotating block (31) is fixedly connected with a placement net cylinder (32), the top surface of the rotating block (31) is rotatably installed with a stirring blade (33), the bottom surface of the stirring blade (33) is provided with a movable groove (34), and the inner side of the movable groove (34) is provided with a first rubber The bottom surface of the rotating block (31) is fixedly connected to a gear shaft (36), a lifting frame (37) is slidably mounted on the inner side of the movable groove (34), a second rubber pad (38) is arranged on the top surface of the lifting frame (37), a connecting rod (39) is fixedly connected to the bottom surface of the lifting frame (37), a second spring (310) is fixedly connected to the outer side of the upper end of the connecting rod (39), and a positioning frame (311) is fixedly mounted on the upper end of the inner wall of the impregnation cylinder (28).
4. A production process for improving the strength and thermal conductivity of graphite materials according to claim 3, characterized in that: An alignment structure (4) is installed inside the stirring structure (3), and the alignment structure (4) comprises a connecting shaft (41), the connecting shaft (41) is fixedly connected to the bottom surface of the impregnation cylinder (28), a gear plate (42) is fixedly connected to the outer wall of the connecting shaft (41), a slot (43) is provided on the bottom surface of the connecting shaft (41), a third spring (44) is fixedly connected to the inner top surface of the slot (43), a connecting arm (45) is fixedly connected to the bottom end of the third spring (44), and a positioning rod (46) is fixedly connected to the bottom of the outer wall of the connecting shaft (41).
5. A production process for improving the strength and thermal conductivity of graphite materials according to claim 2, characterized in that: The bottom surface of the rotating pad (14) is in contact with the top surface of the impregnation cylinder (28); the output end of the motor (22) passes through the fixed plate (21); the positioning plate (23) and the insertion rod (24) are both located on the upper side of the fixed plate (21); the insertion rod (24) is inserted into the inside of the slot (43); and the gear ring plate (26) is slidably mounted on the inner wall of the cylinder (1).
6. A production process for improving the strength and thermal conductivity of graphite materials according to claim 3, characterized in that: The rotating block (31) is provided with four groups, and four groups of stirring blades (33) are installed on the rotating block (31). The placement net cylinder (32) is located inside the four groups of stirring blades (33). The upper ends of the stirring blades (33) are rotatably connected to the positioning frame (311), and the four groups of gear shafts (36) are all meshed with the gear plate (42).
7. A production process for improving the strength and thermal conductivity of graphite materials according to claim 3, characterized in that: The bottom end of the lifting frame (37) is movably mounted on the inner side of the rotating block (31), the second rubber pad (38) cooperates with the first rubber pad (35), the bottom end of the connecting rod (39) is fixedly connected to the connecting arm (45), and one end of the second spring (310) is fixedly connected to the inner wall of the rotating block (31).
8. A production process for improving the strength and thermal conductivity of graphite materials according to claim 4, characterized in that: The connecting arm (45) is in a "cross" shape, and the connecting arm (45) passes through the side wall of the connecting shaft (41). The connecting arm (45) is slidably mounted on the inner side of the slot (43).
9. A production process for improving the strength and thermal conductivity of graphite materials according to claim 4, characterized in that: The slot (43) is matched with the insertion rod (24), and the bottom end of the positioning rod (46) passes through the positioning plate (23).
Citation Information
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