Method for continuously collecting 2-chloropropane from halogenated hydrocarbon and control device

By performing a reflux reaction in the continuous acquisition of 2-chloropropane in halogenated hydrocarbons and controlling the injection ratio of hydrogen chloride and isopropanol by using a flow control device, the problem of difficult control of the injection ratio of hydrogen chloride and isopropanol in the prior art is solved, and the problem of the difficulty in controlling the injection ratio of hydrogen chloride and isopropanol in the prior art is improved. The extraction efficiency and finished product quality of 2-chloropropane are obtained.

CN119143568APending Publication Date: 2024-12-17JIANGXI KEYUAN BIOPHARM
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Patent Information

Application Number
CN202411044086.8
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-07-31
Publication Date
2024-12-17

AI Technical Summary

Technical Problem

In the existing continuous extraction of 2-chloropropane by halogenated hydrocarbons, the injection ratio of hydrogen chloride and isopropanol is difficult to control in a timely manner, resulting in limited extraction efficiency.

Method used

A method for continuously harvesting 2-chloropropane of halogenated hydrocarbons is designed. By performing a reflux reaction in an enamel reactor, and using a flow control device to control the injection ratio of hydrogen chloride and isopropanol, combined with a control device to ensure the balance of flow, including A belt is used to connect the first and second wheel bodies to adjust the valve pipe flow rate to ensure the stable proportion of the material in the reactor.

Benefits of technology

Through continuous reflux reaction and distillation treatment, the extraction efficiency of 2-chloropropane is significantly improved, ensuring the quality and reaction effect of the finished product.

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Abstract

The invention relates to the technical field of chemical engineering, in particular to a method for continuously collecting 2-chloropropane from halogenated hydrocarbon and a control device, and the control device comprises a communication mechanism and a control mechanism arranged on the communication mechanism; the communicating mechanism comprises a first valve pipe and a second valve pipe, and the first valve pipe and the second valve pipe are connected through a containing box. The control mechanism comprises a round box arranged on the containing box, a conduction assembly arranged in the round box and a movable assembly arranged on the conduction assembly, the first wheel body and the second wheel body can be effectively connected through the arrangement of the belt, the belt is driven to rotate in the rotating process of the second wheel body, and therefore the first wheel body and the second wheel body can be effectively connected; the first wheel body can rotate along with the second wheel body in the process of rotating the second wheel body, the flow difference between the first wheel body and the second wheel body is prevented from being too large, the other valve body is adjusted along with the single valve body when the single valve body is adjusted, and the situation that the reaction effect is affected due to the too large proportion difference of materials introduced into the enamel rectifying still at the same time is avoided.
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Description

Technical Field

[0001] The invention relates to the technical field of chemical engineering, in particular to a method and a control device for continuously collecting 2-chloropropane from halogenated hydrocarbons. Background Art

[0002] The continuous reaction method of halogenated hydrocarbons is very important in organic synthesis, especially in the formation of new carbon-carbon bonds. Transition metal-catalyzed coupling reactions are one of the effective methods for constructing carbon-carbon bonds, among which palladium-catalyzed coupling reactions are particularly favored because of their mild reaction conditions and excellent efficiency.

[0003] The existing continuous extraction of 2-chloropropane by halogenated hydrocarbons has limited extraction efficiency, so we designed a method for continuous collection of 2-chloropropane by halogenated hydrocarbons;

[0004] When continuously extracting 2-chloropropane, hydrogen chloride and isopropanol need to be injected into the enameled reactor in equal proportions. The flow rate needs to be controlled according to the amount of solution inside the enameled reactor tower. However, hydrogen chloride and isopropanol are injected through two pipes. When the flow rate of one pipe changes, the change of the other pipe cannot be updated in time, which will cause the injection ratio to change. Therefore, we designed a control device. Summary of the invention

[0005] The purpose of this section is to summarize some aspects of embodiments of the present invention and briefly introduce some preferred embodiments. Some simplifications or omissions may be made in this section and the specification abstract and the invention title of this application to avoid blurring the purpose of this section, the specification abstract and the invention title, and such simplifications or omissions cannot be used to limit the scope of the present invention.

[0006] In view of the problems that the above-mentioned or prior art methods for continuously collecting 2-chloropropane from halogenated hydrocarbons and control devices for continuously extracting 2-chloropropane have limited extraction efficiency and it is difficult to control the injection ratio of hydrogen chloride and isopropanol, the present invention is proposed.

[0007] Therefore, the object of the present invention is to provide a method and a control device for continuously collecting 2-chloropropane from halogenated hydrocarbons.

[0008] In order to solve the above technical problems, the present invention provides the following technical solutions: a method for continuously collecting 2-chloropropane from halogenated hydrocarbons, comprising introducing a hydrochloric acid solution and isopropanol into an enameled reactor, performing a reflux reaction, and collecting a crude 2-chloropropane product; introducing hydrogen chloride and isopropanol into the enameled reactor through a flow control device; continuing the reflux reaction; continuously collecting the crude 2-chloropropane product from the top discharge layer of the enameled reactor; and obtaining 2-chloropropane by treating the crude 2-chloropropane product.

[0009] As a preferred embodiment of the method for continuously collecting 2-chloropropane from halogenated hydrocarbons of the present invention, the temperature of the reflux reaction is controlled at 85°C to 87°C, and hydrogen chloride and isopropanol are introduced when the reflux in the enameled reactor is less than 200 L / h.

[0010] As a preferred embodiment of the method for continuously collecting 2-chloropropane from halogenated hydrocarbons of the present invention, the crude 2-chloropropane product is washed with water in an enamel water washing kettle and then introduced into an enamel distillation kettle, and the washed crude 2-chloropropane product is rectified in an enamel distillation kettle to obtain a finished 2-chloropropane product.

[0011] The beneficial effects of the method for continuously collecting 2-chloropropane from halogenated hydrocarbons of the present invention are as follows: the present invention continuously collects materials through continuous reflux reaction, and the crude 2-chloropropane collected during the reflux process can be obtained after washing and distillation, and the device adopts a continuous collection method for collection to achieve better extraction efficiency.

[0012] In order to solve the above technical problems, the present invention provides the following technical solutions: a control device, including a connecting mechanism and a control mechanism arranged on the connecting mechanism; the connecting mechanism includes a first valve tube and a second valve tube, and the first valve tube and the second valve tube are connected through a containing box; the control mechanism includes a round box arranged on the containing box, a conduction component arranged in the round box, and a movable component arranged on the conduction component.

[0013] As a preferred solution of the control device of the present invention, the conduction component includes a first wheel body and a second wheel body respectively arranged on the first valve tube and the second valve tube, a belt is arranged between the first wheel body and the second wheel body, an inner side of the first wheel body is provided with a built-in limit column and a reset ring, an external ring is arranged outside the reset ring, a clamping seat is fixedly connected to the inner wall of the external ring, and docking grooves are arranged on both sides of the clamping seat.

[0014] As a preferred solution of the control device of the present invention, wherein: the built-in limit column is slidably connected to the first wheel body, the number of the built-in limit columns is multiple, and the multiple built-in limit columns are distributed in a circular array between the reset ring and the inner wall of the first wheel body, and the reset ring is fixedly connected to the built-in limit column.

[0015] As a preferred solution of the control device of the present invention, wherein: the conduction component also includes a mounting groove arranged on the first wheel body, a positioning column is arranged on the inner wall of the mounting groove, a bracket is sleeved on the outside of the positioning column, and the bracket has inner claws and outer claws on both sides respectively, and the mounting groove is provided with a resistance surface and a accommodating surface corresponding to the inner claw, and the outer claw is adapted to the docking groove.

[0016] As a preferred solution of the control device of the present invention, the positioning column is connected to the installation slot through a torsion spring, there are multiple positioning columns, and the multiple positioning columns are distributed in a circular array inside the installation slot, and a gap is provided between the positioning column and the bracket.

[0017] As a preferred solution of the control device of the present invention, the movable component includes a sliding groove and a guide groove arranged inside the round box, a reset belt is provided at the center of the sliding groove, both ends of the reset belt are fixedly connected to a slide seat, a slide cylinder is provided on the top of the slide seat, a pull rope is provided at the end of the slide seat away from the reset belt, the pull rope is limited in the round box by a guide frame, and a swivel is provided on the outside of the pull rope.

[0018] As a preferred solution of the control device of the present invention, there are two guide grooves, which are located on both sides of the inner wall of the round box, both sides of the guide groove are arc-shaped, the guide frame is located at the center between the sliding grooves, and the sliding seat is slidably connected to the sliding groove.

[0019] Beneficial effects of the control device of the present invention: the present invention can effectively connect the first wheel body and the second wheel body through the setting of the belt, and drive the belt to rotate during the rotation of the second wheel body. During the rotation of the second wheel body, the first wheel body can follow the rotation to avoid excessive flow difference between the first wheel body and the second wheel body. When adjusting a single valve body, the other valve body follows the adjustment to avoid excessive difference in the proportion of materials introduced simultaneously into the enameled distillation kettle and affecting the reaction effect. BRIEF DESCRIPTION OF THE DRAWINGS

[0020] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the accompanying drawings required for use in the description of the embodiments will be briefly introduced below. Obviously, the accompanying drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other accompanying drawings can be obtained based on these accompanying drawings without paying creative labor.

[0021] Figure 1 The figure is a schematic diagram of the process for continuously collecting 2-chloropropane from halogenated hydrocarbons.

[0022] Figure 2 It is a schematic diagram of the overall structure of the control device.

[0023] Figure 3 It is a partial cross-sectional view of the overall structure of the control device.

[0024] Figure 4 It is a schematic cross-sectional view of the control mechanism of the control device.

[0025] Figure 5 It is a schematic cross-sectional view of the conducting components of the control device.

[0026] Figure 6 It is a schematic cross-sectional view of the first wheel body of the control device.

[0027] Figure 7 This is a schematic diagram of the interior of the first wheel body of the control device.

[0028] Figure 8 Schematic diagram of the external ring structure of the control device.

[0029] Fig. 9 Schematic diagram of the support structure of the control device.

[0030] Fig.10 for Fig. 9 Enlarged view of point A in the middle. DETAILED DESCRIPTION

[0031] In order to make the above-mentioned objects, features and advantages of the present invention more obvious and easy to understand, the specific implementation methods of the present invention are described in detail below in conjunction with the accompanying drawings.

[0032] In the following description, many specific details are set forth to facilitate a full understanding of the present invention, but the present invention may also be implemented in other ways different from those described herein, and those skilled in the art may make similar generalizations without violating the connotation of the present invention. Therefore, the present invention is not limited to the specific embodiments disclosed below.

[0033] Secondly, the term "one embodiment" or "embodiment" as used herein refers to a specific feature, structure, or characteristic that may be included in at least one implementation of the present invention. The term "in one embodiment" that appears in different places in this specification does not necessarily refer to the same embodiment, nor does it refer to a separate or selective embodiment that is mutually exclusive with other embodiments.

[0034] Example 1, reference Figure 1 , which is the first embodiment of the present invention, provides a method for continuously collecting 2-chloropropane from halogenated hydrocarbons, comprising introducing hydrochloric acid solution and isopropanol into an enameled reactor, wherein the volume ratio of the hydrochloric acid solution and the isopropanol is 100:91, performing a reflux reaction, collecting crude 2-chloropropane, and collecting crude 2-chloropropane from the discharge layer of the enameled reactor after refluxing for two to five hours;

[0035] Hydrogen chloride and isopropanol are introduced into the enameled reactor through the flow control device M. The flow control device M ensures the introduction ratio of hydrogen chloride and isopropanol. When the introduction speed of hydrogen chloride is regulated, the introduction speed of isopropanol is adjusted at the same ratio, so that the device can adjust the flow rate in equal proportion.

[0036] The reflux reaction is continued; the crude 2-chloropropane is continuously collected from the top discharge layer of the enameled reactor; the crude 2-chloropropane is treated to obtain 2-chloropropane.

[0037] The temperature of the reflux reaction is controlled at 85°C to 87°C. When the reflux in the enameled reactor is less than 200 L / h, hydrogen chloride and isopropanol are introduced. The crude 2-chloropropane product is washed with water in the enameled water washing reactor and then introduced into the enameled distillation reactor. The washed crude 2-chloropropane product is rectified in the enameled distillation reactor to obtain the finished 2-chloropropane product.

[0038] Furthermore, isopropanol as a solvent has a relatively low boiling point of only 82.5° C., and the temperature of the reflux reaction needs to be controlled to be higher than 85° C. to stabilize the reflux reaction.

[0039] During operation, the stirring motor of the reactor on the enameled reactor is first turned on, and the hydrochloric acid solution and isopropanol are introduced into the enameled reactor at a volume ratio of 100:91 for reflux reaction. During the reflux reaction, the reflux flow rate is controlled at 220 L / h. At this time, the crude 2-chloropropane is collected at 50 L / h. Due to the continuous extraction of the material inside the enameled reactor, the reflux flow rate will gradually decrease. When the reflux is less than 200 L / h, hydrogen chloride and isopropanol are introduced into the enameled reactor, and the reflux flow rate of the reflux reaction is controlled to be above 220 L / h and the crude 2-chloropropane is continuously collected. The collected crude 2-chloropropane can be washed with water and distilled to obtain a finished product. During the washing process, the pH value of the solution is maintained between 5 and 7.

[0040] Example 2, reference Figure 2-10 , which is the second embodiment of the present invention. Different from the previous embodiment, the flow control device M includes a connecting mechanism 100 and a control mechanism 200 arranged on the connecting mechanism 100; the connecting mechanism 100 includes a first valve tube 101 and a second valve tube 102, and the first valve tube 101 and the second valve tube 102 are connected through a containing box 103; the control mechanism 200 includes a round box 201 arranged on the containing box 103, a conduction component 202 arranged in the round box 201, and a movable component 203 arranged on the conduction component 202.

[0041] Specifically, the setting of the connecting mechanism 100 can effectively limit the material inside it, the setting of the first valve tube 101 and the second valve tube 102 can control the flow conditions inside it, the setting of the accommodating box 103 can effectively protect the valve bodies in the first valve tube 101 and the second valve tube 102, the setting of the round box 201 is convenient for better protecting the conduction component 202 and the movable component 203 inside it, the setting of the conduction component 202 can effectively connect the first valve tube 101 with the second valve tube 102, and the setting of the movable component 203 can effectively control the movable component 203, so as to select whether to enable the movable component 203 according to needs.

[0042] The transmission component 202 includes a first wheel body 202a and a second wheel body 202b respectively arranged on the first valve tube 101 and the second valve tube 102, a belt 202c is arranged between the first wheel body 202a and the second wheel body 202b, a built-in limiting column 202d and a reset ring 202e are arranged on the inner side of the first wheel body 202a, and an external ring 202f is arranged on the outer side of the reset ring 202e, the built-in limiting column 202d is slidably connected to the first wheel body 202a, the sliding stroke of the built-in limiting column 202d is less than one centimeter, the cross-section of the built-in limiting column 202d is circular, the built-in limiting column 202d is fixedly connected to the reset ring 202e, and the reset ring 202e The reset ring 202e is made of elastic material, and moves under the action of external pressure. During the contraction of the reset ring 202e, the built-in limit column 202d will be driven to move until it moves to the limit position of the moving stroke of the built-in limit column 202d. The inner wall of the external ring 202f is fixedly connected with a clamping seat 202g, and the reset ring 202e is located at the bottom of the inner side of the external ring 202f. The upper and lower ends of the external ring 202f are both in contact with the inner wall of the first wheel body 202a, and the outer wall of the external ring 202f is in contact with the inner wall of the belt 202c. Docking grooves 202h are provided on both sides of the clamping seat 202g. The setting of the docking grooves 202h facilitates better contact with the outer claws 202m. The built-in limiting column 202d is slidably connected to the first wheel body 202a. There are multiple built-in limiting columns 202d, which are distributed in a ring array between the reset ring 202e and the inner wall of the first wheel body 202a. The reset ring 202e is fixedly connected to the built-in limiting column 202d.

[0043] Furthermore, the configuration of the first wheel body 202a and the second wheel body 202b can effectively control the flow of the corresponding first valve tube 101 and the second valve tube 102, the configuration of the belt 202c can effectively connect the first wheel body 202a and the second wheel body 202b, the configuration of the clamping seat 202g facilitates better adaptation of the outer claw 202m, and during operation, the second wheel body 202b can be driven to rotate while the first wheel body 202a is rotated, and the configuration of the built-in limit column 202d can effectively limit the reset ring 202e.

[0044] The conducting component 202 further comprises a mounting groove 202i disposed on the first wheel body 202a, a positioning column 202j is disposed on the inner wall of the mounting groove 202i, a bracket 202k is sleeved on the outside of the positioning column 202j, and the bracket 202k has inner claws 202l and outer claws 202m on both sides, the mounting groove 202i is provided with a contact surface 202n and a receiving surface 202o corresponding to the inner claw 202l, and the outer claw 202m is adapted to the docking groove 202h. The positioning column 202j is connected to the mounting groove 202i through a torsion spring, and the number of the positioning columns 202j is multiple, and the multiple positioning columns 202j are distributed in the mounting groove 202i in a ring array, and a gap is provided between the positioning column 202j and the bracket 202k.

[0045] Among them, the installation groove 202i is located in the middle of the first wheel body 202a, and the cross-section of the installation groove 202i is annular. The setting of the installation groove 202i can effectively limit the positioning column 202j. The setting of the bracket 202k can drive the first wheel body 202a to rotate during the rotation of the second wheel body 202b. When the second wheel body 202b rotates, the flow of the first valve tube 101 at the bottom of the first wheel body 202a can be effectively adjusted. The setting of the outer claw 202m can effectively drive the inner claw 202l to enter the docking groove 202h.

[0046] The rest of the structure is the same as that of Example 1.

[0047] When the flow rates of the first valve tube 101 and the second valve tube 102 need to be adjusted simultaneously, in order to avoid the situation where the flow rate of the other side is maintained at the same level when the valve body on one side is adjusted;

[0048] First, the driving ring 203h on the movable component 203 is rotated, so that the movable component 203 tensions the belt 202c. The belt 202c is in a tensioned state under the limiting effect of the movable component 203. The second wheel body 202b on the second valve tube 102 is rotated. The second wheel body 202b drives the second valve tube 102 to rotate during the rotation of the second wheel body 202b, thereby adjusting the flow inside the second valve tube 102.

[0049] At the same time, the second wheel body 202b rotates, and the belt 202c is driven to rotate during the rotation of the second wheel body 202b. At this time, the belt 202c squeezes the external ring 202f on the first wheel body 202a, causing the external ring 202f to deform, thereby driving the reset ring 202e to move and deform at the same time. The clamping seat 202g moves toward the direction of the outer claw 202m under the action of the reset ring 202e. When the belt 202c rotates, the external ring 202f is driven to rotate. During the rotation of the external ring 202f, the clamping seat 202g is driven to rotate. During the rotation of the clamping seat 202g, the outer claw 202m is driven to move. After the outer claw 202m is resisted, it drives the bracket 202k to rotate. During the rotation of the bracket 202k, the inner claw 202l is driven to contact the accommodating surface 202o. The inner claw 202l applies force to drive the first wheel body 202a to rotate. During the rotation of the first wheel body 202a, the valve of the first valve pipe 101 is driven to rotate, thereby changing the valve flow.

[0050] In summary, the setting of the belt 202c can effectively connect the first wheel body 202a and the second wheel body 202b, and drive the belt 202c to rotate during the rotation of the second wheel body 202b, so that the first wheel body 202a can follow the rotation during the rotation of the second wheel body 202b, avoiding a large flow difference between the first wheel body 202a and the second wheel body 202b. During use, the second wheel body 202b drives the first wheel body 202a to rotate to ensure a certain degree of twisting, which makes it difficult to accurately grasp the specific flow of the valve body. When the movable component 203 fails, the valve bodies corresponding to the first wheel body 202a and the second wheel body 202b are in an independent state, and the flow can be accurately adjusted as needed.

[0051] Example 3, reference Figures 2 to 10 , which is the third embodiment of the present invention. Different from the previous embodiment, the movable component 203 includes a sliding groove 203a and a guide groove 203b arranged inside the round box 201, a reset belt 203c is provided at the center of the sliding groove 203a, both ends of the reset belt 203c are fixedly connected with a slide seat 203e, a slide cylinder 203d is provided on the top of the slide seat 203e, and a pull rope 203f is provided at the end of the slide seat 203e away from the reset belt 203c. The pull rope 203f is limited in the round box 201 by a guide frame 203g, and a swivel 203h is provided on the outside of the pull rope 203f.

[0052] Furthermore, the groove depth of the sliding groove 203a is not less than five millimeters, the reset belt 203c is located at the top center of the sliding groove 203a, the reset belt 203c is woven from elastic fibers, both ends of the sliding seat 203e are arc-shaped, the top of the sliding seat 203e is rotatably connected to the slide cylinder 203d, the pull rope 203f is rotatably connected to the sliding seat 203e, the slide cylinder 203d is located inside the belt 202c wheel, both sides of the guide groove 203b are arc-shaped, the pull rope 203f is located inside the guide groove 203b, the inner wall of the swivel 203h is fixedly connected to the pull rope 203f, and the outer wall of the slide cylinder 203d is in contact with the inner wall of the guide frame 203g.

[0053] There are two guide grooves 203b, which are located on both sides of the inner wall of the round box 201. Both sides of the guide groove 203b are arc-shaped. The guide frame 203g is located at the center between the sliding groove 203a and the guide groove 203b, and the sliding seat 203e is slidably connected to the sliding groove 203a.

[0054] The rest of the structure is the same as that of Example 2.

[0055] When in use, the swivel 203h is rotated, and the pull rope 203f is driven to move during the rotation of the swivel 203h. A slight angular deviation will occur in the movement of the pull rope 203f. At this time, the inner wall of the clamping seat 202g is in contact with the outer wall of the pull rope 203f. The pull rope 203f drives the slide 203e to move under the limiting action of the clamping seat 202g. The two slides 203e located in the sliding groove 203a move toward the end away from the reset belt 203c at the same time. The reset belt 203c stretches and accumulates elastic potential energy. The belt 202c is tightened during the movement of the slide 203e, so that the inner wall of the belt 202c drives the external movement to fit the outer wall of the outer claw 202m.

[0056] In summary, the setting of the slide 203e and the sliding groove 203a facilitates better limiting the slide 203d. During the operation, the outer wall of the slide 203d fits against the inner wall of the belt 202c. During the movement of the slide 203d, the middle part of the belt 202c can be effectively driven to move to both sides. The setting of the pull rope 203f can effectively drive the slide 203e to move. When the swivel 203h is rotated, the pull rope 203f will follow the movement, thereby driving the slide 203e and the slide 203d to move. During the movement of the slide 203d, the belt 202c can be effectively tensioned.

[0057] Importantly, it should be noted that the construction and arrangement of the present application shown in a plurality of different exemplary embodiments are only exemplary. Although only a few embodiments are described in detail in this disclosure, it should be readily understood by those who refer to this disclosure that many modifications are possible (e.g., the size, scale, structure, shape and proportion of various elements, and parameter values ​​(e.g., temperature, pressure, etc.), installation arrangement, use of materials, color, directional changes, etc.) without substantially departing from the novel teachings and advantages of the subject matter described in the application. For example, the element shown as integrally formed can be composed of multiple parts or elements, the position of the element can be inverted or otherwise changed, and the nature or number or position of the discrete element can be changed or changed. Therefore, all such modifications are intended to be included in the scope of the present invention. The order or sequence of any process or method steps can be changed or reordered according to alternative embodiments. In the claims, any "device plus function" clause is intended to cover the structure of performing the function described herein, and is not only structurally equivalent but also equivalent structure. Without departing from the scope of the present invention, other replacements, modifications, changes and omissions can be made in the design, operating conditions and arrangement of the exemplary embodiments. Therefore, the invention is not limited to a specific embodiment, but extends to numerous modifications still falling within the scope of the appended claims.

[0058] Additionally, in order to provide a concise description of exemplary embodiments, all features of an actual embodiment (ie, those features that are not relevant to the best mode presently contemplated for carrying out the invention or those that are not relevant to implementing the invention) may not be described.

[0059] It will be appreciated that in the development of any actual implementation, as in any engineering or design project, numerous implementation-specific decisions may be made. Such a development effort may be complex and time-consuming, but will be a routine task of design, fabrication, and production for those of ordinary skill having the benefit of this disclosure without undue experimentation.

[0060] It should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention rather than to limit it. Although the present invention has been described in detail with reference to the preferred embodiments, those skilled in the art should understand that the technical solutions of the present invention may be modified or replaced by equivalents without departing from the spirit and scope of the technical solutions of the present invention, which should all be included in the scope of the claims of the present invention.

Claims

1. A method for continuously collecting 2-chloropropane from halogenated hydrocarbons, characterized in that: The method comprises introducing a hydrochloric acid solution and isopropanol into an enameled reactor, performing a reflux reaction, and collecting a crude 2-chloropropane product; The hydrogen chloride and isopropanol are introduced into the enameled reactor through a flow control device (M); Continuous reflux reaction; Continuously collect crude 2-chloropropane from the top discharge layer of the enameled reactor; The crude 2-chloropropane is treated to obtain 2-chloropropane.

2. The method for continuously collecting 2-chloropropane from halogenated hydrocarbons as claimed in claim 1, characterized in that: The temperature of the reflux reaction is controlled at 85° C. to 87° C., and when the reflux in the enameled reactor is less than 200 L / h, hydrogen chloride and isopropanol are introduced.

3. The method for continuously collecting 2-chloropropane from halogenated hydrocarbons as claimed in claim 2, characterized in that: The crude 2-chloropropane product is washed with water in an enamel water washing kettle and then introduced into an enamel distillation kettle. The washed crude 2-chloropropane product is rectified in an enamel distillation kettle to obtain a finished 2-chloropropane product.

4. A control device, characterized in that: The flow control device (M) comprises a connecting mechanism (100) and a control mechanism (200) arranged on the connecting mechanism (100); The communication mechanism (100) comprises a first valve tube (101) and a second valve tube (102), wherein the first valve tube (101) and the second valve tube (102) are connected via a containing box (103); The control mechanism (200) comprises a round box (201) arranged on the containing box (103), a conducting component (202) arranged in the round box (201), and a movable component (203) arranged on the conducting component (202).

5. The control device according to claim 4, characterized in that: The transmission component (202) comprises a first wheel body (202a) and a second wheel body (202b) which are respectively arranged on the first valve tube (101) and the second valve tube (102); a belt (202c) is arranged between the first wheel body (202a) and the second wheel body (202b); an inner side of the first wheel body (202a) is provided with a built-in limit column (202d) and a reset ring (202e); an outer side of the reset ring (202e) is provided with an external ring (202f); an inner wall of the external ring (202f) is fixedly connected with a clamping seat (202g); and docking grooves (202h) are arranged on both sides of the clamping seat (202g).

6. The control device according to claim 5, characterized in that: The built-in limiting posts (202d) are slidably connected to the first wheel body (202a); there are a plurality of built-in limiting posts (202d); the plurality of built-in limiting posts (202d) are distributed in a ring array between the reset ring (202e) and the inner wall of the first wheel body (202a); and the reset ring (202e) is fixedly connected to the built-in limiting posts (202d).

7. The control device according to claim 6, characterized in that: The conducting component (202) further comprises a mounting groove (202i) arranged on the first wheel body (202a), a positioning column (202j) being arranged on the inner wall of the mounting groove (202i), a bracket (202k) being sleeved on the outside of the positioning column (202j), an inner claw (202l) and an outer claw (202m) being respectively arranged on both sides of the bracket (202k), a contact surface (202n) and a receiving surface (202o) being arranged on the mounting groove (202i) corresponding to the inner claw (202l), and the outer claw (202m) being adapted to the docking groove (202h).

8. The control device according to claim 7, characterized in that: The positioning column (202j) is connected to the mounting groove (202i) via a torsion spring. There are multiple positioning columns (202j), which are distributed in a ring array inside the mounting groove (202i). A gap is provided between the positioning column (202j) and the bracket (202k).

9. The control device according to claim 8, characterized in that: The movable component (203) comprises a sliding groove (203a) and a guide groove (203b) arranged inside the round box (201); a reset belt (203c) is arranged at the center of the sliding groove (203a); both ends of the reset belt (203c) are fixedly connected to a sliding seat (203e); a sliding cylinder (203d) is arranged on the top of the sliding seat (203e); a pull rope (203f) is arranged at one end of the sliding seat (203e) away from the reset belt (203c); the pull rope (203f) is limited in position in the round box (201) by a guide frame (203g); and a swivel (203h) is arranged outside the pull rope (203f).

10. The control device according to claim 9, characterized in that: There are two guide grooves (203b) located on both sides of the inner wall of the round box (201); both sides of the guide groove (203b) are arc-shaped; the guide frame (203g) is located at the center between the sliding groove (203a) and the guide groove (203b); and the sliding seat (203e) is slidably connected to the sliding groove (203a).