Filler and production equipment

By using specific formulas of fillers and production equipment in high-temperature furnaces, the problem of low repair efficiency of cracks in the furnace lining is solved, automatic repair and mechanical performance are achieved, and service life is extended and maintenance frequency is reduced.

CN119285335AInactive Publication Date: 2025-01-10HENAN TIANLI THERMOTECHNICAL EQUIP CO LTD
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Patent Information

Application Number
CN202411804427.7
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-12-10
Publication Date
2025-01-10
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

During the use of high-temperature furnaces, due to the high-temperature sintering of refractory bricks, the existing high-temperature coating materials are inefficient in construction and difficult to effectively repair, resulting in shortening of the service life of the furnace and frequent maintenance.

Method used

A filler formula is adopted, including components A and components B, which consists of methyl cellulose, talc powder, alumina powder, ceramic fibers, silicone oil and diluents, and component B is a silicon sol, by adding rings Oxygen resin/molybdenum disulfide composites to improve bonding strength and fluidity, crack repair is carried out in combination with special production equipment.

Benefits of technology

It realizes automatic repair of the furnace lining in high temperature environment, reduces the probability of cracks, improves the mechanical properties and construction efficiency of the filler, extends the service life of the furnace, and reduces the number of repairs and costs.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention discloses a filler formula and production equipment. The filler formula comprises a component A and a component B, the component A is a main agent, and the component B is an adhesive; the mass ratio of the component A to the component B is (9: 0.5)-(9: 1.5); the component A is prepared from the following components in parts by mass: 1.5 to 2.5 parts of methyl cellulose, 1 to 2 parts of talcum powder, 18 to 24 parts of aluminum oxide powder, 5 to 7 parts of ceramic fiber, 0.5 to 1.5 parts of silicone oil, 50 to 65 parts of diluent and 0.1 to 0.3 part of visual agent; the component B comprises the following components in parts by mass: 8-13 parts of silica sol; after proportioning according to a formula, the device is used for injecting into a crack of a thermal insulation layer to fill and level up an original crack; in the using process of the furnace kiln, automatic drying and sintering are achieved, and the heat preservation effect is achieved.
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Description

Technical Field

[0001] The invention belongs to the technical field of furnace maintenance, and in particular relates to a filler and production equipment. Background Art

[0002] The blast furnace is made of steel plates as the shell, and the shell is lined with refractory bricks. The blast furnace body is divided into five parts from top to bottom: throat, body, waist, belly, and hearth. Due to the advantages of good technical and economic indicators of blast furnace smelting, simple process, large production volume, high labor production efficiency, and low energy consumption, this smelting method occupies the vast majority of the world's smelting field.

[0003] When high-temperature furnaces are in use, due to the high temperature, high-temperature resistant fillers will be applied on the surface of the lining refractory bricks to ensure the durability and fire resistance of the high-temperature furnaces. However, during the operation of high-temperature furnaces, the insulation materials undergo multiple high-temperature sintering, which will cause linear shrinkage, a shrinkage rate of -3‰, and cracks, until cracks appear, causing fire (temperature) leakage, reducing the use effect and service life of the high-temperature furnaces, and causing the working environment to become harsh.

[0004] The current high-temperature resistant coating materials generally need to be applied manually during construction, and when cracks or cracks appear in the furnace lining, they can only be applied on the crack surface. It is difficult to effectively fill and paint the inside of the crack. After painting, the coating will shrink when it undergoes high-temperature sintering again, resulting in poor gap repair effect. The same crack needs to be repaired and painted repeatedly, the construction efficiency is low, and the construction effect needs to be improved. Summary of the invention

[0005] In view of the shortcomings of the prior art, the purpose of the present invention is to provide a filler and a production equipment, which at least solves one of the problems of the background technology.

[0006] The present invention provides the following technical solutions: A filler comprising a component A and a component B; Component A is the main agent, and component B is the adhesive; The mass ratio of component A: component B is 9:0.5-9:1.5; Component A includes the following components by weight: 1.5-2.5 parts of methyl cellulose, 1-2 parts of talc, 18-24 parts of alumina powder, 5-7 parts of ceramic fiber, 0.5-1.5 parts of silicone oil, 50-65 parts of diluent, and 0.1-0.3 parts of visual agent; component B includes 8-13 parts of silica sol by weight.

[0007] Preferably, component A further comprises a mass component: 15-28 parts of epoxy resin / molybdenum disulfide compound, and the mass ratio of epoxy resin to molybdenum disulfide in the epoxy resin / molybdenum disulfide compound satisfies 240:0.8-240:1.5.

[0008] Preferably, the preparation method of the epoxy resin / molybdenum disulfide composite is as follows: in the first step, molybdenum disulfide is pretreated, an appropriate amount of molybdenum disulfide powder is weighed and added to an autoclave, and then an appropriate amount of 2.5M butyl lithium n-hexane solution is added; the autoclave is filled with argon and sealed, and then placed in an oven at 90° C. and heated for 12 hours; the obtained product is filtered and washed with n-hexane 5 times; the vacuum-dried product is then hydrolyzed in an appropriate amount of water, and ultrasonically treated at room temperature for 4 hours, thereby obtaining a monolayer molybdenum disulfide sol suspension; In the second step, the molybdenum disulfide sol suspension obtained in the first step is adjusted to neutral with dilute hydrochloric acid, centrifuged and washed five times with distilled water, the molybdenum disulfide solid content is determined, the molybdenum disulfide mixture is washed with ethanol and centrifuged five times, and then washed twice with acetone, and finally acetone is used as a solvent to preserve the molybdenum disulfide after opening, and heated in an oven for 24 hours to obtain the opened molybdenum disulfide; The third step is to weigh an appropriate amount of molybdenum disulfide and add it to an appropriate amount of acetone, and ultrasonically treat it for 2 hours to form a uniform dispersion; then weigh an appropriate amount of epoxy resin and polypropylene glycol diglycidyl ether and add them to the above dispersion, and perform high-speed mechanical stirring and ultrasonic treatment at 40°C for 2 hours to form a uniform mixture; then transfer the above mixture to a 120°C oil bath environment, vacuum and high-speed stirring for 2 hours to remove acetone in the mixture; after the above mixture is cooled to room temperature, vacuum ultrasonic stirring is performed for 5 minutes; bubbles are removed under vacuum conditions, poured into a homemade polytetrafluoroethylene mold, cured at 75°C for 2 hours and then cured at 120°C for 8 hours, then cooled to room temperature, and demolded to obtain an epoxy resin / molybdenum disulfide composite.

[0009] Preferred. A filler production equipment, comprising a shell, stirring teeth are arranged inside the shell, storage bin one and storage bin two are arranged on the top of the shell, an auger pipe is arranged near the bottom of the shell, one end of the auger pipe is connected to a motor, the other end of the auger pipe is connected to a feed pipe, the other end of the feed pipe is connected to a homogenizer one, the homogenizer one is rotatably connected to the homogenizer two, and the end of the homogenizer two is connected to a discharge pipe; the stirring teeth are connected to a first motor, the first motor is a servo motor, the servo motor is arranged on the outside of the shell, and is rotatably connected to the shell; an auger conveyor is arranged in the auger pipe, the auger conveyor is driven by a second motor, and the second motor adopts a servo motor; the feed pipe adopts an extrusion tube; the storage bin one and the storage bin two are connected to the inside of the shell, and valves are arranged at the bottom of the storage bin one and the storage bin two.

[0010] Preferably, the homogenizing member 1 is a cylindrical structure, and a plurality of discs are sequentially arranged inside the homogenizing member 1 along the length direction, and a central hole is arranged in the center of the disc; the radius of the homogenizing member 1 is R, the vertical distance from the edge of the disc to the side wall of the central hole is d1, and the distance from the center of the central hole to the side wall of the hollow is d2; then the value range of d1 / R is 0.38-0.65; the value range of d1 / d2 satisfies 0.85-1.23; the distance between the two discs is d3, and the value range of d3 / d2 satisfies 1.15-2.35; the radial length of the outer circumference of the disc is greater than the radial length of the inner wall, and the two sides of the disc are concave structures; the angle θ between the radial extension line at the center of the central hole and the connecting line between the center of the central hole and the outer circumferential side edge of the disc satisfies 5°-23°.

[0011] Preferably, the homogenizing member 1 and the homogenizing member 2 are provided with a transition tube body, the transition tube body is a cylindrical structure, one end of the transition tube body is connected to the homogenizing member 2, and the other end is rotatably connected to the homogenizing member 1, a graphite packing ring is sealed between the homogenizing member 1 and the transition tube body, and the liquid material is sealed by the graphite packing ring, and rotation is achieved at the same time, a T-shaped block is provided on the outer side wall of one end of the homogenizing member 1 close to the transition tube body, and two L-shaped blocks are provided on the end of the transition tube body close to the homogenizing member 1, and a block formed between the two L-shaped blocks The central angle of the arc is 45°; the T-shaped block can be engaged with the L-shaped block; the outer wall of one end of the homogenizer located inside the transition tube body is evenly provided with multiple material passages in the same plane, and the inner wall of the transition tube body is evenly provided with multiple blocking blocks in the same plane, and the blocking blocks can seal and block the material passages; the end of the homogenizer located inside the transition tube body is provided with a cross-shaped groove, and a plurality of material holes are provided inside the groove; the outer wall of the transition tube body is provided with at least one coarse material pipe, and the other end of the coarse material pipe is connected to the discharge pipe.

[0012] Preferably, a material plate is provided at one end of the transition pipe body away from the homogenizer one, and a cross-shaped flexible block is provided on the material plate. The flexible block is made of rubber and can block the material hole one. A plurality of cross-shaped material holes two are also provided on the material plate. The material hole two and the flexible block are cross-arranged and form an angle of 45° with each other. The material hole two can be connected with the material hole one.

[0013] Preferably, the second homogenizing member includes a cylinder, a first material tray is provided at one end of the cylinder near the transition pipe body, the other side of the first material tray is connected to the second material tray, the other end of the second material tray is connected to the third material tray, the other end of the third material tray is connected to the box body one, a box body two is provided inside the box body one, the other end of the box body two is connected to a discharge pipe, the discharge pipe extends out of the cylinder, and the discharge pipe is connected to the discharge pipe; the diameters of the first material tray, the second material tray, and the third material tray decrease successively, and the first material tray, the second material tray, the third material tray, the box body one, the box body two, and the discharge pipe are connected in sequence.

[0014] Preferably, at least one material guide groove 1 is provided on the side of the first material tray close to the material plate, the material guide groove 1 is in an annular structure, and a plurality of first material guide holes are arranged inside the material guide groove 1; a material guide groove 2 is provided on the side of the second material tray close to the first material tray, the material guide groove 2 is connected with the first material guide holes, the material guide groove 2 is in an annular structure, and a plurality of second material guide holes are arranged inside the material guide groove 2; a material guide groove 3 is provided on the side of the third material tray close to the second material tray, the material guide groove 3 is connected with the second material guide holes, the material guide groove 3 is in an annular structure, and a third material guide hole is arranged inside the material guide groove 3; the third material guide hole is connected with a material through pipe, the material through pipe is arranged inside the box body 1, and the other end of the material through pipe is connected with the box body 2.

[0015] Preferably, an inner tube is provided inside the second box body, and a conical tube is provided on the outer side of the inner tube, and the end of the conical tube close to the discharge tube has a smaller diameter; the end of the inner tube away from the discharge tube is connected to a central through tube, and the central through tube is connected to the material guide groove of the third material tray; the through tube is connected to the end with a larger diameter of the conical tube, and at least one through hole is provided on the side wall of the end of the inner tube close to the small diameter of the conical tube, and the through hole connects the conical tube and the inner tube; an annular block is provided at the end of the inner tube close to the discharge tube, and the interior of the annular block is a hollow structure, and the discharge pipe is arranged inside the annular block, and the discharge pipe is connected to the inner tube.

[0016] Preferably, the coarse material pipe is connected to the discharge pipe through a discharge pipe, and a baffle is provided at one end of the coarse material pipe located inside the discharge pipe. The baffle is rotatably connected to the discharge pipe through a hinge, and the hinge is a spring hinge.

[0017] Preferably, in order to achieve the purpose of rapid sintering, the talc powder is used as a solid lubricant with a particle size of 320 mesh, and the alumina powder is used as a sintering refractory carrier with a particle size of 320 mesh.

[0018] Preferably, the mass ratio of component A:component B can be 9:0.5, 9:0.6, 9:0.7, 9:0.8, 9:0.9, 9:1, 9:1.1, 9:1.2, 9:1.3, 9:1.4, 9:1.5; the mass ratio of epoxy resin and molybdenum disulfide in the epoxy resin / molybdenum disulfide composite can be 240:0.8, 240:0.9, 240:1, 240:1.1, 240:1.2, 240:1.3, 240:1.4, 240:1.5.

[0019] In addition, by adding epoxy resin / molybdenum disulfide composite to the filler, the molybdenum disulfide contained therein has a high melting point and can melt in a high temperature environment of 2100 degrees, melting from a solid state to a molten state. Especially for coating fillers in high-temperature furnaces, when they are applied to the cracks and then burned at high temperature, after the water is increased, talcum powder is used as a lubricant and silica sol is used as an adhesive. After the filler coating is initially solidified, due to thermal expansion and contraction, and after the water evaporates, tiny cracks will be generated, which are invisible to the naked eye. Over time, the cracks become cracks and cracks. However, after adding molybdenum disulfide, molybdenum disulfide can melt into a molten state at a high temperature of 2136 degrees, increase in volume, and have a certain fluidity. It can carry silica sol, alumina powder, and ceramic fiber to move a small distance, and can well fill cracks that are invisible to the naked eye, thereby achieving the purpose of automatic repair of tiny cracks in the furnace lining; improving the service life of the furnace lining, reducing the number of maintenance times, and saving maintenance costs.

[0020] Through reasonable improvements, this formula not only improves the mechanical properties of existing high-temperature fillers and improves various indicators of the fillers, but also enables the furnace lining to automatically repair tiny cracks in a high-temperature environment and reduce the probability of cracks. The viscosity is moderate and crack repair construction can be carried out through the production equipment of this solution.

[0021] Compared with the prior art, the present invention has the following beneficial effects: The present invention discloses a filler and production equipment. After being mixed according to the formula ratio, the equipment is used to inject into the cracks of the insulation layer to fill the plain cracks. During the use of the furnace, the filler is automatically dried and sintered to play a role in heat preservation. It not only improves the mechanical properties of the existing high-temperature filler and improves all indicators of the filler, but also enables the furnace lining to automatically repair tiny cracks in a high-temperature environment and reduce the probability of cracks. The viscosity is moderate, and the production equipment of the present solution can be used to carry out crack repair construction, so that the filling is more substantial and the effect is better, further improving the construction efficiency. BRIEF DESCRIPTION OF THE DRAWINGS

[0022] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following briefly introduces the drawings required for use in the embodiments. It should be understood that the following drawings only show certain embodiments of the present invention and therefore should not be regarded as limiting the scope. For ordinary technicians in this field, other related drawings can be obtained based on these drawings without creative work.

[0023] Figure 1 It is an overall schematic diagram of the production equipment of the present invention.

[0024] Figure 2 It is a cross-sectional schematic diagram of a homogeneous member of the present invention.

[0025] Figure 3 It is a schematic diagram of the disk layout of the present invention.

[0026] Figure 4 It is a structural schematic diagram of the second homogeneous member of the present invention.

[0027] Figure 5 It is a schematic diagram of the transition pipe structure of the present invention.

[0028] Figure 6 It is a schematic cross-sectional view of a material plate of the present invention.

[0029] Figure 7 The present invention Figure 4 A is a schematic diagram of the partially enlarged structure.

[0030] Figure 8 It is a schematic diagram of the first material tray structure of the present invention.

[0031] Fig. 9 It is a schematic diagram of the second material tray structure of the present invention. DETAILED DESCRIPTION

[0032] In order to make the purpose, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0033] Therefore, the following detailed description of the embodiments of the present invention provided in the accompanying drawings is not intended to limit the scope of the invention claimed for protection, but merely represents selected embodiments of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0034] In addition, in the present invention, descriptions such as "first" and "second" are only used for descriptive purposes, and do not specifically refer to the order or sequence, nor are they used to limit the present invention. They are only used to distinguish components or operations described with the same technical terms, and cannot be understood as indicating or implying their relative importance or implicitly indicating the number of technical features indicated. Therefore, the features defined as "first" and "second" may explicitly or implicitly include at least one of the features. In addition, the technical solutions and technical features between the various embodiments can be combined with each other, but they must be based on the ability of ordinary technicians in the field to implement them. When the combination of technical solutions is contradictory or cannot be implemented, it should be considered that such a combination of technical solutions does not exist and is not within the scope of protection required by the present invention.

[0035] Embodiment 1: refer to Figure 1-3 , a filler comprising a component A and a component B; Component A is the main agent, and component B is the adhesive; the mass ratio of component A to component B is 9:1; Component A includes the following components by weight: 2 parts of methyl cellulose, 1.5 parts of talc, 21 parts of alumina powder, 6 parts of ceramic fiber, 1 part of silicone oil, 58.3 parts of diluent, and 0.2 parts of visual agent; component B includes by weight: 10 parts of silica sol; the diluent is water, and the visual agent is green pigment.

[0036] Component A also includes a mass component: 20 parts of epoxy resin / molybdenum disulfide compound, and the mass ratio of epoxy resin to molybdenum disulfide in the epoxy resin / molybdenum disulfide compound meets 240:1.

[0037] In order to achieve the purpose of rapid sintering, talcum powder is used as a solid lubricant with a particle size of 320 mesh, and alumina powder is used as a sintering refractory carrier with a particle size of 320 mesh.

[0038] The mass ratio of component A:component B can be 9:0.5, 9:0.6, 9:0.7, 9:0.8, 9:0.9, 9:1, 9:1.1, 9:1.2, 9:1.3, 9:1.4, 9:1.5; the mass ratio of epoxy resin and molybdenum disulfide in the epoxy resin / molybdenum disulfide composite can be 240:0.8, 240:0.9, 240:1, 240:1.1, 240:1.2, 240:1.3, 240:1.4, 240:1.5.

[0039] The preparation method of the epoxy resin / molybdenum disulfide composite is as follows: in the first step, molybdenum disulfide is pretreated, an appropriate amount of molybdenum disulfide powder is weighed and added to an autoclave, and then an appropriate amount of 2.5M butyl lithium n-hexane solution is added; the autoclave is filled with argon and sealed, and then placed in an oven at 90°C for heating for 12 hours; the obtained product is filtered and washed with n-hexane for 5 times; the vacuum-dried product is then hydrolyzed in an appropriate amount of water, and ultrasonically treated at room temperature for 4 hours, thereby obtaining a monolayer molybdenum disulfide sol suspension; In the second step, the molybdenum disulfide sol suspension obtained in the first step is adjusted to neutral with dilute hydrochloric acid, centrifuged and washed five times with distilled water, the molybdenum disulfide solid content is determined, the molybdenum disulfide mixture is washed with ethanol and centrifuged five times, and then washed twice with acetone, and finally acetone is used as a solvent to preserve the molybdenum disulfide after opening, and heated in an oven for 24 hours to obtain the opened molybdenum disulfide; The third step is to weigh an appropriate amount of molybdenum disulfide and add it to an appropriate amount of acetone, and ultrasonically treat it for 2 hours to form a uniform dispersion; then weigh an appropriate amount of epoxy resin and polypropylene glycol diglycidyl ether and add them to the above dispersion, and perform high-speed mechanical stirring and ultrasonic treatment at 40°C for 2 hours to form a uniform mixture; then transfer the above mixture to a 120°C oil bath environment, vacuum and high-speed stirring for 2 hours to remove acetone in the mixture; after the above mixture is cooled to room temperature, vacuum ultrasonic stirring is performed for 5 minutes; bubbles are removed under vacuum conditions, poured into a homemade polytetrafluoroethylene mold, cured at 75°C for 2 hours and then cured at 120°C for 8 hours, then cooled to room temperature, and demolded to obtain an epoxy resin / molybdenum disulfide composite.

[0040] Specifically, by adding epoxy resin / molybdenum disulfide composite to the filler of the present scheme, the thermal and mechanical properties of the filler can be improved, so that the filler of the present scheme has better bonding strength and tensile strength in a high temperature environment, and can further reduce the cracks and cracks in the kiln lining. The reasonable addition amount of molybdenum disulfide is verified by comparative experiments. The comparative experiments are as follows: Under the premise that the other groups of the present formula are classified to have the same quality, the molybdenum disulfide content of the control group is set to 0, the molybdenum disulfide content in experimental group 1 is 0.3wt%, the molybdenum disulfide content in experimental group 2 is 0.6wt%, the molybdenum disulfide content in experimental group 3 is 0.9wt%, the molybdenum disulfide content in experimental group 4 is 1.2wt%, and the molybdenum disulfide content in experimental group 5 is 1.5wt%; the finished filler is obtained by stirring with the equipment recorded in this scheme, and the experimental results are as follows:

[0041] The above experimental results show that the tensile strength, tensile modulus, elongation at break and bonding strength are all improved by adding molybdenum disulfide compared with not adding molybdenum disulfide; and further show that when the content of molybdenum disulfide reaches 0.6wt%, the various properties of the filler basically reach the optimal level, and when the amount of molybdenum disulfide increases, the various performance indicators of the filler gradually decrease, and when the content of molybdenum disulfide is greater than 1.2, the tensile strength, tensile modulus and elongation at break of the filler are all lower than those of the control group, that is to say, the addition of molybdenum disulfide will have a counter-effect, but the bonding strength at 1600° is still higher than that of the control group; therefore, when the content of molybdenum disulfide is 0.6wt%, the various performance indicators of the filler reach the optimal level, which helps to improve the mechanical and thermal properties of the filler.

[0042] Through reasonable improvements, this formula not only improves the mechanical properties of existing high-temperature fillers and improves various indicators of the fillers, but also enables the furnace lining to automatically repair tiny cracks in a high-temperature environment and reduce the probability of cracks. The viscosity is moderate and crack repair construction can be carried out through the production equipment of this solution.

[0043] Specifically, by adding an epoxy resin / molybdenum disulfide composite to the filler, the molybdenum disulfide contained therein has a high melting point and can melt in a high temperature environment of 2100 degrees, melting from a solid state to a molten state. Especially for coating fillers in high-temperature furnaces, when they are applied to the cracks and then burned at high temperature, after the water evaporates, talcum powder is used as a lubricant and silica sol is used as an adhesive. After the filler coating is initially solidified, due to thermal expansion and contraction, and after the water evaporates, tiny cracks will be generated, which are invisible to the naked eye. Over time, the cracks become cracks and cracks. However, after adding molybdenum disulfide, the molybdenum disulfide can melt into a molten state at a high temperature of 2136 degrees, increase in volume, and have a certain fluidity. It can carry silica sol, alumina powder, and ceramic fiber to move a small distance, and can well fill cracks that are invisible to the naked eye, thereby achieving the purpose of automatic repair of tiny cracks in the furnace lining; the service life of the furnace lining is improved, and the number of maintenance times can be reduced, saving maintenance costs.

[0044] Embodiment 2: See also Figure 1-3A filler production equipment comprises a shell 1, a stirring tooth is arranged inside the shell 1, a storage bin 1 4 and a storage bin 2 5 are arranged on the top of the shell 1, an auger pipe 2 is arranged near the bottom of the shell 1, one end of the auger pipe 2 is connected to a motor, the other end of the auger pipe 2 is connected to a feeding pipe 7, the other end of the feeding pipe 7 is connected to a homogenizer 1 8, the homogenizer 1 8 is rotatably connected to a homogenizer 2 9, and the end of the homogenizer 2 9 is connected to a discharge pipe 10; the stirring tooth is connected to a first motor 3, the first motor 3 is a servo motor, the servo motor is arranged on the outside of the shell 1, and is rotatably connected to the shell 1; an auger conveyor is arranged in the auger pipe 2, the auger conveyor is driven by a second motor 6, and the second motor 6 adopts a servo motor; the feeding pipe 7 adopts an extrusion tube; the storage bin 1 4 and the storage bin 2 5 are connected to the inside of the shell 1, and valves are arranged at the bottom of the storage bin 1 4 and the storage bin 2 5.

[0045] The homogenous member 8 is a cylindrical structure, and a plurality of disks 81 are sequentially arranged inside the homogenous member 8 along the length direction, and a central hole 82 is arranged in the center of the disk 81; the radius of the homogenous member 8 is R, the vertical distance from the edge of the disk 81 to the side wall of the central hole 82 is d1, and the distance from the center of the central hole 82 to the side wall of the central hole is d2; then the value range of d1 / R is 0.38-0.65; the value range of d1 / d2 satisfies 0.85-1.23; the distance between the two disks 81 is d3, then the value range of d3 / d2 satisfies 1.15-2.35; the radial length of the outer circumference of the disk 81 is greater than the radial length of the inner wall, and the two sides of the disk 81 are concave structures; the angle θ between the radial extension line at the center of the central hole 82 and the connecting line between the center of the central hole 82 and the outer circumferential side edge of the disk 81 satisfies 5°-23°.

[0046] The homogenizer 1 8 and the homogenizer 2 9 are provided with a transition tube body 92, which is a cylindrical structure. One end of the transition tube body 92 is connected to the homogenizer 2 9, and the other end is rotatably connected to the homogenizer 1 8. A graphite packing ring is sealed between the homogenizer 1 8 and the transition tube body 92, and the liquid material is sealed by the graphite packing ring, and rotation is achieved at the same time. A T-shaped block 84 is provided on the outer wall of one end of the homogenizer 8 close to the transition tube body 92, and two L-shaped blocks 89 are provided on one end of the transition tube body 92 close to the homogenizer 1 8. The center angle of the arc formed between the two L-shaped blocks 89 is 4 5°; the T-shaped clamping block 84 can be clamped with the L-shaped blocking block 89; the outer side wall of one end of the homogenizing member 8 located inside the transition tube body 92 is evenly provided with a plurality of feeding ports 85 in the same plane, and the inner side wall of the transition tube body 92 is evenly provided with a plurality of shielding blocks 94 in the same plane, and the shielding blocks 94 can seal and block the feeding ports 85; the end of the homogenizing member 8 located inside the transition tube body 92 is provided with a cross-shaped groove 86, and a plurality of material holes 87 are provided inside the groove 86; the outer side wall of the transition tube body 92 is provided with at least one coarse material pipe 93, and the other end of the coarse material pipe 93 is connected to the discharge pipe 10.

[0047] Specifically, the production equipment provided by the present technical solution can achieve the purpose of production at any time and use at any time during production, and can well prevent the produced filler from being bonded and solidified due to long stirring time, thereby affecting normal use; the provided storage bin 1 4 and storage bin 2 5 are respectively used to place component A and component B. During production, equal proportions of materials are placed in the shell 1, and the stirring teeth are driven by the first electrode to rotate for stirring. After stirring, the materials are transported to the feed pipe 7 through the provided Jiaolong conveyor, and are sprayed out through the homogenizer 1 8, the homogenizer 2 9 and the discharge pipe 10. The discharge pipe 10 is movably connected to the homogenizer 2 9 by screws, which is convenient for cracks of different widths. Replace the discharge pipe 10 with different diameters; use the storage bin 1 4 and the storage bin 2 5 provided in the equipment to store the adhesive tube and other raw materials separately, and can mix them in time when using, which can effectively prevent the prepared filler from being bonded and solidified due to too long construction time, and is more convenient for construction; through the movable discharge pipe 10, replacing the discharge pipe 10 with different diameters is convenient for repairing cracks of different widths, so that the discharge pipe 10 can penetrate into the cracks for construction and filling. Compared with the traditional manual construction method, it not only improves the construction efficiency, but also can be constructed from the inside of the cracks, so that the paint can be completely filled in every corner of the cracks, and the filling effect is better.

[0048] Specifically, the homogenizing member 1 8 and the homogenizing member 2 9 can be provided to fully mix the material output from the feed pipe 7, thereby improving the dispersion of the filler. Because when the material passes through the feed pipe 7, the alumina powder, talcum powder, and ceramic fiber have high density and gravity, and will be deposited in the lower layer of the feed pipe 7. The transportation speed is relatively slow, resulting in poor dispersion of the filler. Finally, the filler ratio discharged from the discharge pipe 10 changes, affecting the overall performance of the filler. Therefore, by providing the homogenizing member 1 8 and the homogenizing member 2 9, the filler passing through the feed pipe 7 can be fully re-mixed to prevent stratification and sedimentation, thereby ensuring the dispersion of the discharge material in the discharge pipe 10 and improving the construction performance of the filler. The homogenizing process of the homogenizing member 8 is as follows: a plurality of disks 81 are arranged at intervals on the inner wall of the homogenizing member 8, the outer circumference of the disk 81 is connected to the inner wall of the homogenizing member, a central hole 82 is arranged at the center of the disk 81, and a homogenizing cavity 83 is formed between two adjacent disks 81. When the upstream fluid material passes through the central hole 82, it is filled in the homogenizing cavity 83. The material near the edge of the homogenizing cavity 83 is blocked by the disk 81, and the material is blocked by the disk 81. Due to the inertia, a reverse flow is formed. The reverse flow of the material is opposite to the direction of the subsequent material entering from the central hole 82. After the two fluids meet, a vortex is formed in the homogenizing cavity 83. The material in the lower layer is mixed with the material in the upper layer by the vortex. The material in the layer is stirred to form a stirring effect, so that the liquid filler has better dispersion and more uniform mixing; and by limiting the relationship between the radius R of the homogenizing member 8, the vertical distance d1 from the edge of the disk 81 to the side wall of the middle hole 82, and the distance d2 from the center of the middle hole 82 to the side wall of the middle hole, the diameter of the middle hole 82 becomes smaller, which can increase the flow rate of the material in the middle hole 82, and can better form a vortex, and the vortex speed is faster and the mixing effect is better; and through the concave setting of the disk 81, according to the vortex theory, the speed and size of the vortex are controlled by controlling the concave curvature of the disk 81, that is, the radial extension line at the center of the middle hole 82 and the connecting line between the center of the middle hole 82 and the outer peripheral edge of the disk 81. The smaller angle between the disk 81 and the disc 81 helps to increase the rotation speed and uniformity of the vortex, further improve the mixing effect of the materials, and ensure that various materials are fully mixed; in addition, according to the law of conservation of energy, the disk 81 has a certain concave curvature, which can reduce the flow resistance and pressure loss, but if the concave curvature is too large, it will lead to insufficient reverse water flow power, affecting the formation and stability of the vortex; therefore, by limiting the angle θ between the radial extension line at the center of the middle hole 82 and the connecting line between the center of the middle hole 82 and the outer peripheral edge of the disk 81 to meet 5°-23°, that is, the concave curvature of the disk 81, it can well ensure the speed and size of the vortex and ensure the mixing effect of various materials.

[0049] Embodiment three: See also Figure 4-9On the basis of the second embodiment, a material plate 88 is provided at one end of the transition tube body 92 away from the homogenizer 8, and a cross-shaped flexible stopper 881 is provided on the material plate 88. The flexible stopper 881 is made of rubber and can block the material hole 87. A plurality of cross-shaped material holes 87 are also provided on the material plate 88. The material hole 87 and the flexible stopper 881 are cross-arranged and form an angle of 45° with each other. The material hole 87 can be connected with the material hole 87. The homogenizing member 2 9 includes a cylinder 91, a first material tray 95 is provided at one end of the cylinder 91 near the transition tube body 92, the other side of the first material tray 95 is connected to the second material tray 98, the other end of the second material tray 98 is connected to the third material tray 911, the other end of the third material tray 911 is connected to a box body 1 915, a box body 2 917 is provided inside the box body 1 915, the other end of the box body 2 917 is connected to a discharge pipe 918, the discharge pipe 918 extends out of the cylinder 91, and the discharge pipe 918 is connected to the discharge pipe 10; the diameters of the first material tray 95, the second material tray 98, and the third material tray 911 decrease successively, and the first material tray 95, the second material tray 98, the third material tray 911, the box body 1 915, the box body 2 917, and the discharge pipe 918 are connected in sequence.

[0050] At least one material guide groove 96 is provided on the side of the first material tray 95 close to the material plate 88. The material guide groove 96 is of an annular structure, and a plurality of first material guide holes 97 are arranged inside the material guide groove 96. A second material guide groove 99 is provided on the side of the second material tray 98 close to the first material tray 95. The material guide groove 99 is connected to the first material guide holes 97, and the material guide groove 99 is of an annular structure. A plurality of second material guide holes 910 are arranged inside the material guide groove 99. A third material tray 911 is provided with a material guide groove 3 912 on the side close to the second material tray 98. The material guide groove 3 912 is connected to the second material guide holes 910, and the material guide groove 3 912 is of an annular structure, and a third material guide hole 913 is arranged inside the material guide groove 3 912. The third material guide hole 913 is connected to a material through pipe 916, and the material through pipe 916 is arranged inside the box body 1 915, and the other end of the material through pipe 916 is connected to the box body 2 917. An inner tube 9172 is provided inside the box body 917, and a tapered tube 9171 is provided on the outer side of the inner tube 9172. The end of the tapered tube 9171 close to the discharge tube 918 has a small diameter; the end of the inner tube 9172 away from the discharge tube 918 is connected to the middle tube 914, and the middle tube 914 is connected to the guide groove 912 of the third material tray 911; the feed pipe 916 is connected to the end with a large diameter of the tapered tube 9171, and at least one through hole 9173 is provided on the side wall of the end of the inner tube 9172 close to the tapered tube 9171 with a small diameter, and the through hole 9173 connects the tapered tube 9171 and the inner tube 9172; an annular block 9174 is provided at the end of the inner tube 9172 close to the discharge tube 918, and the interior of the annular block 9174 is a hollow structure, and the discharge tube 918 is arranged inside the annular block 9174, and the discharge tube 918 is connected to the inner tube 9172. The coarse material pipe 93 is connected to the discharge pipe 10 through the discharge pipe 918. A baffle 931 is provided at one end of the coarse material pipe 93 located inside the discharge pipe 918. The baffle 931 is rotatably connected to the discharge pipe 918 through a hinge, and the hinge is a spring hinge.

[0051] The homogenizing process of the homogenizing member 2 9 is that the material passes through the first material tray 95, the second material tray 98, and the third material tray 911 in sequence, and passes through the material guide groove 1 96, the first material guide hole 97, the material guide groove 2 99, the second material guide hole 910, the material guide groove 3 912, and the third material guide hole 913; when the viscous material is sprayed into the material guide groove 1 96 through the transition tube body 92, a preliminary collision occurs. When the viscous material flows in the material guide groove 1 96, the expansion and contraction changes of the cross-sections of the material guide groove 1 96 and the first material guide hole 97 cause the viscous material to produce strong turbulence under a lower pressure, which can further achieve material homogenization. At the same time, the changing flow channel cross-sections between the material guide groove 1 96, the first material guide hole 97, the material guide groove 2 99, the second material guide hole 910, the material guide groove 3 912, and the third material guide hole 913 increase the collision frequency and collision effect between the material fluid and the wall, and further improve the mixing effect of the viscous material.

[0052] Specifically, through the rotation setting of the homogenizing member 8 and the transition pipe body 92, four blocking blocks 94 are arranged inside the transition pipe body 92, and the corresponding homogenizing member 8 is provided with four feeding ports 85, the feeding ports 85 and the blocking blocks 94 can correspond to each other, and the homogenizing member 8 is limited to rotate 45° by the T-shaped block 84 and the two L-shaped blocks 89; when the crack of the kiln lining is wide, the material hole 87 of the homogenizing member 8 is blocked by the flexible block 881 on the material plate 88, and at the same time, the feeding port 85 and the coarse material pipe 93 are connected. The gap between the homogenizing member 8 and the transition pipe body 92 is connected, and the material in the homogenizing member 8 enters the discharge pipe 918 and the discharge pipe 10 through the rough material pipe 93, and is quickly discharged from the discharge pipe 10. It should be understood that the diameter of the rough material pipe 93 is larger than the diameter of the material hole 87; it can quickly fill wide cracks, increase the speed of crack filling, and increase the construction speed; when the gap of the kiln lining is small, the homogenizing member 8 is rotated, and the four material ports 85 are blocked by four blocking blocks 9 4 is blocked, the material hole 1 87 is connected with the material hole 2 87, the material in the homogenizer 1 8 enters the homogenizer 2 9, passes through the first material tray 95, the second material tray 98, the third material tray 911, and finally enters the inside of the tapered tube 9171 and the inner tube 9172 through the material pipe 916 and the middle through tube 914, and the path of the material is shortened by the tapered tube 9171 and the through hole 9173, the viscous material is accelerated, and finally discharged quickly through the discharge pipe 918 with a small diameter, and a movable baffle 931 is provided on the inner side of the discharge pipe 918 connected to the rough material pipe 93, which is closed by pressure to prevent the material from entering the rough material pipe 93 from the discharge pipe 918. It should be understood that the baffle 931 can be opened by the pressure in the rough material pipe 93, which meets the small demand for viscous material while improving its injection speed, can better penetrate into the small cracks, and better adhere to the inner wall of the cracks, the filling is more substantial, the effect is better, and the purpose of one machine with multiple uses is achieved.

[0053] Other technical solutions not described in detail in the present invention are all existing technologies in the field and will not be described in detail here.

[0054] The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. For those skilled in the art, the present invention may have various changes and modifications. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the scope of protection of the present invention.

Claims

1. A filler, characterized in that: It includes component A and component B; Component A is the main agent, and component B is the adhesive; The mass ratio of component A: component B is 9:0.5-9:1.5; Component A includes the following components by weight: 1.5-2.5 parts of methyl cellulose, 1-2 parts of talc, 18-24 parts of alumina powder, 5-7 parts of ceramic fiber, 0.5-1.5 parts of silicone oil, 50-65 parts of diluent, and 0.1-0.3 parts of visual agent; The mass proportion of component B includes: 8-13 parts of silica sol.

2. A filler according to claim 1, characterized in that: Component A also includes mass components: 15-28 parts of epoxy resin / molybdenum disulfide compound, and the mass ratio of epoxy resin to molybdenum disulfide in the epoxy resin / molybdenum disulfide compound meets 240:0.8-240:1.

5.

3. A filler according to claim 2, characterized in that: The preparation method of the epoxy resin / molybdenum disulfide composite is as follows: in the first step, molybdenum disulfide is pretreated, an appropriate amount of molybdenum disulfide powder is weighed and added to an autoclave, and then an appropriate amount of 2.5M butyl lithium n-hexane solution is added; the autoclave is filled with argon and sealed, and then placed in an oven at 90°C for heating for 12 hours; the obtained product is filtered and washed with n-hexane for 5 times; the vacuum-dried product is then hydrolyzed in an appropriate amount of water, and ultrasonically treated at room temperature for 4 hours, thereby obtaining a monolayer molybdenum disulfide sol suspension; In the second step, the molybdenum disulfide sol suspension obtained in the first step is adjusted to neutral with dilute hydrochloric acid, centrifuged and washed five times with distilled water, the molybdenum disulfide solid content is determined, the molybdenum disulfide mixture is washed with ethanol and centrifuged five times, and then washed twice with acetone, and finally acetone is used as a solvent to preserve the molybdenum disulfide after opening, and heated in an oven for 24 hours to obtain the opened molybdenum disulfide; The third step is to weigh an appropriate amount of molybdenum disulfide and add it to an appropriate amount of acetone, and ultrasonically treat it for 2 hours to form a uniform dispersion; then weigh an appropriate amount of epoxy resin and polypropylene glycol diglycidyl ether and add them to the obtained dispersion, and perform high-speed mechanical stirring and ultrasonic treatment at 40°C for 2 hours to form a uniform mixture; then transfer the above mixture to a 120°C oil bath environment, vacuum and high-speed stirring for 2 hours to remove acetone in the mixture; after the above mixture is cooled to room temperature, vacuum ultrasonic stirring is performed for 5 minutes; bubbles are removed under vacuum conditions, poured into a homemade polytetrafluoroethylene mold, cured at 75°C for 2 hours and then cured at 120°C for 8 hours, then cooled to room temperature, and demolded to obtain an epoxy resin / molybdenum disulfide composite.

4. A filler production device for producing the filler according to any one of claims 1 to 3, characterized in that: The invention comprises a shell (1), wherein stirring teeth are arranged inside the shell (1), a material storage bin 1 (4) and a material storage bin 2 (5) are arranged on the top of the shell (1), an auger pipe (2) is arranged near the bottom of the shell (1), one end of the auger pipe (2) is connected to a motor, the other end of the auger pipe (2) is connected to a material delivery pipe (7), the other end of the material delivery pipe (7) is connected to a homogenizing member 1 (8), the homogenizing member 1 (8) is rotatably connected to a homogenizing member 2 (9), and the end of the homogenizing member 2 (9) is connected to a discharge pipe (10); The mixing teeth are connected to a first motor (3), the first motor (3) being a servo motor, which is arranged outside the housing (1) and is rotatably connected to the housing (1); an auger conveyor is arranged inside the auger pipe (2), the auger conveyor is driven by a second motor (6), and the second motor (6) is a servo motor; the material conveying pipe (7) is an extruded pipe made of rubber material; the first storage bin (4) and the second storage bin (5) are connected to the inside of the housing (1), and valves are arranged at the bottom of the first storage bin (4) and the second storage bin (5).

5. A filler production equipment according to claim 4, characterized in that: The homogenizing member (8) is a cylindrical structure, and a plurality of disks (81) are arranged in sequence inside the homogenizing member (8) along the length direction, and a central hole (82) is arranged at the center of the disk (81); the radius of the homogenizing member (8) is R, the vertical distance from the edge of the disk (81) to the side wall of the central hole (82) is d1, and the distance from the center of the central hole (82) to the side wall of the hollow is d2; then the value range of d1 / R is 0.38-0.65; d1 / d2 The value range satisfies 0.85-1.23; the distance between the two disks (81) is d3, and the value range of d3 / d2 satisfies 1.15-2.35; the radial length of the outer circumference of the disk (81) is greater than the radial length of the inner wall, and the two sides of the disk (81) are inwardly concave; the angle θ between the radial extension line at the center of the middle hole (82) and the connecting line between the center of the middle hole (82) and the outer circumferential side edge of the disk (81) satisfies 5°-23°.

6. A filler production equipment according to claim 5, characterized in that: The homogenizing member 1 (8) and the homogenizing member 2 (9) are provided with a transition tube body (92), the transition tube body (92) being a cylindrical structure, one end of the transition tube body (92) being connected to the homogenizing member 2 (9), and the other end being rotatably connected to the homogenizing member 1 (8), a graphite packing ring being provided between the homogenizing member 1 (8) and the transition tube body (92) for sealing, the liquid material being sealed by the graphite packing ring while achieving rotation, a T-shaped clamping block (84) being provided on the outer side wall of the end of the homogenizing member 1 (8) close to the transition tube body (92), and two L-shaped stoppers (89) being provided on the end of the transition tube body (92) close to the homogenizing member 1 (8), the center angle of the arc formed between the two L-shaped stoppers (89) being 4 5°; the T-shaped clamping block (84) can be clamped with the L-shaped blocking block (89); the outer wall of one end of the homogenizing member (8) located inside the transition tube body (92) is evenly provided with a plurality of material passage openings (85) in the same plane, and the inner wall of the transition tube body (92) is evenly provided with a plurality of blocking blocks (94) in the same plane, and the blocking blocks (94) can seal and block the material passage openings (85); the end of the homogenizing member (8) located inside the transition tube body (92) is provided with a cross-shaped groove (86), and the groove (86) is provided with a plurality of material holes (87); the outer wall of the transition tube body (92) is provided with at least one coarse material pipe (93), and the other end of the coarse material pipe (93) is connected to the discharge pipe (10).

7. A filler production equipment according to claim 6, characterized in that: A material plate (88) is provided at one end of the transition pipe body (92) away from the homogenizing member 1 (8), and a cross-shaped flexible stopper (881) is provided on the material plate (88). The flexible stopper (881) is made of rubber and can block the material hole 1 (87). The material plate (88) is also provided with a plurality of cross-shaped material holes 2 (87). The material holes 2 (87) and the flexible stopper (881) are cross-arranged to form an angle of 45° with each other, and the material holes 2 (87) can be connected to the material hole 1 (87).

8. A filler production equipment according to claim 6, characterized in that: The homogenizing member 2 (9) comprises a cylinder (91), wherein a first material tray (95) is provided at one end of the cylinder (91) near the transition tube body (92), the other side of the first material tray (95) is connected to a second material tray (98), the other end of the second material tray (98) is connected to a third material tray (911), the other end of the third material tray (911) is connected to a box body 1 (915), a box body 2 (917) is provided inside the box body 1 (915), the other end of the box body 2 (917) is connected to a discharge pipe (918), the discharge pipe (918) extends out of the cylinder (91), and the discharge pipe (918) is connected to a discharge pipe (10); the diameters of the first material tray (95), the second material tray (98), and the third material tray (911) decrease in sequence, and the first material tray (95), the second material tray (98), the third material tray (911), the box body 1 (915), the box body 2 (917), and the discharge pipe (918) are connected in sequence.

9. A filler production equipment according to claim 8, characterized in that: At least one material guide groove (96) is provided on a side of the first material tray (95) close to the material plate (88), the material guide groove (96) is annular in structure, and a plurality of first material guide holes (97) are provided inside the material guide groove (96); a second material guide groove (99) is provided on a side of the second material tray (98) close to the first material tray (95), the material guide groove (99) is connected to the first material guide hole (97), the material guide groove (99) is annular in structure, and a plurality of second material guide holes (910) are provided inside the material guide groove (99); A third material guide groove (912) is provided on one side of the third material tray (911) close to the second material tray (98); the third material guide groove (912) is connected to the second material guide hole (910); the third material guide groove (912) is an annular structure; a third material guide hole (913) is provided inside the third material guide groove (912); the third material guide hole (913) is connected to a material passage pipe (916); the material passage pipe (916) is provided inside the first box body (915); the other end of the material passage pipe (916) is connected to the second box body (917).

10. A filler production device according to claim 9, characterized in that: An inner tube (9172) is provided inside the second box body (917), and a conical tube (9171) is provided outside the inner tube (9172); the end of the conical tube (9171) close to the discharge tube (918) has a smaller diameter; the end of the inner tube (9172) away from the discharge tube (918) is connected to a central tube (914), and the central tube (914) is connected to the third material guide groove (912) of the third material tray (911); the material through tube (916) is connected to the end of the conical tube (9171) with a larger diameter. At least one through hole (9173) is provided on the side wall of the end of the inner tube (9172) close to the tapered tube (9171) with a smaller diameter, and the through hole (9173) connects the tapered tube (9171) and the inner tube (9172). An annular block (9174) is provided on the end of the inner tube (9172) close to the discharge tube (918), and the interior of the annular block (9174) is a hollow structure. The discharge tube (918) is arranged inside the annular block (9174), and the discharge tube (918) is in communication with the inner tube (9172).

Citation Information

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