Nuclear magnetic resonance spectrum processing method and spectrum device

By adopting a semi-separated design and mobile display in a portable nuclear magnetic resonance analyzer, the problem of separation operation of display equipment and analyzer in the prior art is solved, ensuring the safety and stability of the spectrometer, and improving the overall efficiency of the equipment.

CN119534527APending Publication Date: 2025-02-28QINGDAO UNIV OF SCI & TECH
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Patent Information

Application Number
CN202411763529.9
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-12-03
Publication Date
2025-02-28

AI Technical Summary

Technical Problem

During use, the existing portable NMR analyzer is troublesome to separate the display device from the analyzer, and it is easy to damage when the analyzer is moved.

Method used

A method and mapping device for nuclear magnetic resonance maps are designed, and the semi-separated design is adopted. The display is electrically connected to the spectrometer. The display is movable and sealed and stored when not in use, ensuring that the sealing and protective structure of the spectrometer is not affected.

Benefits of technology

It realizes convenient operation of the monitor and safe use of the spectrometer, reduces the risk of loss during the movement of the equipment, and improves the stability and heat dissipation effect of the equipment through structures such as cooling fans and filters.

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Abstract

The invention discloses a nuclear magnetic resonance spectrum processing method and a spectrum device, and relates to the technical field of detection.The nuclear magnetic resonance spectrum processing device comprises an equipment main body structure, the equipment main body structure comprises a lower shell, an upper shell, a magnet cabinet, a sample injection pipe, a radio frequency cabinet, an industrial personal computer and a displayer; the device is characterized in that cooling fans are fixedly inserted into the tops of the radio frequency cabinet and the industrial personal computer, four filter screens are fixedly mounted at the bottoms of the outer sides of the radio frequency cabinet and the industrial personal computer, the display and the spectrometer are electrically connected together, and the display and the spectrometer are designed in a semi-separated manner. The operation and watching of the display cannot influence the sealing protection structure of the spectrometer, and the use safety of the spectrometer is ensured; and the display capable of being movably operated is sealed and stored in the storage groove when not in use, so that the loss caused by accidents in the movement process of the map generation equipment is reduced.
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Description

Technical Field

[0001] The present invention relates to the field of detection technology, in particular to a method for processing a nuclear magnetic resonance spectrum and a spectrum device. Background Art

[0003] In order to cope with the lack of effective detection technology and standards for edible oil, various portable detection devices have appeared on the market. For example, the utility model disclosed in the existing patent application No.: 201520787744.2 discloses a nuclear magnetic resonance analyzer, which includes a portable box and a magnet cabinet, wherein the portable box is provided with a handle, an online analysis device and an external display are provided in the portable box, a magnet cabinet is provided on the online analysis device, and a mobile detection device is provided on the magnet cabinet.

[0004] However, when using a portable nuclear magnetic resonance analyzer, since the display device needs to be conveniently used outside the analyzer, when the analyzer and the display device are completely separated, the two need to be temporarily connected during use, which is inconvenient to operate; when the display device is fixedly installed on the outside of the analyzer, the analyzer is prone to damage during movement. Summary of the invention

[0005] The object of the present invention is to provide a method and device for processing nuclear magnetic resonance spectra to solve the problems raised in the prior art.

[0006] To achieve the above-mentioned purpose, the present invention provides the following technical solutions: a method for processing a nuclear magnetic resonance spectrum and a spectrum device, comprising a main structure of the equipment, the main structure of the equipment comprising a lower shell, an upper shell, a magnet cabinet, an injection tube, a radio frequency cabinet, an industrial computer and a display, characterized in that: a cooling fan is fixedly inserted on the top of the radio frequency cabinet and the industrial computer, four filters are fixedly installed on the bottom of the outer side of the radio frequency cabinet and the industrial computer, a feed hole, an exhaust groove three and an exhaust groove four are opened on the top of the upper shell, a storage groove is opened on one side of the upper shell, a display support structure is arranged inside the storage groove, the display support structure comprises a protective shell, a motion card board and two plug-in boards, the display is fixedly installed inside the protective shell, the top of the motion card board is opened with an exhaust groove one and an exhaust groove two, a position control component is arranged between the two plug-in boards and the motion card board, a position fixing component is arranged between the protective shell and the motion card board, and an automatic cleaning component is arranged between the bottom of the protective shell and the upper shell.

[0007] Preferably, a plurality of mounting grooves are provided on both sides of the top of the lower shell and on both sides of the bottom of the upper shell, a fixing plug plate is provided inside the mounting groove of the upper shell, the fixing plug plate is fixedly connected to the upper shell, a bolt is threadedly connected to one side of the fixing plug plate, a thread groove is provided on one side of the mounting groove of the lower shell, and the thread groove is formed on the outer side of the lower shell.

[0008] Preferably, the magnet cabinet, radio frequency cabinet and industrial computer are all fixedly installed inside the lower shell, the sampling tube is installed on the top of the magnet cabinet, the feed hole is arranged on the top of the sampling tube, the exhaust groove three is arranged on the top of one of the cooling fans, and the exhaust groove four is arranged on the top of the other cooling fan.

[0009] Preferably, the industrial computer is provided with a DDS, a PSG and an ADC, and a plurality of pressure relief valves are fixedly provided at the bottom of the outer side of the lower shell.

[0010] Preferably, the position control component includes a biaxial pneumatic cylinder, which is fixedly inserted at a position on one side of the moving card plate away from the protective shell, and connecting cross plates are fixedly installed at both ends of the biaxial pneumatic cylinder, and the connecting cross plates are fixedly connected to the adjacent plug-in plates, and two supporting round rods are inserted on one side of the plug-in plate, and the supporting round rods are fixedly connected to the moving card plate.

[0011] Preferably, a U-shaped frame 2 is sleeved on the outer side of one end of the plug-in board away from the moving card plate, and the U-shaped frame 2 is fixedly connected to the upper shell body, and two U-shaped frames 1 are arranged on the side of the protective shell close to the plug-in board, and a limiting baffle is fixedly connected to one side of the U-shaped frame 1 away from the exhaust groove 2, and the U-shaped frame 1 is fixedly connected to the upper shell body.

[0012] Preferably, the fixing component includes a metal rod and an installation cavity, the metal rod is fixedly installed on one side of the protective shell, the installation cavity is formed on one side of the moving card plate, the metal rod is inserted into the installation cavity, the outer fixed sleeve of the metal rod is provided with two installation bearings, the outer ring of the installation bearing is fixedly connected to the moving card plate, the outer sleeve of the metal rod is provided with an electromagnet and a plurality of rubber sleeves, the outer wall of the electromagnet and the rubber sleeve are fixedly connected to the moving card plate.

[0013] Preferably, a rubber handle is fixedly connected to one side of the protective shell away from the metal rod, the rubber handle is arranged on the outside of the storage slot, a rubber pad is arranged at the bottom of one end of the storage slot away from the plug board, and the rubber pad is fixedly connected to the upper shell.

[0014] Preferably, the automatic cleaning component includes a storage trough, which is formed on the upper shell and connected to the interior of the receiving tank, a waste box is inserted into the storage trough, one end of the waste box is fixedly connected to an ear plate, a scraper is provided on one side of the top of the waste box, the scraper is fixedly connected to the upper shell, a support shaft is provided on the side of the scraper away from the waste box, a sponge sleeve and two one-way bearings are provided on the outer fixed sleeve of the support shaft, the outer rings of the two one-way bearings are fixedly connected to the upper shell, a plurality of support frames are provided at the bottom of the inner cavity of the receiving tank, both ends of the support frames are rotatably connected to the upper shell, and the movable clamping plate is set to a T shape.

[0015] The working method of the graph processing system includes the following steps: Step 1: The map generating device is powered on, the double-axis pneumatic cylinder works and contracts, the plug-in board leaves the inside of the U-shaped frame 2 set on the outside, and the U-shaped frame 2 loses its fixed limiting function on the plug-in board; Step 2: Pull the protective case out of the storage slot. After the movement of the plug board is blocked by the limit baffle, the display is completely out of the storage slot. Step 3: Rotate the protective case to adjust the display rotation angle; Step 4: Control the display support structure to enter the working state, the electromagnet is fixed together with the iron metal rod through magnetic force, the double-axis pneumatic cylinder works to push the two plug-in boards into the two U-shaped frames, and the relative position between the display and the upper shell is fixed; Step 5: insert the bottom end of the glass tube containing the oil sample to be tested into the injection tube through the feed hole, and the oil sample to be tested enters the detection cavity inside the magnet cabinet; Step 6: The display controls the spectrum generating device to work and complete the formation and analysis of the nuclear magnetic resonance spectrum; Step 7: Pull out the glass tube of the oil sample to be tested, insert a new glass tube of the oil sample to be tested into the magnet cabinet, and repeat the above step 6; Step 8: After the detection of multiple samples is completed, the electromagnet is controlled to stop working, and the user rotates the protective shell to control the contraction of the double-axis pneumatic cylinder, and the double-axis pneumatic cylinder drives the two plug-in boards to leave the inside of the two U-shaped frames.

[0016] Compared with the prior art, the present invention has the following beneficial effects: 1. In the present application, the display for analyzing the external spectrum and the spectrometer composed of an industrial computer, DDS, PSG, and ADC for generating the nuclear magnetic resonance spectrum together constitute a spectrum device. The display and the spectrometer are electrically connected together, and the display and the spectrometer are semi-separated, so that the operation and viewing of the display will not affect the sealed protection structure of the spectrometer, thereby ensuring the safety of the spectrometer; and the movable display is also sealed and stored in the storage slot when not in use, thereby reducing the loss caused by accidents during the movement of the spectrum generating equipment.

[0017] 2. In the present application, two cooling fans are fixedly inserted on the RF cabinet and the industrial computer respectively. When the RF cabinet and the industrial computer are working, the two cooling fans are controlled to draw air from the RF cabinet and the industrial computer, and the hot air is discharged through the heat dissipation channel or the exhaust channel to cool down and dissipate the inside of the RF cabinet and the industrial computer, thereby improving the working stability of the RF cabinet and the industrial computer. After the internal air pressure of the sealed box composed of the lower shell and the upper shell is reduced due to the exhaust of the cooling fan, the pressure relief valve releases the pressure to allow outside air to enter the sealed box. The cooling fan, filter, pressure relief valve and other structures cooperate to form a simple air dispersion cycle to complete the heat dissipation protection work for the RF cabinet and the industrial computer.

[0018] 3. When the present application is used, the force generated when the monitor leaves and enters the storage slot is utilized to complete the cleaning of the monitor and the sponge cover, thereby ensuring the cleanliness of the monitor and making it convenient for the staff to watch the monitor. BRIEF DESCRIPTION OF THE DRAWINGS

[0019] Figure 1 It is a structural schematic diagram of the present invention; Figure 2 It is a structural schematic diagram of the lower shell of the present invention; Figure 3 For the present invention Figure 2 A magnified view of the structure at A; Figure 4 It is a structural schematic diagram of the heat dissipation fan of the present invention; Figure 5 It is a structural schematic diagram of the filter screen of the present invention; Figure 6 It is a schematic diagram of the partial structure of the upper shell of the present invention; Figure 7 For the present invention Figure 6 A magnified view of the structure at B; Figure 8 It is a structural schematic diagram of the display support structure of the present invention; Fig. 9 For the present invention Figure 8 A magnified view of the structure at C; Fig.10 It is a structural schematic diagram of the upper shell of the present invention; Fig.11 It is a schematic diagram of the partial structure of the scraper of the present invention; Fig.12 It is a structural schematic diagram of the sports card board of the present invention; Fig.13 It is a schematic structural diagram of the metal rod of the present invention.

[0020] Numbers in the figure: 1. Main structure of the equipment; 11. Lower shell; 12. Upper shell; 13. Installation groove; 14. Threaded groove; 15. Fixed plug plate; 16. Bolt; 17. Magnet cabinet; 18. Sample injection tube; 19. RF cabinet; 110. Industrial computer; 111. Filter; 112. Cooling fan; 113. DDS; 114. PSG; 115. ADC; 116. Display; 117. Storage slot; 2. Display support structure; 21. Protective shell; 22. Rubber handle; 24. Support frame; 25. Sports card board; 26. Exhaust slot 1; 27. Exhaust groove two; 28, installation cavity; 29, metal rod; 210, installation bearing; 211, rubber sleeve; 212, electromagnet; 213, U-shaped frame one; 214, limit baffle; 215, plug-in board; 216, U-shaped frame two; 217, support round rod; 218, connecting cross plate; 219, double-axis pneumatic cylinder; 220, rubber pad; 221, sponge sleeve; 222, support shaft; 223, one-way bearing; 224, scraper; 225, storage trough; 226, waste box; 227, ear plate; 3, feed hole; 4, exhaust groove three; 5, exhaust groove four; 6, pressure relief valve. DETAILED DESCRIPTION

[0021] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0022] Example: Figure 1-Figure 13As shown, the present invention provides a method for processing a nuclear magnetic resonance spectrum and a technical solution of a spectrum device, including a device main structure 1, the device main structure 1 includes a lower shell 11, an upper shell 12, a magnet cabinet 17, a sample injection tube 18, a radio frequency cabinet 19, an industrial computer 110 and a display 116, the radio frequency cabinet 19 and the industrial computer 110 are both fixedly inserted with a cooling fan 112 on the top, the radio frequency cabinet 19 and the industrial computer 110 are both fixedly installed with four filter screens 111 on the outer bottom of the radio frequency cabinet 19 and the industrial computer 110, a feed hole 3, an exhaust slot 4 and an exhaust slot 5 are opened on the top of the upper shell 12, and the upper shell 19 is provided with a plurality of cooling fans 112, and the cooling fans 112 are fixedly installed on the top of the upper shell 12. A storage groove 117 is provided on one side of the body 12, and a display support structure 2 is arranged inside the storage groove 117. The display support structure 2 includes a protective shell 21, a motion card board 25 and two plug-in boards 215. The display 116 is fixedly installed inside the protective shell 21. An exhaust groove 1 26 and an exhaust groove 27 are provided on the top of the motion card board 25. A position control component is provided between the two plug-in boards 215 and the motion card board 25. A position fixing component is provided between the protective shell 21 and the motion card board 25. An automatic cleaning component is provided between the bottom of the protective shell 21 and the upper shell 12.

[0023] Specifically, a plurality of mounting grooves 13 are provided on both sides of the top of the lower shell 11 and on both sides of the bottom of the upper shell 12. A fixing plug plate 15 is provided inside the mounting groove 13 provided in the upper shell 12. When the upper shell 12 is installed on the top of the lower shell 11, the fixing plug plate 15 fixedly connected to the upper shell 12 is controlled to be inserted into the mounting groove 13 provided in the lower shell 11; and a threaded groove 14 is provided on one side of the mounting groove 13 provided in the lower shell 11. The threaded groove 14 is formed on the lower shell 11. The bolt 16 threadedly connected on the fixing plug plate 15 is rotated so that the bolt 16 partially rotates into the threaded groove 14. The bolt 16 is threadedly installed with the lower shell 11. 16 installs the fixed plug plate 15 and the lower shell 11 together to complete the installation of the upper shell 12 and the lower shell 11. The lower shell 11 and the upper shell 12 installed together by bolts 16 can be quickly installed and disassembled, which is convenient for operating and maintaining the magnet cabinet 17, the radio frequency cabinet 19 and the industrial computer 110 fixedly installed inside the lower shell 11, and the sampling tube 18 is installed on the top of the magnet cabinet 17, the feeding hole 3 opened on the upper shell 12 is arranged on the top of the sampling tube 18, the exhaust groove three 4 opened on the upper shell 12 is arranged on the top of one of the cooling fans 112, and the exhaust groove four 5 opened on the upper shell 12 is arranged on the top of the other cooling fan 112.

[0024] When it is necessary to use a spectrum generating device composed of the lower housing 11, the upper housing 12, the magnet cabinet 17, the radio frequency cabinet 19, the industrial computer 110, and the DDS 113, PSG 114 and ADC 115 inserted in the industrial computer 110, the specific steps of the spectrum processing method of the spectrum generating device are as follows: Step 1: Turn on the power supply for the atlas generating device. At this time, the display support structure 2 set inside the storage slot 117 opened on one side of the upper shell 12 is energized. At this time, the position control component set between the two plug-in boards 215 and the motion card board 25 works, and the double-axis pneumatic cylinder 219 in the position control component works and contracts. The two ends of the double-axis pneumatic cylinder 219 fixedly inserted at a position away from the protective shell 21 on one side of the motion card board 25 contract, and the connecting cross plates 218 fixedly installed at both ends of the double-axis pneumatic cylinder 219 move toward the motion card board 25 at the same time. The connecting cross plate 218 drives the fixedly connected plug-in board 215 to move, so that the plug-in board 215 leaves from the U-shaped frame 216 set on the outside, and the U-shaped frame 216 fixedly connected to the upper shell 12 loses the fixed limiting effect on the plug-in board 215. The motion card board 25 and the protective shell 21 fixed to the motion card board 25 lose the limit and can move. The display 116 fixedly connected inside the protective shell 21 loses the limit, and the display 116 enters the waiting state.

[0025] Step 2: The user holds the rubber handle 22 fixedly connected to one side of the protective shell 21, and pulls the rubber handle 22 arranged on the outside of the storage groove 117 to pull the protective shell 21 out of the storage groove 117, and two U-shaped frames 213 are arranged on the side of the protective shell 21 close to the plug-in board 215, and a limit baffle 214 is fixedly connected to the side of the U-shaped frame 213 away from the exhaust groove 27. The two U-shaped frames 213 fixedly connected to the upper shell 12 and the limit baffle 214 fixedly connected to one of the U-shaped frames 213 cannot move. Therefore, the moving protective shell 21 drives the moving card plate 25, the dual-axis pneumatic cylinder 219 and the two plug-in boards 215 to move. When the plug-in board 215 on the same side of the limit baffle 214 moves and is blocked by the limit baffle 214, the protective shell 21 completely leaves the storage groove 117, and the display 116 completely leaves the storage groove 117.

[0026] Step 3: Rotate the protective shell 21. Since the metal rod 29 in the fixing assembly is fixedly installed on one side of the protective shell 21, the metal rod 29 is inserted into the mounting cavity 28 formed on the moving card plate 25, and the outer rings of the two mounting bearings 210 fixedly sleeved on the outside of the metal rod 29 are fixedly connected to the moving card plate 25, the protective shell 21 forms a transmission relationship with the moving card plate 25 through the metal rod 29 and the two mounting bearings 210. Therefore, after the staff rotates the protective shell 21, the protective shell 21 drives the display 116 to rotate on one side of the moving card plate 25, and the electric The magnet 212 and the outer walls of multiple rubber sleeves 211 are fixedly connected to the motion card plate 25. There is a large friction between the multiple rubber sleeves 211 and the metal rod 29, which controls the rotation speed of the metal rod 29 and the protective shell 21, making it convenient for the staff to accurately adjust the rotation angle of the display 116. After the staff stops operating the protective shell 21 and the display 116, the display 116 and the protective shell 21 hover in place; therefore, the staff can rotate the display 116 to an angle that is convenient for viewing and then release it, and the display 116 will automatically hover in the corresponding position.

[0027] Step 4: Control the display support structure 2 to enter the working state through the display 116. At this time, the electromagnet 212 works. The working electromagnet 212 is adsorbed and fixed together with the iron metal rod 29 through magnetic force, so that the metal rod 29 is fixed and cannot rotate. Control the double-axis pneumatic cylinder 219 to work. The double-axis pneumatic cylinder 219 works to push the two plug-in plates 215 into the two U-shaped frames 213. Finally, the two plug-in plates 215 are against the two U-shaped frames 213 at the same time. With the cooperation of the two moving card plates 25 and the two U-shaped frames 213, the moving card plate 25 cannot move inside the storage slot 117, so that the relative position between the display 116 and the upper shell 12 is fixed.

[0028] Step 5: After the moving card plate 25 and the protective shell 21 move, the plug-in board 215 moves and the inside of the feed hole 3 loses its obstruction. At this time, the sampling tube 18 installed on the top of the magnet cabinet 17 is connected to the outside through the feeding hole 3. The staff can insert the bottom end of the glass tube containing the oil sample to be tested into the inside of the sampling tube 18 through the feeding hole 3, so that the glass tube containing the oil sample to be tested is partially inserted into the inside of the magnet cabinet 17, so that the oil sample to be tested enters the detection cavity inside the magnet cabinet 17.

[0029] Step 6: The display 116 is used to control the spectrum generating device to work. DDS113, PSG114 and ADC115 are inserted into the PCI slot of the industrial computer 110; DDS113 receives the parameters sent by the industrial computer 110 and generates a radio frequency signal, and PSG114 modulates the radio frequency signal into the required square wave, which is transmitted to the radio frequency power amplifier module inside the feed hole 3 connected to PSG114 for power amplification, and the radio frequency coil in the display support structure 2 excites the oil sample according to the amplified square wave to generate a nuclear magnetic resonance phenomenon. After receiving the nuclear magnetic resonance signal, the radio frequency coil in the display support structure 2 generates the nuclear magnetic resonance The signal is transmitted to the preamplifier in the feed hole 3 for power amplification. After amplification, the nuclear magnetic resonance signal is transmitted to ADC115 by the feed hole 3. ADC115 converts the nuclear magnetic resonance signal into a digital signal through the control of the pulse sequence in PSG114. The digital signal is sent to the industrial computer 110, and then the industrial computer 110 converts the digital signal into a transverse relaxation time spectrum. The transverse relaxation time spectrum is transmitted to the display 116 and compared with the transverse relaxation time spectrum of the authentic oil in the database of the display 116. The analysis result is displayed on the display 116, and the formation and analysis of the nuclear magnetic resonance spectrum can be completed.

[0030] Step 7: Pull out the glass tube of the oil sample to be tested, insert a new glass tube of the oil sample to be tested into the magnet cabinet 17, and repeat the above step 6.

[0031] Step 8: After the detection of multiple samples is completed, the electromagnet 212 is controlled to stop working through the display 116, and the user rotates the protective shell 21 to align the protective shell 21 with the storage slot 117, and controls the double-axis pneumatic cylinder 219 to contract. The double-axis pneumatic cylinder 219 drives the two plug-in plates 215 to leave the two U-shaped frames 213 and push the protective shell 21 into the storage slot 117; finally, the map generating device is powered off, at which time the double-axis pneumatic cylinder 219 is powered off and restored to the extended state, and the plug-in plate 215 moves back to the inside of the U-shaped frame 216 to limit the protective shell 21.

[0032] In summary, in the present application, the display 116 for analyzing the external spectrum and the spectrometer composed of the industrial computer 110, DDS113, PSG114, and ADC115 for generating the nuclear magnetic resonance spectrum together constitute a spectrum device. The display 116 and the spectrometer are electrically connected together, and the display 116 and the spectrometer are semi-separated, so that the operation and viewing of the display 116 will not affect the sealed protection structure of the spectrometer, thereby ensuring the safety of the spectrometer; and the movable display 116 is also sealed and stored in the storage slot 117 when not in use, thereby reducing losses caused by accidents during the movement of the spectrum generating equipment.

[0033] A cooling fan 112 is fixedly inserted on the top of the RF cabinet 19 and the industrial computer 110. After the protective shell 21 leaves the storage slot 117, the exhaust slot 1 26 moves to align with the exhaust slot 3 4. The exhaust slot 1 26 and the exhaust slot 3 4 form an exhaust channel connected to the outside world, and the exhaust slot 3 4 opened on the upper shell 12 is set on the top of one of the cooling fans 112. At this time, the top of the cooling fan 112 is connected to the outside world through the exhaust channel; After the protective shell 21 leaves the storage slot 117, the second exhaust slot 27 moves to align with the fourth exhaust slot 5. The second exhaust slot 27 and the fourth exhaust slot 5 form a heat dissipation channel connected to the outside world. The fourth exhaust slot 5 opened on the upper shell 12 is set on the top of another heat dissipation fan 112. The top of the heat dissipation fan 112 is connected to the outside world through the heat dissipation channel. Two cooling fans 112 are fixedly inserted on the RF cabinet 19 and the industrial computer 110 respectively. When the RF cabinet 19 and the industrial computer 110 are working, the two cooling fans 112 are controlled to extract air from the RF cabinet 19 and the industrial computer 110, and the hot air is discharged through the heat dissipation channel or the exhaust channel to cool down the inside of the RF cabinet 19 and the industrial computer 110, thereby improving the working stability of the RF cabinet 19 and the industrial computer 110; Four filters 111 are fixedly installed at the bottom of the outer side of the RF cabinet 19 and the industrial computer 110. The filter 111 filters the gas entering the RF cabinet 19 or the industrial computer 110 to prevent dust and impurities from entering the RF cabinet 19 or the industrial computer 110, and a plurality of pressure relief valves 6 are fixedly inserted at the bottom of the outer side of the lower shell 11. When the internal air pressure of the sealed box composed of the lower shell 11 and the upper shell 12 is reduced due to the exhaust of the cooling fan 112, the pressure relief valve 6 releases the pressure to allow outside air to enter the sealed interior. The cooling fan 112, the filter 111, the pressure relief valve 6 and other structures cooperate to form a simple air dispersion cycle, thereby completing the heat dissipation protection work for the RF cabinet 19 and the industrial computer 110.

[0034] In addition, such as Fig.10 As shown, when the protective shell 21 returns to the storage groove 117, the feed hole 3 is cut off by one of the plug-in plates 215, the exhaust groove three 4 is cut off by the moving card plate 25, and the exhaust groove four 5 is cut off by the protective shell 21, so that the lower shell 11 and the upper shell 12 are restored to a sealed state.

[0035] In addition, such as Fig.12 As shown, two supporting round rods 217 are inserted on the plug-in board 215, and the supporting round rods 217 are fixedly connected to the moving card plate 25. The two supporting round rods 217 support and limit the plug-in board 215 so that the plug-in board 215 can only move horizontally, thereby ensuring stable cooperation between the plug-in board 215 and the U-shaped frame 216.

[0036] In addition, such as Figure 8 and Fig. 9As shown, a rubber pad 220 is provided at the bottom of one end of the storage slot 117 away from the plug board 215. The rubber pad 220 is fixedly mounted on the upper shell 12. The rubber pad 220 applies a certain friction force to the protective shell 21 to ensure that the protective shell 21 is sealed inside the storage slot 117, thereby improving the safety of the sealed storage of the display 116.

[0037] In addition, such as Figure 6 , Figure 7 , Figure 8 and Fig. 9 As shown, the storage tank 225 in the automatic cleaning component is formed on the upper shell 12 and is connected to the inside of the storage tank 117. A scraper 224 is arranged on one side of the top of the waste box 226 inserted in the storage tank 225. The scraper 224 is fixedly connected to the upper shell 12, and a support shaft 222 is arranged on the side of the scraper 224 away from the waste box 226. A sponge sleeve 221 and two one-way bearings 223 are provided on the outer fixed sleeve of the support shaft 222. The outer rings of the two one-way bearings 223 distributed at both ends of the support shaft 222 are fixedly connected to the upper shell 12, and the one-way bearings 223 can only rotate in one direction.

[0038] When the protective shell 21 drives the display 116 to leave the storage slot 117, the display 116 applies a rotational force to the rubber sleeve 211 and the support shaft 222. At this time, the rotation direction of the support shaft 222 is the self-locking direction of the one-way bearing 223, so the rubber sponge sleeve 221 cannot rotate to clean the display 116. When the protective shell 21 and the display 116 move toward the storage groove 117, the display 116 applies a rotational force to the rubber sleeve 211 and the support shaft 222. At this time, the force rotation direction of the support shaft 222 is the rotation direction of the outer ring of the one-way bearing 223. At this time, the rubber sleeve 211 rotates and is cleaned by the scraper 224. The inclined scraper 224 guides the impurities into the waste box 226 inside the storage groove 225. The force generated by the display 116 leaving the storage groove 117 and entering the storage groove 117 is used to complete the cleaning of the display 116 and the sponge sleeve 221, thereby ensuring that the display 116 is clean and convenient for the staff to watch the display 116.

[0039] An ear plate 227 is fixedly connected to one end of the waste box 226. The staff hooks the hollow ear plate 227 with a hook and pulls the waste box 226, which is interference fit with the upper shell 12, out of the storage tank 225 to clean the impurities inside the waste box 226.

[0040] In addition, such as Figure 8As shown, a plurality of support frames 24 are arranged at the bottom of the inner cavity of the storage groove 117, and both ends of the support frames 24 are rotatably connected to the upper shell 12. The support frames 24 support the T-shaped motion card plate 25 and the protective shell 21 to avoid friction between the display 116 inside the protective shell 21 and the upper shell 12, thereby protecting the display 116.

[0041] It will be apparent to those skilled in the art that the invention is not limited to the details of the exemplary embodiments described above and that the invention can be implemented in other specific forms without departing from the spirit or essential features of the invention. Therefore, the embodiments should be considered exemplary and non-limiting in all respects, and the scope of the invention is defined by the appended claims rather than the foregoing description, and it is intended that all variations falling within the meaning and scope of the equivalent elements of the claims be included in the invention. Any reference numeral in a claim should not be considered as limiting the claim to which it relates.

Claims

1. A nuclear magnetic resonance spectrum device, comprising a device main structure (1), wherein the device main structure (1) comprises a lower shell (11), an upper shell (12), a magnet cabinet (17), a sample injection tube (18), a radio frequency cabinet (19), an industrial computer (110) and a display (116), characterized in that: A cooling fan (112) is fixedly inserted on the top of the radio frequency cabinet (19) and the industrial computer (110); four filters (111) are fixedly installed on the bottom of the outer sides of the radio frequency cabinet (19) and the industrial computer (110); a feed hole (3), an exhaust slot three (4) and an exhaust slot four (5) are provided on the top of the upper shell (12); a storage slot (117) is provided on one side of the upper shell (12); a display support structure (2) is provided inside the storage slot (117); the display support structure (2) includes a protective The invention relates to a protective shell (21), a motion card board (25) and two plug-in boards (215), wherein the display (116) is fixedly mounted inside the protective shell (21), the motion card board (25) is provided with a first exhaust groove (26) and a second exhaust groove (27) on the top, a position control component is arranged between the two plug-in boards (215) and the motion card board (25), a position fixing component is arranged between the protective shell (21) and the motion card board (25), and an automatic cleaning component is arranged between the bottom of the protective shell (21) and the upper shell (12).

2. The nuclear magnetic resonance spectrum device according to claim 1, characterized in that: A plurality of mounting grooves (13) are provided on both sides of the top of the lower shell (11) and on both sides of the bottom of the upper shell (12); a fixing plug plate (15) is provided inside the mounting groove (13) provided in the upper shell (12); the fixing plug plate (15) is fixedly connected to the upper shell (12); a bolt (16) is threadedly connected to one side of the fixing plug plate (15); a thread groove (14) is provided on one side of the mounting groove (13) provided in the lower shell (11); the thread groove (14) is formed on the outer side of the lower shell (11).

3. The nuclear magnetic resonance spectrum device according to claim 1, characterized in that: The magnet cabinet (17), the radio frequency cabinet (19) and the industrial computer (110) are all fixedly installed inside the lower shell (11); the sample injection tube (18) is installed on the top of the magnet cabinet (17); the feed hole (3) is arranged on the top of the sample injection tube (18); the exhaust groove three (4) is arranged on the top of one of the cooling fans (112); and the exhaust groove four (5) is arranged on the top of another cooling fan (112).

4. The nuclear magnetic resonance spectrum device according to claim 1, characterized in that: The industrial computer (110) is provided with a DDS (113), a PSG (114) and an ADC (115), and a plurality of pressure relief valves (6) are fixedly provided on the bottom of the outer side of the lower housing (11).

5. The nuclear magnetic resonance spectrum device according to claim 1, characterized in that: The position control component comprises a double-axis pneumatic cylinder (219), the double-axis pneumatic cylinder (219) being fixedly inserted at a position on one side of the moving card plate (25) away from the protective shell (21), and connecting transverse plates (218) being fixedly installed at both ends of the double-axis pneumatic cylinder (219), the connecting transverse plates (218) being fixedly connected to the adjacent plug-in plates (215), and two supporting round rods (217) being inserted at one side of the plug-in plates (215), and the supporting round rods (217) being fixedly connected to the moving card plate (25).

6. The nuclear magnetic resonance spectrum device according to claim 5, characterized in that: A second U-shaped frame (216) is sleeved on the outer side of one end of the plug board (215) away from the moving card plate (25), and the second U-shaped frame (216) is fixedly connected to the upper shell (12). Two first U-shaped frames (213) are provided on the side of the protective shell (21) close to the plug board (215), and a limit stopper (214) is fixedly connected to the side of the first U-shaped frame (213) away from the second exhaust groove (27), and the first U-shaped frame (213) is fixedly connected to the upper shell (12).

7. The nuclear magnetic resonance spectrum device according to claim 1, characterized in that: The fixing assembly comprises a metal rod (29) and a mounting cavity (28), wherein the metal rod (29) is fixedly mounted on one side of the protective shell (21), the mounting cavity (28) is formed on one side of the moving card plate (25), the metal rod (29) is inserted into the mounting cavity (28), the outer fixed sleeve of the metal rod (29) is provided with two mounting bearings (210), the outer rings of the mounting bearings (210) are fixedly connected to the moving card plate (25), the outer sleeve of the metal rod (29) is provided with an electromagnet (212) and a plurality of rubber sleeves (211), and the outer walls of the electromagnet (212) and the rubber sleeve (211) are both fixedly connected to the moving card plate (25).

8. The nuclear magnetic resonance spectrum device according to claim 1, characterized in that: A rubber handle (22) is fixedly connected to a side of the protective shell (21) away from the metal rod (29); the rubber handle (22) is arranged outside the storage groove (117); a rubber pad (220) is arranged at the bottom of an end of the storage groove (117) away from the plug board (215); the rubber pad (220) is fixedly connected to the upper shell (12).

9. The nuclear magnetic resonance spectrum device according to claim 1, characterized in that: The automatic cleaning component comprises a material storage tank (225), wherein the material storage tank (225) is formed on the upper shell (12) and communicates with the interior of the storage tank (117), a waste box (226) is inserted into the material storage tank (225), one end of the waste box (226) is fixedly connected to an ear plate (227), and a scraper (224) is arranged on one side of the top of the waste box (226), and the scraper (224) is fixedly connected to the upper shell (12). A support shaft (222) is provided on one side away from the waste box (226); a sponge sleeve (221) and two one-way bearings (223) are provided on the outer fixed sleeve of the support shaft (222); the outer rings of the two one-way bearings (223) are fixedly connected to the upper shell (12); a plurality of support frames (24) are provided at the bottom of the inner cavity of the storage groove (117); both ends of the support frames (24) are rotatably connected to the upper shell (12); and the moving card plate (25) is arranged in a T shape.

10. A spectrum processing system working method, applicable to a spectrum device for a nuclear magnetic resonance spectrum as claimed in any one of claims 1 to 9, characterized in that: The steps include: Step 1: The atlas generating device is powered on, the dual-axis pneumatic cylinder (219) works and contracts, the plug-in board (215) moves away from the inside of the U-shaped frame (216) sleeved on the outside, and the U-shaped frame (216) loses its fixed limiting function on the plug-in board (215); Step 2: Pull the protective shell (21) out of the storage slot (117), and after the movement of the plug board (215) is blocked by the limit baffle (214), the display (116) completely leaves the storage slot (117); Step 3: Rotate the protective case (21) to adjust the rotation angle of the display (116); Step 4: Control the display support structure (2) to enter the working state, the electromagnet (212) is fixed together with the iron metal rod (29) by magnetic force, the double-axis pneumatic cylinder (219) works to push the two plug-in boards (215) to be inserted into the two U-shaped frames (213), and the relative position between the display (116) and the upper shell (12) is fixed; Step 5: insert the bottom end of the glass tube containing the oil sample to be tested into the interior of the sample injection tube (18) through the feed hole (3), and the oil sample to be tested enters the detection cavity inside the magnet cabinet (17); Step 6: The display (116) controls the spectrum generating device to work, and completes the formation and analysis of the nuclear magnetic resonance spectrum; Step 7: Pull out the glass tube of the oil sample to be tested, insert a new glass tube of the oil sample to be tested into the magnet cabinet (17), and repeat the above step 6; Step 8: After the detection of multiple samples is completed, the electromagnet (212) is controlled to stop working, and the user rotates the protective shell (21) to control the double-axis pneumatic cylinder (219) to contract, and the double-axis pneumatic cylinder (219) drives the two plug-in boards (215) to leave the inside of the two U-shaped frames (213).

Citation Information

Patent Citations

  • Nuclear magnetic resonance

    CN205015300U