Graphene hyaluronic acid mask and preparation method thereof

Abstract

The invention discloses a graphene hyaluronic acid mask and a preparation method thereof.The mask is composed of a component A and a component B. The component A is prepared from, by weight, 0.1-0.5 part of biomass graphene; 30 to 38 parts of hyaluronic acid; 13-18 parts of a bletilla striata extract; 11 to 15 parts of a calendula extract; 6-13 parts of a ginseng extract; 3-7 parts of glycerol; 12-17 parts of a chrysanthemum extract; 20 to 25 parts of argireline; 2 to 5 parts of deionized water; 3 to 7 parts of propylene glycol; the component B is graphene film cloth, and the component B is used as a carrier for bearing the component A. The biomass graphene as the component A and the graphene mask cloth as the component B have good compatibility, the biomass graphene and the graphene mask cloth as the component B have good compatibility, and the loaded bletilla striata extract, calendula extract, ginseng extract and chrysanthemum extract are easy to absorb.

Description

Technical Field

[0001] The present invention relates to the technical field of cosmetics, and in particular to a graphene hyaluronic acid facial mask and a preparation method thereof. Background Art

[0002] Facial mask is an important part of skin care. Applying facial mask regularly according to the characteristics of various skin types can degrease oily skin, shrink large pores, restore luster to dry and wrinkled skin, and inhibit inflammation of acne skin. After using the facial mask, the skin looks refreshed, smooth, white and tender. This is because when the facial mask is applied to the skin, the mask and the skin have affinity. As the mask gradually dries, the skin temperature rises, blood circulation speeds up, the skin tightens and the tension increases, the sebum and water secreted by the skin reversely penetrate into the stratum corneum, making the epidermis soft and stretchable, the pores instinctively open, and the effective ingredients in the facial mask penetrate into the skin and are absorbed by it. At the same time, the facial mask is tightly connected to the skin. When the facial mask is removed, the aging keratin on the skin and the deep dirt in the pores are also taken off at the same time, making the skin fresh and clean.

[0003] The principle of the facial mask is to use the short time it covers the face to temporarily isolate the outside air and pollution, increase skin temperature, expand skin pores, promote sweat gland secretion and metabolism, increase skin oxygen content, and help the skin eliminate the products of epidermal cell metabolism and accumulated oil substances. The moisture in the facial mask penetrates into the stratum corneum of the skin's epidermis, making the skin soft, and the skin naturally bright and elastic.

[0004] With the improvement of people's quality of life and people's pursuit of beauty, the types of cosmetics are becoming more and more diverse. At present, Chinese medicine mask is one of the effective whitening solutions in the field of cosmetology. In particular, some Chinese medicine extracts have good detoxification, freckle removal, repair and beauty effects, and are gradually being used in masks.

[0005] Chinese patent document CN104706566A discloses a papaya seed oil anti-wrinkle sleeping mask, which is composed of papaya seed oil, sodium hyaluronate, collagen, ginseng extract, dipotassium glycyrrhizinate, glycerin, propylene glycol, honey, vitamins, carbomer, triethanolamine, ethyl paraben and Jema BP. By combining the efficacy of the mask, the health care function of papaya is integrated into it, but its formula contains carbomer, which is prone to skin poisoning after long-term use, which is not conducive to skin health, and the efficacy data of this mask is relatively weak.

[0006] Chinese patent document CN103784381A discloses an anti-inflammatory facial mask liquid, which is composed of raw materials such as green tea powder, glycerol, cucumber extract, fresh milk and mint leaf extract. The prepared facial mask liquid can effectively relieve skin inflammation, is non-irritating to the skin, and is suitable for sensitive skin. However, the facial mask liquid has a single function and does not meet the requirements of modern people.

[0007] Chinese patent document CN104644510A discloses a facial mask liquid that promotes skin regeneration and anti-allergy, and the facial mask liquid is composed of hyaluronic acid, tranexamic acid, methyl hesperidin, carboxymethyl glucan, wheat protein hydrolyzate, light bamboo leaf extract, scutellaria extract, salvia root extract, ginger extract, aloe extract, wild chrysanthemum extract, atractylodes extract and 1,2-hexanediol. The prepared facial mask liquid can regulate the immune system from endogenous anti-inflammatory, and can activate the repair ability of the skin itself, and the skin is comfortable after use, and facial erythema can be improved, which is suitable for various groups of people to use. However, the facial mask liquid contains tranexamic acid, and the phenomenon of skin poisoning is prone to occur in long-term use, which greatly limits the application of the facial mask liquid.

[0008] Chinese patent document CN112716863A discloses a graphene rose essence facial mask and a preparation method thereof, the facial mask is composed of component A and component B, and the composition of component A is as follows by weight: 18-22 parts of rose extract; 15-18 parts of Ganoderma lucidum stock solution; 12-17 parts of chrysanthemum extract; 11-15 parts of hexapeptide; 1-3 parts of white tuckahoe; 2-5 parts of hyaluronic acid; 0.1-0.5 parts of allantoin; 0.1-0.3 parts of hydroxyethyl cellulose; 41-75 parts of deionized water; component B is a graphene membrane cloth, and component B is used as a carrier to carry the component A. However, its compatibility still has room for improvement. Summary of the invention

[0009] In view of this, the object of the present invention is to provide a graphene hyaluronic acid mask and a preparation method thereof, which has good skin compatibility and can continuously moisturize and whiten.

[0010] The technical solutions adopted are:

[0011] A graphene hyaluronic acid facial mask, which consists of component A and component B. In parts by weight, the composition of component A is as follows:

[0012] Biomass graphene 0.1-0.5 parts;

[0013] 30-38 parts of hyaluronic acid;

[0014] 13-18 parts of Bletilla striata extract;

[0015]

[0016] Component B is a graphene membrane cloth, and component B serves as a carrier to carry component A.

[0017] Furthermore, the calendula extract is obtained by the following preparation method: fresh calendula petals are placed in a distillation kettle, and then 3-4 times the weight of water is added for distillation, and the distillation temperature is controlled to be 100-120° C. and the pressure is 6-8 MPa to obtain the calendula extract.

[0018] Furthermore, the chrysanthemum extract is obtained by the following preparation method: fresh chrysanthemum petals are placed in a distillation kettle, and then 1-2 times the weight of water is added for distillation, and the distillation temperature is controlled to be 100-120° C. and the pressure is 4-5 MPa to obtain the chrysanthemum extract.

[0019] Furthermore, the ginseng extract is prepared by the following method: crushing the ginseng root, adding 3-4 times the weight of deionized water, soaking for 1-2 hours, ultrasonically extracting for 30-40 minutes, filtering, centrifuging, taking the supernatant and concentrating it to obtain the ginseng extract.

[0020] Furthermore, the bletilla striata extract is prepared by the following method: crushing the bletilla striata root, adding 2-3 times of deionized water by weight, soaking for 1-2 hours, ultrasonically extracting for 40-50 minutes, filtering, centrifuging, taking the supernatant and concentrating it to obtain the bletilla striata extract.

[0021] A method for preparing the above-mentioned graphene hyaluronic acid facial mask of the present invention comprises the following steps:

[0022] S1. Mix hyaluronic acid, hexapeptide, glycerin, propylene glycol and deionized water, and stir at a speed of 2000-2500 r / min to form a mixture A;

[0023] S2. Pump mixture A into an emulsifier, stir at a speed of 1500-2000r / min, at a temperature of 50-60°C, homogenize for 5-10 minutes, keep warm for 50-60min, then stir and cool down;

[0024] S3. The mixture A is cooled to 25-30 ° C, and Bletilla striata extract, Calendula officinalis extract, ginseng extract and chrysanthemum extract are added to the mixture A, and the mixture is stirred and discharged to form a mixture B;

[0025] S4. Add biomass graphene to mixture B at a speed of 3000-4000 r / min and stir for 60-70 min to fully disperse the biomass graphene to obtain mixture C;

[0026] S5. Fill the mixture C into the mask bag containing the graphene membrane cloth, and squeeze it so that the mixture C is fully carried in the graphene mask cloth.

[0027] In the above scheme,

[0028] Biomass graphene has the following functions:

[0029] First of all, antibacterial effect is one of the important functions of biomass graphene in facial masks. Graphene can induce the bacterial cell membrane to fall off and adhere to the graphene, thereby killing the bacteria. This has a significant antibacterial effect on harmful bacteria such as Escherichia coli, Staphylococcus aureus, and Candida albicans, and has a good preventive and improvement effect on acne skin. In addition, graphene also has bactericidal and anti-inflammatory effects, which can effectively control the growth of facial mites and other bacteria, increase skin immunity, promote skin water and oil balance, and refine pores.

[0030] Secondly, adsorption is also a major feature of biomass graphene in facial masks. Graphene has a porous structure and can adsorb heavy metal ions such as copper, zinc, cobalt, nickel, lead, chromium, arsenic, etc., effectively removing heavy metals and makeup residues on the skin surface. This feature enables graphene masks to deeply cleanse the skin, purify pores, and shrink pores.

[0031] In addition, promoting skin absorption is another important role of biomass graphene. Biomass graphene and graphene membrane cloth combined with loaded Bletilla striata extract, Calendula officinalis extract, Ginseng extract and Chrysanthemum extract are easily absorbed, keep the face moisturized, continuously promote skin absorption, and effectively improve the skin.

[0032] Finally, environmental friendliness is also one of the advantages of using biomass graphene in facial masks. The raw materials needed to produce graphene are mainly plant straw, which is very safe and environmentally friendly to use. Graphene masks can be effectively degraded by the natural environment after use, and even help improve the soil.

[0033] Hexapeptide is a small molecule protein composed of 6 amino acids. The functions of hexapeptide are: it can quickly and effectively smooth out wrinkles between the eyebrows, eyes, face and neck, prevent wrinkles, promote cell regeneration and improve aging skin quality.

[0034] Hyaluronic acid can store water, moisturize, promote metabolism, and reduce scars. Hyaluronic acid, also known as hyaluronic acid, can store water, make the skin more elastic, and also has a moisturizing effect.

[0035] The graphene mask cloth in component B has a strong adsorption capacity due to its rich porous structure. It can absorb heavy metals and PM2.5 that are stained on the face due to exposure to bad air, and can also absorb dirt and makeup residues in the skin. It has the characteristics of strong adsorption, far-infrared emission, antibacterial and antibacterial, negative ion generation, and natural environmental protection.

[0036] The graphene contained in the graphene mask cloth has sharp edges that can pierce the cell walls and cell membranes of bacteria and extract phospholipid molecules on the cell membranes on a large scale. The unique two-dimensional structure of graphene enables it to interact strongly with phospholipid molecules, causing a large number of phospholipid molecules to detach from the cell membrane.

[0037] The graphene mask cloth can raise the skin's average temperature by up to 1.9°C, open the user's skin pores, and improve the absorption of rose extract, chrysanthemum extract and Ganoderma lucidum essence, thereby continuously transporting the absorbed rose extract, chrysanthemum extract and Ganoderma lucidum essence to the skin through the skin-friendly layer, achieving continuous moisturizing and whitening effects.

[0038] The biomass graphene in component A is well compatible with the graphene mask cloth in component B.

[0039] The effects of Bletilla striata extract are as follows:

[0040] Whitening: Bletilla striata extract is rich in saponins and multiple vitamins, which can inhibit the formation and diffusion of melanin, thereby achieving a whitening effect.

[0041] Moisturizing: The polysaccharides in Bletilla striata extract can form a moisturizing film, lock in moisture, and have a significant moisturizing effect.

[0042] Lightens spots: Bletilla striata extract can promote skin metabolism, inhibit melanin synthesis, and thus lighten spots.

[0043] Anti-inflammatory and soothing: The ingredients in Bletilla striata extract have anti-inflammatory effects, which can reduce inflammation and edema of the skin and achieve a soothing effect.

[0044] Promote wound healing: Bletilla striata extract helps accelerate the regeneration of skin cells, promote wound healing and reduce scar formation.

[0045] Firming skin: Bletilla striata extract has a certain astringent effect, which can help tighten the skin and make it firmer and more elastic.

[0046] Calendula extract has the following effects:

[0047] Soothing and repairing: The flavonoids in calendula extract have sedative and anti-inflammatory effects, which can reduce skin inflammation and relieve discomfort symptoms such as redness, swelling, and itching. In addition, its ingredients can inhibit the release of histamine and reduce the occurrence of allergic reactions.

[0048] Hydrating and moisturizing: Calendula extract has a good moisturizing effect, which can increase the moisture in the skin, relieve dry skin and keep the skin hydrated. Its ability to lock in moisture and moisturize helps maintain the moisture balance of the skin, making the skin softer and more elastic.

[0049] Antibacterial and anti-inflammatory: Calendula extract has an inhibitory effect on a variety of bacteria and fungi, which can help prevent and treat skin infections and reduce skin inflammation. This is especially beneficial for sensitive skin and damaged skin.

[0050] Whitening and brightening: Vitamin C and other antioxidant ingredients in calendula extract can inhibit the production of melanin, help brighten the skin, and reduce spots and dullness. Long-term use of products containing calendula extract can gradually improve uneven skin tone and make the skin brighter.

[0051] Ginseng extract has the following effects:

[0052] Nourishing the skin and promoting cell regeneration: Ginseng extract is rich in a variety of nutrients, such as ginsenosides, amino acids, polysaccharides and trace elements, which can nourish the skin, promote cell regeneration and repair, make the skin smooth and delicate, and have anti-aging effects. In addition, the bioactive substances in ginseng extract, such as ginsenotriol and ginseng phospholipids, can promote skin metabolism, improve skin blood circulation and metabolic capacity, thereby providing comprehensive nourishment and deep care.

[0053] Regulates water-oil balance and soothes skin: Ginseng extract can regulate the water-oil balance of the skin, reduce oil secretion, and improve skin quality. It can also soothe the skin, reduce stress and irritation on the skin, and make the skin healthier. In addition, the anti-inflammatory ingredients in ginseng extract, such as ginsenosides Rg3 and Rb1, can effectively inhibit skin inflammation, reduce symptoms such as skin redness, swelling, itching and pain, and help keep the skin healthy.

[0054] Antioxidant and anti-aging: Antioxidants in ginseng extract, such as ginsenosides and root bark polysaccharides, can fight against free radical damage, improve skin quality, slow down the aging process, and make the skin younger and more elastic. It can also deeply nourish the skin, repair damaged stratum corneum, lock in moisture, achieve a long-lasting moisturizing effect, and shrink pores, making the skin more hydrated and delicate.

[0055] The effects of chrysanthemum extract are as follows:

[0056] Moisturizing: The flavonoids and amino acids in chrysanthemum extract can penetrate deep into the skin, promote skin cell metabolism, enhance moisturizing ability, and make the skin soft, delicate and hydrated.

[0057] Antioxidant: Flavonoids have significant antioxidant effects, which can effectively neutralize free radicals, slow down the skin aging process, and reduce the appearance of wrinkles and sagging.

[0058] Anti-inflammatory: The anti-inflammatory ingredients in chrysanthemum extract can reduce skin inflammation, relieve allergic symptoms, promote wound healing, and are suitable for sensitive skin.

[0059] Soothing and anti-allergic: Its antibacterial and anti-inflammatory effects can prevent allergies, repair damaged skin, reduce the occurrence of red blood vessels and acne, and make the skin more stable and healthy.

[0060] Glycerin plays a major role in moisturizing and nourishing in facial masks, and also plays a certain role as a solvent in facial mask formulas. Glycerin is a natural moisturizer that can absorb moisture from the air and lock moisture on the skin surface, thereby keeping the skin moisturized. It is especially suitable for dry and dehydrated skin. In addition, glycerin also has antioxidant, skin repair and skin irritation relief effects, which can help slow down the skin aging process, promote the skin's natural repair process, and reduce skin irritation.

[0061] The effects of propylene glycol are as follows:

[0062] Moisturizing: Propylene glycol is a moisturizer that also plays a certain role as a solvent in the mask formula. Propylene glycol can absorb moisture from the air and help the skin stay hydrated, preventing dryness and peeling. Adding propylene glycol to the mask formula can improve the mask's moisturizing effect, prevent moisture loss, and achieve moisturizing effects by increasing the water content of the stratum corneum and improving skin permeability.

[0063] Promote skin barrier repair: Since propylene glycol has a certain permeability, it can help promote the skin to absorb nutrients, thereby promoting the repair of the skin barrier. Using a mask containing propylene glycol can promote the skin to absorb beneficial ingredients and help repair the skin barrier.

[0064] Anti-inflammatory: Propylene glycol has the effects of inhibiting the release of inflammatory mediators and reducing capillary dilation, so it can play an anti-inflammatory role. For people with sensitive skin or prone to inflammation, choosing a mask containing propylene glycol can help relieve skin discomfort.

[0065] Antibacterial: Propylene glycol has a certain antibacterial effect, which works by interfering with the synthesis of bacterial cell walls and disrupting their metabolic processes. Using a mask containing propylene glycol can help reduce the number of facial bacteria and prevent acne and other problems.

[0066] Auxiliary whitening: Propylene glycol can promote epidermal cell renewal, accelerate melanin metabolism, and has an antioxidant effect, which helps to lighten spots. Regular care with a mask that is formulated with an appropriate amount of propylene glycol and is suitable for skin tone adjustment can help achieve a whitening effect.

[0067] Deionized water is water that has had all ions (including charged molecules) removed from it. It is a highly pure water with a very low salt content that can quickly penetrate deep into the skin to replenish moisture. Adding deionized water to the mask formula, in addition to playing a certain role as a solvent, can also help the skin lock moisture in the skin, forming a protective film that keeps the skin hydrated for a long time.

[0068] The beneficial effects of the present invention are:

[0069] The biomass graphene of component A and the graphene mask cloth of component B of the present invention not only have good compatibility, but also have a synergistic effect, making the loaded bletilla striata extract, calendula extract, ginseng extract and chrysanthemum extract easier to absorb, keeping the face moisturized, continuously promoting skin absorption, and effectively improving the skin. DETAILED DESCRIPTION

[0070] The present invention is described in detail below through specific examples, but the use and purpose of these exemplary implementation modes are only used to illustrate the present invention, and do not constitute any form of limitation on the actual protection scope of the present invention, nor limit the protection scope of the present invention to them.

[0071] If no specific techniques or conditions are specified in the examples, the techniques or conditions described in the literature in the field or the product instructions are used. If no manufacturer is specified for the reagents or instruments used, they are all conventional products that can be purchased commercially.

[0072] Unless otherwise specified, the contents of the components in the following examples and comparative examples are all in parts by weight.

[0073] Example 1

[0074] The graphene hyaluronic acid mask of this embodiment is composed of the following component A and component B, and the composition of component A is as follows:

[0075]

[0076] Component B is graphene membrane cloth, and component B serves as a carrier to carry component A.

[0077] The calendula extract is obtained by the following preparation method: fresh calendula petals are placed in a distillation kettle, and then 3-4 times the weight of water is added for distillation, and the distillation temperature is controlled to be 100-120° C. and the pressure is 6-8 MPa to obtain the calendula extract.

[0078] The chrysanthemum extract is obtained by the following preparation method: fresh chrysanthemum petals are placed in a distillation kettle, and then 1-2 times the weight of water is added for distillation, and the distillation temperature is controlled to be 100-120° C. and the pressure is 4-5 MPa to obtain the chrysanthemum extract.

[0079] The ginseng extract is prepared by the following method: after crushing the ginseng root, adding 3-4 times of deionized water by weight, soaking for 1-2 hours, ultrasonic extraction for 30-40 minutes, filtering, centrifuging, taking the supernatant and concentrating it to obtain the ginseng extract.

[0080] The bletilla striata extract is prepared by the following method: after the bletilla striata root is crushed, 2-3 times of its weight of deionized water is added, and the mixture is soaked for 1-2 hours, ultrasonically extracted for 40-50 minutes, filtered, centrifuged, and the supernatant is concentrated to obtain the bletilla striata extract.

[0081] The preparation method of the graphene hyaluronic acid facial mask of this embodiment comprises the following steps:

[0082] S1. Mix hyaluronic acid, hexapeptide, glycerin, propylene glycol and deionized water, and stir at a speed of 2000-2500 r / min to form a mixture A;

[0083] S2. Pump mixture A into an emulsifier, stir at a speed of 1500-2000r / min, at a temperature of 50-60°C, homogenize for 5-10 minutes, keep warm for 50-60min, then stir and cool down;

[0084] S3. The mixture A is cooled to 25-30 ° C, and the bletilla extract, calendula extract, ginseng extract and chrysanthemum extract are added to the mixture A, and the mixture is stirred and discharged to form a mixture B;

[0085] S4. Add biomass graphene to mixture B at a speed of 3000-4000 r / min and stir for 60-70 min to fully disperse the biomass graphene to obtain mixture C;

[0086] S5. Fill the mixture C into the mask bag containing the graphene membrane cloth, and squeeze it so that the mixture C is fully carried in the graphene mask cloth.

[0087] Example 2

[0088] Referring to Example 1, the difference from Example 1 is that in the graphene hyaluronic acid mask of this embodiment, the composition of component A is as follows:

[0089]

[0090] Example 3

[0091] Referring to Example 1, the difference from Example 1 is that in the graphene hyaluronic acid mask of this embodiment, the composition of component A is as follows:

[0092]

[0093] Comparative Example 1

[0094] Referring to Example 2, the difference from Example 2 is that the facial mask of this embodiment does not use graphene facial mask cloth, but uses ordinary non-woven facial mask cloth as component B.

[0095] Comparative Example 2

[0096] Referring to Example 2, the difference from Example 2 is that the mask of this embodiment does not use biomass graphene, and the amount of deionized water is 4.3 parts. There is no S4 in the preparation step, and the mixture B is directly filled into the mask bag containing the graphene membrane cloth, and squeezed so that the mixture B is fully carried in the graphene mask cloth.

[0097] In vitro antibacterial experiments were conducted on the facial masks prepared in Examples 1-3 and Comparative Examples 1-2. The results are shown in Table 1.

[0098] Table 1

[0099]

[0100] The criteria for judging the qualitative results of in vitro antibacterial assay are as follows: an inhibition zone diameter less than 8 mm is insensitive (-), 8 to 13 mm is low sensitivity (+), 13 to 19 mm is moderately sensitive (++), and more than 19 mm is highly sensitive (+++).

[0101] It can be seen from Table 1 above that compared with Comparative Examples 1 and 2, the biomass graphene of component A of the present invention and the graphene mask cloth of component B not only have good compatibility, but also have a synergistic effect, which also makes the loaded Bletilla striata extract, Calendula officinalis extract, ginseng extract and chrysanthemum extract easier to absorb, keeps the face moisturized, continuously promotes skin absorption, and effectively improves the skin.

[0102] The facial masks of Examples 1-3 were tested for sensory, physical, chemical and hygienic indicators with reference to standard QB / T 2872-2017. The test results are shown in Table 2.

[0103] Table 2

[0104]

[0105]

[0106] The series of detailed descriptions listed above are only specific descriptions of feasible embodiments of the present invention. They are not intended to limit the scope of protection of the present invention. All equivalent embodiments or changes that do not deviate from the technical spirit of the present invention should be included in the scope of protection of the present invention.

Claims

1. A graphene hyaluronic acid facial mask, characterized in that: It consists of component A and component B. By weight, the composition of component A is as follows: Component B is a graphene membrane cloth, and component B serves as a carrier to carry component A.

2. The graphene hyaluronic acid facial mask according to claim 1, characterized in that: The calendula extract is obtained by the following preparation method: fresh calendula petals are placed in a distillation kettle, and then 3-4 times the weight of water is added for distillation, and the distillation temperature is controlled to be 100-120° C. and the pressure is 6-8 MPa to obtain the calendula extract.

3. The graphene hyaluronic acid facial mask according to claim 1, characterized in that, The chrysanthemum extract is obtained by the following preparation method: fresh chrysanthemum petals are placed in a distillation kettle, and then 1-2 times the weight of water is added for distillation, and the distillation temperature is controlled to be 100-120° C. and the pressure is 4-5 MPa to obtain the chrysanthemum extract.

4. The graphene hyaluronic acid facial mask according to claim 1, characterized in that: The ginseng extract is prepared by the following method: after crushing the ginseng root, adding 3-4 times of deionized water by weight, soaking for 1-2 hours, ultrasonic extraction for 30-40 minutes, filtering, centrifuging, taking the supernatant and concentrating it to obtain the ginseng extract.

5. The graphene hyaluronic acid facial mask according to claim 1, characterized in that: The bletilla striata extract is prepared by the following method: after the bletilla striata root is crushed, 2-3 times of deionized water by weight is added, and the root is soaked for 1-2 hours, ultrasonic extraction is performed for 40-50 minutes, filtration is performed, centrifugation is performed, and the supernatant is concentrated to obtain the bletilla striata extract.

6. A method for preparing the graphene hyaluronic acid facial mask according to any one of claims 1 to 5, characterized in that: The steps include: S1. Mix hyaluronic acid, hexapeptide, glycerin, propylene glycol and deionized water, and stir at a speed of 2000-2500 r / min to form a mixture A; S2. Pump mixture A into an emulsifier, stir at a speed of 1500-2000r / min, at a temperature of 50-60°C, homogenize for 5-10 minutes, keep warm for 50-60min, then stir and cool down; S3. The mixture A is cooled to 25-30 ° C, and Bletilla striata extract, Calendula officinalis extract, ginseng extract and chrysanthemum extract are added to the mixture A, and the mixture is stirred and discharged to form a mixture B; S4. Add biomass graphene to mixture B at a speed of 3000-4000 r / min and stir for 60-70 min to fully disperse the biomass graphene to obtain mixture C; S5. Fill the mixture C into the mask bag containing the graphene membrane cloth, and squeeze it so that the mixture C is fully carried in the graphene mask cloth.

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