Ferulic acid preparation enzymolysis equipment and method

By introducing a circulating feed pipe and a liftable crushing platform into the enzymatic hydrolysis equipment, the problems of material deposition and agglomeration in the enzymatic hydrolysis equipment were solved, realizing the efficient extraction and automated production of ferulic acid, and improving production efficiency and economic benefits.

CN121136813APending Publication Date: 2025-12-16HEZE XINDA BIOTECHNOLOGY CO LTD
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Patent Information

Application Number
CN202511546276.4
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-10-28
Publication Date
2025-12-16

AI Technical Summary

Technical Problem

Existing enzymatic hydrolysis equipment for ferulic acid preparation suffers from a single stirring method, which leads to the deposition and accumulation of dense solid enzymatic hydrolysis raw materials at the bottom of the reaction tank, forming clumps and affecting the extraction rate and production efficiency.

Method used

An enzymatic hydrolysis device was designed, comprising a circulating material pipe, a lifting crushing arc plate, and a crushing mechanism. Through the forced circulation of the circulating material pipe and the lifting crushing platform, material deposition is avoided, and online real-time crushing of agglomerates is achieved, ensuring uniform mixing and full enzymatic hydrolysis.

Benefits of technology

It effectively prevents the static accumulation of materials at the bottom of the tank, improves the extraction efficiency of ferulic acid and the utilization rate of raw materials, realizes automated operation, reduces energy consumption, and improves production efficiency and economic benefits.

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Abstract

The invention relates to the technical field of ferulic acid preparation, and discloses ferulic acid preparation enzymolysis equipment and method, and the ferulic acid preparation enzymolysis equipment comprises an enzymolysis tank, a circulating material pipe, a conical material plate, a filter screen, a liftable crushing arc plate and a rolling crushing mechanism. The invention aims to solve the technical problems of insufficient enzymolysis and low extraction rate caused by easy accumulation and caking of raw materials at the tank bottom due to insufficient stirring in the existing enzymolysis equipment. The core is that forced circulation of materials is achieved through the circulating material pipe and the spiral conveying mechanism, and deposition is prevented; caked materials are separated by a filter screen on a conical material plate and are guided to an annular platform formed by crushing arc plates; and finally, the cakes are thoroughly crushed through the grinding and crushing mechanism, so that the cakes participate in the enzymolysis reaction again. According to the method, online integration of crushing and enzymolysis processes is realized, the contact efficiency of materials and enzyme liquid is remarkably improved, the extraction rate of ferulic acid and the product quality are effectively improved, and meanwhile, the method has the advantages of high automation degree, energy conservation and consumption reduction.
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Description

TECHNICAL FIELD

[0001] The application belongs to the technical field of ferulic acid preparation, and particularly relates to a ferulic acid preparation enzymatic hydrolysis device and method. BACKGROUND

[0002] Ferulic acid is a natural antioxidant and anti-inflammatory agent widely used in the food, pharmaceutical and cosmetic industries, and it is usually obtained by hydrolyzing ferulic acid ester bonds in plant raw materials through enzymatic hydrolysis. The core equipment of the enzymatic hydrolysis process is the enzymatic hydrolysis reactor, and its performance directly determines the extraction efficiency and product yield of ferulic acid.

[0003] In the prior art, the enzymatic hydrolysis device for preparing ferulic acid usually uses a reactor with a stirring device. Specifically, the device includes a tank body, a feed inlet and an enzyme addition port are arranged on the upper part of the tank body, a discharge port is arranged on the lower part of the tank body, and a mechanical stirring paddle (such as an anchor type or paddle type stirrer) driven by a motor is installed at the central position in the tank. When working, the raw material slurry containing ferulic acid precursors (such as rice bran and wheat bran) and specific enzyme preparations (such as ferulic acid esterase) are fed into the tank through the feed inlet, and the motor is started to drive the stirring paddle to rotate in one direction, so as to uniformly mix the raw materials and enzyme liquid, and perform enzymatic hydrolysis reaction under the set temperature and pH conditions.

[0004] However, the existing enzymatic hydrolysis device has obvious defects. The most important defect is that due to the single stirring mode and the existence of stirring dead angles, the solid enzymatic raw materials with high density (such as bran particles) are prone to deposit and accumulate in the central area of the bottom of the reactor. During the enzymatic hydrolysis reaction, these deposited raw materials will adhere to each other due to their own viscosity and the viscosity of the enzymatic hydrolysis products, forming clumps that are difficult to break up. The mass transfer barrier is formed inside the clumps, and the enzyme liquid outside cannot effectively penetrate into the inside to fully contact with the substrate, resulting in that the internal ferulic acid precursors cannot be fully hydrolyzed, and finally causing problems such as decreased extraction rate, raw material waste, prolonged reaction period, increased energy consumption, etc., which seriously restricts the production efficiency and reduces the economic benefits. SUMMARY

[0005] The purpose of the embodiment of the application is to provide a ferulic acid preparation enzymatic hydrolysis device and method, which aims to solve the above problems.

[0006] The application is achieved as follows: a ferulic acid preparation enzymatic hydrolysis device, comprising an enzymatic hydrolysis tank, further comprising: a circulating pipe fixedly arranged at the center of the enzymatic hydrolysis tank, a feeding port arranged at the bottom of the circulating pipe, a discharging port arranged at the side wall near the top of the circulating pipe, a conical bottom of the enzymatic hydrolysis tank, a conveying mechanism arranged in the circulating pipe for conveying materials upward; a conical material plate fixedly arranged in the enzymatic hydrolysis tank, a filter screen arranged on the conical material plate, a plurality of broken arc plates one uniformly arranged at the edge of the conical material plate, and a broken arc plate two arranged between every two broken arc plates one; a lifting mechanism arranged in the enzymatic hydrolysis tank, the lifting mechanism being used for driving the plurality of broken arc plates two to move up and down, the plurality of broken arc plates one and the plurality of broken arc plates two forming a ring-shaped broken platform after the plurality of broken arc plates two move upward, and a rolling and crushing mechanism arranged in the enzymatic hydrolysis tank, the rolling and crushing mechanism being used for crushing the materials collected on the broken platform.

[0007] Further technical solutions, the top of the enzymatic hydrolysis tank is fixedly provided with a feeding pipe, the bottom of the enzymatic hydrolysis tank is fixedly provided with a discharging pipe, and a check valve is arranged on the discharging pipe.

[0008] Further technical solutions, the conveying mechanism comprises a rotating shaft rotatably connected at the center of the circulating pipe, a helical blade fixedly arranged on the side wall of the rotating shaft, a motor one fixedly arranged at the top of the enzymatic hydrolysis tank, and a rotating end of the motor one fixedly connected with the top of the rotating shaft.

[0009] Further technical solutions, the rolling and crushing mechanism comprises a rotating ring rotatably arranged in the enzymatic hydrolysis tank, at least one guide groove one arranged at the bottom of the rotating ring, a rolling block vertically and slidably connected in the guide groove one, a compression spring one fixedly arranged at the top of the rolling block, and a tail end of the compression spring one fixedly arranged in the compression spring one, and a rotating assembly arranged on the side wall of the enzymatic hydrolysis tank and used for driving the rotating ring to rotate.

[0010] Further technical solutions, the rotating assembly comprises an outer gear ring fixedly embedded on the side wall of the rotating ring, a motor two fixedly arranged on the side wall of the enzymatic hydrolysis tank, a rotating end of the motor two fixedly provided with a gear, and the gear engaged with the outer gear ring, and an avoiding groove arranged on the side wall of the enzymatic hydrolysis tank and used for avoiding the engagement between the gear and the outer gear ring.

[0011] Further technical solutions, the lifting mechanism comprises a mounting frame slidably connected on the side wall of the circulating pipe, the plurality of broken arc plates two uniformly fixedly arranged on the edge of the mounting frame, a telescopic piece fixedly arranged on the top of the enzymatic hydrolysis tank through a support, a connecting frame fixedly arranged at the telescopic end of the telescopic piece, and the connecting frame connected with the mounting frame.

[0012] Further technical solutions, a conical guide plate is fixedly arranged on the connecting frame, the conical guide plate is arranged above the conical material plate, a scraper is arranged above the filter screen, and the scraper is fixedly arranged on the rotating ring.

[0013] Further technical solutions, the inner wall of the enzymatic tank is provided with a locking groove, a locking rod is radially slidably connected to the mounting frame, a transmission assembly is arranged on the mounting frame, and the transmission assembly drives the locking rod to slide radially on the mounting frame by moving up and down through the connecting frame.

[0014] Further technical solutions, the transmission assembly includes two sink grooves and guide grooves arranged in sequence from top to bottom in the mounting frame, the two sink grooves and guide grooves are communicatively arranged, a stepped sliding sleeve is vertically and slidably connected in the second guide groove, a compression spring two is fixedly arranged on the top of the stepped sliding sleeve, the end of the compression spring two is fixedly arranged in the sink groove, a transmission shaft is fixedly arranged on the side wall of the stepped sliding sleeve, and one end of the locking rod is provided with an inclined long hole, and the transmission shaft is slidably connected in the long hole.

[0015] A ferulic acid preparation enzymatic method based on the above-mentioned ferulic acid preparation enzymatic equipment, comprising the following steps: S1, during the enzymatic reaction, the enzymatic material at the bottom of the enzymatic tank enters the circulating pipe from the feed port, and the conveying mechanism sends the enzymatic material at the bottom of the circulating pipe out from the discharge port; S2, the enzymatic material falls on the conical material plate, the unblocked enzymatic material passes through the filter screen, and the blocked enzymatic material is collected by the filter screen and falls on the crushing platform formed by the plurality of crushing arc plates one and the plurality of crushing arc plates two; S3, the rolling crushing mechanism crushes the collected material on the crushing platform; S4, after the rolling crushing of the blocked enzymatic material is completed, the lifting mechanism drives the plurality of crushing arc plates two to move downward, the crushing arc plates one and the crushing arc plates two are misaligned and form a gap, and the crushed enzymatic material moves downward Compared with the prior art, the beneficial effects of the present application are: 1. Effectively prevent the bottom from accumulating and blocking: By arranging the built-in circulating pipe and the conveying mechanism (screw blade), the material deposited at the bottom of the tank can be actively lifted upward and re-sprayed to the upper part of the reaction system, forming a forced circulation flow, breaking the dead angle existing in the traditional stirring, and fundamentally avoiding the static accumulation of the material at the bottom, significantly reducing the risk of blocking; 2. Realize the online real-time crushing of the blocked material: The ring-shaped crushing platform composed of the lifting crushing arc plates and the rolling crushing mechanism are innovatively designed. The filter screen can intercept and collect the blocks formed in the reaction liquid and guide them to the crushing platform. The rolling block continuously rolls and crushes the blocks under the action of the pressure spring, solving the core pain point that the blocks in the traditional equipment cannot be dispersed by the stirring paddle, ultimately affecting the overall enzymatic effect; 3. Improved enzymatic efficiency and product yield: By forced circulation, the material is more evenly contacted with the enzyme solution, and at the same time, the generated clumps can be timely crushed, eliminating the mass transfer barrier, so that the ferulic acid precursor can be fully enzymatically hydrolyzed, thereby significantly improving the extraction efficiency of ferulic acid and the utilization rate of raw materials; 4. High degree of automation, reducing manual intervention: The entire circulation, filtration, crushing and unloading process can be programmed controlled by motor and telescopic parts, realizing the automatic operation of continuous or batch processing, not only reducing the labor intensity, but also ensuring the controllability and stability of the production process.

[0016] 5. Energy saving: By promoting uniform mixing and sufficient reaction of the material, it is expected to shorten the reaction time required to achieve the same enzymatic effect, thereby reducing energy consumption and meeting the requirements of green production. BRIEF DESCRIPTION OF DRAWINGS

[0017] Figure 1 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 2 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 1 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 3 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 2 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 4 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 3 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 5 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 4 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 6 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 5 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 7 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application; Figure 3 A structure diagram of the enzyme hydrolysis device and method for preparing ferulic acid provided by the present application.

[0018] In the drawings: 101, enzyme hydrolysis tank; 102, unloading pipe; 103, feeding pipe; 104, circulating pipe; 105, feeding port; 106, discharging port; 107, conical guide plate; 108, filter screen; 109, crushing arc plate one; 110, crushing arc plate two; 111, scraper; 112, conical guide plate; 2, conveying mechanism; 201, rotating shaft; 202, spiral blade; 203, motor one; 3, rolling crushing mechanism; 301, rotating ring; 302, guide groove one; 303, rolling block; 304, compression spring one; 4, rotating assembly; 401, outer tooth ring; 402, gear; 403, motor two; 5, lifting mechanism; 501, connecting frame; 502, mounting frame; 503, telescopic part; 601, locking groove; 602, locking rod; 7, transmission assembly; 701, guide groove two; 702, sink groove; 703, stepped sliding sleeve; 704, compression spring two; 705, transmission shaft; 706, long hole. DETAILED DESCRIPTION

[0019] In order to make the purpose, technical scheme and advantages of the present application more clear, the present application is further described in detail below in combination with the drawings and examples. It should be understood that the specific examples described herein are only used to explain the present application and do not limit the present application.

[0020] The specific implementation of the present application is described in detail below in combination with specific examples.

[0021] As Figure 1 shown, an enzyme hydrolysis equipment for preparing ferulic acid provided by an embodiment of the present application, comprising an enzyme hydrolysis tank 101, further comprising: a circulating pipe 104 fixedly arranged at the center of the enzyme hydrolysis tank 101, wherein the bottom of the circulating pipe 104 is provided with a feeding port 105, the sidewall near the top of the circulating pipe 104 is provided with a discharging port 106, the bottom of the enzyme hydrolysis tank 101 is conically arranged, and the circulating pipe 104 is provided with a conveying mechanism 2 for conveying materials upward; the enzyme hydrolysis tank 101 is fixedly provided with a conical material plate 107, the conical material plate 107 is provided with a filter screen 108, and the edge of the conical material plate 107 is uniformly provided with a plurality of broken arc plates one 109, and a broken arc plate two 110 is arranged between every two broken arc plates one 109; the enzyme hydrolysis tank 101 is provided with a lifting mechanism 5, the lifting mechanism 5 is used to drive the plurality of broken arc plates two 110 to move up and down, after the plurality of broken arc plates two 110 move upward, the plurality of broken arc plates one 109 and the plurality of broken arc plates two 110 form a broken platform in a ring shape, the enzyme hydrolysis tank 101 is provided with a rolling and crushing mechanism 3, the rolling and crushing mechanism 3 is used to crush the materials collected on the broken platform; the top of the enzyme hydrolysis tank 101 is fixedly provided with a feeding pipe 103, the bottom of the enzyme hydrolysis tank 101 is fixedly provided with a discharging pipe 102, and the discharging pipe 102 is provided with a check valve.

[0022] In the embodiment of the present application, the enzymatic raw material is supplied into the enzymatic tank 101 through the feeding pipe 103, and when the enzymatic reaction is carried out, the enzymatic material at the bottom of the enzymatic tank 101 enters the circulating material pipe 104 from the feeding port 105, the conveying mechanism 2 sends the enzymatic material at the bottom of the circulating material pipe 104 out from the discharging port 106, the enzymatic material falls on the conical material plate 107, the un-caked enzymatic material passes through the filter screen 108, thereby promoting the circulation of the enzymatic material from top to bottom, avoiding the accumulation of the enzymatic material at the bottom of the enzymatic tank 101, promoting the flow of the enzymatic material, the caked enzymatic material is collected by the filter screen 108 and falls on the crushing platform formed by the plurality of the first crushing arc plates 109 and the plurality of the second crushing arc plates 110, the crushing mechanism 3 crushes the material collected on the crushing platform, after the crushing of the caked enzymatic material is completed, the lifting mechanism 5 drives the plurality of the second crushing arc plates 110 to move downward, the first crushing arc plates 109 and the second crushing arc plates 110 are misaligned and form a gap, the crushed enzymatic material moves downward, thereby completing a crushing process of the caked enzymatic material, avoiding the insufficient enzymatic reaction caused by the caking or insufficient crushing of the enzymatic material, after the enzymatic reaction is completed, the non-return valve on the discharging pipe 102 is opened, and the raw material in the enzymatic tank 101 is discharged.

[0023] As shown in Figure 2 , Figure 3 and Figure 4 , as a preferred embodiment of the present application, the conveying mechanism 2 comprises a rotating shaft 201 rotatably connected at the axis in the circulating material pipe 104, a spiral blade 202 is fixed on the side wall of the rotating shaft 201, a motor one 203 is fixed on the top of the enzymatic tank 101, and the rotating end of the motor one 203 is fixedly connected with the top of the rotating shaft 201.

[0024] In the embodiment of the present application, the motor one 203 drives the rotating shaft 201 to rotate, the rotating shaft 201 drives the spiral blade 202 to rotate, the rotating spiral blade 202 generates the lifting force to push the enzymatic raw material in the circulating material pipe 104 to move upward, when the enzymatic reaction is completed, the motor one 203 is reversed, and the reversed spiral blade 202 generates the downward pushing force to assist the discharging.

[0025] As shown in Figure 2 , Figure 3 and Figure 7As shown, in a preferred embodiment of the present invention, the crushing and grinding mechanism 3 includes a rotating ring 301 rotatably connected inside the enzymatic hydrolysis tank 101. At least one guide groove 302 is provided at the bottom of the rotating ring 301. A crushing block 303 is vertically slidably connected within the guide groove 302. A compression spring 304 is fixedly mounted on the top of the crushing block 303, and the end of the compression spring 304 is fixedly mounted inside the compression spring 304. A rotating mechanism for driving the rotating ring 301 to rotate is provided on the side wall of the enzymatic hydrolysis tank 101. Component 4; The rotating component 4 includes an external gear ring 401 embedded and fixed on the side wall of the rotating ring 301, and a second motor 403 fixed on the side wall of the enzymatic hydrolysis tank 101. A gear 402 is fixed on the rotating end of the second motor 403. The gear 402 meshes with the external gear ring 401. An avoidance groove is provided on the side wall of the enzymatic hydrolysis tank 101 to avoid the meshing of the gear 402 with the external gear ring 401. A scraper 111 is provided above the filter screen 108 and is fixed on the rotating ring 301.

[0026] In this embodiment of the invention, when crushing agglomerated raw materials, motor 403 drives gear 402 to rotate, gear 402 drives external gear ring 401 to rotate, external gear ring 401 drives rotating ring 301 to rotate, rotating ring 301 drives crushing block 303 and scraper 111 to rotate, and compression spring 304 pushes crushing block 303 downward, so that crushing block 303 and crushing platform crush agglomerated raw materials. When rotating ring 301 drives scraper 111 to rotate, scraper 111 pushes agglomerated raw materials collected on filter screen 108, promoting agglomerated raw materials to fall quickly onto crushing platform.

[0027] like Figure 1 , Figure 4 and Figure 5 As shown, in a preferred embodiment of the present invention, the lifting mechanism 5 includes a mounting frame 502 slidably connected to the side wall of the circulating material pipe 104, a plurality of the crushing arc plates 110 being uniformly fixed on the edge of the mounting frame 502, a telescopic member 503 being fixedly mounted on the top of the enzymatic hydrolysis tank 101 via a bracket, a connecting frame 501 being fixedly mounted on the telescopic end of the telescopic member 503, and the connecting frame 501 being connected to the mounting frame 502; a conical guide plate 112 is fixedly mounted on the connecting frame 501, and the conical guide plate 112 is located above the conical material plate 107.

[0028] In this embodiment of the invention, when the telescopic member 503 retracts, the telescopic member 503 drives the connecting frame 501 to move upward, the connecting frame 501 drives the mounting frame 502 and the conical guide plate 112 to move upward, the mounting frame 502 drives multiple crushing arc plates 110 to move upward, and multiple crushing arc plates 109 and multiple crushing arc plates 110 form an annular crushing platform, and the conical guide plate 112 is located above the discharge port 106; When the telescopic part 503 is extended, the telescopic part 503 drives the connecting frame 501 to move downward, the connecting frame 501 drives the mounting frame 502 and the conical guide plate 112 to move downward, the mounting frame 502 drives the plurality of broken arc plates two 110 to move downward, the plurality of broken arc plates one 109 and the plurality of broken arc plates two 110 are dislocated, which facilitates the downward movement of the crushed raw materials, and the conical guide plate 112 moves below the discharge port 106, the enzyme raw materials discharged from the discharge port 106 are guided by the conical guide plate 112 and fall on the broken arc plate one 109 and the broken arc plate two 110, the enzyme raw materials flush the broken arc plate one 109 and the broken arc plate two 110, which facilitates the downward movement of the crushed enzyme raw materials on the broken arc plate one 109 and the broken arc plate two 110, and avoids the enzyme raw materials remaining on the broken arc plate one 109 and the broken arc plate two 110.

[0029] As shown in Figures 4-7 As a preferred embodiment of the present application, a locking groove 601 is arranged on the inner wall of the enzyme tank 101, a locking rod 602 is radially and slidingly connected to the mounting frame 502, a transmission assembly 7 is arranged on the mounting frame 502, and the transmission assembly 7 drives the locking rod 602 to radially slide on the mounting frame 502 by moving the connecting frame 501 up and down.

[0030] In the embodiment of the present application, when the telescopic part 503 is retracted, the telescopic part 503 drives the connecting frame 501 to move upwards, the connecting frame 501 drives the stepped sliding sleeve 703 to move upwards, the stepped sliding sleeve 703 drives the mounting frame 502 to move upwards through the compression spring 704, the mounting frame 502 drives the plurality of broken arc plates two 110 to move upwards, until the plurality of broken arc plates one 109 and the plurality of broken arc plates two 110 form a ring-shaped crushing platform, when the plurality of broken arc plates two 110 cannot continue to move upwards, the connecting frame 501 continues to drive the stepped sliding sleeve 703 to move upwards, the compression spring 704 is gradually compressed, the stepped sliding sleeve 703 drives the transmission shaft 705 to move upwards relative to the mounting frame 502 and the locking rod 602, the transmission shaft 705 pushes the locking rod 602 through the long hole 706, the locking rod 602 moves to the locking groove 601 on the inner wall of the enzymatic tank 101, until the end of the locking rod 602 is inserted into the locking groove 601, the stepped sliding sleeve 703 moves to the top of the guide groove two 701 and cannot continue to move, by inserting the end of the locking rod 602 into the locking groove 601, the support effect of the broken arc plates two 110 can be improved, so that the plurality of broken arc plates one 109 and the plurality of broken arc plates two 110 form a stable ring-shaped crushing platform; When the telescopic part 503 is extended, the telescopic part 503 drives the connecting frame 501 to move downwards, the connecting frame 501 drives the stepped sliding sleeve 703 to move downwards, at this time the compression spring 704 is gradually extended, the height of the mounting frame 502 and the locking rod 602 remains unchanged, the stepped sliding sleeve 703 drives the transmission shaft 705 to move downwards, the transmission shaft 705 moving downwards pulls the locking rod 602 to move horizontally through the long hole 706, until the locking rod 602 is separated from the locking groove 601, the stepped sliding sleeve 703 moves to the bottom of the guide groove two 701, the stepped sliding sleeve 703 drives the mounting frame 502 to move downwards again, the mounting frame 502 drives the plurality of broken arc plates two 110 to move downwards, the plurality of broken arc plates one 109 and the plurality of broken arc plates two 110 are out of position, which facilitates the downward movement of the crushed raw materials.

[0031] An enzyme hydrolysis method for preparing ferulic acid, based on the enzyme hydrolysis equipment for preparing ferulic acid described above, comprising the following steps: S1, during the enzyme hydrolysis reaction, the enzyme hydrolysis material at the bottom of the enzymatic tank 101 enters the circulating material pipe 104 from the feed port 105, and the conveying mechanism 2 sends the enzyme hydrolysis material at the bottom of the circulating material pipe 104 out from the discharge port 106; S2, the enzyme hydrolysis material falls on the conical material plate 107, the enzyme hydrolysis material that is not caked passes through the filter screen 108, and the caked enzyme hydrolysis material is collected by the filter screen 108 and falls on the ring-shaped crushing platform formed by the plurality of broken arc plates one 109 and the plurality of broken arc plates two 110; S3, the crushing mechanism 3 crushes the material collected on the crushing platform; S4, after the crushing of the caked enzymatic hydrolysis material is finished, the lifting mechanism 5 drives multiple broken arc plate two 110 to move downward, the broken arc plate one 109 and the broken arc plate two 110 are dislocated and form a gap, and the crushed enzymatic hydrolysis material moves downward.

[0032] The above merely describes the preferred embodiments of the present application and is not used to limit the present application, and any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present application shall be included in the protection scope of the present application.

Claims

1. An enzymatic hydrolysis device for the preparation of ferulic acid, comprising an enzymatic hydrolysis tank, characterized in that, Also includes: The enzymatic hydrolysis tank has a circulating material pipe fixed at the center of the shaft. The bottom of the circulating material pipe has a feed inlet and the side wall near the top of the circulating material pipe has a discharge outlet. The bottom of the enzymatic hydrolysis tank is conical. The circulating material pipe is equipped with a conveying mechanism for conveying materials upward. The enzymatic hydrolysis tank is equipped with a conical material plate, a filter screen is installed on the conical material plate, and multiple crushing arc plates are evenly arranged at the edge of the conical material plate. A crushing arc plate is arranged between every two crushing arc plates. The enzymatic hydrolysis tank is equipped with a lifting mechanism, which is used to drive multiple crushing arc plates II to move up and down. After the multiple crushing arc plates II move upward, the multiple crushing arc plates I and the multiple crushing arc plates II form a ring-shaped crushing platform. The enzymatic hydrolysis tank is equipped with a crushing and grinding mechanism, which is used to crush the material collected on the crushing platform.

2. The enzymatic hydrolysis equipment for preparing ferulic acid according to claim 1, characterized in that, The top of the enzymatic hydrolysis tank is fixed with a feed pipe, and the bottom of the enzymatic hydrolysis tank is fixed with a discharge pipe, on which a check valve is installed.

3. The enzymatic hydrolysis equipment for preparing ferulic acid according to claim 1, characterized in that, The conveying mechanism includes a rotating shaft located at the center of the circulating material pipe, with spiral blades fixed on the side wall of the rotating shaft, and a motor fixed on the top of the enzymatic hydrolysis tank. The rotating end of the motor is fixedly connected to the top of the rotating shaft.

4. The enzymatic hydrolysis equipment for preparing ferulic acid according to claim 1, characterized in that, The crushing mechanism includes a rotating ring rotatably connected inside the enzymatic hydrolysis tank. At least one guide groove is provided at the bottom of the rotating ring. A crushing block is vertically slidably connected inside the guide groove. A compression spring is fixed at the top of the crushing block. The end of the compression spring is fixed inside the compression spring. A rotating assembly for driving the rotating ring to rotate is provided on the side wall of the enzymatic hydrolysis tank.

5. The enzymatic hydrolysis equipment for preparing ferulic acid according to claim 4, characterized in that, The rotating assembly includes an external gear ring embedded and fixed on the side wall of the rotating ring, and a second motor fixed on the side wall of the enzymatic hydrolysis tank. The rotating end of the second motor is fixed with a gear that meshes with the external gear ring. The side wall of the enzymatic hydrolysis tank is provided with a clearance groove to avoid the meshing of the gear and the external gear ring.

6. The enzymatic hydrolysis equipment for preparing ferulic acid according to claim 1, characterized in that, The lifting mechanism includes a mounting frame that slides on the side wall of the circulating material pipe, multiple crushing arc plates that are evenly fixed on the edge of the mounting frame, and a telescopic component that is fixed to the top of the enzymatic hydrolysis tank via a bracket. A connecting frame is fixed to the telescopic end of the telescopic component, and the connecting frame is connected to the mounting frame.

7. The enzymatic hydrolysis apparatus for preparing ferulic acid according to claim 4 or 6, characterized in that, A conical guide plate is fixed on the connecting frame, and the conical guide plate is located above the conical material plate. A scraper is provided above the filter screen and is fixed on the rotating ring.

8. The enzymatic hydrolysis apparatus for preparing ferulic acid according to claim 6, characterized in that, The inner wall of the enzymatic hydrolysis tank is provided with a locking groove, and a locking rod is radially slidably connected to the mounting frame. The mounting frame is provided with a transmission component, which drives the locking rod to slide radially on the mounting frame by moving the connecting frame up and down.

9. The enzymatic hydrolysis equipment for preparing ferulic acid according to claim 8, characterized in that, The transmission assembly includes a recessed groove and a guide groove 2 arranged sequentially from top to bottom within the mounting frame. The recessed groove and the guide groove 2 are connected. A stepped sliding sleeve is vertically slidably connected within the guide groove 2. A compression spring 2 is fixedly mounted on the top of the stepped sliding sleeve. The end of the compression spring 2 is fixedly mounted within the recessed groove. A transmission shaft is fixedly mounted on the side wall of the stepped sliding sleeve. One end of the locking rod is provided with an inclined elongated hole, and the transmission shaft is slidably connected within the elongated hole.

10. A method for the enzymatic hydrolysis of ferulic acid, based on the enzymatic hydrolysis equipment for the preparation of ferulic acid according to any one of claims 1-9, characterized in that, Includes the following steps: S1. During the enzymatic hydrolysis reaction, the enzymatic hydrolysate at the bottom of the enzymatic hydrolysis tank enters the circulating material pipe from the feed inlet, and the conveying mechanism sends the enzymatic hydrolysate at the bottom of the circulating material pipe out from the discharge outlet. S2. The enzymatically hydrolyzed material falls onto the conical material plate. Unagglomerated enzymatically hydrolyzed material passes through the filter screen, while agglomerated enzymatically hydrolyzed material is collected by the filter screen and falls onto the annular crushing platform formed by multiple crushing arc plates one and multiple crushing arc plates two. S3. The crushing and grinding mechanism crushes the material collected on the crushing platform. S4. After the agglomerated enzymatic hydrolysate is crushed, the lifting mechanism drives multiple crushing arc plates II to move downwards. The crushing arc plate I and the crushing arc plate II are misaligned and form a gap, allowing the crushed enzymatic hydrolysate to move downwards.