Phenol recycling device

By designing a phenol recycling device including heating seat, circulation pump, kettle body, condenser, filter cylinder, filter member and agitating component, the problem of poor phenol recycling quality in the acid ester production process is solved, and high efficiency is achieved phenol recycling and filtration reduces environmental pollution and material waste.

CN222445400UActive Publication Date: 2025-02-11YUJIANG COUNTY CHANGSHENG CHEM CO LTD
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Patent Information

Application Number
CN202421203952.9
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-05-30
Publication Date
2025-02-11
Estimated Expiration
2034-05-30

AI Technical Summary

Technical Problem

The water vapor with phenol produced during the acid ester production process contains catalyst impurities, which is difficult to purify, resulting in poor quality of phenol recycling and direct emissions will cause environmental pollution and waste of materials.

Method used

A phenol recycling device is designed, including a heating seat, a circulation pump, a kettle body, a condenser, a filter cylinder, a filter member and agitating assembly. The phenol waste liquid is filtered through the filter cylinder, and the agitating assembly and a heating assembly are used to improve the Purification efficiency and circulating purification through a circulation pump.

Benefits of technology

It improves the effect of phenol recycling and treatment, reduces the impurities involved in the internal, ensures the recycling quality, and can easily replace and clean the filter structure, improving the processing efficiency.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a phenol recycling device, which belongs to the technical field of phenol recycling and comprises a mounting rack, a heating seat is mounted at the bottom of the mounting rack, a kettle body for purifying and recycling phenol waste liquid is assembled in the heating seat, and a stirring component for assisting in recycling the phenol waste liquid is arranged in the kettle body; the two sides of the top of the kettle body are connected with a condenser and a filtering guide cylinder respectively, a filtering piece for filtering the phenol waste liquid before recycling is arranged in the filtering guide cylinder, and positioning assemblies for locking and fixing the filtering piece are arranged on the two sides of the filtering guide cylinder; the bottom of the heating seat is connected with a circulating pump for circularly purifying phenol waste liquid in the kettle body; according to the phenol recycling device, the phenol recycling treatment effect can be further improved, in the phenol recycling process, phenol is filtered, impurities entrained in the phenol are reduced, the recycling quality is guaranteed, the filtering structure can be conveniently replaced and cleaned, and the treatment efficiency is improved.
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Description

Technical Field

[0001] The utility model relates to the technical field of phenol recovery, in particular to a phenol recovery and utilization device. Background Art

[0002] Phenol is a colorless needle-shaped crystal with a special smell. It is toxic and can be used as an important raw material for the production of certain resins, bactericides, preservatives and drugs (such as aspirin). It can also be used for disinfecting surgical instruments and treating excrement, skin sterilization, itching and otitis media. Therefore, it is an important raw material for medical drugs.

[0003] In the process of producing certain acid esters, water vapor containing phenol is generated. However, this part of phenol usually contains catalyst impurities and is difficult to purify in general industrial devices. Therefore, this part of phenol is not very suitable as a chemical raw material. However, phenol is highly toxic, and direct discharge will cause environmental pollution and waste of materials. Therefore, the aqueous solution of phenol needs to be recycled to reduce environmental pollution. However, direct recycling of phenol is likely to affect the quality of phenol recycling. Therefore, we need to propose a phenol recycling device. Utility Model Content

[0004] The purpose of the utility model is to provide a phenol recovery and utilization device, which can further improve the effect of phenol recovery and treatment, and filter the phenol during the phenol recovery process to reduce the impurities entrained inside and ensure the quality of recovery. The filter structure can also be easily replaced and cleaned to improve the treatment efficiency, so as to solve the problems raised in the above-mentioned background technology.

[0005] To achieve the above-mentioned purpose, the utility model provides: a phenol recovery and utilization device, comprising a mounting frame, a heating seat is installed at the bottom of the mounting frame, a kettle body for purifying and recovering phenol waste liquid is assembled inside the heating seat, a stirring component for assisting the recovery of phenol waste liquid is arranged inside the kettle body; a condenser and a filter guide are respectively connected to the top two sides of the kettle body, a filter element for filtering the phenol waste liquid before recovery is arranged inside the filter guide, and positioning components for locking and fixing the filter element are arranged on both sides of the filter guide; a circulating pump for circulating and purifying the phenol waste liquid inside the kettle body is connected to the bottom of the heating seat.

[0006] Preferably, the stirring assembly includes: a connecting shaft rotatably installed inside the kettle body, and a servo motor installed on the top of the kettle body; wherein the output end of the servo motor is transmission-connected to the top of the connecting shaft, and the bottom surface of the connecting shaft is connected to a stirring rod.

[0007] Preferably, a heating coil for heating the kettle body is arranged inside the heating seat, the condenser is connected to the kettle body through a condenser pipe, and the filter guide cylinder is connected to the kettle body through a feed pipe.

[0008] Preferably, a feed pipe is connected to the bottom of the heating seat, a fixing plate is connected to the bottom of the mounting frame, the circulating pump is installed on the surface of the fixing plate, and an input end of the circulating pump is connected to the feed pipe through a pipeline.

[0009] Preferably, the output end of the circulation pump is connected to the feed pipe through a delivery pipe, and the surface of the delivery pipe is connected to one side of the mounting frame through a fixing sleeve.

[0010] Preferably, the positioning assembly includes: fixed blocks connected to both sides of the filter guide tube, and an adjustment plate slidably connected to the inner wall of the fixed block; wherein, a plug-in plate is connected to the surface of the adjustment plate, and the ends of the plug-in plate are movably inserted into both sides of the filter element, and assembly blocks are provided on both sides of the filter element.

[0011] Preferably, a locking spring is provided inside the fixing block, both ends of the locking spring are connected to the surface of the adjusting plate, assembly slots are provided on both sides of the inner wall of the filter guide cylinder, and the assembly block is slidably inserted into the inner wall of the assembly slot.

[0012] Compared with the prior art, the beneficial effects of the utility model are:

[0013] The utility model adopts the arrangement of structures such as a heating seat, a circulation pump, a kettle body, a condenser, a filter guide cylinder, a filter element, a stirring assembly and a positioning assembly, and injects phenol waste liquid into the kettle body through the filter guide cylinder. During the injection process, the phenol waste liquid will filter impurities therein through the filter element, thereby improving the quality of recovery. When replacement and maintenance are required later, the plug-in plate can be retracted into the interior of the fixed block through the adjustment plate to release the locking effect of the filter element, and the filter element can be conveniently taken out and replaced from the interior of the filter guide cylinder to ensure the filtering effect. The servo motor drives the connecting shaft to rotate so that the stirring rod stirs the interior of the kettle body, further improving the effect of the heating seat on heating the phenol waste liquid, cooperating with the condenser to recover the phenol gas from the outlet, and at the same time, the purified raw liquid can be transported through the circulation pump, and the purification process is performed again, thereby further improving the recovery effect of phenol in the raw liquid. BRIEF DESCRIPTION OF THE DRAWINGS

[0014] Figure 1 It is a schematic diagram of the overall structure of the utility model;

[0015] Figure 2 This is a schematic diagram of the heating seat structure of the utility model;

[0016] Figure 3 This is a schematic diagram of the kettle structure of the utility model;

[0017] Figure 4 This is a schematic diagram of the filter guide structure of the utility model.

[0018] In the figure: 1. mounting frame; 2. heating seat; 3. heating coil; 4. feeding pipe; 5. fixing plate; 6. fixing sleeve; 7. circulating pump; 8. conveying pipeline; 9. kettle body; 10. connecting shaft; 11. stirring rod; 12. servo motor; 13. condenser; 14. condenser; 15. feeding pipe; 16. filter guide cylinder; 17. assembly slot; 18. filter element; 19. assembly block; 20. fixing block; 21. adjusting plate; 22. plug-in board; 23. locking spring. DETAILED DESCRIPTION

[0019] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0020] See also Figure 1-4 The utility model provides: a phenol recovery and utilization device, comprising a mounting frame 1, a heating seat 2 is mounted at the bottom of the mounting frame 1, a kettle 9 for purifying and recovering phenol waste liquid is assembled inside the heating seat 2, a stirring assembly for assisting the recovery of phenol waste liquid is arranged inside the kettle 9; a condenser 14 and a filter guide 16 are respectively connected to the top two sides of the kettle 9, a filter element 18 for filtering the phenol waste liquid before recovery is arranged inside the filter guide 16, and positioning assemblies for locking and fixing the filter element 18 are arranged on both sides of the filter guide 16; a circulating pump 7 for circulating and purifying the phenol waste liquid inside the kettle 9 is connected to the bottom of the heating seat 2.

[0021] It is worth noting that, by arranging the structures such as the heating seat 2, the circulating pump 7, the kettle body 9, the condenser 14, the filter guide 16, the filter element 18, the stirring assembly and the positioning assembly, the effect of the phenol recovery treatment can be further improved, and in the process of phenol recovery, it can be filtered to reduce the impurities entrained inside, thereby ensuring the quality of recovery, and the filter structure can be conveniently replaced and cleaned to improve the efficiency of the treatment.

[0022] Specifically, the stirring assembly includes: a connecting shaft 10 rotatably installed inside the kettle body 9, and a servo motor 12 installed on the top of the kettle body 9; wherein the output end of the servo motor 12 is connected to the top of the connecting shaft 10 by transmission, and the bottom surface of the connecting shaft 10 is connected to a stirring rod 11. The kettle body 9 is an area for treating phenol waste liquid, and the connecting shaft 10 is a transmission structure driven by the servo motor 12, thereby driving the stirring rod 11 to stir the phenol waste liquid, thereby improving the effect of phenol recovery.

[0023] The heating base 2 is provided with a heating coil 3 for heating the kettle body 9, the condenser 14 is connected to the kettle body 9 through the condenser tube 13, and the filter guide 16 is connected to the kettle body 9 through the feed pipe 15. The bottom of the heating base 2 is connected to the feed pipe 4, the bottom of the mounting frame 1 is connected to the fixing plate 5, the circulating pump 7 is installed on the surface of the fixing plate 5, and the input end of the circulating pump 7 is connected to the feed pipe 4 through a pipeline. The output end of the circulating pump 7 is connected to the feed pipe 15 through the delivery pipe 8, and the surface of the delivery pipe 8 is connected to one side of the mounting frame 1 through the fixing sleeve 6.

[0024] In addition, the heating coil 3 is the heating seat 2 that heats the phenol waste liquid inside the kettle body 9, the filter guide tube 16 is a structure that filters impurities from the injected phenol waste liquid, the feed pipe 15 is a structure that connects the conveying pipeline 8, the feed pipe 15, the condenser 13 and the discharge pipe 4 are all provided with electromagnetic control valves, the heating seat 2 is a structure for assembling the heating coil 3, the heating coil 3 is used to heat and distill the waste liquid inside the kettle body 9, and the fixing sleeve 6 fixes the conveying pipeline 8 to prevent shaking.

[0025] The positioning assembly includes: a fixed block 20 connected to both sides of the filter guide 16, and an adjustment plate 21 slidably connected to the inner wall of the fixed block 20; wherein, a plug-in plate 22 is connected to the surface of the adjustment plate 21, and the ends of the plug-in plate 22 are movably inserted on both sides of the filter element 18, and both sides of the filter element 18 are provided with assembly blocks 19. A locking spring 23 is provided inside the fixed block 20, and both ends of the locking spring 23 are connected to the surface of the adjustment plate 21. Assembly slots 17 are provided on both sides of the inner wall of the filter guide 16, and the assembly block 19 is slidably inserted into the inner wall of the assembly slot 17.

[0026] Furthermore, the filter guide 16 is a structure for installing the filter element 18, the fixing block 20 is a component for assembling the plug-in board 22, so that the plug-in board 22 can be used to plug and position the filter element 18, and the filter element 18 has a filtering effect when phenol waste liquid is injected into the filter guide 16. The assembly block 19 is a structure for assembling the filter element 18 in cooperation with the assembly slot 17, and the locking spring 23 acts on the adjustment plate 21, so that the plug-in board 22 on the surface of the adjustment plate 21 is inserted into the two sides of the filter element 18 to ensure the stability and sealing of the filter element 18 when in use.

[0027] The phenol waste liquid is injected into the kettle body 9 through the filter guide 16. During the injection process, the phenol waste liquid will filter the impurities therein through the filter element 18, thereby improving the recovery quality. When replacement and maintenance are required later, the plug-in plate 22 can be retracted into the fixed block 20 through the adjustment plate 21 to release the locking effect of the filter element 18, and the filter element 18 can be conveniently taken out and replaced from the filter guide 16 to ensure the filtering effect. The servo motor 12 drives the connecting shaft 10 to rotate, so that the stirring rod 11 stirs the inside of the kettle body 9, further improving the effect of the heating seat 2 on the heating treatment of the phenol waste liquid, cooperating with the condenser 14 to recover the phenol gas from the outlet, and at the same time, the purified raw liquid can be transported by the circulating pump 7, and purified again, thereby further improving the phenol recovery effect in the raw liquid.

[0028] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A phenol recovery and utilization device, characterized in that: include: A mounting frame (1), a heating seat (2) being mounted at the bottom of the mounting frame (1), a kettle (9) for purifying and recovering phenol waste liquid being installed inside the heating seat (2), and a stirring component for assisting in recovering phenol waste liquid being arranged inside the kettle (9); The top sides of the kettle body (9) are respectively connected to a condenser (14) and a filter guide cylinder (16), the interior of the filter guide cylinder (16) is provided with a filter element (18) for filtering the phenol waste liquid before recovery, and the two sides of the filter guide cylinder (16) are provided with positioning components for locking and fixing the filter element (18); The bottom of the heating seat (2) is connected to a circulation pump (7) for circulating and purifying the phenol waste liquid inside the kettle body (9).

2. A phenol recovery and utilization device according to claim 1, characterized in that: The stirring assembly comprises: Rotating a connecting shaft (10) installed inside the kettle body (9), and A servo motor (12) mounted on the top of the kettle body (9); The output end of the servo motor (12) is drivingly connected to the top end of the connecting shaft (10), and the bottom surface of the connecting shaft (10) is connected to a stirring rod (11).

3. A phenol recovery and utilization device according to claim 1, characterized in that: A heating coil (3) for heating the kettle body (9) is arranged inside the heating seat (2); the condenser (14) is connected to the kettle body (9) via a condenser pipe (13); and the filter guide cylinder (16) is connected to the kettle body (9) via a feed pipe (15).

4. A phenol recovery and utilization device according to claim 3, characterized in that: The bottom of the heating seat (2) is connected to a feed pipe (4), the bottom of the mounting frame (1) is connected to a fixing plate (5), the circulating pump (7) is mounted on the surface of the fixing plate (5), and the input end of the circulating pump (7) is connected to the feed pipe (4) through a pipeline.

5. A phenol recovery and utilization device according to claim 4, characterized in that: The output end of the circulation pump (7) is connected to the feed pipe (15) through a delivery pipe (8), and the surface of the delivery pipe (8) is connected to one side of the mounting frame (1) through a fixing sleeve (6).

6. A phenol recovery and utilization device according to claim 1, characterized in that: The positioning component includes: a fixing block (20) connected to both sides of the filter guide cylinder (16), and An adjustment plate (21) slidably connected to the inner wall of the fixing block (20); The surface of the adjustment plate (21) is connected to a plug-in plate (22), the ends of the plug-in plate (22) are movably inserted into two sides of the filter element (18), and both sides of the filter element (18) are provided with assembly blocks (19).

7. A phenol recovery and utilization device according to claim 6, characterized in that: A locking spring (23) is arranged inside the fixing block (20), and two ends of the locking spring (23) are connected to the surface of the adjustment plate (21). Both sides of the inner wall of the filter guide cylinder (16) are provided with assembly slots (17), and the assembly block (19) is slidably inserted into the inner wall of the assembly slot (17).