Continuous rectification device for benzotriazole production

By designing a continuous distillation device for benzotriazole production, using components such as fans and deflectors, the problem of low practicality of conventional distillation equipment is solved, and efficient condensation and separation of benzotriazole is achieved, and the distillation efficiency is improved.

CN222623684UActive Publication Date: 2025-03-18NANTONG BOTAO CHEM
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Patent Information

Application Number
CN202421293734.9
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-06-07
Publication Date
2025-03-18
Estimated Expiration
2034-06-07

AI Technical Summary

Technical Problem

Conventional distillation equipment has complex structure, which makes it less useful and makes it difficult to efficiently purify benzotriazole.

Method used

A continuous distillation device for the production of benzotriazole is designed, including a fan, air guide frame, air guide groove, baffle, air collecting hood and collection hopper. The blowing of the fan is heated and heated by the fan, and the air flow is guided into an S-shaped flow using the deflector, increasing the length of the condensation path, and achieving efficient condensation and separation of benzotriazole.

Benefits of technology

The heat dissipation efficiency of the air conductor tank and baffle is improved, the condensation effect of benzotriazole is enhanced, and the practicality and efficiency of the distillation device are improved.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a continuous rectification device for benzotriazole production, which belongs to the technical field of benzotriazole production equipment, and comprises a fan, the front end of the fan is fixedly connected with an air guide frame, the inside of the air guide frame is uniformly and fixedly connected with air guide grooves, the outer ends of the air guide grooves are fixedly connected with baffle plates, and the baffle plates are fixedly connected with the air guide grooves. The upper ends of the gas guide groove and the baffle are fixedly connected with a gas collecting hood, and the lower ends of the gas guide groove and the baffle are fixedly connected with a collecting hopper. The air guide frame comprises a fixed frame and a shell, and the fixed frame is fixedly connected with the shell. Evaporated gas is discharged into the gas collecting hood, concentrated into the gas guide groove through the gas collecting hood and discharged outwards through the material collecting hopper, in the process, the fan is used for blowing gas to the gas guide groove and the baffle, heated air is blown out, and meanwhile normal-temperature air is fed in, so that the heat dissipation efficiency of the gas guide groove and the baffle is improved, and the heat dissipation efficiency is improved. And benzotriazole in the gas guide groove and the baffle is conveniently condensed and discharged downwards through the collection hopper.
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Description

Technical Field

[0001] The utility model belongs to the technical field of benzotriazole production equipment, in particular to a continuous distillation device used for benzotriazole production. Background Art

[0002] Benzotriazole needs to be purified by distillation equipment. Distillation is a separation process that uses the different volatilities of the components in a mixture to separate the components. Commonly used equipment includes plate distillation towers and packed distillation towers.

[0003] A distillation tower is a tower-type gas-liquid contact device for distillation. By utilizing the different volatilities of the components in the mixture, that is, the different vapor pressures of the components at the same temperature, the light components and low-boiling substances in the liquid phase are transferred to the gas phase, while the high-boiling and heavy components in the gas phase are transferred to the liquid phase, thereby achieving the purpose of separation. Due to the complex distillation structure of conventional distillation towers, the practicality of conventional distillation equipment is relatively low.

[0004] Therefore, we propose a continuous distillation device for benzotriazole production to solve the above problems. Utility Model Content

[0005] The utility model aims to solve the problem of low practicability of conventional distillation equipment and proposes a continuous distillation device for benzotriazole production.

[0006] In order to achieve the above purpose, the utility model adopts the following technical solutions:

[0007] A continuous distillation device for the production of benzotriazole includes a fan, the front end of the fan is fixedly connected to an air guide frame, the interior of the air guide frame is evenly fixedly connected to an air guide groove, the outer end of the air guide groove is fixedly connected to a baffle, the upper ends of the air guide groove and the baffle are fixedly connected to an air collecting hood, and the lower ends of the air guide groove and the baffle are fixedly connected to a collecting hopper. The evaporated gas is discharged into the air collecting hood, collected into the air guide groove through the air collecting hood, and discharged outward through the collecting hopper. During the process, the fan is used to blow air to the air guide groove and the baffle to blow out the heated air, and at the same time, normal temperature air is sent in, so as to increase the heat dissipation efficiency of the air guide groove and the baffle, and facilitate the condensation of the benzotriazole in the air guide groove and the baffle to be discharged downward through the collecting hopper.

[0008] Preferably, the air guide frame comprises a fixing frame and a shell, and the fixing frame is fixedly connected to the shell. When the fan delivers air into the shell, the shell conveniently guides the airflow to pass through the air guide groove and the baffle.

[0009] Preferably, the air guide groove includes a groove body and a guide plate, and the guide plate is distributed at the inner end of the groove body. When the evaporated gas enters the groove body, the guide plate is used to guide the airflow into an S-shaped flow, and the condensed liquid is discharged downward along the guide plate, which is convenient for increasing the length of the condensation path.

[0010] Preferably, the gas collecting hood includes a hood body and a first sealing grid, wherein the first sealing grid is fixedly connected to the lower end of the hood body. When the evaporated gas enters the hood body, it is guided into the tank body through the hood body, so that the evaporated gas enters the tank body, thereby facilitating the collection of the evaporated gas into the gas guide groove.

[0011] Preferably, the gas collecting hood further comprises a docking nozzle, the docking nozzle is fixedly connected to the hood body, and the internal spaces of the hood body and the docking nozzle are in communication, and the docking nozzle facilitates the pipeline to be externally connected to the evaporating vessel.

[0012] Preferably, the collecting hopper comprises a second sealing grid and a hopper, wherein the second sealing grid is fixedly connected to the upper end of the hopper. When the liquid and gas pass through the second sealing grid and enter the hopper, they are conveniently discharged outward through the hopper.

[0013] Preferably, the collecting hopper further comprises a discharge nozzle, which is fixedly connected to the lower end of the hopper. The target container is placed under the discharge nozzle to facilitate the collection of liquid discharged from the collecting hopper.

[0014] In summary, the technical effects and advantages of the utility model are as follows:

[0015] 1. The evaporated gas is discharged into the gas collecting hood, and then concentrated into the air guide groove through the gas collecting hood, and discharged outward through the collecting hopper. During the process, the fan is used to blow air into the air guide groove and the baffle to blow out the heated air, and at the same time, the normal temperature air is sent in to increase the heat dissipation efficiency of the air guide groove and the baffle, so as to facilitate the condensation of benzotriazole in the air guide groove and the baffle to be discharged downward through the collecting hopper.

[0016] 2. After the evaporated gas enters the tank, the guide plate is used to guide the airflow into an S-shaped flow, and the condensed liquid is discharged downward along the guide plate, which is convenient for increasing the length of the condensation path.

[0017] 3. After the evaporated gas enters the cover body, it is guided into the tank body through the cover body, so that the evaporated gas enters the tank body, which is convenient for concentrating the evaporated gas into the gas guide tank. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 It is a schematic diagram of the overall structure of the utility model;

[0019] Figure 2 This is a schematic diagram of the wind guide frame structure of the utility model;

[0020] Figure 3 This is a schematic diagram of the air guide groove structure of the utility model;

[0021] Figure 4 This is a schematic diagram of the structure of the gas collecting hood of the utility model;

[0022] Figure 5 It is a schematic diagram of the structure of the collecting hopper of the utility model.

[0023] In the figure: 1. fan; 2. air guide frame; 3. air guide trough; 4. air collecting hood; 5. collecting hopper; 6. baffle; 21. fixing frame; 22. outer shell; 31. trough body; 32. guide plate; 41. hood body; 42. first sealing grid; 43. docking nozzle; 51. second sealing grid; 52. hopper; 53. discharge nozzle. DETAILED DESCRIPTION

[0024] The technical solutions in the utility model embodiments will be described clearly and completely below in conjunction with the drawings in the utility model embodiments. Obviously, the described embodiments are only part of the utility model embodiments, rather than all of the embodiments.

[0025] Reference Figure 1 A continuous distillation device for producing benzotriazole includes a fan 1, a front end of the fan 1 is fixedly connected to an air guide frame 2, the inside of the air guide frame 2 is evenly fixedly connected to an air guide groove 3, the outer end of the air guide groove 3 is fixedly connected to a baffle 6, the upper ends of the air guide groove 3 and the baffle 6 are fixedly connected to an air collecting hood 4, and the lower ends of the air guide groove 3 and the baffle 6 are fixedly connected to a collecting hopper 5.

[0026] Reference Figure 1 and 2 The air guide frame 2 includes a fixed frame 21 and a shell 22. The fan 1 is fixedly connected to the inner end of the fixed frame 21, and the fixed frame 21 is fixedly connected to the shell 22. When the fan 1 supplies air into the shell 22, the airflow is guided through the air guide groove 3 and the baffle 6 by the shell 22.

[0027] Reference Figure 1 , 2 3, the air guide groove 3 includes a groove body 31 and a guide plate 32, the lower end of the groove body 31 is fixedly connected to the inner end of the shell 22, and the guide plate 32 is distributed at the inner end of the groove body 31. After the evaporated gas enters the groove body 31, the guide plate 32 is used to guide the airflow into an S-shaped flow, and the condensed liquid is discharged downward along the guide plate 32.

[0028] Reference Figure 1 , 34, the gas collecting cover 4 includes a cover body 41 and a first sealing grid 42, the first sealing grid 42 is sealed at the gap outside the air guide groove 3 and the baffle 6, the internal space of the cover body 41 is connected to the internal space of the tank body 31, and the first sealing grid 42 is fixedly connected to the lower end of the cover body 41. After the evaporated gas enters the cover body 41, it is introduced into the tank body 31 through the cover body 41, so that the evaporated gas enters the tank body 31.

[0029] Reference Figure 1 and 4 The gas collecting hood 4 further comprises a docking nozzle 43, which is connected to an external evaporation vessel pipeline, and the docking nozzle 43 is fixedly connected to the hood body 41, and the internal spaces of the hood body 41 and the docking nozzle 43 are in communication. The docking nozzle 43 is used for connecting to an external evaporation vessel.

[0030] Reference Figure 1 , 3 5, the collecting hopper 5 includes a second sealing grid 51 and a hopper 52, the second sealing grid 51 is sealed at the lower outer end of the tank body 31 and the baffle 6, and the second sealing grid 51 is fixedly connected to the upper end of the hopper 52. When the liquid and gas pass through the second sealing grid 51 and enter the hopper 52, they are discharged outward through the hopper 52.

[0031] Reference Figure 1 and 5 The collecting hopper 5 also includes a discharge nozzle 53, which is fixedly connected to the lower end of the hopper 52. The target container is placed under the discharge nozzle 53 to collect the liquid discharged from the collecting hopper 5.

[0032] Working principle: the evaporated gas is discharged into the gas collecting hood 4, and is collected into the air guide groove 3 through the gas collecting hood 4, and discharged outward through the collecting hopper 5. During the process, the fan 1 is used to blow air to the air guide groove 3 and the baffle 6 to blow out the heated air, and at the same time, the air at normal temperature is sent in to increase the heat dissipation efficiency of the air guide groove 3 and the baffle 6, so that the benzotriazole in the air guide groove 3 and the baffle 6 is condensed and discharged downward through the collecting hopper 5.

[0033] The above is only a preferred specific implementation method of the utility model, but the protection scope of the utility model is not limited to it. Any technician familiar with the technical field can make equivalent replacements or changes within the technical scope disclosed by the utility model according to the technical scheme and utility model concept of the utility model, which should be covered by the protection scope of the utility model.

[0034] The description briefly mentions the application direction of the utility model for the prior art that is known to those skilled in the art and has not been changed, and combines it with the utility model to form a complete technology; the description avoids over-popularizing the technology familiar to those skilled in the art, and is used to assist those skilled in the art to quickly understand the main content of the utility model.

Claims

1. A continuous distillation device for the production of benzotriazole, comprising a blower (1), characterized in that: The front end of the fan (1) is fixedly connected to an air guide frame (2), the interior of the air guide frame (2) is evenly fixedly connected to an air guide groove (3), the outer end of the air guide groove (3) is fixedly connected to a baffle (6), the upper ends of the air guide groove (3) and the baffle (6) are fixedly connected to an air collecting hood (4), and the lower ends of the air guide groove (3) and the baffle (6) are fixedly connected to a collecting hopper (5).

2. A continuous distillation device for the production of benzotriazole according to claim 1, characterized in that: The air guide frame (2) comprises a fixing frame (21) and an outer shell (22), and the fixing frame (21) is fixedly connected to the outer shell (22).

3. A continuous distillation device for the production of benzotriazole according to claim 1, characterized in that: The air guide groove (3) comprises a groove body (31) and a guide plate (32), and the guide plate (32) is distributed at the inner end of the groove body (31).

4. A continuous distillation device for the production of benzotriazole according to claim 1, characterized in that: The gas collecting hood (4) comprises a hood body (41) and a first sealing grid (42), wherein the first sealing grid (42) is fixedly connected to the lower end of the hood body (41).

5. A continuous distillation device for the production of benzotriazole according to claim 4, characterized in that: The air collecting hood (4) further comprises a docking nozzle (43), wherein the docking nozzle (43) is fixedly connected to the hood body (41), and the internal spaces of the hood body (41) and the docking nozzle (43) are in communication.

6. A continuous distillation device for the production of benzotriazole according to claim 1, characterized in that: The collecting hopper (5) comprises a second sealing grid (51) and a hopper (52), wherein the second sealing grid (51) is fixedly connected to the upper end of the hopper (52).

7. A continuous distillation device for the production of benzotriazole according to claim 6, characterized in that: The collecting hopper (5) further comprises a discharge nozzle (53), and the discharge nozzle (53) is fixedly connected to the lower end of the hopper (52).