A multifunctional online detection and analysis instrument and detection and analysis method

Through a multi-functional online detection analyzer combining reflection and transmission lighting mechanisms, the limitations of measurement of insoluble components and multi-component solution in liquids in the prior art are solved, and simultaneous online detection is realized, which improves detection efficiency and quality and avoids Safety and quality issues.

CN111678890BActive Publication Date: 2024-12-31EVAN TECH (HANGZHOU) CO LTD
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Patent Information

Application Number
CN202010747931.3
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2020-07-30
Publication Date
2024-12-31
Estimated Expiration
2040-07-30

AI Technical Summary

Technical Problem

Existing detection analyzers have limitations when measuring the content of insoluble components and multi-component solutions in liquids, and it is difficult to achieve online inspection of the two principles of instruments on the same time, resulting in safety production, product quality and ecological environment problems.

Method used

A multi-functional online detection analyzer is designed, combining reflected light and transmittance light mechanisms, using CCD, processor and laser emitting tubes to simultaneously detect the content of dissolved substances and solid substances online through refractive index and absorbance, and manually or The automatic adjustment mechanism adapts to different materials.

Benefits of technology

The two principles are implemented to achieve simultaneous online testing, which improves the quality and efficiency of detection and analysis, avoids safety and quality problems caused by excessive or low content of individual substances, and reduces the deviation of inaccurate detection and compensation calculation.

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Abstract

The invention discloses a multifunctional online detection analyzer, comprising a shell installed on a pipeline, a PCB board installed in the shell and a CCD connected to the PCB, a processor, a temperature sensor, and a detector installed on the pipeline for transmitting detection results to the processor; its characteristics also include a lighting assembly and a lighting adjustment mechanism installed in the shell; by combining the reflective lighting mechanism and the transmissive lighting mechanism together and cooperating with the processor, the problem of simultaneous online detection of two principle instruments is achieved, thereby avoiding production safety problems, product quality problems and ecological environment problems caused by excessively high or low content of a single substance.
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Description

Technical Field

[0001] The present invention relates to the field of detection and analysis instruments, and in particular to a multifunctional online detection and analysis instrument and a detection and analysis method. Background Art

[0002] In the prior art, in the detection analyzer, the measurement of refractive index can reflect the total content of dissolved matter, but it has limitations in measuring the content of insoluble active ingredients in the liquid, especially for solutions with multiple components and no correlation between the components; the light absorption measurement method determines the content of the total active ingredients in the liquid by the light absorption rate, but the light absorption rate of different substances varies greatly. It is often used to measure the content of specific components or the total content of solid-liquid mixtures in multi-component solutions. However, the measurement results are greatly affected by the changes in different components due to the different absorption rates, and there are also great limitations in practical applications; and if two instruments based on the same principle are used for simultaneous measurement, there are problems: the instrument cost is high and two instruments are required; the installation is complicated and time-consuming. The cost is high, two installations are required, and more space is occupied, because it is very important to ensure the long-term stable operation of online analytical instruments under appropriate process conditions. In the process, there are not many very suitable locations, so the resources of suitable installation locations are also limited. Different instruments only output their own measurement results, and the corresponding compensation calculation process requires users to calculate in their own control system, which will increase additional costs. In addition, the output result of the instrument is the final calculation result, not the original signal. There are often many compensation calculations in the calculation process, and the output result cannot reflect the real-time situation of the measured medium. The compensation calculation methods of different instruments are quite different, so using the final output result of the instrument to calculate in the control system may lead to large deviations;

[0003] In industrial production, many chemical substances have high reaction risks. If they cannot be detected and analyzed in time, excessively high or low content of a single substance may lead to production safety problems, product quality problems and ecological environment problems. Therefore, in view of the problems in the current prior art, the present invention proposes an improvement on the detector in the prior art. Summary of the invention

[0004] The purpose of the present invention is to solve the problem in the prior art that instruments based on two principles are concentrated on the product and cannot detect materials online at the same time, as well as the problems of production safety, product quality and ecological environment caused thereby, and propose a multifunctional online detection and analysis instrument; secondly, to facilitate the adjustment and maintenance of the detector when adapting to the detection and analysis of different materials, thereby improving the quality and efficiency of the detection and analysis.

[0005] To achieve the above-mentioned purpose, the present invention proposes a multifunctional online detection analyzer, including a shell installed on a pipeline, a PCB board installed in the shell and a CCD connected to the PCB, a processor, a temperature sensor, and a detector installed on the pipeline for transmitting the detection results to the processor; its characteristics also include a lighting assembly and a lighting adjustment mechanism installed in the shell.

[0006] Furthermore, the total lighting components are reflective lighting mechanisms and transmissive lighting mechanisms.

[0007] Furthermore, the reflective lighting mechanism and the transmissive lighting mechanism both include a light source mounted on a PCB board, a lighting lens and a prism mounted on a housing, and a lighting adjustment mechanism matched with the light source and the lighting lens.

[0008] Furthermore, the lighting adjustment mechanism is divided into a manual adjustment mechanism and an automatic adjustment mechanism.

[0009] Preferably, the manual adjustment mechanism includes a bracket, a lighting lens cover threadedly connected to the bracket, an adjustment slot provided on the lighting lens cover, and an adjustment tool inserted into the adjustment slot.

[0010] Preferably, the automatic adjustment mechanism comprises a micro motor, a transmission gear mounted on the micro motor, and a reduction gear meshing with the transmission gear.

[0011] Preferably, the transmission lighting mechanism further comprises a light guide sleeve mounted on the lighting lens, the light source of the transmission lighting mechanism is a laser emitting tube, and the laser emitting tube is provided with an adjusting gear for adjusting the laser.

[0012] Furthermore, the shell is divided into a lower shell and an end cover, the lower shell and the end cover are provided with bolt connection holes, insulating terminals and sealing rings are provided between the lower shell and the end cover, and the lower shell is also provided with a temperature sensor cavity.

[0013] A detection and analysis method of a multifunctional online detection and analysis instrument, characterized in that it includes the following:

[0014] a) Refraction analysis: The light source passes through the lighting lens, hits the prism, and is reflected by the prism into another lighting lens. The reflected light source signal is collected by the CCD. The CCD transmits the collected light source signal to the processor for analysis. The refractive index is calculated by analyzing the obtained light source signal, and the content of dissolved substances is obtained by calculating the refractive index;

[0015] b) Transmission analysis: The laser emitting tube emits laser light, which is focused by the light guide sleeve. The laser passes through the material in the pipeline through the light-collecting lens and prism and is projected onto the detector. After receiving the signal, the detector detects and analyzes it. The transmittance is obtained by analyzing the light source signal attenuated when the laser passes through the pipeline material, and the content of solid materials in the pipeline is obtained by calculating the absorbance. The content of dissolved substances and solid substances is calculated by calculating the refractive index and absorbance, and the content of other substances is obtained by subtracting the content of dissolved substances and solid substances from the total amount.

[0016] The beneficial effects of the present invention are as follows: by combining the reflective lighting mechanism and the transmissive lighting mechanism together and coordinating with the processor, the problem of simultaneous online detection of two principle instruments is achieved, avoiding production safety problems, product quality problems and ecological environment problems caused by excessively high or low content of a single substance.

[0017] By adjusting the mechanism, the distance between the lighting lens, the light source and the prism can be adjusted to facilitate the detection and analysis of different materials, thereby avoiding the need to adapt to different light requirements of different materials, thereby further improving the quality and efficiency of the detection and analysis.

[0018] The transmission lighting mechanism uses a laser emitting tube to emit the light source, which solves the problem in the prior art that the light source needs to be converted into parallel light through a conversion mechanism, thereby avoiding the problem of inaccurate detection caused by the attenuation of the light source during conversion, thereby reducing the assembly space and production cost of the light source conversion mechanism in the detection analyzer; and the size of the emitted light source can be adjusted through the laser emitting tube to adapt to different types of materials. BRIEF DESCRIPTION OF THE DRAWINGS

[0019] Figure 1 This is a schematic diagram of the structure of Embodiment 1 of the present invention;

[0020] FIG2 is a schematic diagram of the overall structure of Example 1 of the present invention;

[0021] Figure 3 This is a schematic diagram of the PCB board structure of the patent of this invention;

[0022] Figure 4 This is a schematic diagram of the structure of the second embodiment of the present invention.

[0023] Figure 5 It is a schematic diagram of the structure of the manual adjustment mechanism of the patent of the present invention;

[0024] Figure 6 It is a schematic diagram of the lighting lens structure of the reflective lighting mechanism of the patent of the present invention;

[0025] Figure 7 It is a schematic diagram of the lighting lens structure of the invention patented transmission lighting mechanism;

[0026] Figure 8 It is a schematic diagram of the structure of the third embodiment of the present invention;

[0027] Fig. 9 It is a schematic diagram of the overall structure of the third embodiment of the present invention;

[0028] Fig.10 It is a schematic diagram of the automatic adjustment mechanism of the patent of the present invention. DETAILED DESCRIPTION

[0029] The present invention will be further described in detail below in conjunction with the accompanying drawings and embodiments. The following embodiments are used to illustrate the present invention but are not intended to limit the scope of the present invention. Example 1

[0030] See also Figures 1 to 3 A multifunctional online detection analyzer comprises a shell 1 installed on a pipeline, a PCB board 2 installed in the shell and a CCD 201 connected to the PCB board 2, a processor 202, a temperature sensor 203 and a detector 204 installed on the pipeline for transmitting detection results to the processor; it is also characterized by a lighting assembly 3 installed in the shell 1; the lighting assembly 3 is divided into a reflection lighting mechanism 301 and a transmission lighting mechanism 302; the reflection lighting mechanism 301 and the transmission lighting mechanism 302 both comprise a light source 303 installed on the PCB 2, a lighting lens 304 and a prism 305 installed on the shell 1 and the light source 303.

[0031] The housing 1 is divided into a lower housing 101 and an end cover 102. Bolt connection holes 103 are provided on the lower housing 101 and the end cover 102. Insulating terminals 104 and sealing rings 105 are provided between the lower housing 101 and the end cover 102. The insulators are divided into upper insulators mounted on the end cover 102 and lower insulators mounted on the lower housing 101. The sealing rings are mounted on both sides between the lower housing 101 and the end cover 102 to seal and insulate the PCB board from both sides of the outer housing. The temperature sensor 203 on the PCB board is inserted into the temperature sensor cavity 106 on the lower housing to measure the temperature, thereby facilitating the calculation of the refractive index and the absorbance at different temperatures, and detecting the temperature stability of the material. The PCB board is fitted with a sealing ring and placed between the upper and lower insulators. The bolts are inserted into the bolt connection holes in the end cover through the PCB and connected to the bolt connection holes on the lower housing. The PCB board is fixed by tightening the bolts. The temperature sensor 203 is inserted into the temperature sensor cavity 106 on the lower housing to be electrically connected to the PCB board.

[0032] When the detector is used for detection, refraction analysis: the light source passes through the lighting lens, hits the prism, and is reflected into another lighting lens through the prism. The reflected light source signal is collected by the CCD. The CCD transmits the collected light source signal to the processor for analysis. The refractive index is calculated by analyzing the light source signal obtained, and the content of dissolved substance A is obtained by calculating the refractive index; transmission analysis: the laser emitting tube emits laser, the laser is focused by the light guide sleeve, the laser passes through the material in the pipeline through the lighting lens and the prism, and hits the detector. After the detector receives the signal, it detects and analyzes it. The transmittance is obtained by analyzing the light source signal attenuated when the laser passes through the pipeline material, and the content of solid material B in the pipeline is obtained by calculating the transmittance; the content of dissolved substance A and the content of solid substance B are calculated by calculating the refractive index and the transmittance, and then the content of substance C is obtained by subtracting the content of dissolved substance and the content of solid substance from the total amount. Example 2

[0033] See also Figures 3 to 7 Compared with Example 1, this embodiment is different from Example 1 in that a manual lighting adjustment mechanism is provided on the reflective lighting mechanism, and the manual adjustment mechanism includes a bracket 403, a lighting lens cover 404 with a lighting lens threadedly connected to the bracket 403, an adjustment groove 405 provided on the lighting lens cover 404, and an adjustment tool 406 inserted into the adjustment groove 405; the adjustment tool 406 is inserted into the adjustment groove 405 provided on the lighting lens cover 404, and the lens cover is placed in the bracket 403, and then the adjustment tool is screwed to drive the lighting lens cover 404 with a lighting lens to adjust the optimal distance with the light source and the prism to improve the lighting effect, thereby ensuring that the detection result is more accurate. Example 3

[0034] See also Figure 3 and Figures 4 to 10Compared with Example 2, the present embodiment is different in that an automatic light source adjustment mechanism is added to the transmission lighting mechanism. The automatic adjustment mechanism 402 includes a micro motor 407 connected to the PCB board wire installed on a fixed column, a transmission gear 408 installed on the micro motor 407, and a reduction gear 409 meshing with the transmission gear 408. The reduction gear is connected and fixed to the reduction gear fixing column through a rotating shaft; the transmission lighting mechanism 302 also includes a light guide sleeve 306 installed on the lighting lens 304. The light source of the transmission lighting mechanism 302 is a laser emitting tube 307. An adjusting gear 308 for adjusting the laser is provided; the function of the light guide sleeve is to protect the laser beam and prevent the laser beam from diffusing and affecting the detection effect; the automatic adjustment mechanism adjusts the size of the laser beam emitted by the laser emitting tube, specifically by controlling the rotation of the micro motor to drive the transmission gear to rotate, and the transmission gear drives the reduction gear on the reduction gear fixing column to rotate, and the reduction gear and the adjusting gear for adjusting the size of the light beam are meshed with each other, so that the reduction gear drives the retrieval gear to rotate to adjust the size of the laser beam, so that the emitted laser beam can be changed according to the characteristics of the detected material, so that its application is more extensive and adapts to the detection and analysis of more materials.

[0035] The above embodiments are intended to illustrate the present invention, not to limit the present invention. Any solution that is a simple transformation of the present invention belongs to the protection scope of the present invention.

Claims

1. A multifunctional online detection analyzer, comprising a housing (1) mounted on a pipeline, a PCB (2) mounted in the housing, a CCD (201) connected to the PCB (2), a processor (202), a temperature sensor (203), and a detector (204) mounted on the pipeline for transmitting detection results to the processor; the characteristic of the multifunctional online detection analyzer is that it also comprises a lighting assembly (3) and a lighting adjustment mechanism mounted in the housing (1); the lighting assembly (3) is divided into a reflection lighting mechanism (301) and a transmission lighting mechanism (302), and the lighting adjustment mechanism is mounted on the lighting assembly; the reflection lighting mechanism (301) and the transmission lighting mechanism (302) both comprise a light source (303) mounted on the PCB (2), a lighting lens (304) and a prism (305) mounted on the housing (1); the lighting adjustment mechanism is further divided into a manual adjustment mechanism (401) and an automatic adjustment mechanism (402); the manual adjustment mechanism comprises a bracket (403), a lighting lens threadedly connected to the bracket (403), and a prism (305) mounted on the housing (1). The automatic adjustment mechanism (402) comprises a micro motor (407), a transmission gear (408) mounted on the micro motor (407), and a reduction gear (409) meshing with the transmission gear (408); the transmission lighting mechanism (302) further comprises a light guide sleeve (306) mounted on the lighting lens (304); the The light source (303) of the transmission lighting mechanism (302) is a laser emitting tube, and an adjusting gear (308) for adjusting the laser is provided on the laser emitting tube; the housing (1) is divided into a lower housing (101) and an end cover (102), and bolt connection holes (103) are provided on the lower housing (101) and the end cover (102), and an insulating terminal (104) and a sealing ring (105) are provided between the lower housing (101) and the end cover (102), and a temperature sensor cavity (106) is also provided on the lower housing.

2. The detection and analysis method of a multifunctional online detection and analysis instrument according to claim 1, characterized in that: The steps include: a) Refraction analysis: The light source passes through the lighting lens, hits the prism, and is reflected by the prism into another lighting lens. The reflected light source signal is collected by the CCD. The CCD transmits the collected light source signal to the processor for analysis. The refractive index is calculated by analyzing the obtained light source signal, and the content of dissolved substances is obtained by calculating the refractive index. b) Transmission analysis: The laser emitting tube emits laser, which is focused by the light guide sleeve. The laser passes through the material in the pipeline through the light-collecting lens and prism and is projected onto the detector. After receiving the signal, the detector detects and analyzes it. By analyzing the light source signal that is blocked when the laser passes through the pipeline material, the absorbance is obtained. By calculating the absorbance, the content of solid material in the pipeline is obtained; the content of dissolved matter and solid matter is calculated by calculating the refractive index and the absorbance; and the content of other substances is obtained by subtracting the content of dissolved matter and solid matter from the total amount.