A soothing and moisturizing composition, facial mask and preparation method thereof
A synergistic composition of natural extracts in a facial mask addresses the shortcomings of traditional skin care by enhancing moisturizing and soothing effects, offering long-lasting hydration and improved skin barrier function.
Patent Information
- Application Number
- CN202410724628.X
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-06-05
- Publication Date
- 2024-12-27
- Estimated Expiration
- 2044-06-05
AI Technical Summary
Existing skin care products fail to provide both long-lasting moisturizing and soothing effects, with traditional moisturizers like glycerin and hyaluronic acid having poor permeability and short-lasting effects, and soothing methods like cold compresses offering only temporary relief.
A composition comprising hydrolyzed sclerotium gum, porphyra polysaccharide, and goldenseal extract, combined with aloe barbadensis leaf extract, forsythia extract, and zanthoxylum bungeanum fruit extract, formulated into a facial mask to enhance moisturizing and soothing effects through synergistic mechanisms.
The composition achieves enhanced moisturizing and soothing effects, providing anti-inflammatory and antibacterial benefits, suitable for all skin types, especially dry and sensitive skin, with long-lasting moisture retention and improved skin barrier function.
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Abstract
Description
Technical Field
[0001] The invention belongs to the field of skin care functional products, and specifically relates to a soothing and moisturizing composition, a facial mask and a preparation method thereof. Background Art
[0002] In the field of skin care, moisturizing and soothing are the two issues that consumers are most concerned about. Although traditional skin care products meet the need for moisturizing to a certain extent, they are still insufficient in soothing the skin and reducing external stimuli. The skin is a natural barrier between the body and the environment. By maintaining an effective epidermal barrier to protect the body from environmental influences, it can not only resist external factors, but also prevent the body from losing water. The hydration level not only affects the visible skin state, such as the softness of the skin, but also affects the cell metabolism, enzyme activity and signal transduction in the epidermis. Therefore, sufficient skin hydration is essential to maintaining skin health, and moisturizing is an important part of basic skin care.
[0003] The water content of the normal stratum corneum is 20%-35%. When the water content of the stratum corneum drops below 10%, the skin barrier function will be damaged and secondary problems such as skin allergies, irritation and inflammation will be caused. Therefore, developing a product that can provide both moisturizing and soothing effects is of great significance to meet the skin care needs of modern consumers.
[0004] In terms of moisturizing technology, although traditional moisturizing ingredients such as glycerin and butylene glycol have certain moisturizing effects, they often fail to meet the needs of modern consumers for deep skin moisturizing. In addition, although some new moisturizers such as hyaluronic acid and seaweed extracts can provide better moisturizing effects, the use of a single ingredient often has problems such as poor permeability and short-lasting moisturizing effects. Therefore, it is necessary to develop a composition composed of multiple natural plant extracts and high-efficiency moisturizers, and form a skin care system with high permeability and long-lasting moisturizing through scientific proportioning.
[0005] In terms of soothing technology, skin sensitivity, redness and swelling have become common skin problems for modern consumers. Although traditional soothing methods such as cold compresses and ointments can temporarily relieve skin discomfort, the long-term effect is not ideal. Therefore, it is necessary to develop a composition with soothing effect, which can effectively soothe the skin and reduce the damage to the skin caused by external stimuli through the active ingredients in natural plant extracts. Summary of the invention
[0006] In view of the deficiencies in the prior art, the purpose of the present invention is to provide a composition consisting of a variety of natural plant extracts and a high-efficiency moisturizer, and to prepare a composition and a product thereof with dual moisturizing and soothing effects through scientific proportioning and preparation methods.
[0007] To achieve the above object, the present invention discloses the following technical solutions:
[0008] In a first aspect, the present invention provides a soothing and moisturizing composition, comprising the following components in parts by mass:
[0009]
[0010] The moisturizing and synergistic component consists of hydrolyzed sclerotium gum, porphyra polysaccharide and goldenseal extract.
[0011] Preferably, the mass ratio of the hydrolyzed sclerotium gum, the water-based laver polysaccharide, and the goldenseal extract is 1:(0.02-0.05):(1.6-1.9).
[0012] Preferably, the preparation method of the Glehnia littoralis extract comprises the following steps:
[0013] S1. Take the melon seeds gold powder and filter it to obtain the melon seeds gold powder;
[0014] S2. Add ethanol aqueous solution, reflux extraction, filter, and obtain filtrate A;
[0015] S3. The remaining residue was extracted by reflux in distilled water and filtered to obtain filtrate B. The filtrates A and B were combined and the combined filtrate was concentrated under reduced pressure to a water content of ≤30% to obtain a concentrated solution of melon seeds;
[0016] S4. Take papain and add it to the Guazijin concentrated solution. At the same time, add ethanol aqueous solution to the Guazijin concentrated solution. Let it stand overnight, filter it, and vacuum dry it to obtain the Guazijin extract.
[0017] Further preferably, the filtration mesh number in step S1 is ≥60 mesh;
[0018] The concentration of the ethanol aqueous solution in step S2 is ≥95 v / v%, the reflux temperature is ≥85°C, the number of reflux extractions is 2 times, and the extraction time for each time is 1.5 h;
[0019] The water bath reflux extraction temperature in step S3 is ≥95°C, the reflux extraction times are 2 times, each extraction time is 2 hours, and the combined filtrate is concentrated under reduced pressure at ≤50°C.
[0020] More preferably, the enzymatic activity of papain in step S4 is ≥300 U / g, the added amount is ≥3% of the mass of the concentrated solution, and the concentration of the ethanol aqueous solution is ≥95 v / v%.
[0021] In a second aspect, the present invention provides a soothing and moisturizing facial mask, comprising a facial mask paper and an impregnation liquid, wherein the impregnation liquid comprises the soothing and moisturizing composition of the first aspect and a solvent;
[0022] The soothing and moisturizing composition is added in an amount of ≤3 wt % in the soaking liquid.
[0023] Preferably, the impregnation liquid further contains a thickener, a preservative, a pH adjuster, and an antioxidant.
[0024] Further preferably, the thickener is acrylic acid (ester) / C10-30 alkyl acrylate cross-linked polymer;
[0025] The preservative is at least one of p-hydroxyacetophenone and phenoxyethanol;
[0026] The moisturizer is at least one of butylene glycol, propylene glycol, allantoin, and sodium hyaluronate;
[0027] The solvent is water;
[0028] The pH regulator is triethanolamine;
[0029] The antioxidant is at least one of vitamin C and water-soluble vitamin E.
[0030] In a third aspect, the present invention provides a method for preparing the soothing and moisturizing facial mask according to the second aspect, comprising the following steps:
[0031] (1) mixing the soothing and moisturizing composition, a thickener, a preservative, a solvent, a pH adjuster, and an antioxidant in a certain proportion to obtain an impregnation solution;
[0032] (2) Taking a facial mask paper and immersing it in the immersion liquid to obtain the soothing and moisturizing facial mask.
[0033] In a fourth aspect, the present invention provides use of the soothing and moisturizing composition described in the first aspect in the preparation of a skin care product with soothing and / or moisturizing effects.
[0034] In the present invention:
[0035] Aloe barbadensis leaf extract is rich in various amino acids, vitamins and minerals, and has significant moisturizing, calming and repairing effects; it can help the skin retain moisture and reduce water loss, while also repairing and soothing damaged skin.
[0036] Forsythia extract has multiple biological activities such as anti-inflammatory, antibacterial and antioxidant; it can help reduce skin inflammation, promote skin health, and also has a certain improvement effect on acne skin.
[0037] Zanthoxylum bungeanum fruit extract is rich in various bioactive ingredients, such as volatile oils, flavonoids, etc. It has antibacterial, anti-inflammatory and analgesic effects. It can enhance the permeability of the product and has a certain soothing effect on sensitive skin.
[0038] As a basic moisturizing ingredient, the aloe barbadensis leaf extract provides lasting moisture to the skin, while the forsythia extract and the prickly ash fruit extract help the skin maintain a healthy state and reduce external factors of water loss through their anti-inflammatory and antibacterial effects. The hydrolyzed sclerotium gum, the water-front temple porphyra polysaccharide and the melon seed gold extract in the moisturizing and synergistic components complement the aloe barbadensis leaf extract through different moisturizing mechanisms, and jointly enhance the moisturizing effect of the product. The present invention proves through experiments that the moisturizing and synergistic components composed of the hydrolyzed sclerotium gum, the water-front temple porphyra polysaccharide and the melon seed gold extract can further promote the moisturizing effect of the aloe barbadensis leaf extract.
[0039] Beneficial effects of the present invention:
[0040] 1. The moisturizing enhancing component provided in the present application has a promoting effect on the moisturizing performance of the aloe vera leaf extract. When the moisturizing enhancing component is used in combination with the aloe vera leaf extract, it exhibits a better water-retaining and moisturizing effect;
[0041] 2. The soothing and moisturizing composition provided by the present invention achieves excellent moisturizing effect through synergistic enhancement among various ingredients, and at the same time has certain anti-inflammatory and antibacterial effects, and is suitable for all skin types, especially dry and sensitive skin. DETAILED DESCRIPTION
[0042] In order to better understand the present invention, the present invention is further described below in conjunction with specific examples, wherein the terms used in the examples are for describing specific embodiments and do not constitute limitations on the scope of protection of the present invention.
[0043] In the present invention:
[0044] Aloe barbadensis leaf extract is Aloe barbadensis leaf extract, INCI name is ALOE BARBADENSIS LEAF EXTRACT, purchased from Xi'an Kangnuo Chemical Co., Ltd.
[0045] Aloe vera extract is aloe vera (ALOE VERA) extract, INCI name is ALOE BARBADENSIS LEAFEXTRACT, purchased from Xi'an Kangnuo Chemical Co., Ltd.
[0046] The Forsythia suspensa extract is Forsythia suspensa extract, with the INCI name of FORSYTHIA SUSPENSA EXTRACT, purchased from Shaanxi Hengxi Biotechnology Co., Ltd.
[0047] Zanthoxylum bungeanum fruit extract is Zanthoxylum bungeanum fruit extract, INCI name is ZANTHOXYLUM BUNGEANUM FRUIT EXTRACT, purchased from Xi'an Kangnuo Chemical Co., Ltd.
[0048] The hydrolyzed sclerotium gum is hydrolyzed sclerotium (SCLEROTIUM ROLFSSII) gum, with the INCI name of HYDROLYZED SCLEROTIUM GUM, purchased from Nanjing Bermuda Biotechnology Co., Ltd.
[0049] APHANOTHECE SACRUM polysaccharide is APHANOTHECE SACRUM polysaccharide, INCI name is APHANOTHECE SACRUM POLYSACCHARIDES, purchased from Jiangsu Jufeng Chemical Technology Co., Ltd.
[0050] Polygala japonica extract is Polygala japonica extract, the INCI name is POLYGALA JAPONICA EXTRACT, and Polygala japonica medicinal materials were purchased from the Qingping Market in Liwan District, Guangzhou.
[0051] Water-soluble vitamin E is compounded with 36% PEG-40 hydrogenated castor oil, 30% PEG-50 hydrogenated castor oil, 20% tocopherol acetate, 8% propylene glycol, and 6% nonylphenol polyether-20, and is purchased from Beijing Belliles Biotechnology Co., Ltd.
[0052] The remaining raw materials are commercially available.
[0053] The experimental methods in the following examples without specifying specific conditions are usually carried out under conventional conditions or under conditions recommended by the manufacturer. Unless otherwise specified, percentages and parts are calculated by weight.
[0054] Preparation of Guazijin Extract:
[0055] Step (1), taking the dried whole plant of Glehnia littoralis, crushing it with a grinder, and filtering it with a 60-mesh sieve to obtain Glehnia littoralis powder;
[0056] Step (2), adding 95 v / v% ethanol aqueous solution, wherein the material-water ratio is 1:6, reflux extraction at 85° C. for 2 times, each time for 1.5 hours, filtering, evaporating the medicinal residue, adding distilled water at 95° C. water bath reflux extraction for 2 times, each time for 2 hours, wherein the mass ratio of medicinal residue to distilled water is 1:10, filtering, combining the filtrate, and concentrating the filtrate under reduced pressure at 50° C. to a water content of ≤30%, thereby obtaining a melon seed gold concentrate;
[0057] Step (3), taking papain with an enzyme activity of ≥300U / g, adding an amount of 3% of the mass of the concentrated solution, and adding 95v / v% ethanol aqueous solution to the concentrated solution, the volume ratio of ethanol aqueous solution to the concentrated solution is 1:1, standing overnight, filtering, and vacuum drying to obtain the melon seed gold extract for later use.
[0058] Example 1
[0059] Preparation of moisturizing and enhancing components:
[0060] Weigh the raw materials according to the mass ratio in Table 1 and mix them evenly to obtain the moisturizing and enhancing component.
[0061] Table 1 Moisturizing and enhancing component raw material mass ratio
[0062]
[0063] Note: “-” in the table means not added.
[0064] Sample preparation:
[0065] Table 2 Sample raw material mass ratio
[0066]
[0067]
[0068] Note: “-” in the table means not added.
[0069] Moisture retention test:
[0070] Test plan: Weigh 0.500g of Aloe vera leaf extract and samples 1-10 in glass culture dishes, add 0.200g of distilled water evenly, place the glass culture dishes in a desiccator with color-changing silica gel (relative humidity 0%) at 25°C, and weigh the culture dishes and samples at 12, 24, 36, and 48 hours. The results of moisture retention are shown in Table 3.
[0071] Calculate the moisturizing rate according to the following formula:
[0072]
[0073] Where: W 4 is the mass of the initial culture dish and sample, g; W 3 is the mass of the culture dish and sample after a specific time, g.
[0074] Table 3 Moisture retention rate results
[0075]
[0076]
[0077] Result analysis:
[0078] According to Table 3, under a dry environment, the moisture content of the 11 samples decreases rapidly, and the loss of moisture begins to slow down with the extension of time. Compared with the single aloe vera leaf extract, samples 1-3 have better moisturizing effects at various time points; compared with samples 4-10, samples 1-3 have better moisturizing effects at various time points; the moisturizing enhancing component provided in the present application has a promoting effect on the moisturizing performance of the aloe vera leaf extract, and the moisturizing enhancing component exhibits better water-retaining and moisturizing effects when used in combination with the aloe vera leaf extract.
[0079] Example 2
[0080] Preparation of soothing and moisturizing composition:
[0081] Weigh the raw materials in parts by mass according to Table 4 and mix them evenly to obtain a soothing and moisturizing composition.
[0082] Table 4 Soothing and moisturizing composition raw materials
[0083] Composition 1 Composition 2 Composition 3 Composition 4 Composition 5 Aloe Barbadensis Leaf Extract 10 13 15 13 13 Forsythia suspensa extract 3 4 5 - 4 Zanthoxylum bungeanum fruit extract 1.4 1.6 1.7 1.6 - Moisturizing ingredients 2.62 2.74 2.95 2.74 2.74 Moisturizing and enhancing component number 3 3 3 3 3
[0084] Note: “-” in the table means not added.
[0085] Performance Test:
[0086] Inflammatory factor inhibition experiment
[0087] Samples to be tested: Take a certain amount of soothing and moisturizing compositions 1-5, and dilute them to 0.5wt%, 1wt%, and 3wt% respectively with physiological saline.
[0088] Experimental method: RAW264.7 macrophages were used as the research object, and the cell inflammation model was established by stimulating the cells with lipopolysaccharide (LPS) (bacterial endotoxin). Macrophages were inoculated into 12-well plates and incubated in an incubator at 37°C and 5% CO. 2 After incubation for 24 h under ventilation conditions, the samples to be tested were added, and LPS (1 μg / mL) was added 2 h later, which was recorded as T 1 , and set up a group without adding diluent and only adding LPS, denoted as T 总 The group without LPS and only with diluent was recorded as T 0 , stimulated for 24 hours, collected the supernatant, centrifuged and tested. The ELISA kit was used to analyze the release level of the pro-inflammatory inflammatory factor TNF-α of RAW264.7.
[0089] The TNF-α inhibition rate was calculated by the following formula:
[0090] TNF-α inhibition rate (%) = [(T 总 -T1 ) / (T 总 -T 0 )]×100%.
[0091] The higher the TNF-α inhibition rate, the better the anti-inflammatory and soothing effect of the soothing and moisturizing composition. The TNF-α inhibition test results are shown in Table 5.
[0092] Table 5 TNF-α inhibition rate
[0093]
[0094] Result analysis:
[0095] According to the results in Table 5, as the concentration of the soothing and moisturizing composition increases, the inhibition rate of anti-inflammatory factors gradually increases, proving that the soothing and moisturizing compositions 1-3 provided by the present invention have obvious inhibitory effects on the inflammatory factor TNF-α, showing a certain gradient dependence, among which the inhibition rates of composition 3 at concentrations of 3wt%, 1wt%, and 0.5wt% on the inflammatory factor TNF-α are as high as 32.481%, 24.297%, and 20.212%, respectively, having good anti-inflammatory and soothing effects; the Forsythia suspensa extract and Zanthoxylum bungeanum fruit extract in the soothing and moisturizing composition have better anti-inflammatory and soothing effects when used in combination than when used alone.
[0096] Example 3
[0097] Preparation of Soothing and Moisturizing Mask Infusion:
[0098] Weigh the raw materials according to the mass percentage in Table 6;
[0099] Step (1), dispersing and soaking sodium hyaluronate, allantoin, acrylic acid (ester) / C10-30 alkyl acrylate cross-linked polymer and p-hydroxyacetophenone with butylene glycol and propylene glycol, adding them into water, heating and stirring, heating to 85° C., and keeping the temperature for 20 minutes to obtain a mixture A;
[0100] Step (2), dissolving triethanolamine completely with water to obtain a mixture B;
[0101] Step (3), cooling mixture A to 60° C., adding mixture B, and stirring at a speed of 200-300 r / min to obtain mixture AB;
[0102] Step (4), cooling the mixture AB to 45° C., adding vitamin C, water-soluble vitamin E, soothing and moisturizing composition 3 and phenoxyethanol, stirring and dispersing them uniformly at 45° C. and a rotation speed of 600 r / min, and filtering through a 100-mesh filter to obtain a soothing and moisturizing facial mask impregnation liquid;
[0103] Step (5), taking the mask paper and immersing it in the immersion liquid to obtain a soothing and moisturizing mask.
[0104] Table 6 Raw materials and conditions for preparing the impregnation solution
[0105]
[0106]
[0107] Note: The units in the table are mass percentage.
[0108] Performance Test:
[0109] Human skin patch test:
[0110] The impregnation solution prepared above was subjected to the human skin patch test in accordance with the "2022 Technical Specifications for Safety of Cosmetics".
[0111] The skin reaction was observed according to the standard at 30 minutes (after the indentation disappears), 24 hours and 48 hours, and the observation results were recorded. See Table 7.
[0112] Table 7 Human safety test results
[0113] serial number 30min 24h 48h Impregnation liquid 1 Level 0, 30 players Level 0, 30 players Level 0, 30 players Impregnation liquid 2 Level 0, 30 players Level 0, 30 players Level 0, 30 players Impregnation liquid 3 Level 0, 30 players Level 0, 30 players Level 0, 30 players
[0114] Skin water loss reduction test:
[0115] The level of transepidermal water loss (TEWL value) is an important indicator for evaluating the strength of skin barrier function.
[0116] The TEWL value is measured by a transepidermal water loss tester.
[0117] The impregnation solutions 1-3 prepared above were used as test samples.
[0118] Fifteen subjects aged 20-40 with dry skin were selected and divided into three groups. Each test sample was repeated 5 times and the average value was taken. A 3×3 cm mark was made on the inner side of the forearms of both hands of the subjects. 2 Test area: Multiple areas can be marked on the same arm, with an interval of 1 cm. Test samples and blank controls are randomly distributed on the left and right arms. Capacitive skin analyzer is used to measure the test area and control area. Each area is measured 15 times in parallel, first measuring the blank value of each test area, and then measuring the blank value of each test area at 0.5g / 9cm 2The amount is evenly applied in the test area. The skin moisture content of the test area and the blank control area is measured 1, 2, 4, and 8 hours after application (measured at this time during verification). No products (cosmetics or topical medicines) can be used on the test area 2-3 days before. The test environment temperature is controlled at 25±1℃, and the relative humidity is 40±5%. Before the test, the arms of the subjects are wiped with pure water at about 36℃, and the subjects are asked to sit quietly in the test environment for 30 minutes before the test. According to the experimental design, the TEWL values of each time period are measured separately, and the reduction in skin moisture loss at each time point is calculated. The greater the reduction in skin moisture loss, the better the effect of skin barrier repair. The results are shown in Table 8.
[0119] Calculation formula:
[0120] Reduction in skin water loss = [(T0-T1) / T0] x 100%
[0121] Where: T1 is the TEWL corresponding to the test group at each time point, and T0 is the TEWL corresponding to the blank control group at each time point.
[0122] Table 8 Reduction in skin water loss (%)
[0123] Group\Time 1h 2h 4h 8h Example 1 23.62 22.78 19.65 18.06 Example 2 25.27 23.35 21.54 20.32 Example 3 26.19 23.62 22.13 21.27
[0124] Lactic acid sting evaluation:
[0125] 1. Test principle: Research shows that the occurrence of skin sensitivity is a complex process involving skin barrier, skin nervous system, and skin immune cells. Under the combined effects of internal and external factors, the skin barrier function is damaged, causing an increase in sensory nerve afferent signals, leading to an enhanced skin response to external stimuli and triggering skin immune inflammatory reactions. The score of the lactic acid sting test before and after using the product can directly reflect the product's repairing effect on the skin barrier function.
[0126] The present invention tests the skin barrier repairing effect of the soothing and moisturizing facial mask by evaluating the lactic acid stinging before and after using the product.
[0127] 2. Test Method
[0128] Test environment: The test environment temperature is 22±1℃, the humidity is 50±5%, and real-time dynamic detection is performed;
[0129] Test volunteers: aged between 35 and 45 years old (excluding pregnant or lactating women), a total of 15 people, 5 people in each group; no serious systemic diseases, no immunodeficiency or autoimmune diseases; no history of severe allergies to skin care cosmetics; no use of hormone drugs and immunosuppressants in the past month; no participation in other clinical trials; use of test drugs as required and complete information; all volunteers should fill out an informed consent form before the test.
[0130] Test steps:
[0131] Preparation before the test: Do not use any products (cosmetics or topical medications) on the test area 2-3 days before.
[0132] Test process: The subjects sit quietly in a constant temperature and humidity room for 30 minutes, then use equal amounts of 10% lactic acid aqueous solution and distilled water on the left and right nasolabial grooves of the subjects, and ask the subjects about their skin sensation symptoms at 0.5, 2, and 5 minutes, and score them according to a four-point scale: no tingling sensation is 0 points, mild tingling sensation is 1 point, moderate tingling sensation is 2 points, and severe tingling sensation is 3 points. The test of the same volunteer is completed by the same measurement personnel.
[0133] 3. Test results
[0134] Lactic acid stinging improvement rate calculation formula: R = (R1-R2) / R1×100%
[0135] Where:
[0136] R: improvement rate of lactic acid stinging; R1: lactic acid stinging score before using the soothing moisturizing mask; R2: lactic acid stinging score after using the soothing moisturizing mask for 28 days; lactic acid stinging score = 0.5min+2min+5min stinging score.
[0137] The experimental results are shown in Table 9.
[0138] Table 9 Lactic acid stinging improvement rate
[0139] Group Lactic acid stinging improvement rate (%) Mask 1 (corresponding impregnation solution 1) 63.72 Mask 2 (corresponding to impregnation solution 2) 68.43 Mask 3 (corresponding to impregnation solution 3) 72.17
[0140] Result analysis:
[0141] 1. According to the test results in Table 8, as the concentration of the soothing and moisturizing composition increases, the moisturizing effect of the soothing and moisturizing mask becomes better. When the experiment is carried out for 8 hours, the moisturizing performance of the composition still has a good effect, indicating that the composition provided by the present invention can form a long-lasting and stable water-locking barrier on the surface of the skin;
[0142] 2. According to the test results in Table 9, the soothing and moisturizing facial mask provided by the present invention has excellent moisturizing, soothing and anti-inflammatory effects, and improves and repairs the skin barrier function.
[0143] Although the specific embodiments of the present invention are described above, it should be understood by those skilled in the art that this is only for illustration and the protection scope of the present invention is defined by the appended claims. Those skilled in the art may make various changes or modifications to these embodiments without departing from the principles and essence of the present invention, but these changes and modifications all fall within the protection scope of the present invention.
Claims
1. A soothing and moisturizing composition, characterized in that: By mass, it includes the following components: 10-15 parts of aloe barbadensis leaf extract; 3-5 parts of Forsythia suspensa extract; 1.4-1.7 parts of Zanthoxylum bungeanum fruit extract; 2.62-2.95 parts of moisturizing and enhancing components; The moisturizing and synergistic component is composed of hydrolyzed sclerotium gum, porphyra polysaccharide and goldenseal extract; The mass ratio of the hydrolyzed sclerotium gum, the suiqiansi laver polysaccharide, and the melon seed gold extract is 1: (0.02-0.05): (1.6-1.9); The preparation method of the Melon Seed Gold Extract comprises the following steps: (1) Take the dried whole plant of Glehnia littoralis, grind it into powder using a grinder, and filter it through a 60-mesh sieve to obtain Glehnia littoralis powder; (2) Add 95 v / v% ethanol aqueous solution, where the material-water ratio is 1:6, reflux extract at 85°C for 2 times, each time for 1.5 h, filter, evaporate the residue, add distilled water at 95°C water bath for reflux extraction for 2 times, each time for 2 h, where the mass ratio of the residue to distilled water is 1:10, filter, combine the filtrate, and concentrate the filtrate at 50°C under reduced pressure to a water content of ≤30%, to obtain Guazijin concentrate; (3) Take papain with an enzyme activity of ≥300 U / g and add it in an amount of 3% of the mass of the concentrate. At the same time, add 95 v / v% ethanol aqueous solution to the concentrate in a volume ratio of 1:
1. Let it stand overnight, filter, and vacuum dry to obtain the golden melon seed extract.
2. A soothing and moisturizing facial mask, comprising a facial mask paper and an impregnation liquid, characterized in that: The impregnation liquid comprises the soothing and moisturizing composition of claim 1 and a solvent; The soothing and moisturizing composition is added in an amount of ≤3 wt % in the immersion liquid.
3. The soothing and moisturizing facial mask according to claim 2, characterized in that: The impregnation liquid also contains a thickener, a preservative, a pH regulator, an antioxidant and a moisturizer.
4. The soothing and moisturizing facial mask according to claim 3, characterized in that: The thickener is acrylic acid (ester) / C10-30 alkyl acrylate cross-linked polymer; The preservative is at least one of p-hydroxyacetophenone and phenoxyethanol; The moisturizer is at least one of butylene glycol, propylene glycol, allantoin, and sodium hyaluronate; The solvent is water; The pH regulator is triethanolamine; The antioxidant is at least one of vitamin C and water-soluble vitamin E.
5. The method for preparing the soothing and moisturizing facial mask according to claim 4, characterized in that: The following steps are involved: (1) Mixing the soothing and moisturizing composition, a thickener, a preservative, a solvent, a pH adjuster, an antioxidant and a moisturizer according to a proportion to obtain an impregnation solution; (2) Taking a facial mask paper and immersing it in an immersion liquid to obtain the soothing and moisturizing facial mask.
6. Use of the soothing and moisturizing composition according to claim 1 in the preparation of a skin care product with soothing and / or moisturizing effects.
Citation Information
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