Clean and environment-friendly biological fuel oil-diesel oil alternative fuel and preparation method thereof
Clean and environmentally friendly biofuel-diesel alternative fuel prepared by scientifically combining various compounds, the problem of exhaust emission pollution of fuel motor vehicles is solved, efficient combustion and low emissions are achieved, strict national exhaust emission standards are met, and the shelf life of the product is extended.
Patent Information
- Application Number
- CN202411259587.8
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-10
- Publication Date
- 2024-12-10
AI Technical Summary
Existing fuel-powered motor vehicles have exceeded the standard pollutants, and traditional purification equipment cannot effectively purify carbon monoxide and hydrocarbon gases, resulting in serious environmental pollution and it is difficult to meet the latest national and local exhaust emission standards.
Using a clean and environmentally friendly biofuel-diesel alternative fuel, through scientific compatibility with isooctyl nitrate, isopropyl ether, n-octanol, high-carbon fatty alcohol, polymethoxydimethyl ether, Fischer-Tropsch wax, castor oil, Glycerol oxalate, diisoamyl oxalate, 2-ethylhexyl nitrate, sodium dodecyl sulfonate, vinyl acetate, isopropanol and energy-saving and energizing combustion aids, prepared by thermal preparation and compounding of the mixture to form Biofuel with high cetane number and low sulfur content is used to replace traditional diesel.
The biofuel-diesel alternative fuel is fully burned during the combustion process, reducing exhaust smoke emissions and achieving higher cleaning results. It meets the National VI diesel standard, has a sulfur content lower than the national standard, and has a shelf life of more than 3 years, which significantly improves the environment. Pollution problem.
Smart Images

Figure CN119101544A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the field of diesel substitute fuel, and in particular to a clean and environmentally friendly biofuel-diesel substitute fuel and a preparation method thereof. Background Art
[0002] With the continuous maturity of automobile industry technology, the number of fuel-burning motor vehicles is increasing day by day. Exhaust emissions are becoming more and more serious. The main source of environmental pollutants is the engine exhaust of fuel-burning motor vehicles. Exhaust emissions from fuel vehicles account for more than 30% of environmental pollutants. These exhausts contain a large amount of harmful gases and inhalable particulate matter such as sulfides, nitrides, carbon, and lead. These exhaust emissions are distributed in the air 0.5 to 3 meters above the ground, seriously polluting the living environment of human beings and threatening human health.
[0003] In order to achieve the goal of "carbon peak and carbon neutrality", we should first start from the field of science and technology and vigorously develop technologies and measures for environmental governance. We should solve the bottleneck technologies of environmental governance, energy conservation and emission reduction, innovate and develop key products, and intensify efforts to promote clean, environmentally friendly, energy-saving and emission reduction industries.
[0004] In order to control the harm caused by exhaust emissions of fuel vehicles to the environment and humans, many countries in the world have formulated increasingly stringent exhaust emission standards and regulations for fuel vehicles. Installing a three-effect purifier and an electronic injection closed-loop controller on the exhaust system of fuel vehicles is one of the effective measures to solve automobile exhaust pollution. However, most of these devices can only purify particulate media, and have little effect on purifying carbon monoxide and hydrocarbon gases, and cannot play a very effective purification role. In order to better achieve the purification of fuel vehicle exhaust to meet the latest national six and Beijing six standards, in view of the phenomenon of excessive exhaust emission pollutants from fuel vehicles on the market and the stubborn problem of environmental pollution control, through years of research and experiments, the present invention summarizes a clean and environmentally friendly biofuel-diesel alternative fuel and its preparation method. Summary of the invention
[0005] In order to solve the problem of excessive exhaust pollutants from fuel-powered motor vehicles on the market and the stubborn problem of environmental pollution control, the present invention provides a clean and environmentally friendly biofuel-diesel alternative fuel and a preparation method thereof.
[0006] The present invention is realized by the following technical scheme: A clean and environmentally friendly biofuel-diesel alternative fuel, comprising the following raw materials:
[0007] Isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax, castor oil, glycerin, mixed alcohol, diisoamyl oxalate, 2-ethylhexyl nitrate, sodium dodecyl sulfonate, vinyl acetate, isopropanol, energy-saving and efficiency-enhancing combustion aid.
[0008] As a further improvement of the technical solution of the present invention, the clean and environmentally friendly biofuel-diesel alternative fuel comprises the following raw materials in parts by weight:
[0009] 3-5 parts of isooctyl nitrate, 4-6 parts of diisopropyl ether, 5-7 parts of n-octanol, 2-4 parts of high carbon number fatty alcohol, 29-31 parts of polymethoxy dimethyl ether, 13-15 parts of Fischer-Tropsch wax, 5-7 parts of castor oil, 3-5 parts of glycerol sesquioxide, 9-11 parts of mixed alcohol, 3-5 parts of diisoamyl oxalate, 5-8 parts of 2-ethylhexyl nitrate, 4-7 parts of sodium dodecyl sulfonate, 3-5 parts of vinyl acetate, 7-9 parts of isopropanol, and 1-2 parts of energy-saving and efficiency-enhancing combustion aid.
[0010] Furthermore, a clean and environmentally friendly biofuel-diesel alternative fuel is made from the following raw materials:
[0011] Isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax, castor oil, glycerin, mixed alcohol, diisoamyl oxalate, 2-ethylhexyl nitrate, sodium dodecyl sulfonate, vinyl acetate, isopropanol, energy-saving and efficiency-enhancing combustion aid.
[0012] The present invention also provides a clean and environmentally friendly biofuel-diesel alternative fuel, which is made from the following raw materials in parts by weight:
[0013] 3-5 parts of isooctyl nitrate, 4-6 parts of diisopropyl ether, 5-7 parts of n-octanol, 2-4 parts of high carbon number fatty alcohol, 29-31 parts of polymethoxy dimethyl ether, 13-15 parts of Fischer-Tropsch wax, 5-7 parts of castor oil, 3-5 parts of glycerol sesquioxide, 9-11 parts of mixed alcohol, 3-5 parts of diisoamyl oxalate, 5-8 parts of 2-ethylhexyl nitrate, 4-7 parts of sodium dodecyl sulfonate, 3-5 parts of vinyl acetate, 7-9 parts of isopropanol, and 1-2 parts of energy-saving and efficiency-enhancing combustion aid.
[0014] As a further improvement of the technical solution of the present invention, the mixed alcohol is a mixture of methanol, propane and butane.
[0015] The present invention further provides a method for preparing the clean and environmentally friendly biofuel-diesel alternative fuel, comprising the following steps:
[0016] Step 1: Preparation of component A: Place isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax and castor oil in a reactor at 110°C for 4 hours and transfer to a stirring tank for standby use;
[0017] Step 2: Preparation of component B: Add glycerol, mixed alcohol, diisoamyl oxalate and 2-ethylhexyl nitrate into a reaction kettle in sequence, heat to 100°C, react for 4 hours and transfer to a stirring tank for standby use;
[0018] Step 3: Sodium dodecyl sulfate, vinyl acetate, isopropyl alcohol and energy-saving and synergistic combustion improver are sent to the reactor for physical reaction at 100°C for 4 hours and then transferred to the stirring tank for standby use;
[0019] Step 4: Put the prepared components A and B and the refined components into a stirring tank and stir and mix them for 1 hour. After circulating the physical and chemical process for 4 hours, the finished product tank area is obtained.
[0020] The clean and environmentally friendly biofuel-diesel alternative fuel and its preparation method provided by the present invention have the following advantages compared with the prior art:
[0021] The disadvantages of traditional diesel fuel are incomplete combustion, easy coking and carbonization, and serious tail gas emission pollution. Therefore, how to solve its defects, improve its calorific value, make it burn fully, improve the cleaning effect, and reduce tail gas smoke emissions has become a key technical difficulty at present, and its bottleneck technology has not yet had an innovative breakthrough. The present invention provides a clean and environmentally friendly biofuel-diesel alternative fuel, which is formed by thermally blending a composite mixture based on the scientific compatibility of new biofuel-diesel alternative fuel materials. After more than 5 years of multiple tests and market sales and use inspections, its shelf life can reach more than 3 years.
[0022] The present invention belongs to clean fuel renewable energy, can completely replace petrochemical gasoline, diesel, boiler fuel oil, ship fuel, and is a biofuel-diesel substitute fuel completely independent of fossil fuels.
[0023] Compared with vehicle exhaust cleaners and national standard gasoline, clean and environmentally friendly biofuel-diesel alternative fuel has three advanced technical features
[0024]
[0025] BRIEF DESCRIPTION OF THE DRAWINGS
[0026] The accompanying drawings, which are incorporated in and constitute a part of this specification, illustrate embodiments consistent with the invention and, together with the description, serve to explain the principles of the invention.
[0027] In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, for ordinary technicians in this field, other drawings can be obtained based on these drawings without paying any creative work.
[0028] Figure 1This is the inspection report of the clean and environmentally friendly biofuel-diesel alternative fuel described in Example 1 of the present invention. From this inspection report, it can be seen that the distillation gap of the present invention is uniform and full, reaching the National VI diesel standard, and ensuring the power. Its flash point reaches the National VI diesel standard, and the sulfur content (mass fraction)% is 0.003, which is lower than the national standard. Therefore, it is cleaner and more environmentally friendly than the National VI standard diesel. DETAILED DESCRIPTION
[0029] In order to more clearly understand the above-mentioned objectives, features and advantages of the present invention, the scheme of the present invention will be further described below. It should be noted that the embodiments of the present invention and the features in the embodiments can be combined with each other without conflict.
[0030] In the following description, many specific details are set forth to facilitate a full understanding of the present invention, but the present invention may also be implemented in other ways different from those described herein; it is obvious that the embodiments in the specification are only part of the embodiments of the present invention, rather than all of the embodiments.
[0031] The present invention provides a clean and environmentally friendly biofuel-diesel alternative fuel, comprising the following raw materials:
[0032] Isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax, castor oil, glycerin, mixed alcohol, diisoamyl oxalate, 2-ethylhexyl nitrate, diisopropyl ether, sodium dodecyl sulfonate, vinyl acetate, isopropyl alcohol, energy-saving and efficiency-enhancing combustion aid.
[0033] In some embodiments of the present invention, additives capable of improving the comprehensive performance of diesel alternative fuels may be added to the above raw materials.
[0034] As a further improvement of the technical solution of the present invention, the clean and environmentally friendly biofuel-diesel alternative fuel comprises the following raw materials in parts by weight:
[0035] 3-5 parts of isooctyl nitrate, 4-6 parts of diisopropyl ether, 5-7 parts of n-octanol, 2-4 parts of high carbon number fatty alcohol, 29-31 parts of polymethoxy dimethyl ether, 13-15 parts of Fischer-Tropsch wax, 5-7 parts of castor oil, 3-5 parts of glycerol sesquioxide, 9-11 parts of mixed alcohol, 3-5 parts of diisoamyl oxalate, 5-8 parts of 2-ethylhexyl nitrate, 4-7 parts of sodium dodecyl sulfonate, 3-5 parts of vinyl acetate, 7-9 parts of isopropanol, and 1-2 parts of energy-saving and efficiency-enhancing combustion aid.
[0036] Furthermore, a clean and environmentally friendly biofuel-diesel alternative fuel is made from the following raw materials:
[0037] Isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax, castor oil, glycerin, mixed alcohol, diisoamyl oxalate, 2-ethylhexyl nitrate, sodium dodecyl sulfonate, vinyl acetate, isopropanol, energy-saving and efficiency-enhancing combustion aid.
[0038] The present invention also provides a clean and environmentally friendly biofuel-diesel alternative fuel, which is made from the following raw materials in parts by weight:
[0039] 3-5 parts of isooctyl nitrate, 4-6 parts of diisopropyl ether, 5-7 parts of n-octanol, 2-4 parts of high carbon number fatty alcohol, 29-31 parts of polymethoxy dimethyl ether, 13-15 parts of Fischer-Tropsch wax, 5-7 parts of castor oil, 3-5 parts of glycerol sesquioxide, 9-11 parts of mixed alcohol, 3-5 parts of diisoamyl oxalate, 5-8 parts of 2-ethylhexyl nitrate, 4-7 parts of sodium dodecyl sulfonate, 3-5 parts of vinyl acetate, 7-9 parts of isopropanol, and 1-2 parts of energy-saving and efficiency-enhancing combustion aid.
[0040] As a further improvement of the technical solution of the present invention, the mixed alcohol is a mixture of methanol, propane and butane. Preferably, the mixed alcohol is a mixture of 25wt% methanol, 45wt% propane and 30wt% butane.
[0041] The present invention further provides a method for preparing the clean and environmentally friendly biofuel-diesel alternative fuel, comprising the following steps:
[0042] Step 1: Preparation of component A: Place isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax, and castor oil in a reactor at 110° C. for reaction for 4 hours and transfer to a stirring tank for standby use;
[0043] Step 2: Preparation of component B: Add glycerol, mixed alcohol, diisoamyl oxalate and 2-ethylhexyl nitrate into a reaction kettle in sequence, heat to 100°C, react for 4 hours and transfer to a stirring tank for standby use;
[0044] Step 3: Sodium dodecyl sulfate, vinyl acetate, isopropyl alcohol and energy-saving and synergistic combustion improver are sent to the reactor for physical reaction at 100°C for 4 hours and then transferred to the stirring tank for standby use;
[0045] Step 4: Put the prepared components A and B and the refined components into a stirring tank and stir and mix them for 1 hour. After circulating the physical and chemical process for 4 hours, the finished product tank area is obtained.
[0046] The physicochemical properties and effects of each raw material in the present invention are briefly described as follows:
[0047] Isooctyl nitrate: It can increase the cetane number of diesel, improve the combustion performance of diesel, shorten the ignition time, reduce the ignition point, improve the thermal power of locomotives, and save fuel significantly. Application: It is used in diesel fuel, especially in secondary processed diesel to increase its cetane number. The effect of addition varies depending on the base oil. Generally, adding 0.1%-0.3% of isooctyl nitrate can increase the cetane number by 2-9 units. It can also be used as an organic solvent. It is used in the present invention to improve the combustibility and anti-explosion properties.
[0048] Diisopropyl ether: It is miscible in most organic solvents such as alcohol, ether, benzene, chloroform, etc. It has the function of being compatible with various formulation components in the present invention.
[0049] n-Octanol: It is a colorless flammable liquid with a special odor, which is miscible with most organic solvents. In the present invention, it is miscible with the auxiliary agents of each component, and can be called a highly compatible combustion aid.
[0050] High carbon number fatty alcohol: easily soluble in organic solvents such as n-butanol, isopropanol, ether, chloroform, ethanol, benzene, petroleum ether, cyclohexane, acetone, methanol, etc. It can be mixed with polyoxymethylene dimethyl ether to form the best multi-soluble solvent.
[0051] Polymethoxy dimethyl ether: It is a clean fuel. In the present invention, it can improve the lubrication performance of oil products, has good miscibility with fuel oil, and is very suitable as a diesel additive component. Polymethoxy dimethyl ether has a relatively high oxygen content, which can reach up to 51% at most, and an average cetane number of 76, which can improve the combustion efficiency of diesel in the engine. When added to diesel, it can significantly reduce pollutant emissions, reduce sulfide, CO and NOx emissions, and reduce tail gas pollution. Polymethoxy dimethyl ether is currently the best environmentally friendly solvent in the field of solvents. It is a very clean and environmentally friendly solvent oil that is sulfur-free, aromatic-free, benzene-free, and chlorine-free. As a solvent mother liquor, it has alcohol-soluble, ether-soluble, and fat-soluble multi-solubility and compatibility. It is currently the world's best universal solvent and an important component for diesel addition and replacement.
[0052] Fischer-Tropsch wax: Fischer-Tropsch wax is a methylene polymer, an alkane polymer synthesized from hydrocarbon-based syngas or natural gas. It mainly relies on high-quality and cheap raw materials from coal chemical industry for iron-based or cobalt-based synthesis. It is one of the base oils for formulating biofuel-diesel alternative fuel.
[0053] Castor oil: Castor oil is a vegetable oil with good lubricating properties. It can reduce friction and wear between mechanical parts and extend the service life. Castor oil contains more unsaturated fatty acids, which can be used as a rust inhibitor to protect the metal surface and prevent metal oxidation and corrosion. It has high drying and weather resistance, and can enhance the adhesion and durability of coatings and paints. Castor oil can also be used as a solvent, and the polyunsaturated fatty acids in castor oil can be used as additives for oil products. It can improve the softness, ductility and toughness of oil products and improve their service life. Castor oil can be used as a raw material for biofuel. Due to its high unsaturated fatty acid content, castor oil methyl ester is used as a diesel substitute. It is used as a biological raw material in the present invention.
[0054] Glycerol of kuehne acid: It is a saturated fatty acid ester, a special diluent, emulsifier stabilizer, solubilizer and preservative. It is colorless, odorless, transparent, has good stability and is durable in storage. It is used as a biological raw material in the present invention.
[0055] Mixed alcohol: It is a synthetic modifier using polymethoxy dimethyl ether as solvent. Propane, butane and methanol are mixed in a certain proportion to make methanol physically react and change its alkalinity. After the synthetic denaturant physically reacts with the molecular structure of methanol, a new molecular structure chain is formed under the action of polymethoxy dimethyl ether molecules, which effectively inhibits the secondary acid discharge of methanol during combustion, so that the acid is completely physicochemically transformed during combustion. Mixed alcohol has the advantages of cleanliness and environmental protection, safety and anti-explosion, strong power, low energy consumption rate, good versatility, low corrosiveness and low price. Thus, the purpose of modifying methanol raw materials is achieved. The corrosiveness of oil products to engines is greatly reduced.
[0056] Diisoamyl oxalate: It is a new type of diesel cetane number improver. It has obvious advantages in replacing traditional nitrate additives. It does not produce nitrogen oxides (NOx) when burned, does not corrode equipment, does not pollute the environment, and meets the requirements of environmentally friendly products. In the present invention, it is used to improve the octane number, promote combustion, and eliminate smoke, especially when mixed with isooctyl nitrate, the effect is better.
[0057] 2-Ethylhexyl nitrate: Cetane number improver, a class of compounds that easily decompose free particles, so it can accelerate the speed of the chain reaction when diesel fuel is ignited. It can promote the rapid oxidation of diesel, so it can improve the ignition characteristics of diesel. It can increase the chain initiation rate of diesel during the combustion process. It promotes the rapid oxidation of diesel and improves its ignition performance. At the same time, it is also the most economical and effective important component for improving tail gas emissions.
[0058] Sodium dodecyl sulfate: It is easy to biodegrade, with a biodegradability of more than 90%, and has little environmental pollution. The purpose of adding it in the present invention is to dissolve carbon molecules in the physical and chemical process, to achieve full combustion, and to play a role in fuel purification.
[0059] Vinyl acetate: soluble in alcohol, acetone, benzene, chloroform. In the present invention, it is used as an intermediate and adhesive for smoke suppressants, pour point depressants, and thickeners.
[0060] Isopropyl alcohol: As a solvent, it is a relatively cheap solvent in industry. It can mix freely with water and has a stronger solubility for lipophilic substances than ethanol. It is an extractant and can be used as an antifreeze, a cleaning agent, an additive for blending gasoline and diesel, an antifreeze, a dehydrating agent, etc.
[0061] Energy-saving and efficiency-enhancing combustion aid: This is a patented technology (CN105062589A) that the inventor has successfully applied for an invention patent for. The product is added to clean and environmentally friendly biofuel to improve its calorific value, burn fully, clean up coking and carbon deposits, and achieve energy-saving and efficiency-enhancing combustion-supporting effects. The fuel cleanliness is reduced to more than 99%, which is basically a zero emission effect.
[0062] The clean and environmentally friendly biofuel-diesel alternative fuel described in the present invention has a shelf life of more than 3 years. For details, please see the following oil quality shelf life comparison table:
[0063] Euro VI, US, China VI0 # Diesel and clean biomass Fuel-diesel alternative Four major fuel quality indicators Standard comparison table
[0064] Product Name: Cetane number Vapor Pressure Sulfur content Shelf life <![CDATA[Euro VI 0 # Diesel]]> 49 80 10 1 year <![CDATA[United States 0 # diesel]]> 40 76 5 1 year <![CDATA[China National VI 0 # Diesel]]> 48-50 88 5 1 year <![CDATA[Clean and Environmentally Friendly Biofuel - Diesel Alternative Fuel 0 # Diesel]]> 50-55 87 3 3 years
[0065] Through the comparison of the quality of four major oil products: Euro VI, US, China National VI diesel and clean and environmentally friendly biofuel-diesel alternative fuel, the indicators are compared. The sixteen values and vapor pressure are higher and better than the Euro VI, US, and China National VI diesel indicators; the sulfur content is much lower than the diesel emission indicators of Euro VI, US, and China National VI; the shelf life of Euro VI, US, and China National VI diesel is 1 year; the shelf life of the clean and environmentally friendly biofuel-diesel alternative fuel of the present invention is more than 3 years. After 5 years of research and development experiments, the product of the present invention has been mass-produced and sold in more than 20 provinces and cities such as Shanxi, Shandong, Henan, Hebei, Hunan, Hubei, and Zhejiang. More than 1 million tons have been sold in the market. The market effect is very good. In order to enable the product to enter the oil sales market of PetroChina and Sinopec, it will make a positive leading role and due contribution to "carbon peak and carbon neutrality".
[0066] The specific embodiments of the present invention are described in detail below.
[0067] Example 1
[0068] The present invention discloses a method for preparing a clean and environmentally friendly biofuel-diesel alternative fuel, which mainly comprises the following steps:
[0069] Step 1: Preparation of component A: 3 parts of isooctyl nitrate, 6 parts of diisopropyl ether, 7 parts of n-octanol, 2 parts of high carbon number fatty alcohol, 29 parts of polymethoxy dimethyl ether, 15 parts of Fischer-Tropsch wax and 7 parts of castor oil are placed in a reactor at 110°C for reaction for 4 hours and then transferred to a stirring tank for standby use;
[0070] Step 2, preparation of component B: 3 parts of glycerol ester, 11 parts of mixed alcohol, 5 parts of diisoamyl oxalate, and 8 parts of 2-ethylhexyl nitrate are added into a reaction kettle in sequence, heated to 100°C, reacted for 4 hours, and then transferred into a stirring tank for standby use; the mixed alcohol is a mixture of 25wt% methanol, 45wt% propane, and 30wt% butane;
[0071] The third step is to send 7 parts of sodium dodecyl sulfate, 5 parts of vinyl acetate, 9 parts of isopropanol and 2 parts of energy-saving and efficiency-enhancing combustion aid into the reactor for physical reaction at 100°C for 4 hours and then transfer them into a stirring tank for standby use.
[0072] Step 4: Put the prepared components A and B and the refined components into a stirring tank and stir and mix them for 1 hour. After 4 hours of circulation and chemical reaction, the finished product tank area is obtained.
[0073] Example 2
[0074] The present invention discloses a method for preparing a clean and environmentally friendly biofuel, namely a diesel alternative fuel, which mainly comprises the following steps:
[0075] Step 1: Preparation of component A: Place 5 parts of isooctyl nitrate, 4 parts of diisopropyl ether, 5 parts of n-octanol, 4 parts of high carbon number fatty alcohol, 31 parts of polymethoxy dimethyl ether, 13 parts of Fischer-Tropsch wax and 5 parts of castor oil in a reactor at 110°C and react for 4 hours, then transfer to a stirring tank for standby use;
[0076] Step 2: Preparation of component B: 5 parts of glycerol ester, 9 parts of mixed alcohol, 3 parts of diisoamyl oxalate and 5 parts of 2-ethylhexyl nitrate are added into a reaction kettle in sequence, heated to 100°C, reacted for 4 hours and transferred into a stirring tank for standby use; the mixed alcohol is a mixture of 25wt% methanol, 45wt% propane and 30wt% butane
[0077] The third step is to send 4 parts of sodium dodecyl sulfate, 3 parts of vinyl acetate, 7 parts of isopropyl alcohol and 1 part of energy-saving and efficiency-enhancing combustion aid into the reactor, carry out physical reaction at 100°C for 4 hours, and then transfer to a stirring tank for standby use.
[0078] Step 4: Put the prepared components A and B and the refined components into a stirring tank and stir and mix them for 1 hour. After 4 hours of circulation and chemical reaction, the finished product tank area is obtained.
[0079] Example 3
[0080] The present invention discloses a method for preparing a clean and environmentally friendly biofuel, namely a diesel alternative fuel, which mainly comprises the following steps:
[0081] Step 1: Preparation of component A: Place 4.5 parts of isooctyl nitrate, 5.5 parts of diisopropyl ether, 5.5 parts of n-octanol, 3 parts of high carbon number fatty alcohol, 31 parts of polymethoxy dimethyl ether, 14 parts of Fischer-Tropsch wax, and 6.5 parts of castor oil in a reactor at 110°C and react for 4 hours, then transfer to a stirring tank for standby use;
[0082] Step 2, preparation of component B: 3.5 parts of glycerol ester, 10 parts of mixed alcohol, 3.5 parts of diisoamyl oxalate and 6.5 parts of 2-ethylhexyl nitrate are added into a reaction kettle in sequence, heated to 100°C, reacted for 4 hours and transferred into a stirring tank for standby use; the mixed alcohol is a mixture of 25wt% methanol, 45wt% propane and 30wt% butane.
[0083] The third step is to send 5.5 parts of sodium dodecyl sulfate, 4 parts of vinyl acetate, 9 parts of isopropanol and 2 parts of energy-saving and efficiency-enhancing combustion aid into the reactor for physical reaction at 100°C for 4 hours and then transfer to a stirring tank for standby use.
[0084] Step 4: Put the prepared components A and B and the refined components into a stirring tank and stir and mix them for 1 hour. After 4 hours of circulation and chemical reaction, the finished product tank area is obtained.
[0085] The above is only a specific implementation of the present invention, which enables those skilled in the art to understand or implement the present invention. Although detailed descriptions are given with reference to the aforementioned embodiments, those skilled in the art should understand that they can still modify the technical solutions recorded in the aforementioned embodiments, or replace some or all of the technical features therein by equivalents; and these modifications or replacements do not make the essence of the corresponding technical solutions deviate from the scope of the technical solutions of the embodiments, and they should all be covered by the protection scope of the claims.
Claims
1. A clean and environmentally friendly biofuel-diesel alternative fuel, characterized in that: Including the following ingredients: Isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax, castor oil, glycerin, mixed alcohol, diisoamyl oxalate, 2-ethylhexyl nitrate, sodium dodecyl sulfonate, vinyl acetate, isopropanol, energy-saving and efficiency-enhancing combustion aid.
2. A clean and environmentally friendly biofuel-diesel alternative fuel, characterized in that: The invention comprises the following raw materials in parts by weight: 3-5 parts of isooctyl nitrate, 4-6 parts of diisopropyl ether, 5-7 parts of n-octanol, 2-4 parts of high carbon number fatty alcohol, 29-31 parts of polymethoxy dimethyl ether, 13-15 parts of Fischer-Tropsch wax, 5-7 parts of castor oil, 3-5 parts of glycerol sesquioxide, 9-11 parts of mixed alcohol, 3-5 parts of diisoamyl oxalate, 5-8 parts of 2-ethylhexyl nitrate, 4-7 parts of sodium dodecyl sulfonate, 3-5 parts of vinyl acetate, 7-9 parts of isopropanol, and 1-2 parts of energy-saving and efficiency-enhancing combustion aid.
3. A clean and environmentally friendly biofuel-diesel alternative fuel, characterized in that: It is made from the following raw materials: Isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax, castor oil, glycerin, mixed alcohol, diisoamyl oxalate, 2-ethylhexyl nitrate, sodium dodecyl sulfonate, vinyl acetate, isopropanol, energy-saving and efficiency-enhancing combustion aid.
4. A clean and environmentally friendly biofuel-diesel alternative fuel, characterized in that: It is made from the following raw materials in parts by weight: 3-5 parts of isooctyl nitrate, 4-6 parts of diisopropyl ether, 5-7 parts of n-octanol, 2-4 parts of high carbon number fatty alcohol, 29-31 parts of polymethoxy dimethyl ether, 13-15 parts of Fischer-Tropsch wax, 5-7 parts of castor oil, 3-5 parts of glycerol sesquioxide, 9-11 parts of mixed alcohol, 3-5 parts of diisoamyl oxalate, 5-8 parts of 2-ethylhexyl nitrate, 4-7 parts of sodium dodecyl sulfonate, 3-5 parts of vinyl acetate, 7-9 parts of isopropanol, and 1-2 parts of energy-saving and efficiency-enhancing combustion aid.
5. A clean and environmentally friendly biofuel-diesel alternative fuel according to any one of claims 1 to 4, characterized in that: The mixed alcohol is a mixture of methanol, propane and butane.
6. A method for preparing a clean and environmentally friendly biofuel-diesel alternative fuel as claimed in any one of claims 5, characterized in that: The steps include: Step 1: Preparation of component A: Place isooctyl nitrate, diisopropyl ether, n-octanol, high carbon number fatty alcohol, polymethoxy dimethyl ether, Fischer-Tropsch wax, and castor oil in a reactor at 110° C. for reaction for 4 hours and transfer to a stirring tank for standby use; Step 2: Preparation of component B: Add glycerol, mixed alcohol, diisoamyl oxalate and 2-ethylhexyl nitrate into a reaction kettle in sequence, heat to 100°C, react for 4 hours and transfer to a stirring tank for standby use; Step 3: Sodium dodecyl sulfate, vinyl acetate, isopropyl alcohol and energy-saving and synergistic combustion improver are sent to the reactor for physical reaction at 100°C for 4 hours and then transferred to the stirring tank for standby use; Step 4: Put the prepared components A and B and the refined components into a stirring tank and stir and mix them for 1 hour. After 4 hours of circulation and chemical reaction, the finished product tank area is obtained.
Citation Information
Patent Citations
Energy-saving synergetic combustion supporting agent, dimethyl ether synthesis fuel gases, and dimethyl ether synthesis fuel oil
CN105062589A
Clean environment-friendly ether diesel oil and preparation method thereof
CN107099347A
Automobile exhaust gas cleaning agent and preparation method thereof
CN108728188A
Environment-friendly automotive alcohol ether diesel for Fischer-Tropsch synthesis liquid wax
CN110218592A
High-flash-point, high-calorific-value and high-safety-coefficient liquid fuel for catering furnace
CN112961713A
