Automatic baking device for distillation cap of titanium sponge reduction reactor
Through the design of the automatic baking device of the distillation cap of the sponge titanium reduction reactor, welding difficulties and safety hazards caused by moisture inside the distillation cap are solved, welding quality and efficiency are improved, and the dryness and airtightness of the distillation cap are ensured.
Patent Information
- Application Number
- CN202411090727.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-08-09
- Publication Date
- 2024-12-10
AI Technical Summary
During the distillation cap welding process of the titanium sponge reduction reactor, the high temperature vaporization of the moisture inside the distillation cap cylinder leads to difficulty in forming the inner port of the welding, affecting the airtightness and bringing safety risks, and reducing welding efficiency.
Design a sponge titanium reduction reactor automatic baking device for distillation cap, including baking chamber, PID temperature controller, U-shaped resistor belt and refractory brick stacking layer, to remove moisture inside the distillation cap through automatic baking, ensuring the distillation cap before welding dry.
It effectively avoids the problems caused by high temperature vaporization of moisture during welding, improves welding quality and airtightness, eliminates safety hazards, simplifies welding preparation work, improves work efficiency and reduces costs.
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Figure CN119103816A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of titanium sponge production equipment, in particular to an automatic baking device for a distillation cap of a titanium sponge reduction reactor. Background Art
[0002] In the "Type I" semi-integrated titanium sponge reduction production process, the MgCl at the tail of the reduction reactor 2 A distillation cap needs to be welded on the discharge pipe to ensure the smooth progress of the distillation process and prevent the leakage of high-temperature melt or the mixing of air, which may cause discoloration of the titanium sponge.
[0003] However, in actual operation, if there is moisture inside the distillation cap cylinder, it will generate high-temperature vaporization during welding, which will not only make it difficult to form the inner welding mouth, but also may affect the airtightness of the discharge device welding mouth, thereby bringing safety hazards and reducing welding work efficiency. Therefore, before welding, it is necessary to ensure that the moisture inside the distillation cap cylinder is fully baked and removed. Summary of the invention
[0004] The purpose of the present invention is to provide an automatic baking device for the distillation cap of a sponge titanium reduction reactor, so as to solve the problem raised in the above background technology that in actual operation, if there is moisture inside the distillation cap cylinder, high-temperature vaporization will occur during welding, which will not only make it difficult to form the welding inner mouth, but may also affect the airtightness of the welding port of the discharge device, thereby bringing safety hazards and reducing the welding work efficiency.
[0005] To achieve the above-mentioned purpose, the present invention provides an automatic baking device for the distillation cap of a sponge titanium reduction reactor, comprising an external shell of the equipment, characterized in that a baking chamber is arranged inside the external shell of the equipment, the inner wall of the baking chamber is installed with ceramic fiber insulation cotton, an electrical control box is arranged at the bottom of the external shell of the equipment, a PID temperature controller is installed on the back of the baking chamber, a number of U-shaped resistance belts are evenly arranged on the inner walls on both sides of the baking chamber, a pad is installed on the bottom inner wall of the baking chamber, the bottom arc end of the U-shaped resistance belt is supported and positioned by the pad, and the front outer walls of the baking chamber and the electrical control box are both installed with warehouse doors.
[0006] As a preferred solution of the present invention, a nylon universal wheel is installed at the bottom of the electrical control box.
[0007] As a preferred solution of the present invention, there are two PID temperature controllers, which are respectively located at the upper and lower parts of the back side of the baking cavity of the external shell of the equipment.
[0008] As a preferred embodiment of the present invention, there are 10 groups of U-shaped resistance belts in total, with 5 groups on each side, so as to ensure that the distillation cap can be heated evenly.
[0009] As a preferred embodiment of the present invention, the outer side wall of the baking chamber is provided with a refractory brick stacking layer with a thickness of 10 cm, and the outside of the refractory brick stacking layer is provided with ceramic fiber insulation wool with a thickness of 10 cm.
[0010] As a preferred embodiment of the present invention, the refractory brick stacking layer and the ceramic fiber insulation wool are separated by a 1 cm steel plate.
[0011] As a preferred solution of the present invention, a sealing cover is provided on the top of the baking chamber, a pressure cover is installed on the top of the sealing cover, the upper end of the U-shaped resistance belt passes through the sealing cover and the pressure cover, and is sleeved with an insulating porcelain bottle.
[0012] As a preferred solution of the present invention, the U-shaped resistance belt comprises a U-shaped electric heating rod, the upper end of the U-shaped electric heating rod is sleeved with an insulating sleeve, and the insulating porcelain bottle sleeve is arranged at the upper end of the insulating sleeve.
[0013] As a preferred embodiment of the present invention, a socket is provided inside the insulating sleeve, the upper part of the U-shaped electric heating rod is inserted into the socket, the outer wall of the insulating sleeve is provided with an external thread, the surfaces of the sealing cover and the pressure cover are provided with threaded holes, and the insulating sleeve is threadedly connected to the threaded holes of the sealing cover and the pressure cover.
[0014] As a preferred embodiment of the present invention, the baking steps are as follows:
[0015] S1. Ensure that the automatic baking device for the distillation cap of the titanium sponge reduction reactor is in good working condition, check whether all parts are intact, clean the distillation cap that needs to be baked, and remove surface impurities;
[0016] S2. Open the door of the baking chamber, place the distillation cap horizontally in the baking chamber, ensure that the inner opening of the distillation cap cylinder is opposite to the heating surface of the U-shaped resistance belt, so that the internal moisture can be completely dried during baking, and close the door of the baking chamber to ensure good sealing;
[0017] S3. Turn on the power of the electrical control box, set the baking temperature and time through the PID temperature controller, set the baking temperature at 250℃-300℃, and maintain it for 10 minutes after the temperature reaches the set temperature;
[0018] S4. After confirming that the baking parameters are set correctly, start the baking program. The electrical control box will control the U-shaped resistance belt to start heating. During the baking process, the PID temperature controller will monitor the temperature in the baking chamber in real time and adjust it as needed to ensure that the temperature is controlled within the set range.
[0019] S5. When the baking time reaches the set value and the temperature maintenance time ends, the baking device will automatically stop heating and wait for the distillation cap to naturally cool to a safe temperature in the baking chamber, then open the door and take out the distillation cap; S6. Check whether the distillation cap is dry after baking to ensure that all the internal moisture has been removed.
[0020] Compared with the prior art, the present invention has the following beneficial effects:
[0021] 1. In the automatic baking device for the distillation cap of the titanium sponge reduction reactor, the moisture inside the distillation cap cylinder is effectively baked to avoid the difficulty in forming the inner mouth of the welding due to high-temperature vaporization of moisture during welding, thereby significantly improving the welding quality. The use of the baking device ensures the complete removal of moisture inside the distillation cap before welding, thereby improving the airtightness of the welding port of the discharge device, effectively preventing leakage of high-temperature melt and mixing of air, and avoiding discoloration of titanium sponge. The use of the device eliminates the safety hazards caused by residual moisture inside the distillation cap, such as problems that may be caused by high-temperature vaporization during welding, and provides a safer environment for the production process.
[0022] 2. In the automatic baking device for the distillation cap of the titanium sponge reduction reactor, the automated baking method simplifies the preparation work before welding, reduces manual intervention, significantly improves work efficiency, and reduces labor costs. The design of the baking device takes into account various needs in practical applications, such as the dual-point control of the PID temperature controller, the uniform distribution of the U-shaped resistance belt, and the composite insulation layer of refractory bricks and ceramic fiber insulation cotton, which enhance the adaptability and durability of the device. The baking device has a simple structure and is easy to operate. The design of the nylon universal wheel makes the equipment more convenient to move and carry. At the same time, all parts of the equipment are easy to inspect and maintain, ensuring the long-term stable operation of the equipment. BRIEF DESCRIPTION OF THE DRAWINGS
[0023] Figure 1 It is a schematic diagram of the overall structure of the present invention;
[0024] Figure 2 It is a schematic diagram of the internal front structure of the present invention;
[0025] Figure 3 It is a schematic diagram of the internal side structure of the present invention;
[0026] Figure 4 It is a schematic diagram of the structure of the U-shaped resistance belt in the present invention;
[0027] Figure 5 It is a schematic diagram of the internal structure of the insulating sleeve in the present invention;
[0028] The meaning of each number in the figure is:
[0029] 1. PID temperature controller; 2. Equipment external shell; 3. U-shaped resistance belt; 31. U-shaped electric heating rod; 32. Insulating sleeve; 321. External thread; 322. Socket; 4. Electrical control box; 5. Nylon universal wheel; 6. Ceramic fiber insulation cotton; 61. Sealing cover; 62. Pressure cover; 63. Pad; 7. Refractory brick stacking layer; 8. Insulating porcelain bottle. DETAILED DESCRIPTION
[0030] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0031] Example 1
[0032] The present invention provides an automatic baking device for a distillation cap of a titanium sponge reduction reactor, such as Figure 1-Figure 5 As shown, the device comprises an external shell 2, a baking chamber is arranged inside the external shell 2, a ceramic fiber thermal insulation cotton 6 is installed on the inner wall of the baking chamber, an electrical control box 4 is arranged at the bottom of the external shell 2, a PID temperature controller 1 is installed on the back of the baking chamber, a plurality of U-shaped resistance bands 3 are evenly arranged on the inner walls of both sides of the baking chamber, a pad 63 is installed on the bottom inner wall of the baking chamber, and the bottom arc end of the U-shaped resistance band 3 is supported and positioned by the pad 63, and the front outer walls of the baking chamber and the electrical control box 4 are both installed with a compartment door, and the inner wall of the baking chamber is installed with ceramic fiber thermal insulation cotton 6. This material has good thermal insulation performance, can effectively reduce heat loss, improve baking efficiency, and reduce energy consumption. A PID temperature controller 1 is installed on the back of the baking chamber, which can accurately control and adjust the temperature in the baking chamber, ensure the temperature stability and uniformity during the baking process, and thus improve the baking quality. A plurality of U-shaped resistance bands 3 are evenly arranged on the inner walls of both sides of the baking chamber. This layout can ensure that the distillation cap is heated evenly during the baking process, avoid local overheating or insufficient temperature, and further improve the baking effect. The bottom arc end of the U-shaped resistance belt 3 is supported and positioned by the pad 63. This design not only ensures the stability of the resistance belt, but also prolongs its service life and reduces damage caused by vibration or displacement. The front outer wall of the baking chamber and the electrical control box 4 are both equipped with doors. This design makes the maintenance and inspection of the equipment more convenient. Necessary operations can be performed without disassembling the entire equipment, reducing maintenance costs and time.
[0033] In this embodiment, nylon universal wheels 5 are installed at the bottom of the electrical control box 4 to facilitate the flexible movement of the equipment.
[0034] Specifically, there are two PID temperature controllers 1, which are located at the upper and lower parts of the back of the baking chamber of the external shell 2 of the device, so as to facilitate the simultaneous control and detection of the temperature on both sides of the upper and lower parts. The PID temperature controller continuously measures and compares the difference between the actual temperature and the set value, and adjusts the output of the actuator (such as the power of the heating element) according to the difference, so that the actual temperature gradually approaches and stabilizes near the set value. Its working principle is based on the basic principle of the feedback control system, combining the three control methods of proportion, integration and differentiation to achieve the best control effect. This is the content of the prior art and will not be described in detail here.
[0035] Furthermore, there are a total of 10 groups of U-shaped resistance belts 3, with 5 groups on each side, which are used to ensure that the distillation cap can be heated evenly. This layout ensures that the distillation cap can be heated evenly during the heating process, avoiding local overheating or insufficient temperature, thereby improving the baking quality and efficiency.
[0036] Furthermore, the outer wall of the baking chamber is provided with a refractory brick stacking layer 7 with a thickness of 10 cm, and the outside of the refractory brick stacking layer 7 is provided with ceramic fiber insulation cotton 6 with a thickness of 10 cm, which ensures a good heat insulation effect. This double-layer insulation structure greatly reduces heat loss, improves the insulation performance of the baking chamber, and reduces energy consumption.
[0037] Furthermore, the refractory brick stacking layer 7 and the ceramic fiber insulation cotton 6 are separated by a 1 cm steel plate. This design not only enhances the structural stability of the baking chamber, but also prevents the insulation material from directly contacting the fire source, thereby improving the safety of the equipment.
[0038] Furthermore, a sealing cover 61 is provided on the top of the baking chamber, a pressure cover 62 is installed on the top of the sealing cover 61, the upper end of the U-shaped resistance belt 3 passes through the sealing cover 61 and the pressure cover 62, and is sleeved with an insulating porcelain bottle 8 to ensure a good insulation effect. This design ensures the sealing of the baking chamber and prevents heat loss. At the same time, the insulating porcelain bottle 8 provides a good insulation effect to ensure the safe operation of the equipment.
[0039] Example 2
[0040] The present invention provides an automatic baking device for a distillation cap of a titanium sponge reduction reactor, such as Figure 1-Figure 5As shown, the device comprises an external shell 2, a baking chamber is arranged inside the external shell 2, a ceramic fiber thermal insulation cotton 6 is installed on the inner wall of the baking chamber, an electrical control box 4 is arranged at the bottom of the external shell 2, a PID temperature controller 1 is installed on the back of the baking chamber, a plurality of U-shaped resistance bands 3 are evenly arranged on the inner walls of both sides of the baking chamber, a pad 63 is installed on the bottom inner wall of the baking chamber, and the bottom arc end of the U-shaped resistance band 3 is supported and positioned by the pad 63, and the front outer walls of the baking chamber and the electrical control box 4 are both installed with a compartment door, and the inner wall of the baking chamber is installed with ceramic fiber thermal insulation cotton 6. This material has good thermal insulation performance, can effectively reduce heat loss, improve baking efficiency, and reduce energy consumption. A PID temperature controller 1 is installed on the back of the baking chamber, which can accurately control and adjust the temperature in the baking chamber, ensure the temperature stability and uniformity during the baking process, and thus improve the baking quality. A plurality of U-shaped resistance bands 3 are evenly arranged on the inner walls of both sides of the baking chamber. This layout can ensure that the distillation cap is heated evenly during the baking process, avoid local overheating or insufficient temperature, and further improve the baking effect. The bottom arc end of the U-shaped resistance belt 3 is supported and positioned by the pad 63. This design not only ensures the stability of the resistance belt, but also prolongs its service life and reduces damage caused by vibration or displacement. The front outer wall of the baking chamber and the electrical control box 4 are both equipped with doors. This design makes the maintenance and inspection of the equipment more convenient. Necessary operations can be performed without disassembling the entire equipment, reducing maintenance costs and time.
[0041] In this embodiment, nylon universal wheels 5 are installed at the bottom of the electrical control box 4 to facilitate the flexible movement of the equipment.
[0042] Specifically, there are two PID temperature controllers 1, which are located at the upper and lower parts of the back of the baking chamber of the external shell 2 of the device, respectively, so as to facilitate simultaneous control and detection of the temperature on both sides of the upper and lower parts. The PID temperature controller continuously measures and compares the difference between the actual temperature and the set value, and adjusts the output of the actuator (such as the power of the heating element) according to the difference, so that the actual temperature gradually approaches and stabilizes near the set value. Its working principle is based on the basic principle of the feedback control system, combining the three control methods of proportion, integration and differentiation to achieve the best control effect. This is the content of the prior art and will not be described in detail here.
[0043] Furthermore, there are a total of 10 groups of U-shaped resistance belts 3, with 5 groups on each side, which are used to ensure that the distillation cap can be heated evenly. This layout ensures that the distillation cap can be heated evenly during the heating process, avoiding local overheating or insufficient temperature, thereby improving the baking quality and efficiency.
[0044] Furthermore, the outer wall of the baking chamber is provided with a refractory brick stacking layer 7 with a thickness of 10 cm, and the outside of the refractory brick stacking layer 7 is provided with ceramic fiber insulation cotton 6 with a thickness of 10 cm, which ensures a good heat insulation effect. This double-layer insulation structure greatly reduces heat loss, improves the insulation performance of the baking chamber, and reduces energy consumption.
[0045] Furthermore, the refractory brick stacking layer 7 and the ceramic fiber insulation cotton 6 are separated by a 1 cm steel plate. This design not only enhances the structural stability of the baking chamber, but also prevents the insulation material from directly contacting the fire source, thereby improving the safety of the equipment.
[0046] Furthermore, a sealing cover 61 is provided on the top of the baking chamber, a pressure cover 62 is installed on the top of the sealing cover 61, the upper end of the U-shaped resistance belt 3 passes through the sealing cover 61 and the pressure cover 62, and is sleeved with an insulating porcelain bottle 8 to ensure a good insulation effect. This design ensures the sealing of the baking chamber and prevents heat loss. At the same time, the insulating porcelain bottle 8 provides a good insulation effect to ensure the safe operation of the equipment.
[0047] Furthermore, the U-shaped resistance belt 3 includes a U-shaped electric heating rod 31 , the upper end of the U-shaped electric heating rod 31 is sleeved with an insulating sleeve 32 , and the insulating porcelain bottle 8 is sleeved on the upper end of the insulating sleeve 32 to facilitate the positioning of the U-shaped electric heating rod 31 .
[0048] Furthermore, a socket 322 is provided inside the insulating sleeve 32, and the upper part of the U-shaped electric heating rod 31 is inserted into the socket 322. The outer wall of the insulating sleeve 32 is provided with an external thread 321, and the surfaces of the sealing cover 61 and the pressure cover 62 are provided with threaded holes. The insulating sleeve 32 is threadedly connected with the threaded holes of the sealing cover 61 and the pressure cover 62, which facilitates the installation and fixation of the insulating sleeve 32. This design makes the installation and fixation of the U-shaped resistance belt more convenient, and is also convenient for subsequent maintenance and replacement.
[0049] Further, the baking steps are as follows:
[0050] S1. Ensure that the automatic baking device for the distillation cap of the titanium sponge reduction reactor is in good working condition, check whether all parts are intact, clean the distillation cap that needs to be baked, and remove surface impurities;
[0051] S2. Open the door of the baking chamber, place the distillation cap horizontally in the baking chamber, ensure that the inner opening of the distillation cap cylinder is opposite to the heating surface of the U-shaped resistance belt, so that the internal moisture can be completely dried during baking, and close the door of the baking chamber to ensure good sealing;
[0052] S3. Turn on the power of the electrical control box, set the baking temperature and time through the PID temperature controller, set the baking temperature at 250℃-300℃, and maintain it for 10 minutes after the temperature reaches the set temperature;
[0053] S4. After confirming that the baking parameters are set correctly, start the baking program. The electrical control box will control the U-shaped resistance belt to start heating. During the baking process, the PID temperature controller will monitor the temperature in the baking chamber in real time and adjust it as needed to ensure that the temperature is controlled within the set range.
[0054] S5. When the baking time reaches the set value and the temperature maintenance time is over, the baking device will automatically stop heating, wait for the distillation cap to cool naturally to a safe temperature in the baking chamber, and then open the door to take out the distillation cap;
[0055] S6. Check whether the distillation cap is dry after baking and ensure that all the internal moisture has been removed.
[0056] Finally, it should be noted that the electrical control box 4 and other components in this embodiment, the electronic components in the above parts are all universal standard parts or parts known to technical personnel in this field, and their structures and principles can be known to technical personnel in this field through technical manuals or through conventional experimental methods. In the idle part of this device, all the above electrical components are connected by wires respectively, and the specific connection means should refer to the working sequence between the electrical components in the above working principle to complete the electrical connection, which are all well-known technologies in the field.
[0057] The above shows and describes the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited by the above embodiments. The above embodiments and descriptions are only preferred examples of the present invention and are not intended to limit the present invention. Without departing from the spirit and scope of the present invention, the present invention may have various changes and improvements, which fall within the scope of the present invention. The scope of protection of the present invention is defined by the attached claims and their equivalents.
Claims
1. An automatic baking device for a distillation cap of a titanium sponge reduction reactor, comprising an outer shell (2) of the device, characterized in that: A baking chamber is arranged inside the outer shell (2) of the device, and ceramic fiber thermal insulation cotton (6) is installed on the inner wall of the baking chamber. An electrical control box (4) is arranged at the bottom of the outer shell (2) of the device, and a PID temperature controller (1) is installed on the back of the baking chamber. A plurality of U-shaped resistance bands (3) are evenly arranged on the inner walls of both sides of the baking chamber, and a pad (63) is installed on the bottom inner wall of the baking chamber. The bottom arc end of the U-shaped resistance band (3) is supported and positioned by the pad (63), and the front outer walls of the baking chamber and the electrical control box (4) are both installed with warehouse doors.
2. The automatic baking device for the distillation cap of a titanium sponge reduction reactor according to claim 1, characterized in that: A nylon universal wheel (5) is installed at the bottom of the electrical control box (4).
3. The automatic baking device for the distillation cap of a titanium sponge reduction reactor according to claim 1, characterized in that: There are two PID temperature controllers (1), which are respectively located at the upper and lower parts of the back side of the baking chamber of the device external shell (2).
4. The automatic baking device for the distillation cap of a titanium sponge reduction reactor according to claim 1, characterized in that: There are a total of 10 groups of U-shaped resistance bands (3), with 5 groups on each side, which are used to ensure that the distillation cap can be heated evenly when heated.
5. The automatic baking device for the distillation cap of a titanium sponge reduction reactor according to claim 1, characterized in that: The outer wall of the baking chamber is provided with a refractory brick stacking layer (7) with a thickness of 10 cm, and the outside of the refractory brick stacking layer (7) is provided with ceramic fiber thermal insulation cotton (6) with a thickness of 10 cm.
6. The automatic baking device for the distillation cap of the titanium sponge reduction reactor according to claim 5, characterized in that: The refractory brick stacking layer (7) and the ceramic fiber thermal insulation wool (6) are separated by a 1 cm steel plate.
7. The automatic baking device for the distillation cap of a titanium sponge reduction reactor according to claim 1, characterized in that: A sealing cover (61) is arranged on the top of the baking chamber, a pressure cover (62) is installed on the top of the sealing cover (61), the upper end of the U-shaped resistance belt (3) passes through the sealing cover (61) and the pressure cover (62), and is sleeved with an insulating porcelain bottle (8).
8. The automatic baking device for the distillation cap of a titanium sponge reduction reactor according to claim 7, characterized in that: The U-shaped resistance belt (3) comprises a U-shaped electric heating rod (31), the upper end of the U-shaped electric heating rod (31) is sleeved with an insulating sleeve (32), and the insulating porcelain bottle (8) is sleeved on the upper end of the insulating sleeve (32).
9. The automatic baking device for the distillation cap of the titanium sponge reduction reactor according to claim 8, characterized in that: The insulating sleeve (32) is provided with a plug hole (322) inside, the upper part of the U-shaped electric heating rod (31) is inserted into the plug hole (322), the outer wall of the insulating sleeve (32) is provided with an external thread (321), the surfaces of the sealing cover (61) and the pressure cover (62) are provided with threaded holes, and the insulating sleeve (32) is threadedly connected with the threaded holes of the sealing cover (61) and the pressure cover (62).
10. The automatic baking device for the distillation cap of a titanium sponge reduction reactor according to claim 1, characterized in that: The baking steps are as follows: S1. Ensure that the automatic baking device for the distillation cap of the titanium sponge reduction reactor is in good working condition, check whether all parts are intact, clean the distillation cap that needs to be baked, and remove surface impurities; S2. Open the door of the baking chamber, place the distillation cap horizontally in the baking chamber, ensure that the inner opening of the distillation cap cylinder is opposite to the heating surface of the U-shaped resistance belt, so that the internal moisture can be completely dried during baking, and close the door of the baking chamber to ensure good sealing; S3. Turn on the power of the electrical control box, set the baking temperature and time through the PID temperature controller, set the baking temperature at 250℃-300℃, and maintain it for 10 minutes after the temperature reaches the set temperature; S4. After confirming that the baking parameters are set correctly, start the baking program. The electrical control box will control the U-shaped resistance belt to start heating. During the baking process, the PID temperature controller will monitor the temperature in the baking chamber in real time and adjust it as needed to ensure that the temperature is controlled within the set range. S5. When the baking time reaches the set value and the temperature maintenance time is over, the baking device will automatically stop heating, wait for the distillation cap to cool naturally to a safe temperature in the baking chamber, and then open the door to take out the distillation cap; S6. Check whether the distillation cap is dry after baking and ensure that all the internal moisture has been removed.
Citation Information
Patent Citations
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