Demulsification degree determinator and demulsification degree determination method

Abstract

The invention relates to the technical field of demulsification degree measuring instruments, in particular to a demulsification degree measuring instrument and a demulsification degree measuring method.The demulsification degree measuring instrument comprises a lifting assembly, the lifting assembly comprises a containing part, a driving part and a conversion part, the driving part is arranged on the containing part, and the conversion part is arranged on the driving part; and the stirring assembly comprises a mounting part, an auxiliary part and a follower, the mounting part is arranged on the conversion part, the auxiliary part is arranged on the driving part, the follower is arranged on the auxiliary part, and an automatic stirring function can be conveniently and rapidly performed according to the number of test tubes needing to be tested through the lifting assembly and the stirring assembly. The stirring time can be controlled according to needs, manual operation is reduced, the operation process is simplified, and the testing efficiency is improved; full-detection process automatic control and detection are completed through the method design, so that the sample detection time is greatly shortened; the target of detecting human resource requirements is reduced, and the stability and accuracy of detection results and the working efficiency are improved.

Description

Technical Field

[0001] The invention relates to the technical field of demulsification degree measuring instruments, and in particular to a demulsification degree measuring instrument and a demulsification degree measuring method. Background Art

[0002] Demulsification is an important indicator to measure the ability of turbine oil to separate from water. When the oil has strong demulsification performance, the oil-water emulsion can be quickly separated in the oil tank, thereby effectively reducing the damage of the oil film, preventing the corrosion of metal parts and delaying the aging of the oil, ensuring the normal operation of the equipment. However, if the demulsification performance is weak, the oil-water emulsion is separated slowly, which will lead to the rupture of the oil film, the corrosion of metal parts, and the acceleration of oil aging. These will increase the friction between parts and may cause equipment overheating or even damage.

[0003] At present, the laboratory usually uses manual operation to test the demulsibility: inject the oil sample and water sample into the measuring cylinder respectively, prepare the emulsion by high-speed stirring, then stop stirring and let it stand for a period of time to observe the oil-water separation process. This process mainly relies on the naked eye observation of the experimenter to determine the state of oil-water separation and the operation is complicated. A stopwatch is used to record the time. This method has obvious limitations, such as the lack of unified specifications and standards, low degree of automation, the test results are greatly affected by subjective factors, and the data stability and accuracy are not ideal. These problems not only reduce the test efficiency, but also increase the result error, which has an adverse effect on subsequent data analysis and quality control. Summary of the invention

[0004] In view of the above problems that the oil-water separation state is mainly determined by naked eye observation of the experimenter and the test operation is complicated, the present invention is proposed.

[0005] Therefore, the object of the present invention is to provide a demulsification degree measuring instrument and a demulsification degree measuring method.

[0006] In order to solve the above technical problems, the present invention provides the following technical solutions: a demulsification degree measuring instrument, comprising:

[0007] A lifting assembly comprises a receiving member, a driving member and a transition member, wherein the driving member is arranged on the receiving member, and the transition member is arranged on the driving member; and

[0008] The stirring component comprises a mounting part, an auxiliary part and a follower part, wherein the mounting part is arranged on the conversion part, the auxiliary part is arranged on the driving part, and the follower part is arranged on the auxiliary part.

[0009] As a preferred solution of the demulsification degree measuring instrument described in the present invention, the accommodating part includes a lifting shell, a heating seat, a placement shell and a treatment pool, the heating seat is arranged on the lifting shell, and the placement shell and the treatment pool are arranged on the heating seat.

[0010] As a preferred solution of the demulsification degree measuring instrument described in the present invention, the driving part includes a servo motor, a first threaded rod, a moving block, a connecting block, a lifting column and a lifting seat, the servo motor is arranged on the lifting shell, the first threaded rod is arranged on the servo motor, the moving block is arranged on the first threaded rod, the connecting block is arranged on the moving block, the lifting column is arranged on the connecting block, and the lifting seat is arranged on the lifting column.

[0011] As a preferred solution of the demulsification degree measuring instrument described in the present invention, the transition member includes a positioning bead, a transition block, a deflection groove, a storage shell, a test tube and a positioning block, the positioning bead and the transition block are arranged on the lifting column, the deflection groove is arranged on the transition block, the storage shell is arranged on the lifting seat, and the test tube and the positioning block are arranged on the storage shell.

[0012] As a preferred solution of the demulsification degree measuring instrument described in the present invention, wherein: the mounting part includes a mounting groove, a displacement groove, a movable arc block, a lifting block, a compression groove, a first spring and an embedded block, the mounting groove and the displacement groove are arranged on the storage shell, the movable arc block is arranged on the displacement groove, the lifting block is arranged on the movable arc block, the compression groove is arranged on the test tube, the first spring is arranged on the compression groove, and the embedded block is arranged on the first spring.

[0013] As a preferred solution of the demulsification degree measuring instrument described in the present invention, the auxiliary parts include a fixed plate, a movable groove, a falling groove, a positioning groove, a first energy storage block, a rotating shaft and a stirring rod, the fixed plate is arranged on the lifting seat, the movable groove, the falling groove and the positioning groove are arranged on the fixed plate, the first energy storage block is arranged on the positioning groove, the rotating shaft is arranged on the first energy storage block, and the stirring rod is arranged on the rotating shaft.

[0014] As a preferred embodiment of the demulsification degree measuring instrument described in the present invention, the follower includes a moving column, a falling block, a passive block, a limiting block, a follower ring, a ball, a second threaded rod and a second energy storage block, the moving column is arranged on the first energy storage block, the falling block, the passive block and the limiting block are arranged on the moving column, the follower ring is arranged on the limiting block, the ball is arranged on the follower ring, the second threaded rod is arranged on the ball, and the second energy storage block is arranged on the second threaded rod.

[0015] A method for measuring demulsification degree, comprising the above-mentioned demulsification degree measuring instrument, comprises the following steps:

[0016] Through preparation and initial setup and water bath heating;

[0017] Then through automatic measurement and result recording and output;

[0018] Finally, automatic cleaning and drying are carried out to complete the whole process of demulsification degree detection.

[0019] As a preferred solution of the method for determining the demulsification degree of the present invention, the lifting component and the stirring component are used to synchronously realize automatic lifting and stirring functions, thereby simplifying the operation process.

[0020] As a preferred solution of the method for determining demulsification degree described in the present invention, water bath heating and constant temperature control use high-precision temperature sensors, intelligent temperature controllers, and high-resolution analog-to-digital conversion and digital-to-analog conversion technologies to ensure accurate control of the water bath temperature.

[0021] The beneficial effects of the present invention are as follows: the lifting assembly and the stirring assembly can conveniently perform the automatic stirring function according to the number of test tubes required for testing, and the stirring time can be controlled according to the needs, which reduces the number of personnel required for operation, simplifies the operation process and improves the test efficiency;

[0022] The entire testing process is automated and controlled through method design to significantly shorten the time for sample testing. This reduces the demand for human resources for testing, frees up labor, and improves the stability, accuracy, and work efficiency of test results. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following briefly introduces the drawings required for use in the description of the embodiments. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.

[0024] Figure 1 The figure is a schematic diagram of the overall structure of an instrument for measuring demulsification degree of the present invention.

[0025] Figure 2 The figure is a schematic cross-sectional view of a demulsification degree measuring instrument of the present invention.

[0026] Figure 3 The present invention is a schematic diagram of the structure of a driving component of a demulsification degree measuring instrument.

[0027] Figure 4The figure is a schematic diagram of the structure of a transition piece of a demulsification degree measuring instrument of the present invention.

[0028] Figure 5 The figure is another schematic diagram of the overall structure of a demulsification degree tester of the present invention.

[0029] Figure 6 The present invention is a schematic diagram of the structure of a stirring component of a demulsification degree tester.

[0030] Figure 7 The present invention is a schematic diagram of the structure of the mounting parts of a demulsification degree measuring instrument.

[0031] Figure 8 The figure is a schematic diagram of the auxiliary parts structure of a demulsification degree measuring instrument of the present invention.

[0032] Fig. 9 The present invention is a schematic diagram of the connection structure of the mounting parts and auxiliary parts of a demulsification degree tester.

[0033] Fig.10 The present invention is a schematic diagram of the follower structure of a demulsification degree measuring instrument.

[0034] Fig.11 The present invention is a schematic diagram of a control and detection system for a method for determining demulsification degree.

[0035] Fig.12 The present invention is a schematic diagram of an automatic cleaning and drying module for a method for determining a demulsification degree. DETAILED DESCRIPTION

[0036] In order to make the above-mentioned objects, features and advantages of the present invention more obvious and easy to understand, the specific implementation methods of the present invention are described in detail below in conjunction with the accompanying drawings.

[0037] In the following description, many specific details are set forth to facilitate a full understanding of the present invention, but the present invention may also be implemented in other ways different from those described herein, and those skilled in the art may make similar generalizations without violating the connotation of the present invention. Therefore, the present invention is not limited to the specific embodiments disclosed below.

[0038] Secondly, the term "one embodiment" or "embodiment" as used herein refers to a specific feature, structure, or characteristic that may be included in at least one implementation of the present invention. The term "in one embodiment" that appears in different places in this specification does not necessarily refer to the same embodiment, nor is it a separate or selective embodiment that is mutually exclusive with other embodiments.

[0039] Secondly, the present invention is described in detail with reference to the schematic diagram. When describing the embodiments of the present invention in detail, for the sake of convenience, the cross-sectional diagrams showing the device structure will not be partially enlarged according to the general scale, and the schematic diagrams are only examples, which should not limit the scope of protection of the present invention. In addition, in actual production, the three-dimensional dimensions of length, width and depth should be included.

[0040] Example 1

[0041] Reference Figure 1 - Figure 5 , which is the first embodiment of the present invention, provides a demulsification degree measuring instrument, which includes a lifting component 100, including a receiving component 101, a driving component 102 and a transition component 103, wherein the driving component 102 is arranged on the receiving component 101, and the transition component 103 is arranged on the driving component 102. Through the interaction between the receiving component 101, the driving component 102 and the transition component 103, the entire device can be lifted and lowered and rotated during the lifting, so that it is convenient for the installation of the test tube 103e and the placement after installation to facilitate subsequent test operations.

[0042] Specifically, the container 101 includes a lifting shell 101a, a heating seat 101b, a placement shell 101c and a treatment pool 101d. The lifting shell 101a is arranged on the operating table and is a rectangular structure. A certain operable space is provided inside to facilitate demulsification degree detection. The heating seat 101b is arranged on the lifting shell 101a. The heating seat 101b is fixedly connected to one side of the lifting shell 101a. The heating seat 101b can be heated in a water bath and temperature controlled. The placement shell 101c and the treatment pool 101d are placed on the lifting shell 101a. d is arranged on the heating seat 101b, the placing shell 101c is fixedly connected to the heating seat 101b, and its position is above the heating seat 101b. The placing shell 101c can be heated by the heating seat 101b. The placing shell 101c is a cylindrical structure, and a plurality of circular holes are arranged therein for the convenience of storing other objects. The processing pool 101d is fixedly connected to one side of the heating seat 101b, and the processing pool 101d can be communicated with the heating seat 101b, so as to facilitate the processing of the heating seat 101b after water bath heating.

[0043] Furthermore, the driving member 102 includes a servo motor 102a, a first threaded rod 102b, a moving block 102c, a connecting block 102d, a lifting column 102e and a lifting seat 102f. The servo motor 102a is arranged on the lifting shell 101a, and the servo motor 102a is fixedly connected in the lifting shell 101a. The first threaded rod 102b is arranged on the servo motor 102a, and the first threaded rod 102b is rotatably connected to the servo motor 102a. The start of the servo motor 102a can make the first threaded rod 102e move. The rod 102b rotates, and the first threaded rod 102b has a certain length and is arranged in the lifting shell 101a. The moving block 102c is arranged on the first threaded rod 102b. The moving block 102c is embedded in the lifting shell 101a. The lifting shell 101a performs a positioning function on the moving block 102c to move up and down. The moving block 102c is connected to the first threaded rod 102b by the moving rod. With the rotation of the first threaded rod 102b, the moving block 102c can be moved up and down. The connecting block 102d is arranged at The connecting block 102d is fixedly connected to the moving block 102c. The connecting block 102d is formed by a rectangular structure with an opening on one side. The opening on one side is for setting other objects on the side. A through hole with a certain diameter is left in the middle of the connecting block 102d to facilitate setting objects thereon. The connecting block 102d can move with the movement of the moving block 102c. The lifting column 102e is set on the connecting block 102d. The lifting column 102e is fixedly connected to the connecting block 10 2d, the lifting column 102e moves with the movement of the connecting block 102d, and the lifting seat 102f is set on the lifting column 102e. The lifting seat 102f is fixedly connected to the lifting column 102e and moves with the movement of the lifting column 102e. The lifting seat 102f is composed of a long rod and a petal-shaped structure connected to the long rod, so that the petal structure corresponds to the circular hole opened in the placement shell 101c, so that the object set on the lifting seat 102f is moved to the placement shell 101c.

[0044] Furthermore, the transition member 103 includes a positioning bead 103a, a transition block 103b, a deflection groove 103c, a storage shell 103d, a test tube 103e and a positioning block 103f. The positioning bead 103a and the transition block 103b are arranged on the lifting column 102e. The positioning bead 103a is fixedly connected to the lifting column 102e. The positioning bead 103a is a round bead structure and is arranged on the bottom side of the lifting column 102e. The transition block 103b is arranged on the upper side of the lifting column 102e and is fixedly connected to the upper side of the lifting shell 101a. The outer side surface of the transition block 103b is a block with a quarter arc structure. The transition block 103b contacts the lifting column 102e. And it does not affect the movement of the lifting column 102e, the deflection groove 103c is arranged on the conversion block 103b, the deflection groove 103c is opened on the conversion block 103b, and presents a certain arc groove with a gradual inclination toward the top of the lifting shell 101a, and the conversion block 103b is arranged corresponding to the side of the connection block 102d with an opening, so that when the lifting column 102e moves to the deflection groove 103c with the positioning bead 103a and then continues to move, it can be deflected 90 degrees during the rise, and the storage shell 103d is arranged on the lifting seat 102f, and the storage shell 103d is fixedly connected to the lifting seat 102f, and presents a petal shape, corresponding to the round hole arranged in the placement shell 101c;

[0045] Among them, the test tube 103e and the positioning block 103f are arranged on the storage shell 103d, and the test tube 103e is movably connected to the storage shell 103d. The reagent to be tested for demulsification degree is placed in the test tube 103e. The number of test tubes 103e is at most four. Each test tube 103e has two protruding ears on both sides of the top for easy operation and installation. The positioning block 103f is fixedly connected to the storage shell 103d, and the positioning block 103f is composed of two arc-shaped rings, and a certain space is left between the two, so that the object on the positioning block 103f can be moved on the storage shell 103d without being affected and can also play a role in assisting movement.

[0046] During operation, the first threaded rod 102b can be rotated by starting the servo motor 102a, driving the moving block 102c and the connecting block 102d to move, so that the lifting column 102e moves with the positioning bead 103a, and when the lifting column 102e moves to the transition block 103b connected to the top of the lifting shell 101a, the positioning bead 103a on the lifting column 102e will be deflected 90 degrees along the deflection groove 103c on the transition block 103b, and the lifting seat 102f on the lifting column 102e will move synchronously, so that the lifting seat 102f can move the storage shell 103d out of the position of the placement shell 101c, thereby facilitating the operation of installing the test tube 103e on the storage shell 103d.

[0047] Example 2

[0048] Reference Figure 1 - Fig.10 , which is the second embodiment of the present invention. This embodiment is different from the first embodiment in that: this device includes a stirring assembly 200, including a mounting member 201, an auxiliary member 202 and a follower 203. The mounting member 201 is arranged on the conversion member 103, the auxiliary member 202 is arranged on the driving member 102, and the follower 203 is arranged on the auxiliary member 202. Through the interaction between the mounting member 201, the auxiliary member 202 and the follower 203, the entire device can be installed with any number of test tubes 103e, and a corresponding number of test tubes 103e can be stirred. The overall operation can reduce the number of personnel, simplify the operation process, and improve the test efficiency and flexibility.

[0049] Specifically, the mounting member 201 includes a mounting groove 201a, a displacement groove 201b, a movable arc block 201c, a lifting block 201d, a compression groove 201e, a first spring 201f and an embedded block 201g. The mounting groove 201a and the displacement groove 201b are arranged on the storage shell 103d. The mounting groove 201a is provided on the storage shell 103d and is located on the bottom side of the storage shell 103d. The mounting groove 201a is adapted to the protruding ear on the test tube 103e, so as to facilitate the initial entry of the test tube 103e into the storage shell 103d. The displacement groove 201b is provided on the storage shell 103d and is located on the upper side of the mounting groove 201a. The depth of the mounting groove 201a is shallower than that of the displacement groove 201b and the length is also shorter. The movable arc block 201c is provided in the displacement groove 201 b, the moving arc block 201c is a semicircular ring structure, which is movably connected on the displacement groove 201b, and the extended part can move between the positioning block 103f and the storage shell 103d, and can move up and down along the inner wall of the lifting seat 102f. The protruding side of the moving arc block 201c is embedded in the displacement groove 201b, and the lifting block 201d is arranged on the moving arc block 201c. The lifting block 201d is fixedly connected to the top of the moving arc block 201c, and the lifting block 201d is a polyhedron, the bottom side is fixedly connected to the moving arc block 201c, the two sides are horizontally arranged, and the top is composed of two inclined surfaces and a plane. The inclined surface close to the center of the storage shell 103d is relatively short, and the force-bearing area is small, so it can be used to push objects, and the objects are pushed to move with the change of the inclined surface;

[0050] The compression groove 201e is arranged on the test tube 103e, the compression groove 201e is opened on the test tube 103e, and is located at a protruding position of the test tube 103e. The first spring 201f is arranged on the compression groove 201e, and the first spring 201f is fixedly connected to the compression groove 201e. The embedded block 201g is arranged on the first spring 201f, and the embedded block 201g is fixedly connected to the first spring 201f. With the connection of the first spring 201f, the embedded block 201g can move in the compression groove 201e. The cross section of the embedded block 201g is a "trapezoidal" structure, and the cross section is composed of two sides. The structure is composed of an arc surface and two horizontal surfaces on both sides which are perpendicular to the arc surface. The embedded block 201g cannot move up and down directly and can only be rotated to move up and down after the retraction of the embedded block 201g. When the test tube 103e moves into the storage tube, it will push the movable arc block 201c to move in the displacement groove 201b. At this time, the embedded block 201g in the test tube 103e will move out of the compression groove 201e due to the action of the first spring 201f and touch the displacement groove 201b to make a sound. At this time, the movable arc block 201c and the embedded block 201g occupy the entire displacement groove 201b so that the test tube 103e will not fall off.

[0051] Furthermore, the auxiliary member 202 includes a fixed plate 202a, a movable groove 202b, a drop groove 202c, a positioning groove 202d, a first energy storage block 202e, a rotating shaft 202f and a stirring rod 202g, the fixed plate 202a is arranged on the lifting seat 102f, the fixed plate 202a is fixedly connected to the lifting seat 102f and is located at the top thereof, the fixed plate 202a is a rectangular structure, the movable groove 202b, the drop groove 202c and the positioning groove 202d are arranged on the fixed plate 202a, the movable groove The fixing plate 202a is provided with a plurality of movable grooves 202c, and the fixing plate 202a is provided with a plurality of movable grooves 202c, and the plurality of movable grooves 202b are provided with a plurality of movable grooves 202c. The plurality of movable grooves 202c are provided with a plurality of movable grooves 202c, and the plurality of movable grooves 202b are provided with a plurality of movable grooves 202c, and the plurality of movable grooves 202b are provided with a plurality of movable grooves 202c, and the plurality of movable grooves 202b are provided with a plurality of movable grooves 202c, and the plurality of movable grooves 202b are provided with a plurality of movable grooves 202c, and the plurality of movable grooves 202d are provided with a plurality of movable grooves 202d, and the plurality of movable grooves 202d are provided with a plurality of movable grooves 202c ... The middle position of the plate 202a allows an object to be placed on the fixed plate 202a. The first energy storage block 202e is arranged on the positioning groove 202d. The first energy storage block 202e is movably connected to the positioning groove 202d. The first energy storage block 202e is cylindrical in shape and a drivable motor is arranged therein. The rotating shaft 202f is arranged on the first energy storage block 202e. The rotating shaft 202f is rotatably connected to the first energy storage block 202e and is connected to the motor on the first energy storage block 202e. The motor The start and stop can be controlled, that is, the rotating shaft 202f can be rotated and stopped. The stirring rod 202g is set on the rotating shaft 202f. The stirring rod 202g is fixedly connected to the rotating shaft 202f. The rotation of the rotating shaft 202f can rotate the stirring rod 202g. The stirring rod 202g is composed of a ring fixed on the rotating shaft 202f and cylindrical rods arranged in a circular array on the ring. There are several stirring rods 202g on one rotating shaft 202f to facilitate stirring the reagent in the test tube 103e.

[0052] Furthermore, the follower 203 includes a moving column 203a, a falling block 203b, a passive block 203c, a limiting block 203d, a follower ring 203e, a ball 203f, a second threaded rod 203g and a second energy storage block 203h. The moving column 203a is arranged on the first energy storage block 202e, and the moving column 203a is movably connected to the first energy storage block 202e. The moving column 203a is arranged in a moving groove 202b on the fixed plate 202a, and the width of the moving column 203a is the same as that of the moving groove 202b. The falling block 203b, the passive block 203c and the limiting block 203d are arranged on the moving column 203a, and the falling block 203b is fixedly connected to the moving column 203a. The falling block 203b is arranged vertically with the moving column 203a, which has the effect of expanding the width of the moving column 203a part so as not to cause the moving column 203a to be separated from the fixed plate Fixed plate 202a, when the falling block 203b moves the moving column 203a into the falling groove 202c with the moving column 203a, the moving column 203a is released from the movement of the fixed plate 202a, and the passive block 203c is fixedly connected to the moving column 203a. The passive block 203c is a block with a certain slope, and the number of passive blocks 203c is only one on the moving column 203a. The passive column can push the passive block 203c to move to one side with the movement of the lifting block 201d on the moving arc block 201c, and at this time, the moving column 203a will move with the falling block 203b into the falling groove 202c. The limiting block 203d is fixedly connected to the moving column 203a and is arranged on the opposite side of the passive block 203c. The width of the limiting block 203d is smaller than that of the moving column 203a, so that the limiting block 203d can move with the movement of the moving column 203a.

[0053] Among them, the follower ring 203e is arranged on the limiting block 203d, and the follower ring 203e is movably connected to the limiting block 203d. A notch corresponding to the limiting block 203d is opened on the follower ring 203e, and the follower ring 203e is a circular ring structure, so that grooves of corresponding diameters and a certain length are opened on the lifting seat 102f and the storage shell 103d. The follower ring 203e can perform an auxiliary role of movement control in the grooves opened in the lifting seat 102f and the storage shell 103d. The ball 203f is arranged on the follower ring 203e, and the ball 203f is fixedly connected to the follower ring 203e and is arranged on the inner side wall of the follower ring 203e. The second threaded rod 203g is arranged on the ball 203f, and the ball 203f can be The second threaded rod 203g moves on the second threaded rod 203g, the second threaded rod 203g is set in the groove opened by the lifting seat 102f and the storage shell 103d, the second energy storage block 203h is set on the second threaded rod 203g, the second energy storage block 203h is fixedly connected to the lifting seat 102f, and is movably connected to the second threaded rod 203g. A motor is set in the second energy storage block 203h, which can control the movement of the second threaded rod 203g at any time, so that the follower ring 203e will be lifted and moved on the second threaded rod 203g under the action of the ball 203f, and the limiting block 203d moved to the follower ring 203e and the moving column 203a connected to the limiting block 203d will be lifted and moved along the moving arc block 201c.

[0054] The remaining structures are the same as those of Example 1.

[0055] Operation process: When the test tube 103e is moved into the storage tube, the movable arc block 201c is pushed to move in the displacement groove 201b. At this time, the embedded block 201g in the test tube 103e moves out of the compression groove 201e due to the action of the first spring 201f and touches the displacement groove 201b to make a sound. At this time, the movable arc block 201c and the embedded block 201g occupy the entire displacement groove 201b so that the test tube 103e will not fall off, and the servo motor 102a can be driven to drive the first threaded rod 102b and the first threaded rod 102b connected to the test tube 103e. The lifting seat 102f and the storage shell 103d are deflected 90 degrees and moved downward, so that the test tube 103e can enter the placement shell 101c, and the test tube 103e is heated by the heating seat 101b to improve the test efficiency. During the installation of the test tube 103e, the lifting block 201d on the moving arc block 201c pushes the passive block 203c to move the falling block 203b and the moving block 102c, and the embedded block 201g on the moving block 102c moves into the follower ring 203e corresponding to the falling groove 202c;

[0056] When the motor on the second energy storage block 203h is started, the moving block 102c and the first energy storage block 202e on the moving block 102c can also move accordingly, so that the rotating shaft 202f and the stirring rod 202g on the first energy storage block 202e can move synchronously, and only the part where the test tube 103e is installed will move accordingly. When the rotating shaft 202f and the stirring rod 202g enter the test tube 103e, the motor on the first energy storage block 202e can be controlled to start so that the rotating shaft 202f rotates and the stirring rod 202g rotates synchronously, so that the reagent in the test tube 103e is stirred, which is convenient for subsequent further detection and observation of the demulsification degree.

[0057] Example 3

[0058] Reference Fig.11 - Fig.12 , as a third embodiment of the present invention, provides a method for determining demulsification degree, comprising the following steps:

[0059] S1, through preparation and initial setup and water bath heating;

[0060] S2, then automatically measure and record and output the results;

[0061] S3. Finally, automatic cleaning and drying are performed to complete the whole process of demulsification degree detection.

[0062] Among them, water bath heating and constant temperature control are composed of temperature sensors, including thermostats, over-temperature protection switches, etc.

[0063] Among them: the temperature sensor adopts 4-wire PT100 to ensure accuracy; the over-temperature protection switch adopts 85℃ temperature protection switch; the thermostat adopts intelligent thermostat. The main parameters are shown in Table 1 below:

[0064] Table 1 Main parameters of intelligent thermostat

[0065]

[0066]

[0067] The water bath thermostatic automatic temperature control module has the functions of water bath temperature control, water temperature value setting, automatic water circulation, real-time temperature display, etc. It adopts PID control technology, and improves the analog-to-digital conversion (A / D) accuracy of the PID circuit to 24 bits, the digital-to-analog conversion (D / A) accuracy to 16 bits, increases the number of floating-point arithmetic bits and increases the minimum control output percentage (OP) to 0.01%, and controls the accuracy of constant temperature control within 0.1%.

[0068] Among them, multiple channels can selectively lift and stir automatically;

[0069] The device is designed to realize functions such as automatic lifting and automatic constant speed stirring after the test tube 103e is installed with selectable channels. Before the test begins, 1-4 test tubes 103e with samples are placed in the test tube 103e installation position. After the test is started, the installed test tube 103e will be moved to the corresponding position first. After the water bath constant temperature time of the sample to be tested reaches 20 minutes, the stirring blade at the corresponding test tube 103e position is controlled to extend into the test tube 103e, and the stirring is started and continued for 5 minutes. After the stirring is completed, the stirring rod 202g is controlled to rise again. Due to the structure of the stirring rod 202g, it is convenient for the emulsion on it to flow back into the test tube 103e.

[0070] Among them, machine vision automatic detection;

[0071] The machine vision automatic detection module adopts the method of industrial camera + visual detection, which is composed of PC host computer, machine vision software, single chip control unit, high-definition camera, etc. It has the functions of automatically judging the end point of oil sample demulsification degree determination and automatically detecting the height of emulsion layer, such as Fig.11 As shown;

[0072] The machine vision detection module consists of a high-definition camera and a host computer equipped with machine vision algorithm software. When the oil sample is stirred, the stirring rod is raised, and the timing starts at the same time. The machine vision detection system also starts to intervene. The camera takes pictures of the real-time status of 1-4 oil samples to be tested at a speed of dozens of frames per second. The pictures are transmitted to the host computer. The host computer software determines the upper and lower positions of the emulsified part through digital detection and boundary detection, and determines the width of the emulsified layer and the position of the lower liquid level of the oil through the distance measurement algorithm. When the width of the emulsified layer is less than or equal to 3mL, the measurement ends, the timing result is obtained, and the pictures taken are stored in the host computer for inspection. The machine vision detection method is used to do these jobs that previously required manual work, completely liberating manpower, thereby realizing truly fully automatic detection.

[0073] Among them, automatic cleaning and drying, such as Fig.12 As shown;

[0074] The automatic cleaning and drying module of the test tube 103e is composed of a cleaning paddle assembly, a switching valve assembly, a pipeline assembly, a dry air generating assembly, a control unit, etc., and has the functions of automatically dropping the cleaning paddle, automatically discharging waste oil / waste cleaning liquid / waste distilled water / waste petroleum ether, automatically adding cleaning liquid / distilled water / petroleum ether, automatically washing the test tube 103e, automatically drying the test tube 103e, and automatically retracting the cleaning paddle;

[0075] After the determination is completed, the equipment automatically drops the cleaning paddle, and the switching valve switches to the waste liquid discharge pipeline to discharge the residual waste oil in the test tube 103e; then, the switching valve switches to the cleaning liquid addition pipeline and introduces 80mL of cleaning liquid, and then starts the cleaning paddle to stir and clean the test tube 103e. After the cleaning is completed, the switching valve switches to the waste liquid discharge pipeline to discharge the waste cleaning liquid; the switching valve switches to the distilled water addition pipeline and introduces 80mL of distilled water, and then starts the cleaning paddle to stir and clean the test tube 103e. After the cleaning is completed, the switching valve switches to the waste liquid discharge pipeline to discharge the waste distilled water; the switching valve switches to the petroleum ether addition pipeline and introduces 80mL of petroleum ether, and then starts the cleaning paddle to stir and clean the test tube 103e. After the cleaning is completed, the switching valve switches to the waste liquid discharge pipeline to discharge the waste petroleum ether; the switching valve switches to the distilled water addition pipeline and adds 80mL of distilled water, and then starts the cleaning paddle to stir and clean the test tube 103e. After the cleaning is completed, the switching valve switches to the waste liquid discharge pipeline to discharge the waste distilled water; repeat this operation to ensure that the oil sample is thoroughly cleaned.

[0076] After the cleaning is completed, the switching valve is switched to the dry air channel, and the dry air generating component is started to blow out 54°C hot air to dry the test tube 103e. After the drying is completed, the cleaning paddle is put away, and the entire detection process of the equipment is completed.

[0077] Among them, automatic timing and printing;

[0078] The automatic timing and printing module consists of a PC host computer, a single-chip control unit, a printer, etc. The timing starts from the injection of 40mL of oil sample and 40mL of distilled water, the constant temperature water bath is set for 20 minutes, and the sample to be tested is stirred for 5 minutes. After stirring, the emulsion separation time is measured until the emulsion layer is less than or equal to 3mL to obtain the demulsification time, and the test results are automatically printed through the printer;

[0079] The demulsification degree of turbine oil is automatically tested by means of a demulsification degree tester, and the entire testing process is automatically controlled and tested, so as to greatly shorten the time for sample testing. At the same time, the influence of manual judgment and manual timing on the test results is eliminated, making the test data more stable and accurate. The test process is made more automatic and intelligent, reducing manpower, lowering human resource requirements, liberating labor, and improving the stability, accuracy and work efficiency of test results.

[0080] It should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention rather than to limit it. Although the present invention has been described in detail with reference to the preferred embodiments, those skilled in the art should understand that the technical solutions of the present invention may be modified or replaced by equivalents without departing from the spirit and scope of the technical solutions of the present invention, which should all be included in the scope of the claims of the present invention.

Claims

1. A demulsification tester, Features: include, A lifting assembly (100) comprises a receiving member (101), a driving member (102) and a transition member (103), wherein the driving member (102) is arranged on the receiving member (101), and the transition member (103) is arranged on the driving member (102); and, The stirring assembly (200) comprises a mounting member (201), an auxiliary member (202) and a follower member (203); the mounting member (201) is arranged on the conversion member (103); the auxiliary member (202) is arranged on the driving member (102); and the follower member (203) is arranged on the auxiliary member (202).

2. The demulsification tester according to claim 1, Features: The accommodating member (101) comprises a lifting shell (101a), a heating seat (101b), a placement shell (101c) and a processing pool (101d); the heating seat (101b) is arranged on the lifting shell (101a), and the placement shell (101c) and the processing pool (101d) are arranged on the heating seat (101b).

3. The demulsification degree measuring instrument according to claim 2, Features: The driving member (102) includes a servo motor (102a), a first threaded rod (102b), a moving block (102c), a connecting block (102d), a lifting column (102e) and a lifting seat (102f), wherein the servo motor (102a) is arranged on the lifting shell (101a), the first threaded rod (102b) is arranged on the servo motor (102a), the moving block (102c) is arranged on the first threaded rod (102b), the connecting block (102d) is arranged on the moving block (102c), the lifting column (102e) is arranged on the connecting block (102d), and the lifting seat (102f) is arranged on the lifting column (102e).

4. The demulsification degree measuring instrument according to claim 3, Features: The transition member (103) includes a positioning bead (103a), a transition block (103b), a deflection groove (103c), a storage shell (103d), a test tube (103e) and a positioning block (103f); the positioning bead (103a) and the transition block (103b) are arranged on the lifting column (102e); the deflection groove (103c) is arranged on the transition block (103b); the storage shell (103d) is arranged on the lifting seat (102f); and the test tube (103e) and the positioning block (103f) are arranged on the storage shell (103d).

5. The demulsification degree measuring instrument according to claim 4, Features: The mounting member (201) comprises a mounting groove (201a), a displacement groove (201b), a movable arc block (201c), a lifting block (201d), a compression groove (201e), a first spring (201f) and an embedded block (201g); the mounting groove (201a) and the displacement groove (201b) are arranged on the storage shell (103d); the movable arc block (201c) is arranged on the displacement groove (201b); the lifting block (201d) is arranged on the movable arc block (201c); the compression groove (201e) is arranged on the test tube (103e); the first spring (201f) is arranged on the compression groove (201e); and the embedded block (201g) is arranged on the first spring (201f).

6. The demulsification degree measuring instrument according to claim 4 or 5, Features: The auxiliary component (202) includes a fixed plate (202a), a movable groove (202b), a drop groove (202c), a positioning groove (202d), a first energy storage block (202e), a rotating shaft (202f) and a stirring rod (202g); the fixed plate (202a) is arranged on the lifting seat (102f); the movable groove (202b), the drop groove (202c) and the positioning groove (202d) are arranged on the fixed plate (202a); the first energy storage block (202e) is arranged on the positioning groove (202d); the rotating shaft (202f) is arranged on the first energy storage block (202e); and the stirring rod (202g) is arranged on the rotating shaft (202f).

7. The demulsification degree measuring instrument according to claim 6, Features: The follower (203) comprises a moving column (203a), a falling block (203b), a passive block (203c), a limiting block (203d), a follower ring (203e), a ball (203f), a second threaded rod (203g) and a second energy storage block (203h); the moving column (203a) is arranged on the first energy storage block (202e); the falling block (203b), the passive block (203c) and the limiting block (203d) are arranged on the moving column (203a); the follower ring (203e) is arranged on the limiting block (203d); the ball (203f) is arranged on the follower ring (203e); the second threaded rod (203g) is arranged on the ball (203f); and the second energy storage block (203h) is arranged on the second threaded rod (203g).

8. A method for measuring demulsification degree, comprising the demulsification degree measuring instrument according to any one of claims 1 to 7, The following steps are involved: Through preparation and initial setup and water bath heating; Then through automatic measurement and result recording and output; Finally, automatic cleaning and drying are carried out to complete the whole process of demulsification degree detection.

9. The method for determining the demulsification degree according to claim 8, Features: The lifting component (100) and the stirring component (200) are used to synchronously realize the automatic lifting and stirring functions, thereby simplifying the operation process.

10. The method for determining the demulsification degree according to claim 9, Features: Water bath heating and constant temperature control use high-precision temperature sensors, intelligent temperature controllers, and high-resolution analog-to-digital conversion and digital-to-analog conversion technologies to ensure accurate control of the water bath temperature.

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