Rectification device for cineole
By using staggered distribution of trays, exhaust, stirring and anti-blocking structures in the distillation tower, the safety hazards and low efficiency of the plate distillation tower due to hole blockage are solved, and a more efficient separation and heating process is achieved. .
Patent Information
- Application Number
- CN202411491169.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-10-24
- Publication Date
- 2024-12-13
- Estimated Expiration
- 2044-10-24
AI Technical Summary
During use, plate distillation towers are prone to blockage of the tube holes due to material condensation and deposition, which may cause explosion or leakage. The existing cleaning methods are inefficient and incomplete.
A distillation device of eucalyptus is designed, using multiple staggered tower trays, exhaust structures, stirring structures and anti-blocking structures. The heat transfer and anti-blocking structures are accelerated through the exhaust structure, and the stirring structures are accelerated. Impurities deposit to ensure the unobstructed holes of the tower plate.
It improves separation efficiency, speeds up the liquid heating speed, avoids blockage of tray holes, reduces the need for unblocking of tray holes, and ensures the safety and efficiency of the distillation process.
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Figure CN119113557A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of distillation and purification, in particular to a distillation device for eucalyptol. Background Art
[0002] Eucalyptus oil is a colorless to light yellow oily liquid with a camphor and refreshing herbal smell. The method for preparing eucalyptus oil is generally steam distillation. Eucalyptus oil is extracted from branches and leaves by steam distillation, and then the eucalyptus oil is further purified by vacuum distillation according to the different boiling points and inclusion vapor pressures of the components in eucalyptus oil.
[0003] During the purification of eucalyptus oil, a plate distillation tower is often used for distillation. The principle of the plate distillation tower is based on the difference in volatility of each component in the mixture, and the separation and purification of the substance are achieved through the close contact of the gas-liquid two phases on the tower plate. The plate distillation tower will condense due to materials during use. Factors such as deposition cause the holes of the tower plate to be blocked. If the holes of the tower plate cannot be cleaned in time, the distillation tower may explode or leak. In the prior art, multiple top plates are installed on the upper side of the tower plate, and the top plates will move up and down during the rotation of the upper side of the tower plate, so as to achieve the dredging of the holes of the tower plate, and scrapers are installed on both sides of the upper and lower sides of the tower plate. However, since there are multiple tower plates in the plate distillation tower, the impurities cleaned from the upper tower plate will fall on the lower tower plate. During the rotation of the scraper on the upper side of the tower plate, the impurities that cannot fall through the holes of the lower tower plate will always accumulate on the outside of the scraper on the upper side of the tower plate, which will cause impurities to remain on the tower plate. Summary of the invention
[0004] The object of the present invention is to provide a rectification device for eucalyptol to solve the problems raised in the above-mentioned background technology.
[0005] To achieve the above object, the present invention provides the following technical solutions: A distillation device for eucalyptol comprises a distillation tower, wherein a plurality of tower plates distributed at equal distances are fixedly installed inside the distillation tower, and the plurality of tower plates are staggeredly distributed, a plurality of circular through holes are opened on the tower plate, a weir plate is fixedly installed on the outer side of the tower plate, and the connection mode between the weir plate and the distillation tower is a fixed connection, and also comprises an exhaust structure for exhausting steam inside the distillation tower, and the exhaust structure is installed at the top of the distillation tower; a stirring structure for stirring liquid inside the distillation tower, and the stirring structure is installed inside the distillation tower and located at the lower end of the distillation tower; an anti-blocking structure for preventing the circular through holes of the tower plate from being blocked, and a plurality of the anti-blocking structures are correspondingly installed on the lower sides of the plurality of tower plates.
[0006] Preferably, the distillation tower includes an exhaust pipe movably embedded in the upper end of the distillation tower, the outer side of the exhaust pipe is movably sleeved with a sleeve seat, and the connection between the sleeve seat and the distillation tower is a fixed connection, the outer side of the sleeve seat is provided with an external thread, the outer side of the exhaust pipe is fixedly sleeved with a limiting ring, the limiting ring can prevent the exhaust pipe from falling into the distillation tower, and the outer ring diameter of the limiting ring is equal to the outer ring diameter of the sleeve seat.
[0007] Preferably, the lower end surface of the limiting ring is movably abutted against the upper end surface of the sleeve seat, the outer side of the exhaust pipe is movably sleeved with a threaded cover, and the threaded cover is located on the upper side of the limiting ring, and the connection between the threaded cover and the sleeve seat is a threaded connection. When the threaded cover is screwed onto the sleeve seat, the exhaust pipe can be fixed to the upper end of the distillation tower, and a plurality of exhaust holes equidistantly distributed around the circumference are provided on the outer side of the exhaust pipe, and the exhaust holes are located on the upper side of the threaded cover.
[0008] Preferably, the upper end of the exhaust pipe is fixedly connected to a top plate, a hydraulic rod is fixedly installed at the center of the top plate, the lower end of the hydraulic rod is fixedly connected to a connecting seat, a piston is fixedly sleeved on the outer side of the connecting seat, and the piston can move up and down inside the exhaust pipe, and the hydraulic rod can drive the piston to move up and down.
[0009] Preferably, the stirring structure includes a cylindrical rod installed at the lower center of the distillation tower, a plurality of stirring rods equidistantly distributed in a circle are fixedly installed on the outer side of the cylindrical rod, the stirring rod is in the shape of an arc, and both ends of the stirring rod are fixedly connected to the cylindrical rod, a supporting seat is installed at the lower end of the cylindrical rod, and the cylindrical rod is rotatably connected to the supporting seat through a bearing, the bearing can reduce the friction between the cylindrical rod and the supporting seat, a plurality of support rods equidistantly distributed in a circle are fixedly installed on the outer side of the supporting seat, and the end of the support rod 1 away from the supporting seat is fixedly connected to the distillation tower.
[0010] Preferably, a cylindrical groove is provided at the center of the upper end of the cylindrical rod, and a threaded groove is provided on the side wall of the cylindrical groove. A long connecting rod is movably embedded in the upper end of the cylindrical rod, and the long connecting rod is plugged and unpluggedly connected to the cylindrical rod through the cylindrical groove. The long connecting rod passes through a plurality of the tower plates and can move up and down inside the distillation tower. A pin ball is fixedly embedded on the outer side of the long connecting rod, and the pin ball is located inside the cylindrical rod. The pin ball is in sliding contact with the cylindrical rod through the threaded groove, and the pin ball can drive the cylindrical rod to rotate through the threaded groove. The upper end of the long connecting rod is provided with an external thread 2.
[0011] Preferably, the long connecting rod is threadedly connected to the connecting seat through the second external thread, and a limiting assembly is installed on the outer side of the long connecting rod near the exhaust structure, and the limiting assembly includes a plurality of convex ribs fixedly embedded on the outer side of the long connecting rod, and the convex ribs are equidistantly distributed around the circumference, and a ring is movably sleeved on the outer side of the convex ribs, and the ring is sleeved on the outer side of the plurality of convex ribs to prevent the long connecting rod from rotating, and a plurality of support rods 2 are fixedly embedded on the outer side of the ring and are equidistantly distributed around the circumference, and the end of the support rod 2 away from the ring is fixedly connected to the distillation tower.
[0012] Preferably, the anti-blocking structure includes a grid plate installed on the lower side of the tower plate, and the grid plate is fixedly sleeved on the outer side of the long connecting rod, and a plurality of vertical poles are fixedly embedded in the upper end of the grid plate, and the number of the vertical poles is equal to the number of circular through holes opened on the tower plate, and the plurality of vertical poles are located on the lower side of the plurality of circular through holes, and a wire brush is fixedly connected to the upper end of the vertical pole, and the wire brush can pass through the tower plate through the circular through hole, and the wire brush is in an umbrella shape, and the umbrella-shaped wire brush can rub the side wall of the circular through hole when it moves downward inside the circular through hole.
[0013] Preferably, a plurality of connection components distributed at equal distances are installed between the grid disk and the inner wall of the distillation tower, the connection component includes a metal spring fixedly embedded in the outer side of the grid disk, a fixing plate is fixedly embedded on the inner wall of the distillation tower corresponding to the connection component, a plurality of blocks distributed at equal distances are fixedly installed on one side of the fixing plate close to the metal spring, the plurality of blocks can cause the metal spring to vibrate during its movement, and the cross-sectional shape of the block is triangular, and the connection between the metal spring and the plurality of blocks is sliding contact.
[0014] Preferably, a connecting pipe is fixedly installed on the upper end of the distillation tower, a cover pipe is installed on the upper end of the connecting pipe, and the cover pipe and the connecting pipe are located on the outside of the exhaust structure, the outsides of the cover pipe and the connecting pipe are fixedly sleeved with flanges, and the cover pipe and the connecting pipe are fixedly connected by the flange and bolts, a conduit 1 connected thereto is fixedly installed on the upper end of the cover pipe, a condenser is installed on the end of the conduit 1 away from the cover pipe, and the cover pipe is rotatably connected to the condenser through a rotary joint, a conduit 2 connected thereto is fixedly installed on the outside of the connecting pipe, and the end of the conduit 2 away from the connecting pipe is fixedly connected to the distillation tower, the conduit 2 can discharge the condensed water between the connecting pipe and the sleeve seat into the distillation tower, and a reflux pipe is fixedly installed on the outside of the distillation tower near its upper end.
[0015] Compared with the prior art, the present invention has the following beneficial effects: 1. The present invention installs an exhaust structure, and the piston in the exhaust structure moves to the lower side of the exhaust hole under the drive of the hydraulic rod, which can block the discharge of steam inside the distillation tower, increase the pressure inside the distillation tower, and make the distillate evaporate under high pressure, which can further improve the separation efficiency.
[0016] 2. The present invention installs and stirs the structure. When the piston in the exhaust structure moves up and down to relieve the pressure of the distillation tower, the long connecting rod in the stirring structure will also move back and forth up and down. In the process of moving up and down, the long connecting rod drives the cylindrical rod and multiple stirring rods to rotate through the threaded groove and the pin ball, which is beneficial to stirring the liquid inside the distillation tower, can speed up the heat transfer efficiency in the liquid, is beneficial to the uniform distribution of heat in the liquid, and accelerates the heating speed of the liquid.
[0017] 3. The present invention installs an anti-blocking structure, and the umbrella-shaped wire brush in the anti-blocking structure can reciprocate up and down with the long connecting rod. The umbrella-shaped wire brush will penetrate the circular through hole on the tower plate during the up and down movement and rub against the side wall of the circular through hole, which can effectively prevent impurities from being deposited in the circular through hole of the tower plate, thereby effectively preventing the circular through hole of the tower plate from being blocked, and there is no need to dredge the circular through hole of the tower plate at a later stage.
[0018] 4. The present invention installs a connecting component, and the metal spring of the connecting component can move up and down with the grid plate. The metal spring can contact multiple blocks during the up and down movement, so that the metal spring and the wire brush produce continuous vibration, which is beneficial to the vibration and diffusion of the liquid in the wire brush, effectively increases the contact area between the liquid phase and the gas phase, facilitates mass transfer, accelerates the mass transfer rate of the components, and makes the distillation in the tower more uniform. BRIEF DESCRIPTION OF THE DRAWINGS
[0019] Figure 1 It is a schematic diagram of the overall structure of the present invention; Figure 2 It is a side sectional schematic diagram of the present invention; Figure 3 This is a schematic diagram of the connection between the stirring structure and the anti-blocking structure of the present invention; Figure 4 Schematic diagram of the connection between the anti-blocking structure and the connecting assembly of the present invention Figure 5 For the present invention Figure 4 A schematic diagram of the enlarged split at center A; Figure 6 It is a schematic diagram of a side section split of the stirring structure of the present invention; Figure 7 This is a schematic diagram of the separation of the cover pipe and the connecting pipe of the present invention; Figure 8 It is a side cross-sectional schematic diagram of the exhaust structure of the distillation tower of the present invention.
[0020] In the figure: 1, distillation tower; 2, tower plate; 3, weir plate; 4, exhaust structure; 401, exhaust pipe; 402, sleeve seat; 403, limit ring; 404, threaded cover; 405, exhaust hole; 406, top plate; 407, hydraulic rod; 408, piston; 409, connecting seat; 5, stirring structure; 501, cylindrical rod; 502, stirring rod; 503, supporting seat; 504, support rod 1; 505, cylindrical groove; 506, threaded groove; 507, Long connecting rod; 508, pin ball; 509, external thread 2; 6, anti-blocking structure; 601, grid plate; 602, vertical pole; 603, wire brush; 7, connecting assembly; 701, metal spring; 702, fixing plate; 703, block; 8, limiting assembly; 801, convex rib; 802, collar; 803, support rod 2; 9, cover pipe; 10, conduit 1; 11, condenser; 12, flange; 13, conduit 2; 14, return pipe; 15, connecting pipe. DETAILED DESCRIPTION
[0021] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0022] Example 1: Please refer to Figure 1-Figure 3 , Figure 7 , Figure 8 The distillation device of eucalyptus tincture shown in the figure includes a distillation tower 1, a plurality of tower plates 2 distributed at equal distances are fixedly installed inside the distillation tower 1, and the plurality of tower plates 2 are staggered, a plurality of circular through holes are opened on the tower plate 2, a weir plate 3 is fixedly installed on the outer side of the tower plate 2, and the connection mode between the weir plate 3 and the distillation tower 1 is a fixed connection, and also includes an exhaust structure 4 for discharging steam inside the distillation tower 1, and the exhaust structure 4 is installed at the top of the distillation tower 1; a stirring structure 5 for stirring the liquid inside the distillation tower 1, the stirring structure 5 is installed inside the distillation tower 1, and is located at the lower end of the distillation tower 1; an anti-blocking structure 6 for preventing the circular through holes of the tower plate 2 from being blocked, and a plurality of anti-blocking structures 6 are correspondingly installed on the lower side of the plurality of tower plates 2.
[0023] The distillation tower 1 includes an exhaust pipe 401 movably embedded in the upper end of the distillation tower 1, and the outer side of the exhaust pipe 401 is movably sleeved with a sleeve seat 402, and the connection between the sleeve seat 402 and the distillation tower 1 is a fixed connection. The outer side of the sleeve seat 402 is provided with an external thread 1, and the outer side of the exhaust pipe 401 is fixedly sleeved with a limiting ring 403. The limiting ring 403 can prevent the exhaust pipe 401 from falling into the distillation tower 1, and the outer circle diameter of the limiting ring 403 is equal to the outer circle diameter of the sleeve seat 402.
[0024] The lower end surface of the limiting ring 403 is movably abutted against the upper end surface of the sleeve seat 402, and the outer side of the exhaust pipe 401 is movably sleeved with a threaded cover 404, and the threaded cover 404 is located on the upper side of the limiting ring 403. The connection between the threaded cover 404 and the sleeve seat 402 is a threaded connection. When the threaded cover 404 is screwed onto the sleeve seat 402, the exhaust pipe 401 can be fixed to the upper end of the distillation tower 1. A plurality of exhaust holes 405 equidistantly distributed in a circle are provided on the outer side of the exhaust pipe 401, and the exhaust holes 405 are located on the upper side of the threaded cover 404.
[0025] The upper end of the exhaust pipe 401 is fixedly connected to a top plate 406, a hydraulic rod 407 is fixedly installed in the center of the top plate 406, the lower end of the hydraulic rod 407 is fixedly connected to a connecting seat 409, a piston 408 is fixedly sleeved on the outer side of the connecting seat 409, and the piston 408 can move up and down inside the exhaust pipe 401, and the hydraulic rod 407 can drive the piston 408 to move up and down.
[0026] A connecting pipe 15 is fixedly installed on the upper end of the distillation tower 1, and a cover pipe 9 is installed on the upper end of the connecting pipe 15, and the cover pipe 9 and the connecting pipe 15 are located on the outside of the exhaust structure 4, and the outsides of the cover pipe 9 and the connecting pipe 15 are fixedly sleeved with flanges 12, and the cover pipe 9 and the connecting pipe 15 are fixedly connected by the flange 12 and bolts, and a conduit 10 interconnected with the cover pipe 9 is fixedly installed on the upper end, and a condenser 11 is installed at the end of the conduit 10 away from the cover pipe 9, and the cover pipe 9 is rotatably connected to the condenser 11 through a rotary joint, and a conduit 2 13 interconnected with the connecting pipe 15 is fixedly installed on the outside of the connecting pipe 15, and the end of the conduit 2 13 away from the connecting pipe 15 is fixedly connected to the distillation tower 1, and the conduit 2 13 can discharge the condensed water between the connecting pipe 15 and the sleeve seat 402 into the distillation tower 1, and a reflux pipe 14 is fixedly installed on the outside of the distillation tower 1 near its upper end.
[0027] Working principle: the eucalyptus oil stock solution is located inside the distillation tower 1, and the distillation tower 1 heats the stock solution through high-temperature steam. During the heating process, the temperature inside the distillation tower 1 gradually increases. At this time, the piston 408 blocks the exhaust pipe 401 of the distillation tower 1, and the pressure inside the distillation tower 1 is increased, so that the fraction evaporates under high pressure, which can further improve the separation efficiency. When the temperature inside the distillation tower 1 reaches a certain value, the hydraulic rod 407 will drive the piston 408 to move up until the piston 408 moves up to the upper side of the exhaust hole 405. At this time, the gas inside the distillation tower 1 is discharged through the exhaust hole 405, and the distillation tower 1 is depressurized. After the distillation tower 1 is depressurized, the hydraulic rod 407 will drive the piston 408 to move down again, which can achieve indirect blocking of the exhaust pipe 401; The steam in the distillation tower 1 is discharged into the conduit 10 through the exhaust hole 405, and after being condensed by the condenser 11, part of the condensate flows back into the distillation tower 1 through the reflux pipe 14. The refluxed condensate flows inside the distillation tower 1 through multiple trays 2. The steam inside the distillation tower 1 passes through the tray 2 through multiple circular through holes during the rising process. During this period, the steam will contact with the condensate flowing on the tray 2. After multiple partial vaporizations and multiple partial condensations, the purpose of completely separating the light and heavy components is achieved. When the hydraulic rod 407 and the piston 408 need to be inspected or replaced, the personnel first remove the cover pipe 9, then rotate the threaded cover 404, rotate the exhaust pipe 401 to make the piston 408 separate from the long connecting rod 507, and then the hydraulic rod 407 and the piston 408 can be disassembled. Example 2: Please refer to Figure 4 , Figure 5 The present embodiment further explains Example 1, the anti-blocking structure 6 includes a grid plate 601 installed on the lower side of the tower plate 2, and the grid plate 601 is fixedly sleeved on the outer side of the long connecting rod 507, and a plurality of vertical rods 602 are fixedly embedded on the upper end of the grid plate 601, and the number of the vertical rods 602 is equal to the number of circular through holes opened on the tower plate 2, and the plurality of vertical rods 602 are located on the lower side of the plurality of circular through holes, and a wire brush 603 is fixedly connected to the upper end of the vertical rod 602, and the wire brush 603 can pass through the tower plate 2 through the circular through hole, and the wire brush 603 is in an umbrella shape, and the umbrella-shaped wire brush 603 can rub the side wall of the circular through hole when it moves downward inside the circular through hole.
[0028] In this embodiment: in the process of the long connecting rod 507 moving up and down with the piston 408, the grid plate 601 will move with the long connecting rod 507. In the process of the grid plate 601 driving multiple wire brushes 603 to move up and down, the wire brush 603 passes through the circular through hole on the tower plate 2, and then the wire brush 603 moves down inside the circular through hole. Since the wire brush 603 is umbrella-shaped, after the umbrella-shaped wire brush 603 moves down inside the circular through hole, the wire brush 603 will be stretched open by the tower plate 2, so that the wire brush 603 contacts and rubs against the side wall of the circular through hole during the downward movement, which can effectively prevent impurities from being deposited in the circular through hole on the tower plate 2, and prevent the circular through hole of the tower plate 2 from being blocked, and there is no need to dredge the circular through hole of the tower plate 2 in the later stage. Example 3: Please refer to Figure 6, this embodiment further explains Example 1, the stirring structure 5 includes a cylindrical rod 501 installed at the center of the lower part of the distillation tower 1, and a plurality of stirring rods 502 equidistantly distributed in a circle are fixedly installed on the outer side of the cylindrical rod 501, the stirring rods 502 are in the shape of an arc, and both ends of the stirring rods 502 are fixedly connected to the cylindrical rod 501, a supporting seat 503 is installed at the lower end of the cylindrical rod 501, and the cylindrical rod 501 is rotatably connected to the supporting seat 503 through a bearing, and the bearing can reduce the friction between the cylindrical rod 501 and the supporting seat 503, and a plurality of support rods 504 equidistantly distributed in a circle are fixedly installed on the outer side of the supporting seat 503, and the end of the support rod 504 away from the supporting seat 503 is fixedly connected to the distillation tower 1.
[0029] A cylindrical groove 505 is provided at the center of the upper end of the cylindrical rod 501, and a threaded groove 506 is provided on the side wall of the cylindrical groove 505. A long connecting rod 507 is movably embedded in the upper end of the cylindrical rod 501, and the long connecting rod 507 is plugged and connected to the cylindrical rod 501 through the cylindrical groove 505. The long connecting rod 507 passes through multiple tower plates 2 and can move up and down inside the distillation tower 1. A pin ball 508 is fixedly embedded on the outer side of the long connecting rod 507, and the pin ball 508 is located inside the cylindrical rod 501. The pin ball 508 is in sliding contact with the cylindrical rod 501 through the threaded groove 506, and the pin ball 508 can drive the cylindrical rod 501 to rotate through the threaded groove 506. An external thread 509 is provided on the upper end of the long connecting rod 507.
[0030] The long connecting rod 507 is threadedly connected to the connecting seat 409 through an external thread 509. A limiting assembly 8 is installed on the outer side of the long connecting rod 507 near the exhaust structure 4. The limiting assembly 8 includes a plurality of convex ribs 801 fixedly embedded on the outer side of the long connecting rod 507, and the convex ribs 801 are equidistantly distributed around the circumference. A ring 802 is movably sleeved on the outer side of the convex ribs 801. The ring 802 is sleeved on the outer side of the plurality of convex ribs 801 to prevent the long connecting rod 507 from rotating. A plurality of support rods 803 equidistantly distributed around the circumference are fixedly embedded on the outer side of the ring 802, and the end of the support rod 803 away from the ring 802 is fixedly connected to the distillation tower 1.
[0031] In this embodiment: the pin ball 508 is located inside the threaded groove 506. When the long connecting rod 507 moves up and down, the long connecting rod 507 and the pin ball 508 cannot rotate due to the restriction of the long connecting rod 507 by the limit assembly 8. Therefore, when the pin ball 508 moves up and down, the pin ball 508 will drive the cylindrical rod 501 and the stirring rod 502 to rotate through the threaded groove 506. Multiple stirring rods 502 rotate inside the distillation tower 1, which is beneficial to stirring the liquid inside the distillation tower 1, can speed up the heat transfer efficiency in the liquid, is beneficial to uniform distribution of heat in the liquid, and accelerates the heating speed of the liquid. Example 4: Please refer to Figure 5This embodiment further explains Example 3: a plurality of connection components 7 distributed at equal distances are installed between the grid disk 601 and the inner wall of the distillation tower 1; the connection component 7 includes a metal spring 701 fixedly embedded on the outer side of the grid disk 601; a fixing plate 702 is fixedly embedded on the inner wall of the distillation tower 1 at the corresponding connection component 7; a plurality of stoppers 703 distributed at equal distances are fixedly installed on one side of the fixing plate 702 close to the metal spring 701; the plurality of stoppers 703 can vibrate the metal spring 701 during its movement, and the cross-sectional shape of the stopper 703 is triangular; the connection between the metal spring 701 and the plurality of stoppers 703 is sliding contact.
[0032] In this embodiment: during the up and down movement of multiple wire brushes 603, steam will flow in the gaps between the wire brushes 603, thereby passing through the circular through holes on the tower plate 2 through the wire brushes 603 to contact the condensate. When the wire brush 603 moves downward from the inside of the circular through holes, some condensate will also be attached to the wire brush 603. Since the multiple blocks 703 can vibrate the metal shrapnel 701 and the multiple wire brushes 603 during the movement of the metal shrapnel 701, the condensate attached to the wire brush 603 can be vibrated and diffused, which effectively increases the contact area between the liquid phase and the gas phase, facilitates mass transfer, accelerates the mass transfer rate of the components, and makes the fractionation in the tower more uniform.
[0033] It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variants thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device.
[0034] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.
Claims
1. A distillation device for eucalyptol, comprising a distillation tower (1), wherein a plurality of trays (2) are fixedly installed inside the distillation tower (1) and are distributed at equal distances, and the plurality of trays (2) are distributed in a staggered manner, a plurality of circular through holes are opened on the trays (2), a weir plate (3) is fixedly installed on the outer side of the trays (2), and the connection between the weir plate (3) and the distillation tower (1) is a fixed connection, characterized in that: Also includes: An exhaust structure (4) for exhausting steam inside the distillation tower (1), the exhaust structure (4) being installed at the top of the distillation tower (1); A stirring structure (5) for stirring the liquid inside the distillation tower (1), wherein the stirring structure (5) is installed inside the distillation tower (1) and is located at the lower end of the distillation tower (1); The anti-blocking structure (6) is used to prevent the circular through hole of the tower plate (2) from being blocked, and a plurality of the anti-blocking structures (6) are correspondingly installed on the lower sides of a plurality of the tower plates (2).
2. A rectification device for eucalyptol according to claim 1, characterized in that: The distillation tower (1) comprises an exhaust pipe (401) movably embedded in the upper end of the distillation tower (1); the exhaust pipe (401) is movably sleeved with a sleeve seat (402) on the outer side, and the sleeve seat (402) and the distillation tower (1) are connected in a fixed manner; the outer side of the sleeve seat (402) is provided with an external thread; the outer side of the exhaust pipe (401) is fixedly sleeved with a limiting ring (403), and the outer ring diameter of the limiting ring (403) is equal to the outer ring diameter of the sleeve seat (402).
3. A rectification device for eucalyptol according to claim 2, characterized in that: The lower end surface of the limiting ring (403) is movably abutted against the upper end surface of the sleeve seat (402); the outer side of the exhaust pipe (401) is movably sleeved with a threaded cover (404), and the threaded cover (404) is located on the upper side of the limiting ring (403); the threaded cover (404) and the sleeve seat (402) are connected in a threaded manner; the outer side of the exhaust pipe (401) is provided with a plurality of exhaust holes (405) equidistantly distributed around the circumference, and the exhaust holes (405) are located on the upper side of the threaded cover (404).
4. A rectification device for eucalyptol according to claim 3, characterized in that: The upper end of the exhaust pipe (401) is fixedly connected to a top plate (406), a hydraulic rod (407) is fixedly installed at the center of the top plate (406), the lower end of the hydraulic rod (407) is fixedly connected to a connecting seat (409), a piston (408) is fixedly sleeved on the outer side of the connecting seat (409), and the piston (408) can move up and down inside the exhaust pipe (401).
5. A rectification device for eucalyptol according to claim 1, characterized in that: The stirring structure (5) comprises a cylindrical rod (501) installed at the center of the lower part of the distillation tower (1), a plurality of stirring rods (502) equidistantly distributed in a circle are fixedly installed on the outer side of the cylindrical rod (501), the stirring rods (502) are in the shape of an arc, and both ends of the stirring rods (502) are fixedly connected to the cylindrical rod (501), a supporting seat (503) is installed at the lower end of the cylindrical rod (501), and the cylindrical rod (501) is rotatably connected to the supporting seat (503) via a bearing, a plurality of supporting rods (504) equidistantly distributed in a circle are fixedly installed on the outer side of the supporting seat (503), and one end of the supporting rod (504) away from the supporting seat (503) is fixedly connected to the distillation tower (1).
6. A rectification device for eucalyptol according to claim 5, characterized in that: A cylindrical groove (505) is provided at the center of the upper end of the cylindrical rod (501), and a threaded groove (506) is provided on the side wall of the cylindrical groove (505). A long connecting rod (507) is movably embedded in the upper end of the cylindrical rod (501), and the long connecting rod (507) is plug-in-pull connected to the cylindrical rod (501) through the cylindrical groove (505). The long connecting rod (507) passes through a plurality of the tower plates (2) and can move up and down inside the distillation tower (1). A pin ball (508) is fixedly embedded on the outer side of the long connecting rod (507), and the pin ball (508) is located inside the cylindrical rod (501). The pin ball (508) is in sliding contact with the cylindrical rod (501) through the threaded groove (506), and an external thread (509) is provided at the upper end of the long connecting rod (507).
7. A rectification device for eucalyptol according to claim 6, characterized in that: The long connecting rod (507) is threadedly connected to the connecting seat (409) via the second external thread (509); a limiting assembly (8) is installed on the outer side of the long connecting rod (507) near the exhaust structure (4); the limiting assembly (8) comprises a plurality of convex ribs (801) fixedly embedded on the outer side of the long connecting rod (507), and the convex ribs (801) are equidistantly distributed around the circumference; a collar (802) is movably sleeved on the outer side of the convex rib (801); a plurality of supporting rods (803) are fixedly embedded on the outer side of the collar (802) and are equidistantly distributed around the circumference; and one end of the supporting rod (803) away from the collar (802) is fixedly connected to the distillation tower (1).
8. A rectification device for eucalyptol according to claim 1, characterized in that: The anti-blocking structure (6) comprises a grid plate (601) installed on the lower side of the tower plate (2), and the grid plate (601) is fixedly sleeved on the outer side of the long connecting rod (507); a plurality of vertical rods (602) are fixedly embedded in the upper end of the grid plate (601), and the number of the vertical rods (602) is equal to the number of circular through holes opened on the tower plate (2); the plurality of vertical rods (602) are located on the lower side of the plurality of circular through holes; a wire brush (603) is fixedly connected to the upper end of the vertical rod (602), and the wire brush (603) can pass through the tower plate (2) through the circular through hole; the shape of the wire brush (603) is umbrella-shaped.
9. A rectification device for eucalyptol according to claim 8, characterized in that: A plurality of connection components (7) distributed at equal distances are installed between the grid plate (601) and the inner wall of the distillation tower (1), the connection component (7) comprising a metal spring (701) fixedly embedded on the outer side of the grid plate (601), a fixing plate (702) fixedly embedded on the inner wall of the distillation tower (1) corresponding to the connection component (7), a plurality of stoppers (703) distributed at equal distances are fixedly installed on one side of the fixing plate (702) close to the metal spring (701), and the cross-sectional shape of the stoppers (703) is triangular, and the connection between the metal spring (701) and the plurality of stoppers (703) is a sliding contact.
10. A rectification device for eucalyptol according to claim 1, characterized in that: A connecting pipe (15) is fixedly mounted on the upper end of the distillation tower (1), a cover pipe (9) is mounted on the upper end of the connecting pipe (15), and the cover pipe (9) and the connecting pipe (15) are located outside the exhaust structure (4), flanges (12) are fixedly sleeved on the outer sides of the cover pipe (9) and the connecting pipe (15), and the cover pipe (9) and the connecting pipe (15) are fixedly connected via the flange (12) and bolts, and a flange (12) is fixedly mounted on the upper end of the cover pipe (9) and connected to the connecting pipe (15). A conduit (10) is connected to the distillation tower (1), the end of the conduit (10) away from the cover pipe (9) is equipped with a condenser (11), and the cover pipe (9) is rotatably connected to the condenser (11) via a rotary joint, a conduit (13) is fixedly installed on the outside of the connecting pipe (15) and is in communication with the conduit, and the end of the conduit (13) away from the connecting pipe (15) is fixedly connected to the distillation tower (1), and a reflux pipe (14) is fixedly installed on the outside of the distillation tower (1) near its upper end.
Citation Information
Patent Citations
Chemical efficient energy-saving high-purity rectifying tower
CN112337126A
Rectifying tower for producing 2,4-dichlorophenol
CN113750560A
Efficient rectification device for mixed hydrocarbon
CN116099225A
System for producing liquid ammonia by rectifying ammonia-containing wastewater in isophthalonitrile-containing production process
CN220182849U
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