Maleic anhydride wastewater treatment method

Abstract

The invention relates to the technical field of wastewater treatment, in particular to a maleic anhydride wastewater treatment method, which comprises the following steps of: proportioning power plant wastewater and maleic anhydride wastewater, coagulating and flocculating to degrade COD (Chemical Oxygen Demand), comprehensively knowing the characteristics of the maleic anhydride wastewater, starting from a reaction mechanism, proportioning by taking existing desulfurization and denitrification wastewater / coal hydrogen production wastewater of a sewage treatment plant as a reaction agent, and preparing the maleic anhydride wastewater. COD (Chemical Oxygen Demand) in water is consumed through coagulation and flocculation, so that up-to-standard discharge of treated water and reuse of reclaimed water are realized. On one hand, the dosage of agents for treating maleic anhydride wastewater is saved, and on the other hand, power plant wastewater treatment difficulty is reduced.

Description

Technical Field

[0001] The invention relates to the technical field of wastewater treatment, in particular to a method for treating maleic anhydride wastewater. Background Art

[0002] n-Butane is partially oxidized by air under the action of vanadium-phosphorus-oxygen catalyst to produce maleic anhydride. The reaction process includes carbon four separation, n-butane oxidation, solvent absorption and analysis, product refining and other processes. When the maleic anhydride device is in operation, the wastewater will contain organic components such as maleic acid, phthalic anhydride, and dibutyl phthalate. These substances are difficult to degrade through biochemical degradation, resulting in an increase in the chemical oxygen demand (COD) of the effluent, that is, a high degree of organic pollution in the water body. Maleic anhydride wastewater needs to be treated and discharged only after it meets the discharge standards. After treatment, the maleic anhydride wastewater is reduced to below 500 mg / L before it can be discharged. In the prior art, the treatment of maleic anhydride wastewater is a common problem, and the cost of adding reagents is high.

[0003] Due to the high hardness and pH value of power plant desulfurization wastewater / coal-to-hydrogen wastewater, in actual operation, blockage of pipelines by hardness removal units and blockage of membranes in the grey water system are common problems. Summary of the invention

[0004] In view of the defects of the prior art, the present invention provides a method for treating maleic anhydride wastewater, which treats maleic anhydride wastewater and desulfurization wastewater in different proportions, which can not only achieve better coagulation and flocculation and COD removal effects, but also consume desulfurization wastewater from power plants to a certain extent, reducing the risk of pipeline blockage by hardness removal units and membrane blockage in the reclaimed water system.

[0005] In order to achieve the above-mentioned purpose, the technical solution provided by the present invention is a method for treating maleic anhydride wastewater, which uses power plant wastewater and maleic anhydride wastewater to mix, coagulate and flocculate to degrade COD.

[0006] Furthermore, a method for treating maleic anhydride wastewater comprises the following steps: Step S100, taking industrial wastewater; Step S200, taking maleic anhydride wastewater; Step S300, mixing the industrial wastewater in step S100 with the maleic anhydride wastewater in step S200; Step S400, stirring and coagulation and flocculation are performed, and the temperature is controlled within the range of 20°C to 30°C.

[0007] Preferably, the pH value of the industrial wastewater in step S100 is 6-9, the hardness is 4000 mg / L, and the temperature is 15°C-35°C.

[0008] Preferably, the pH value of the maleic anhydride wastewater in step S200 is 1-2, and the temperature is 50°C-60°C.

[0009] Preferably, the industrial wastewater in step S100 includes one or more of desulfurization wastewater, denitrification wastewater, and coal-to-hydrogen wastewater.

[0010] Preferably, the maleic anhydride wastewater in step S200 contains one or more of maleic acid, phthalic anhydride and dibutyl phthalate.

[0011] Preferably, the industrial wastewater in step S100 is low-concentration industrial wastewater, and the concentration of the low-concentration desulfurization wastewater is 100 mg / L to 150 mg / L.

[0012] Furthermore, the volume ratio of the maleic anhydride wastewater in step S200 to the low-concentration industrial wastewater in step S100 is 4 / 1.

[0013] Preferably, the industrial wastewater in step S100 is high-concentration desulfurization wastewater, and the concentration of the high-concentration desulfurization wastewater is 1500 mg / L~3000 mg / L.

[0014] Furthermore, the volume ratio of the maleic anhydride wastewater in step S200 to the high-concentration desulfurization wastewater in step S100 is 20 / 1.

[0015] In the above method, the maleic anhydride wastewater treatment method has one, two or three of the following characteristics: First, it can consume the desulfurization wastewater from power plants, reducing the risk of blockage of pipelines in hardness removal units and membrane blockage in the reclaimed water system; Second, it can reduce the use of coagulants in treating maleic anhydride wastewater; Third, remove the difficult-to-degrade organic substances such as acid, phthalic anhydride, and dibutyl phthalate; Fourth, it can remove metal and non-metal ions simultaneously.

[0016] The beneficial effects of the present invention are as follows: firstly, the technology used in the present invention realizes the resource utilization of wastes, and treats and utilizes industrial wastewater including but not limited to desulfurization wastewater from power plants while treating maleic anhydride wastewater; secondly, the present invention treats waste with waste, and utilizes power plant wastewater to treat maleic anhydride wastewater to achieve coagulation, flocculation and removal of difficult-to-degrade organic pollutants, thereby achieving a significant COD removal effect; finally, the present invention reduces the discharge of desulfurization wastewater and thereby simultaneously solves the common problems of pipe blockage of hardness removal units and membrane blockage of reclaimed water systems. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 It is the corresponding COD removal rate line chart of maleic anhydride wastewater and low-concentration desulfurization wastewater after mixing, coagulation and flocculation at different proportions; Figure 2 This is the corresponding effect diagram after mixing, coagulation and flocculation of maleic anhydride wastewater and low-concentration desulfurization wastewater in different proportions; Figure 3 It is the corresponding COD removal rate line chart of maleic anhydride wastewater and high-concentration desulfurization wastewater after mixing, coagulation and flocculation at different proportions; Figure 4 This is the corresponding effect diagram after mixing, coagulation and flocculation of maleic anhydride wastewater and high-concentration desulfurization wastewater in different proportions; Figure 5 This is a schematic diagram of the corresponding colors of maleic anhydride wastewater and high-concentration desulfurization wastewater after mixing, coagulation, flocculation and ozone oxidation in different proportions. DETAILED DESCRIPTION

[0018] In order to make the above-mentioned objects, features and advantages of the present invention more obvious and easy to understand, the specific embodiments of the present invention are described in detail below in conjunction with the accompanying drawings. In the following description, many specific details are set forth to facilitate a full understanding of the present invention. However, the present invention can be implemented in many other ways different from those described herein, and those skilled in the art can make similar improvements without violating the connotation of the present invention, so the present invention is not limited by the specific embodiments disclosed below.

[0019] Chemical Oxygen Demand (COD) is a chemical method to measure the amount of reducing substances that need to be oxidized in a water sample. It is the oxygen equivalent of substances (generally organic matter) that can be oxidized by strong oxidants in wastewater, effluent from wastewater treatment plants and contaminated water. In the study of river pollution and the properties of industrial wastewater, as well as the operation and management of wastewater treatment plants, it is an important and rapidly measurable organic pollution parameter, often represented by the symbol COD. It should be noted that the concentration of desulfurization wastewater in this application is the COD in the desulfurization wastewater.

[0020] Example 1 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of low-concentration 150 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 35°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 56°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 and the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 4 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0021] The COD removal rate of maleic anhydride wastewater was determined to be 84.71%.

[0022] Example 2 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: take a certain amount of low-concentration 150 mg / L desulfurization wastewater, with a pH value of 7, a hardness of 4000 mg / L, and a temperature of 30°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 59°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 with the industrial wastewater in step S100 in a certain proportion, with the volume ratio of the two being 1 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0023] The COD removal rate of maleic anhydride wastewater was determined to be 65.47%.

[0024] Example 3 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of low-concentration 150 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 35°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 56°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 and the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 2 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0025] The COD removal rate of maleic anhydride wastewater was determined to be 78.07%.

[0026] Example 4 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of low-concentration 150 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 35°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 56°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 and the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 3 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0027] The COD removal rate of maleic anhydride wastewater was determined to be 77.81%.

[0028] Example 5 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of low-concentration 150 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 35°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 56°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 with the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 1 / 2; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0029] The COD removal rate of maleic anhydride wastewater was determined to be 68.53%.

[0030] Example 6 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of low-concentration 150 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 35°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 56°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 with the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 1 / 3; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0031] The COD removal rate of maleic anhydride wastewater was determined to be 73.67%.

[0032] Example 7 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of high-concentration 3000 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 30°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 55°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 and the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 20 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0033] The COD removal rate of maleic anhydride wastewater was determined to be 92.75%.

[0034] Example 8 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of high-concentration 3000 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 30°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 55°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 and the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 1 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0035] The COD removal rate of maleic anhydride wastewater was determined to be 79.34%.

[0036] Example 9 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of high-concentration 3000 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 30°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 55°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 and the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 2 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0037] The COD removal rate of maleic anhydride wastewater was determined to be 84.11%.

[0038] Example 10 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of high-concentration 3000 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 30°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 55°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 and the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 3 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0039] The COD removal rate of maleic anhydride wastewater was determined to be 85.59%.

[0040] Embodiment 11 A method for treating maleic anhydride wastewater comprises the following steps: Step S100, selection and use of industrial wastewater: taking a certain amount of high-concentration 3000 mg / L desulfurization wastewater, with a pH value of 8, a hardness of 4000 mg / L, and a temperature of 30°C; Step S200, introduction and use of maleic anhydride wastewater: taking a certain amount of maleic anhydride wastewater, which contains organic components that are difficult to be biodegraded, such as maleic acid, phthalic anhydride, dibutyl phthalate, etc., with a pH value of 1-2 and a temperature of 55°C; Step S300, mixing two kinds of wastewater: mixing the maleic anhydride wastewater in step S200 and the industrial wastewater in step S100 in a certain proportion, with the volume ratio between the two being 40 / 1; Step S400, coagulation and flocculation of mixed wastewater: when mixing and coagulating, the temperature is 25°C, the stirring speed during flocculation is 200 rpm, and the stirring speed used for coagulation is 40 rpm.

[0041] The COD removal rate of maleic anhydride wastewater was determined to be 78.03%.

[0042] pass Figure 1 It can be seen that when low-concentration desulfurization wastewater and maleic anhydride wastewater are mixed, coagulated and flocculated at a volume ratio of 1 / 1, 2 / 1, 3 / 1, 4 / 1, 1 / 2, and 1 / 3, the COD removal rate of maleic anhydride wastewater can be above 60%, and the highest can reach 84.71%. Figure 2 The corresponding flocculation effect can be seen. Figure 2 The flocculation effect and Figure 1 The volume ratios in the figure correspond one to one from left to right.

[0043] Figure 3 It can be seen that when high-concentration desulfurization wastewater and maleic anhydride wastewater are mixed, coagulated and flocculated at a volume ratio of 1 / 1, 2 / 1, 3 / 1, 20 / 1 and 40 / 1, the COD removal rate of maleic anhydride wastewater can be above 70%, and the highest can reach 92.75%. Figure 4 It can be seen that the corresponding coagulation and flocculation conditions are Figure 5 It shows the color of the water after ozone oxidation, and it can be seen that the water is clear and transparent. Figure 4 Flocculation effect and Figure 5The color of the water after ozone oxidation is the same as Figure 3 The volume ratios in the figure correspond one to one from left to right.

[0044] In this embodiment, power plant wastewater and maleic anhydride wastewater are mixed and flocculated to degrade COD, remove a large amount of COD before ozone, reduce ozone consumption, ensure effective ozone addition, and achieve normal function of the depth line. The hard COD problem of maleic anhydride wastewater is solved at a low cost, and the reuse of reclaimed water is realized, thereby ensuring that the discharge is qualified.

[0045] In the description of the present invention, it is to be understood that the terms “center”, “longitudinal”, “lateral”, “length”, “width”, “thickness”, “up”, “down”, “front”, “back”, “left”, “right”, “vertical”, “horizontal”, “top”, “bottom”, “inside”, “outside”, “clockwise”, “counterclockwise”, “axial”, “radial”, “circumferential”, etc., indicating orientations or positional relationships are based on the orientations or positional relationships shown in the accompanying drawings, and are only for the convenience of describing the present invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore should not be understood as limiting the present invention.

[0046] In addition, the terms "first" and "second" are used for descriptive purposes only and should not be understood as indicating or implying relative importance or implicitly indicating the number of the indicated technical features. Therefore, the features defined as "first" and "second" may explicitly or implicitly include at least one of the features. In the description of the present invention, the meaning of "plurality" is at least two, such as two, three, etc., unless otherwise clearly and specifically defined.

[0047] In the present invention, unless otherwise clearly specified and limited, the terms "installed", "connected", "connected", "fixed" and the like should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium, it can be the internal connection of two elements or the interaction relationship between two elements, unless otherwise clearly defined. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.

[0048] In the present invention, unless otherwise clearly specified and limited, the first feature "above" or "below" the second feature may be that the first and second features are in direct contact, or the first and second features are in indirect contact through an intermediate medium. Moreover, the first feature "above", "above" and "above" the second feature may be that the first feature is directly above or obliquely above the second feature, or simply indicates that the first feature is higher in level than the second feature. The first feature "below", "below" and "below" the second feature may be that the first feature is directly below or obliquely below the second feature, or simply indicates that the first feature is lower in level than the second feature. It should be noted that when an element is referred to as "fixed to" or "set on" another element, it may be directly on the other element or there may be a central element. When an element is considered to be "connected" to another element, it may be directly connected to the other element or there may be a central element at the same time. The terms "vertical", "horizontal", "up", "down", "left", "right" and similar expressions used herein are for illustrative purposes only and do not represent the only implementation method.

Claims

1. A method for treating maleic anhydride wastewater, characterized in that: The power plant wastewater and maleic anhydride wastewater are mixed and coagulated to degrade COD.

2. A method for treating maleic anhydride wastewater according to claim 1, characterized in that: The following steps are involved: Step S100, taking industrial wastewater; Step S200, taking maleic anhydride wastewater; Step S300, mixing the industrial wastewater in step S100 with the maleic anhydride wastewater in step S200; Step S400, stirring and coagulation and flocculation are performed, and the temperature is controlled within the range of 20°C to 30°C.

3. A method for treating maleic anhydride wastewater according to claim 2, characterized in that: The industrial wastewater in step S100 has a pH value of 6-9, a hardness of 4000 mg / L, and a temperature of 15°C-35°C.

4. A method for treating maleic anhydride wastewater according to claim 2, characterized in that: The pH value of the maleic anhydride wastewater in step S200 is 1-2, and the temperature is 50°C-60°C.

5. A method for treating maleic anhydride wastewater according to claim 2, characterized in that: The industrial wastewater in step S100 includes one or more of desulfurization wastewater, denitrification wastewater, and coal-to-hydrogen wastewater.

6. A method for treating maleic anhydride wastewater according to claim 2, characterized in that: The maleic anhydride wastewater in step S200 contains one or more of maleic acid, phthalic anhydride, and dibutyl phthalate.

7. A method for treating maleic anhydride wastewater according to any one of claims 1 to 6, characterized in that: The industrial wastewater in step S100 is low-concentration industrial wastewater, and the concentration of the low-concentration desulfurization wastewater is 100 mg / L to 150 mg / L.

8. A method for treating maleic anhydride wastewater according to claim 7, characterized in that: The volume ratio of the maleic anhydride wastewater in step S200 to the low-concentration industrial wastewater in step S100 is 4 / 1.

9. A method for treating maleic anhydride wastewater according to any one of claims 1 to 6, characterized in that: The industrial wastewater in step S100 is high-concentration desulfurization wastewater, and the concentration of the high-concentration desulfurization wastewater is 1500 mg / L~3000 mg / L.

10. A method for treating maleic anhydride wastewater according to claim 9, characterized in that: The volume ratio of the maleic anhydride wastewater in step S200 to the high-concentration desulfurization wastewater in step S100 is 20 / 1.

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