Rose disinfectant formula and preparation process thereof

Abstract

The invention belongs to the technical field of disinfectants, and particularly relates to a rose disinfectant formula and a preparation process thereof. The formula of the rose disinfectant comprises the following components in parts by mass: 0.2-0.3 part of benzalkonium chloride; 0.5 to 1.0 part by mass of tea tree essential oil; 0.2 to 0.5 part by mass of chamomile essential oil; 3.0 to 5.0 parts by mass of glycerin; and 93.2 to 95.8 parts by mass of rose water. According to the formula and the preparation process of the rose disinfectant disclosed by the invention, the pH value and the electrical characteristics of the disinfectant system are measured and regulated on line in the preparation process by adopting the active matter electrode and the pH meter, so that the disinfectant system can be always in a stable state, and an activity reduction reaction between active substances is avoided; the use effect of the disinfectant is favorably improved.

Description

Technical Field

[0001] The present application belongs to the technical field of disinfectants, and specifically relates to a rose disinfectant formula and a production process thereof. Background Art

[0002] Commonly used disinfectants include alcohol disinfectants, iodine-containing disinfectants, quaternary ammonium salt disinfectants, chlorine-containing disinfectants, chlorine dioxide disinfectants, peroxide disinfectants, bromine-containing disinfectants, phenol disinfectants and other 8 types. The most commonly used disinfectants are mainly alcohol disinfectants, chlorine-containing disinfectants, iodine-containing disinfectants, and quaternary ammonium salt disinfectants.

[0003] Alcohol disinfectants: The most common ones are 75% alcohol, which has the characteristics of rapid volatilization and broad-spectrum bactericidal effect. They are suitable for hygienic hand disinfection, surgical hand disinfection, skin disinfection, etc.

[0004] Chlorine-containing disinfectants: such as sodium hypochlorite, calcium hypochlorite, etc. This type of disinfectant has strong oxidizing properties and can quickly kill bacteria, viruses and other pathogens, but it is highly irritating to the skin, eyes, etc.

[0005] Iodine-containing disinfectants: including iodine tincture and iodine tincture. Iodine tincture is suitable for disinfection of surgical hands and skin, surgical incision sites, injection and puncture sites, and neonatal umbilical cord skin, while iodine tincture is suitable for disinfection of surgical sites, injection and puncture sites, and neonatal umbilical cord skin, but not suitable for mucous membranes and damaged skin.

[0006] Quaternary ammonium disinfectants: such as benzalkonium bromide, are mainly used for fabric disinfection, surgical hand disinfection, skin and mucous membrane disinfection. They have the characteristics of broad-spectrum bactericidal effect, good stability and low skin irritation.

[0007] The selection of a suitable disinfectant should be determined according to the specific disinfection requirements and environmental conditions. Existing disinfectant products lack a disinfectant that is suitable for household use, has good sterilization ability, is less irritating to the human body, and has a fragrant smell. Summary of the invention

[0008] In view of this, the present application provides a rose disinfectant formula and a production process thereof to solve all or part of the technical problems described in the background technology section of the present application.

[0009] The rose disinfectant formula provided by this application to solve its technical problem is: Benzalkonium chloride: 0.2 to 0.3 parts by mass; Tea Tree Oil: 0.5 to 1.0 parts by mass; Chamomile Essential Oil: 0.2 to 0.5 parts by mass; Glycerin: 3.0 to 5.0 parts by mass; Rose Water: 93.2 parts by mass to 95.8 parts by mass.

[0010] The disinfectant formula uses tea tree oil, chamomile oil, rose water, glycerin and benzalkonium chloride to not only effectively provide disinfection effects, but also maintain mildness and skin comfort.

[0011] As the main disinfectant ingredient, benzalkonium chloride can effectively kill a variety of bacteria, viruses and fungi within this concentration range, while being relatively less irritating to the skin.

[0012] Tea tree essential oil has good natural antibacterial and anti-inflammatory properties and is suitable for addition to disinfectant formulas; within the range of 0.5 to 1 part by mass, it can exert its antibacterial effect without being overly irritating to the skin.

[0013] Chamomile essential oil has a calming and soothing effect, which can help reduce skin irritation and inflammation. Low concentrations of chamomile essential oil (0.2 to 0.5 parts by weight) can provide a soothing effect without masking the antibacterial effects of other ingredients.

[0014] As a humectant, glycerin can help retain moisture in the skin and prevent dryness and discomfort caused by disinfection; a concentration of 3 to 5 parts by mass can provide sufficient moisturizing effect without affecting the texture of the product.

[0015] Rose water is a gentle base ingredient that provides a mild antibacterial effect, while having a refreshing aroma and mild properties, making it suitable for use in disinfectant formulations.

[0016] Benzalkonium chloride: 0.2 parts by mass; Tea tree essential oil: 0.5 parts by mass; Chamomile essential oil: 0.3 parts by mass; Glycerol: 4 parts by mass; Rose water: 95 parts by mass.

[0017] Benzalkonium chloride: 0.2 parts by mass; Tea tree essential oil: 0.5 parts by mass; Chamomile essential oil: 0.2 parts by mass; Glycerol: 3.0 parts by mass; Rose water: 93.2 parts by mass.

[0018] Benzalkonium chloride: 0.3 parts by mass; Tea tree essential oil: 1.0 parts by mass; Chamomile essential oil: 5.0 parts by mass; Glycerol: 3.0 parts by mass; Rose water: 95.8 parts by mass.

[0019] The rose disinfectant production process adopted by the present application to solve the technical problem includes the following steps: S1, adding 93.2 to 95.8 parts by mass of rose water into a stirring tank; S2, turning on the electric control valves of the benzalkonium chloride storage tank, the tea tree essential oil storage tank, the chamomile essential oil storage tank, and the glycerin storage tank, and uniformly adding benzalkonium chloride, tea tree essential oil, chamomile essential oil, and glycerin to the rose water prepared in step S1 and stirring at a constant temperature; S3, simultaneously detect the active substance electrode potential Eqc and pH of the system; When the pH exceeds the upper limit of the pH scale, the flow rate of the benzalkonium chloride is reduced, and when the pH is below the lower limit of the pH scale, the flow rate of the chamomile essential oil is reduced; When the change in the active substance electrode potential Eqc per unit time exceeds the threshold value Eqc0, the injection of benzalkonium chloride and tea tree essential oil is stopped until the active substance electrode potential Eqc returns to a stable state; S4, according to the control method in S3, adding 0.1 to 0.3 parts by mass of benzalkonium chloride, 0.5 to 1.0 parts by mass of tea tree essential oil, 0.2 to 0.5 parts by mass of chamomile essential oil, and 3.0 to 5.0 parts by mass of glycerin; Among them: the upper limit of pH is pH=5.6, the lower limit of pH is pH=4.1, and the threshold value Eqc0=2mv-4mv; The method for making the active material electrode is as follows: S31, taking at least one of tea tree essential oil active substance, chamomile essential oil active substance, and rose water active substance, adding sodium tetraphenylborate solution with stirring, standing, filtering, washing, and drying to obtain an active mixture; S32, first dissolving the active mixture and PVC powder into tetrahydrofuran, then adding dibutyl phthalate, and drying to obtain an electrode active material, and making the electrode active material into a rose water disinfectant active electrode.

[0020] Beneficial technical effects: 1. Powerful disinfection: Benzalkonium chloride, as the main disinfectant ingredient, can effectively kill a variety of pathogens. Tea tree essential oil supplements the natural antibacterial and antiviral effects, enhancing the overall disinfection effect.

[0021] 2. Gentle and comfortable: Chamomile essential oil provides soothing and calming effects, reducing skin irritation or inflammation caused by the use of disinfectant products. At the same time, rose water and glycerin work together to provide good moisturizing effects and protect the skin from dryness.

[0022] 3. Natural aroma: The combination of tea tree essential oil and chamomile essential oil, plus rose water, provides a natural and refreshing aroma to enhance the user experience.

[0023] 4. Multiple uses: This formula is suitable for hand disinfection as well as disinfection of other body parts or surfaces, and is suitable for home and daily use.

[0024] The technical solution and technical effects of the present application are described in detail below in conjunction with the accompanying drawings and specific implementation methods. BRIEF DESCRIPTION OF THE DRAWINGS

[0025] Figure 1 : Rose water disinfectant production process flow chart; Figure 2 : Schematic diagram of active material electrode structure; Icon Description: 10-electrode shell, 20-electrode head, 30-lead wire. DETAILED DESCRIPTION

[0026] See also Figure 1 The rose disinfectant preparation process disclosed in the present application comprises the following steps: S1, adding 93.2 to 95.8 parts by mass of rose water into a stirring tank; S2, turning on the electric control valves of the benzalkonium chloride storage tank, the tea tree essential oil storage tank, the chamomile essential oil storage tank, and the glycerin storage tank, and uniformly adding benzalkonium chloride, tea tree essential oil, chamomile essential oil, and glycerin to the rose water prepared in step S1 and stirring at a constant temperature; Technical means such as using electric control valves to control fluids and constant temperature stirring are common technical knowledge in this field and will not be elaborated here.

[0027] S3, simultaneously detect the active substance electrode potential Eqc and pH of the system; When the pH exceeds the upper limit of pH, the injection rate of benzalkonium chloride is reduced, and when the pH is lower than the lower limit of pH, the injection rate of chamomile essential oil is reduced; so that the pH of the system is always within the range of 4.1 to 5.6; When the change in the active substance electrode potential Eqc per unit time exceeds the threshold value Eqc0, stop injecting benzalkonium chloride and tea tree essential oil until the active substance electrode potential Eqc returns to a stable state; the threshold value Eqc0 = 2mv-4mv; S4, according to the control method in S3, adding 0.1 to 0.3 parts by mass of benzalkonium chloride, 0.5 to 1.0 parts by mass of tea tree essential oil, 0.2 to 0.5 parts by mass of chamomile essential oil, and 3.0 to 5.0 parts by mass of glycerin; Among them: the upper limit of pH is pH=5.6, the lower limit of pH is pH=4.1, and the threshold value Eqc0=2mv-4mv.

[0028] The purpose of using pH and active substance electrode potential to regulate the production process is to avoid chemical reactions between various active substances when the material concentration, system pH, and system electrode potential change, thereby reducing the biological activity of various ingredients and affecting the bactericidal and disinfecting effect of the disinfectant.

[0029] In the case of benzalkonium chloride and quercetin, the active substance in rose water, the chemical reaction that may occur between benzalkonium chloride and quercetin depends on the reaction conditions, such as pH, temperature, reaction time, and concentration of the two. Under certain conditions, they may undergo ion exchange, addition reaction, or redox reaction. For example, the cationic part of benzalkonium chloride may form an ion pair with the hydroxyl group of quercetin, or a redox reaction may occur between them, resulting in structural changes. For example, in an acidic environment, benzalkonium chloride may be protonated, enhancing its interaction with the hydrophobic part of quercetin. In an alkaline environment, some functional groups of quercetin may be deprotonated, changing its reactivity. Therefore, monitoring and adjusting the pH during the preparation of disinfectants can help maintain the biological activity of various materials and avoid reduced activity due to changes in pH and concentration.

[0030] For example, under certain material concentrations, system pH and system potential, terpenes in tea tree essential oil may interact with the cationic surfactant benzalkonium chloride, resulting in solubility changes or the formation of complexes, thereby affecting its biological activity. In addition, one of the main components of tea tree essential oil is terpinen-4-ol, the content of which can exceed 30%. Benzalkonium chloride may also react with such compounds, affecting its antibacterial effect.

[0031] Chamomile essential oil is mainly a volatile oil composed of various terpenoid compounds, while benzalkonium chloride is a class of cationic surfactants. However, they may affect each other's solubility and physical properties when mixed together. The chemical properties of chamomile essential oil may be affected by pH, and the bactericidal efficacy of benzalkonium chloride may be reduced at extreme pH values. When the two are mixed, chamomile essential oil may affect the surface activity of benzalkonium chloride, thereby affecting its disinfection effect. Conversely, benzalkonium chloride may also affect the solubility and biological activity of certain components in chamomile essential oil. Since chamomile essential oil has antibacterial and antioxidant properties, and benzalkonium chloride has bactericidal effects, theoretically, mixing the two may produce a synergistic effect and enhance each other's antibacterial properties. However, such a mixed use may reduce their respective effectiveness because certain components in chamomile essential oil may interact with benzalkonium chloride, thereby reducing its biological activity.

[0032] Therefore, in the process of making disinfectant, timely control of the pH and electrical properties of the system by utilizing the acid-base and electrical properties of the ingredients themselves helps to ensure that the material concentration, pH and active substance electrode potential Eqc of the system are always in a stable state, and avoid chemical reactions between the active substances of each ingredient to reduce biological activity. At the same time, using active substance electrodes to measure the electrical properties of the system helps to timely understand the dynamic changes in the biological activity of the ingredients in the system. When the active substance electrode potential changes greatly, the injection speed of the ingredients that have a greater impact on the electrical properties is adjusted to avoid mutual reduction of biological activity between the ingredients, ensuring the formation of a synergistic effect of mutual enhancement.

[0033] The method for making the active electrode in this application is: S31, taking at least one of tea tree essential oil active substance, chamomile essential oil active substance, and rose water active substance, adding sodium tetraphenylborate solution with stirring, standing, filtering, washing, and drying to obtain an active mixture; S32, first dissolving the active mixture and PVC powder into tetrahydrofuran, then adding dibutyl phthalate, and drying to obtain an electrode active material, and making the electrode active material into a rose water disinfectant active electrode.

[0034] The active substance can be any one or any combination of tea tree essential oil active substance, chamomile essential oil active substance, and rose water active substance. In addition, multiple active substances can be used in the system to prepare corresponding active substance electrodes, and the dynamic parameters of each active substance electrode can be detected to determine whether the various active substances in the system are in a stable state.

[0035] Take quercetin, one of the active substances in rose water, as an example. Quercetin belongs to the flavonoids and has strong biological and pharmacological activities. It has antioxidant and free radical scavenging, anti-inflammatory, analgesic, hypoglycemic and anti-cancer effects. Prepare quercetin electrode active material according to the above preparation method. Then, make the quercetin electrode active material into active material electrode. Please refer to Figure 2 The electrode generally includes a motor housing 10, an electrode head 20, and a wire 30. The electrode head 20 is made of quercetin electrode active material and is fastened in the electrode housing 10. The wire 30 is connected to the electrode head 20 through a conductive adhesive.

[0036] The rose disinfectant formula and its production process disclosed in the present application can ensure that the disinfectant system is always in a stable state and avoid activity reduction reactions between active substances by using active substance electrodes and pH meters to measure and control the pH and electrical properties of the disinfectant system online during the production process, thereby helping to improve the use effect of the disinfectant.

[0037] The technical scheme and technical effects of the present application are described in detail above in combination with the drawings and specific embodiments of the specification. It should be noted that technicians in this field can also develop other embodiments on this basis; any simple deformation and equivalent substitution that does not deviate from the innovative concept of the present application are covered by the present application and belong to the scope of protection of this patent.

Claims

1. A rose disinfectant formula, comprising: Benzalkonium chloride: 0.1 to 0.3 parts by mass; Tea tree essential oil: 0.5 to 1.0 parts by mass; Chamomile essential oil: 0.2 to 0.5 parts by mass; Glycerin: 3.0 to 5.0 parts by mass; Rose water: 93.2 parts by mass to 95.8 parts by mass.

2. The rose disinfectant formulation according to claim 1, characterized in that: Benzalkonium chloride: 0.2 parts by mass; Tea tree essential oil: 0.5 parts by mass; Chamomile essential oil: 0.3 parts by mass; Glycerol: 4.0 parts by mass; Rose water: 95.0 parts by mass.

3. The rose disinfectant formulation according to claim 1, characterized in that: Benzalkonium chloride: 0.1 parts by mass; Tea tree essential oil: 0.5 parts by mass; Chamomile essential oil: 0.2 parts by mass; Glycerol: 3.0 parts by mass; Rose water: 93.2 parts by mass.

4. The rose disinfectant formulation according to claim 1, characterized in that: Benzalkonium chloride: 0.3 parts by mass; Tea tree essential oil: 1.0 parts by mass; Chamomile essential oil: 5.0 parts by mass; Glycerol: 3.0 parts by mass; Rose water: 95.8 parts by mass.

5. The rose disinfectant formulation according to claim 1, characterized in that: The preparation process of the rose water is: First, fresh rose flowers and pure water are distilled in a distillation tank, and then cooled, condensed, and the oil and water are separated to obtain rose essential oil and rose water.

6. A rose disinfectant production process, characterized in that: Used to prepare the rose disinfectant according to the formula of claim 1; The steps include: S1, adding 93.2 to 95.8 parts by mass of rose water into a stirring tank; S2, turning on the electric control valves of the benzalkonium chloride storage tank, the tea tree essential oil storage tank, the chamomile essential oil storage tank, and the glycerin storage tank, and uniformly adding benzalkonium chloride, tea tree essential oil, chamomile essential oil, and glycerin to the rose water prepared in step S1 and stirring at a constant temperature; S3, simultaneously detect the active substance electrode potential Eqc and pH of the system; When the pH exceeds the upper limit of the pH value, the injection flow rate of the benzalkonium chloride is reduced, and when the pH is below the lower limit of the pH value, the injection flow rate of the chamomile essential oil is reduced; When the change in the active substance electrode potential Eqc per unit time exceeds the threshold value Eqc0, the injection of benzalkonium chloride and tea tree essential oil is stopped until the unit change in the active substance electrode potential Eqc is at the threshold value Eqc0; S4, according to the control method in S3, adding 0.1 to 0.3 parts by mass of benzalkonium chloride, 0.5 to 1.0 parts by mass of tea tree essential oil, 0.2 to 0.5 parts by mass of chamomile essential oil, and 3.0 to 5.0 parts by mass of glycerin; Among them: the upper limit of pH is pH=5.6, the lower limit of pH is pH=4.1, and the threshold value Eqc0=2mv-4mv.

7. The rose disinfectant production process according to claim 6, characterized in that: The method for making the active material electrode is as follows: S31, taking at least one of tea tree essential oil active substance, chamomile essential oil active substance, and rose water active substance, adding sodium tetraphenylborate solution with stirring, standing, filtering, washing, and drying to obtain an active mixture; S32, first dissolving the active mixture and PVC powder into tetrahydrofuran, then adding dibutyl phthalate, and drying to obtain an electrode active material, and making the electrode active material into a rose water disinfectant active electrode.

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