Non-irritating, lifting and tightening mask cloth as well as preparation method and application thereof
By using the laminated structure of the cellulose fiber surface layer, PU fiber intermediate layer and cellulose fiber base layer in the mask cloth, combined with hydrospinning process and adhesive composite technology, the problem of irritation of the existing mask cloth is solved, and the problem of irritation is achieved. A non-irritating, lifting and tightening mask cloth improves user experience and product stability.
Patent Information
- Application Number
- CN202411674368.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-11-21
- Publication Date
- 2025-02-11
AI Technical Summary
The existing facial mask cloth is directly touching the skin when it is made of a water agent mask or a freeze-dried facial mask. Although it has a certain delicate feeling and elasticity, it is highly irritating, resulting in poor consumer experience.
Using the structures of the cellulose fiber surface layer, the elastic PU fiber intermediate layer and the cellulose fiber base layer arranged in sequence, a non-irritating, lifting and tight mask cloth is prepared through hydrospinning process and adhesive composite technology.
The mask fabric is non-irritating, providing good elasticity and skin feel, and the mask fabric structure is more stable through specific processes, avoiding layering and bleaching.
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Figure BDA0005146667010000131 
Figure BDA0005146667010000141
Abstract
Description
Technical Field
[0001] The invention belongs to the technical field of facial mask cloths, and in particular relates to a non-irritating, lifting and firming facial mask cloth and a preparation method and application thereof. Background Art
[0002] Facial mask cloth is a carrier of facial mask essence and can be applied directly to the face. Currently, the most common type of facial mask cloth on the market is non-woven fabric, but its air permeability and elasticity are poor, resulting in poor use effect and comfort. As a result, more and more manufacturers choose elastic fiber to prepare facial mask cloth. The mask cloth produced by elastic fiber can achieve good elasticity after heat shrinkage treatment, which will bring consumers an excellent use experience.
[0003] CN108866813A discloses a method for preparing an elastic water-retaining and moisture-absorbing facial mask cloth, which belongs to the technical field of facial mask cloth preparation. The invention blends activated carbon with polyester to obtain highly elastic and hydrophilic polyester fibers. The crystallinity of viscose fibers prepared using cheap rice bran as raw materials is much lower than that of traditional facial mask cloth raw materials such as cotton and linen. The activated carbon used in the invention is fired at high temperature and without oxygen on bamboo pieces. Since bamboo is acidic, the prepared activated carbon is also acidic. Under acidic conditions, bacterial growth and reproduction will be inhibited, which plays an antibacterial role. The polyester fiber itself has excellent elasticity. After being compounded with the viscose fiber, the gaps between the polyester fibers can be filled, so that the elasticity of the facial mask cloth is enhanced.
[0004] CN109680411A discloses a method for manufacturing a multi-component ultra-fine mask cloth, which forms capillary cavities of different sizes between continuous filament multi-component ultra-fine fibers, so that more capillary gaps are generated on the cloth surface, making the cloth surface fuller, and the amount of liquid carried is greatly increased, which can fully increase the absorption of essence liquid, thereby achieving high elasticity and ultra-flexibility of the ultra-fine mask cloth. At the same time, when the fibers are fully cracked, the fibers are subjected to secondary water softening treatment, making the cloth surface more delicate and good in skin adhesion. At the same time, due to the introduction of PLA, the ultra-fine fiber mask cloth is degradable and more environmentally friendly.
[0005] However, if the mask cloth obtained by the above technology is used as a water-based mask or a freeze-dried mask, the mask cloth directly contacts the skin. Although it has a certain degree of fineness and elasticity, it is highly irritating and will bring a bad user experience to consumers. Therefore, it is very necessary to provide a non-irritating, highly elastic mask cloth, which has a huge market demand and will bring considerable economic benefits. Summary of the invention
[0006] In view of the deficiencies in the prior art, the object of the present invention is to provide a non-irritating, lifting and firming facial mask cloth and a preparation method and application thereof.
[0007] In order to achieve the purpose of the invention, the present invention adopts the following technical solutions:
[0008] In a first aspect, the present invention provides a non-irritating, lifting, and firming facial mask cloth, the facial mask cloth comprising a cellulose fiber surface layer, an elastic middle layer, and a cellulose fiber bottom layer stacked in sequence;
[0009] The materials of the cellulose fiber surface layer and the cellulose fiber bottom layer are both fine-denier viscose fibers, with a fineness of 0.5dtex-1.0dtex (for example, 0.6dtex, 0.7dtex, 0.8dtex, 0.9dtex or 1dtex, etc.) and a length of 38-52mm (for example, 40mm, 42mm, 44mm, 46mm, 48mm or 50mm, etc.);
[0010] The material of the elastic middle layer is PU fiber.
[0011] The present invention adopts PU fiber as the elastic middle layer and cellulose fiber layers on both sides, wherein the middle layer has good elasticity. After being made into a membrane cloth, it can provide good elasticity. The cellulose fiber layer can make the fiber very soft by controlling the fineness. The surface of the prepared membrane cloth is very delicate and soft, and can provide a good skin feel. Since the cellulose fiber layer is in contact with the skin, the final facial mask cloth is very friendly to the skin, has no irritation, and is safer and gentler.
[0012] Preferably, the fine denier viscose fiber includes any one of lyocell fiber, viscose fiber or cuprammonium fiber, or a combination of at least two thereof.
[0013] Preferably, the fineness of the PU fiber is at the micron level.
[0014] Preferably, the longitudinally distributed fiber proportions in the cellulose fiber surface layer and the cellulose fiber bottom layer are independently 60%-80% (for example, 62%, 64%, 66%, 68%, 70%, 72%, 74%, 76% or 78%, etc.), and the transversely distributed fiber proportions are independently 20%-40% (for example, 22%, 24%, 26%, 28%, 30%, 32%, 34%, 36% or 38%, etc.).
[0015] In the present invention, the ductility of the cellulose fiber layer can be improved by setting the distribution ratio of the transverse and longitudinal fibers in the cellulose fiber surface layer or the bottom layer.
[0016] Preferably, the gram weight of the cellulose fiber surface layer and the cellulose fiber bottom layer is independently 10-20 g / m 2 , for example, it can be 11g / m 2 , 13g / m 2 , 15g / m 2, 17g / m 2 or 19g / m 2 wait.
[0017] Preferably, the elastic middle layer has a grammage of 8-15 g / m 2 , for example 8g / m 2 , 9g / m 2 , 10g / m 2 , 11g / m 2 , 12g / m 2 , 13g / m 2 or 14g / m 2 wait.
[0018] Other specific point values within the above numerical ranges can be selected and will not be described in detail here.
[0019] In a second aspect, the present invention provides a method for preparing the non-irritating, lifting, and firming facial mask cloth as described in the first aspect, the preparation method comprising:
[0020] (1) Using fine denier viscose fiber as raw material, preparing a cellulose fiber surface layer and a cellulose fiber bottom layer by carding and spunlace process;
[0021] The elastic middle layer is perforated;
[0022] (2) The upper and lower surfaces of the elastic middle layer are respectively compounded with the cellulose fiber surface layer and the cellulose fiber bottom layer using an adhesive to obtain the non-irritating, lifting and firming facial mask cloth.
[0023] Preferably, the spunlace process in step (1) is performed through six spunlace steps.
[0024] Preferably, the pressures of the first and second hydroentanglement steps are independently 0.5-1.5 MPa, for example, 0.6 MPa, 0.8 MPa, 1 MPa, 1.2 MPa or 1.4 MPa.
[0025] Preferably, the pressure of the third to sixth hydroentanglement steps is 2-3 MPa, for example, 2.1 MPa, 2.3 MPa, 2.5 MPa, 2.7 MPa or 2.9 MPa.
[0026] The spunlace process of the present invention adopts 6 spunlace steps, and at the same time controls the spunlace pressure range of different numbers of steps, so that the entanglement effect of the cellulose fiber layer is better and the uniformity is better. When the pressure of the first two spunlaces is too high, the fiber web is easily broken up, resulting in voids in the fiber web and affecting the surface uniformity. When the pressure of the last four spunlaces is too low, the fiber entanglement is too small, which in turn affects the adsorption effect of the mask cloth on the mask liquid. When the pressure of the last four spunlaces is too high, the fibers between the skin-friendly layers are entangled more tightly and the hardness is high, affecting the skin feel of the product.
[0027] Preferably, the hydroentanglement process in step (1) is followed by a drying process.
[0028] Preferably, the drying temperature is 130-140°C, and the drying time is 5-15 min. For example, the temperature may be 131°C, 133°C, 135°C, 137°C or 139°C, and the drying time may be 6 min, 8 min, 10 min, 12 min or 14 min.
[0029] In the present invention, when the drying temperature is too low, the film cloth cannot be completely dried, and when the temperature is too high, the film cloth is too hard, affecting the skin feel of the mask product. Only when the drying temperature is controlled within the above range can the final mask cloth have a better skin feel.
[0030] Preferably, the adhesive in step (2) is PUR hot melt adhesive.
[0031] Preferably, the amount of the adhesive is 2-5 g / m 2 , for example, it can be 2.5g / m 2 , 3g / m 2 3.5g / m 2 , 4g / m 2 or 4.5g / m 2 wait.
[0032] Preferably, the compounding in step (2) is followed by a standing treatment.
[0033] In the present invention, the middle layer is compounded with the cellulose fiber layers on both sides and then left to stand for a static treatment, so that the layers can be better cross-linked and cured, ensuring that the product will not be delaminated or lint-shed.
[0034] Preferably, the standing temperature is 30-40°C, for example, 31°C, 33°C, 35°C, 37°C or 39°C.
[0035] Preferably, the standing time is 5-10 h, for example, 5 h, 6 h, 7 h, 8 h, 9 h or 10 h.
[0036] Other specific point values within the above numerical ranges can be selected and will not be described in detail here.
[0037] In a third aspect, the present invention provides a use of the non-irritating, lifting, and firming facial mask cloth as described in the first aspect in preparing a facial mask.
[0038] Compared with the prior art, the present invention has the following beneficial effects:
[0039] (1) The present invention uses PU fiber as the elastic middle layer and cellulose fiber layers on both sides, wherein the middle layer has good elasticity. After being made into a membrane cloth, it can provide good elasticity. The cellulose fiber layer can be made very soft by controlling the fineness. The surface of the prepared membrane cloth is very delicate and soft, and can provide a good skin feel. Since the cellulose fiber layer is in contact with the skin, the final mask cloth is very friendly to the skin, has no irritation, and is safer and gentler.
[0040] (2) The present invention uses processes such as spunlace and compounding to make the structure of the mask cloth more stable, and it is not easy to deform or shift when it fits the skin. In addition, by punching the middle layer, it can ensure that the mask liquid in the mask can better infiltrate the entire mask cloth. DETAILED DESCRIPTION
[0041] In order to further explain the technical means and effects adopted by the present invention, the technical solution of the present invention is further described below in conjunction with the preferred embodiments of the present invention, but the present invention is not limited to the scope of the embodiments.
[0042] The raw materials involved in the following examples and comparative examples can be used as long as they are purchased from regular dealers.
[0043] Example 1
[0044] This embodiment provides a non-irritating, lifting and firming facial mask cloth, which comprises a cellulose fiber surface layer, an elastic middle layer and a cellulose fiber bottom layer stacked in sequence;
[0045] The material of the cellulose fiber surface layer is lyocell fiber, with a fineness of 0.8 dtex and a length of 45 mm; the transverse distribution fiber accounts for 30%, and the longitudinal distribution fiber accounts for 70%; the fiber weight is 15 g / m 2 ;
[0046] The material of the cellulose fiber bottom layer is lyocell fiber, with a fineness of 0.8 dtex and a length of 45 mm; the transverse distribution fiber accounts for 30%, and the longitudinal distribution fiber accounts for 70%; the fiber weight is 15 g / m 2 ;
[0047] The elastic middle layer is made of micron-grade PU fiber; the gram weight is 12g / m 2 .
[0048] The preparation method of the facial mask cloth is:
[0049] (1) combing lyocell fibers and then subjecting them to a spunlacing process, wherein the spunlacing process comprises six spunlacing steps, wherein the pressure of the first to second spunlacing steps is independently 1 MPa; the pressure of the third to sixth spunlacing steps is 2.5 MPa, and then drying at 135° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0050] (2) Punch holes in the elastic middle layer, and then apply PUR hot melt adhesive (3 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 35° C. for 8 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0051] Example 2
[0052] This embodiment provides a non-irritating, lifting and firming facial mask cloth, which comprises a cellulose fiber surface layer, an elastic middle layer and a cellulose fiber bottom layer stacked in sequence;
[0053] The material of the cellulose fiber surface layer is viscose fiber, with a fineness of 1 dtex and a length of 40 mm; the transverse distribution fiber accounts for 40%, and the longitudinal distribution fiber accounts for 60%; the fiber weight is 20 g / m 2 ;
[0054] The material of the cellulose fiber bottom layer is viscose fiber, with a fineness of 1 dtex and a length of 40 mm; the transverse distribution fiber accounts for 40%, and the longitudinal distribution fiber accounts for 60%; the fiber weight is 20 g / m 2 ;
[0055] The material of the elastic middle layer is micron-grade PU fiber; the gram weight is 10g / m 2 .
[0056] The preparation method of the facial mask cloth is:
[0057] (1) combing the viscose fibers and then subjecting them to a spunlace process, wherein the spunlace process comprises six spunlace steps, wherein the pressure of the first to second spunlace steps is independently 0.8 MPa; the pressure of the third to sixth spunlace steps is 3 MPa, and then drying at 140° C. for 5 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0058] (2) Punch holes in the elastic middle layer, and then use PUR hot melt adhesive (5 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 40° C. for 5 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0059] Example 3
[0060] This embodiment provides a non-irritating, lifting and firming facial mask cloth, which comprises a cellulose fiber surface layer, an elastic middle layer and a cellulose fiber bottom layer stacked in sequence;
[0061] The material of the cellulose fiber surface layer is cuprammonium fiber, with a fineness of 0.5 dtex and a length of 500 mm; the transverse distribution fiber accounts for 20%, and the longitudinal distribution fiber accounts for 80%; the fiber weight is 10 g / m 2 ;
[0062] The material of the cellulose fiber bottom layer is cuprammonium fiber, with a fineness of 0.5 dtex and a length of 500 mm; the transverse distribution fiber accounts for 20%, and the longitudinal distribution fiber accounts for 80%; the fiber weight is 10 g / m 2 ;
[0063] The elastic middle layer is made of micron-grade PU fiber; the gram weight is 15g / m 2 .
[0064] The preparation method of the facial mask cloth is:
[0065] (1) combing the cuprammonium fiber and then subjecting it to a spunlacing process, wherein the spunlacing process includes six spunlacing steps, wherein the pressure of the first to second spunlacing steps is independently 1.2 MPa; the pressure of the third to sixth spunlacing steps is 2 MPa, and then drying at 130° C. for 15 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0066] (2) Punch holes in the elastic middle layer, and then use PUR hot melt adhesive (2 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 30° C. for 10 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0067] Example 4
[0068] The present embodiment provides a non-irritating, lifting, and firming facial mask cloth. The facial mask cloth differs from that of Embodiment 1 only in that the transversely distributed fibers in the cellulose fiber surface layer and the bottom layer each account for 50%, and the longitudinally distributed fibers each account for 50%. The remaining structures and features are consistent with those of Embodiment 1, and the preparation method refers to that of Embodiment 1.
[0069] Example 5
[0070] The present embodiment provides a non-irritating, lifting, and firming facial mask cloth. The facial mask cloth differs from that of Example 1 only in that the transversely distributed fibers in the cellulose fiber surface layer and the bottom layer account for 90% and the longitudinally distributed fibers account for 10%. The remaining structures and features are consistent with those of Example 1, and the preparation method refers to that of Example 1.
[0071] Example 6
[0072] This embodiment provides a non-irritating, lifting, and firming facial mask cloth, the difference between the facial mask cloth and embodiment 1 is only that the preparation method is:
[0073] (1) combing lyocell fibers and then subjecting them to a spunlace process, wherein the spunlace process comprises five spunlace steps, wherein the pressure of the first to second spunlace steps is independently 1 MPa; the pressure of the third to fifth spunlace steps is 2.5 MPa, and then drying at 135° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0074] (2) Punch holes in the elastic middle layer, and then apply PUR hot melt adhesive (3 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 35° C. for 8 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0075] Example 7
[0076] This embodiment provides a non-irritating, lifting, and firming facial mask cloth, the difference between the facial mask cloth and embodiment 1 is only that the preparation method is:
[0077] (1) combing lyocell fibers and then subjecting them to a spunlace process, wherein the spunlace process comprises seven spunlace steps, wherein the pressure of the first to second spunlace steps is independently 1 MPa; the pressure of the third to seventh spunlace steps is 2.5 MPa, and then drying at 135° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0078] (2) Punch holes in the elastic middle layer, and then apply PUR hot melt adhesive (3 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 35° C. for 8 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0079] Example 8
[0080] This embodiment provides a non-irritating, lifting, and firming facial mask cloth, the difference between the facial mask cloth and embodiment 1 is only that the preparation method is:
[0081] (1) combing lyocell fibers and then subjecting them to a spunlace process, wherein the spunlace process comprises six spunlace steps, wherein the pressure of the first to sixth spunlace steps is independently 1 MPa, and then drying at 135° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0082] (2) Punch holes in the elastic middle layer, and then apply PUR hot melt adhesive (3 g / m2) on the upper and lower surfaces of the elastic middle layer. 2) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 35° C. for 8 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0083] Example 9
[0084] This embodiment provides a non-irritating, lifting, and firming facial mask cloth, the difference between the facial mask cloth and embodiment 1 is only that the preparation method is:
[0085] (1) combing lyocell fibers and then subjecting them to a spunlace process, wherein the spunlace process comprises six spunlace steps, wherein the pressure of the first to sixth spunlace steps is independently 2.5 MPa, and then drying at 135° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0086] Since the pressure of 1-2 water pressures is too high, the fibers cannot form a uniform fiber web under the impact of the water pressure, resulting in more holes and unable to form qualified non-woven fabric products.
[0087] Example 10
[0088] This embodiment provides a non-irritating, lifting, and firming facial mask cloth, the difference between the facial mask cloth and embodiment 1 is only that the preparation method is:
[0089] (1) combing lyocell fibers and then subjecting them to a spunlace process, wherein the spunlace process comprises six spunlace steps, wherein the pressure of the first to second spunlace steps is independently 1 MPa; the pressure of the third to sixth spunlace steps is 4 MPa, and then drying at 135° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0090] (2) Punch holes in the elastic middle layer, and then apply PUR hot melt adhesive (3 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 35° C. for 8 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0091] Embodiment 11
[0092] This embodiment provides a non-irritating, lifting, and firming facial mask cloth, the difference between the facial mask cloth and embodiment 1 is only that the preparation method is:
[0093] (1) combing lyocell fibers and then subjecting them to a spunlace process, wherein the spunlace process comprises six spunlace steps, wherein the pressure of the first to second spunlace steps is independently 1 MPa; the pressure of the third to sixth spunlace steps is 2.5 MPa, and then drying at 120° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0094] (2) Punch holes in the elastic middle layer, and then apply PUR hot melt adhesive (3 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 35° C. for 8 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0095] Example 12
[0096] This embodiment provides a non-irritating, lifting, and firming facial mask cloth, the difference between the facial mask cloth and embodiment 1 is only that the preparation method is:
[0097] (1) combing lyocell fibers and then subjecting them to a spunlace process, wherein the spunlace process comprises six spunlace steps, wherein the pressure of the first to second spunlace steps is independently 1 MPa; the pressure of the third to sixth spunlace steps is 2.5 MPa, and then drying at 150° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0098] (2) Punch holes in the elastic middle layer, and then apply PUR hot melt adhesive (3 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 35° C. for 8 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0099] Example 13
[0100] This embodiment provides a non-irritating, lifting, and firming facial mask cloth, the difference between the facial mask cloth and embodiment 1 is only that the preparation method is:
[0101] (1) combing lyocell fibers and then subjecting them to a spunlacing process, wherein the spunlacing process comprises six spunlacing steps, wherein the pressure of the first to second spunlacing steps is independently 1 MPa; the pressure of the third to sixth spunlacing steps is 2.5 MPa, and then drying at 135° C. for 10 minutes to obtain a cellulose fiber surface layer and a bottom layer;
[0102] (2) Use PUR hot melt adhesive (3 g / m2) on the upper and lower surfaces of the elastic middle layer. 2 ) is compounded with a cellulose fiber surface layer and a bottom layer, and then allowed to stand at 35° C. for 8 hours to obtain the non-irritating, lifting and firming facial mask cloth.
[0103] Comparative Example 1
[0104] This comparative example provides a non-irritating, lifting and firming facial mask cloth. The facial mask cloth is different from Example 1 only in that the material of the elastic middle layer is wood pulp fiber, and the rest of the structure and features are consistent with Example 1. The preparation method refers to Example 1.
[0105] Comparative Example 2
[0106] This comparative example provides a non-irritating, lifting and firming facial mask cloth. The difference between the facial mask cloth and Example 1 is that the materials of the cellulose fiber surface layer and the bottom layer are respectively replaced by fine-denier viscose microfibers with PU fibers. The rest of the structure and characteristics are consistent with Example 1, and the preparation method refers to Example 1.
[0107] Comparative Example 3
[0108] This comparative example provides a non-irritating, lifting and firming facial mask cloth. The facial mask cloth is different from Example 1 only in that the fineness of the lyocell fiber is 0.3 dtex, and the rest of the structure and features are consistent with Example 1. The preparation method refers to Example 1.
[0109] Comparative Example 4
[0110] This comparative example provides a non-irritating, lifting and firming facial mask cloth. The facial mask cloth is different from Example 1 only in that the fineness of the lyocell fiber is 1.5 dtex, and the rest of the structure and features are consistent with Example 1. The preparation method refers to Example 1.
[0111] Test Example 1
[0112] The mask cloths of Examples 1-8, 10-13 and Comparative Examples 1-4 were immersed in water for 20 seconds, and then hung in the air to observe whether there was dripping, and then naturally air-dried to observe whether there was delamination or fuzzing. The results are shown in Table 1.
[0113] Table 1
[0114] Experience Is there any dripping phenomenon? Whether it is layered or fluffy Example 1 no no Example 2 no no Example 3 no no Example 4 no no Example 5 no no Example 6 no no Example 7 yes no Example 8 no yes Example 10 no no Embodiment 11 yes no Example 12 no no Example 13 yes no Comparative Example 1 no no Comparative Example 2 yes no Comparative Example 3 no no Comparative Example 4 no no
[0115] It can be seen from Table 1 that the facial mask cloth prepared by the present invention has good liquid absorption, and through a specific process, the layers will not be delaminated, and there will be no linting or linting.
[0116] Test Example 2
[0117] The mask cloths of Examples 1-8, 10-13 and Comparative Examples 1-4 were soaked in water for 20 seconds, and then 102 volunteers were selected and randomly divided into 17 groups, with 6 people in each group, and the products after the above treatment were tried for 30 minutes, and then sensory evaluation was performed on the softness of the fit, lifting and firming effect, and irritation (the higher the score, the less irritation), using a 5-point system: 4.5 points and above, indicating very good, very satisfactory; 4-4.5 points are good; 3-4 points are moderately acceptable; 3 points or less are not good, unacceptable. The scores of each group are the average values, and the results are shown in Table 2.
[0118] Table 2
[0119]
[0120]
[0121] According to Table 2, the facial mask cloths prepared in Examples 1-3 of the present invention have excellent softness and fit, and have a lifting and firming effect, and do not cause any irritation after use.
[0122] From Examples 6-10, it can be seen that the number of passes and pressure in the spunlace process will affect the softness and lifting and firming effect of the mask cloth;
[0123] It can be seen from Examples 11-12 that the film cloth cannot be completely dried at the drying temperature during the preparation process. When the temperature is too high, the film cloth is too hard, which will affect the skin feel of the mask cloth.
[0124] It can be seen from Comparative Example 1 that when the middle layer is not the PU fiber specified in the present invention, the elasticity of the mask cloth is poor, thereby affecting the lifting and firming effect;
[0125] It can be seen from Comparative Example 2 that when the cellulose layer fiber is PU fiber, the mask cloth is more irritating and the volunteers have a poor experience after using it;
[0126] It can be seen from Comparative Example 4 that when the adsorption of the cellulose fiber layer is greater, the softness and conformability of the mask cloth are poor.
[0127] The applicant declares that the present invention uses the above-mentioned embodiments to illustrate a non-irritating, lifting, and firming facial mask cloth and its preparation method and application, but the present invention is not limited to the above-mentioned embodiments, that is, it does not mean that the present invention must rely on the above-mentioned embodiments to be implemented. Those skilled in the art should understand that any improvement of the present invention, equivalent replacement of the raw materials of the product of the present invention, addition of auxiliary components, selection of specific methods, etc., all fall within the protection scope and disclosure scope of the present invention.
[0128] The preferred embodiments of the present invention are described in detail above. However, the present invention is not limited to the specific details in the above embodiments. Within the technical concept of the present invention, a variety of simple modifications can be made to the technical solution of the present invention, and these simple modifications all belong to the protection scope of the present invention.
[0129] It should also be noted that the various specific technical features described in the above specific embodiments can be combined in any suitable manner without contradiction. In order to avoid unnecessary repetition, the present invention will not further describe various possible combinations.
Claims
1. A non-irritating, lifting and firming facial mask cloth, characterized in that: The facial mask cloth comprises a cellulose fiber surface layer, an elastic middle layer and a cellulose fiber bottom layer which are stacked in sequence; The materials of the cellulose fiber surface layer and the cellulose fiber bottom layer are both fine-denier viscose fibers with a fineness of 0.5dtex-1.0dtex and a length of 38-52mm; The material of the elastic middle layer is PU fiber.
2. The non-irritating, lifting and firming facial mask cloth according to claim 1, characterized in that: The fine denier viscose fiber includes any one of lyocell fiber, viscose fiber or cuprammonium fiber or a combination of at least two thereof; Preferably, the fineness of the PU fiber is at the micron level.
3. The non-irritating, lifting and firming facial mask cloth according to claim 1 or 2, characterized in that: The longitudinally distributed fibers in the cellulose fiber surface layer and the cellulose fiber bottom layer each independently account for 60%-80%, and the transversely distributed fibers each independently account for 20%-40%.
4. The non-irritating, lifting and firming facial mask cloth according to any one of claims 1 to 3, characterized in that: The gram weights of the cellulose fiber surface layer and the cellulose fiber bottom layer are independently 10-20 g / m 2 ; Preferably, the elastic middle layer has a grammage of 8-15 g / m 2 .
5. The method for preparing the non-irritating, lifting and firming facial mask cloth according to any one of claims 1 to 4, characterized in that: The preparation method comprises: (1) Using fine denier viscose fiber as raw material, preparing a cellulose fiber surface layer and a cellulose fiber bottom layer by carding and spunlace process; The elastic middle layer is perforated; (2) The upper and lower surfaces of the elastic middle layer are respectively compounded with the cellulose fiber surface layer and the cellulose fiber bottom layer using an adhesive to obtain the non-irritating, lifting and firming facial mask cloth.
6. The preparation method according to claim 5, characterized in that: The spunlacing process in step (1) is performed through six spunlacing steps; Preferably, the pressures of the first and second hydroentanglement processes are independently 0.5-1.5 MPa; Preferably, the pressure of the third to sixth hydroentanglement processes is 2-3 MPa.
7. The preparation method according to claim 5 or 6, characterized in that: After the spunlacing process in step (1), drying is performed; Preferably, the drying temperature is 130-140° C. and the drying time is 5-15 min.
8. The preparation method according to any one of claims 5 to 7, characterized in that: The adhesive in step (2) is PUR hot melt adhesive; Preferably, the amount of the adhesive is 2-5 g / m 2 .
9. The preparation method according to any one of claims 5 to 8, characterized in that: After the compounding in step (2), the step of standing still is performed; Preferably, the standing temperature is 30-40°C; Preferably, the standing time is 5-10 hours.
10. Use of the non-irritating, lifting and firming facial mask cloth according to any one of claims 1 to 4 in preparing a facial mask.
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