Collagen firming, anti-wrinkle and anti-aging mask and preparation method thereof

Abstract

The invention provides a collagen-containing composition which comprises the following components in parts by weight: 15-30 parts of a collagen mixture, 10-20 parts of a plant extract, 2-4 parts of a vitamin mixture, 1-3 parts of D ribose and 3-7 parts of glucosamine, the collagen mixture is fish scale collagen, deer collagen and bovine bone collagen; the plant extract is an ethanol extract obtained by mixing rhizoma phragmitis, cherries, grapes, liriodendron tulipifera, blueberries, caulis sinomenii and sagittaria sagittifolia; the vitamin mixture is a mixture of vitamin B, vitamin C and vitamin E; when the composition is applied to food, the effects of obviously improving skin and resisting aging can be achieved.

Description

Technical Field

[0001] The present invention relates to the technical field of facial mask preparation, and in particular to a collagen firming, anti-wrinkle and anti-aging facial mask and a preparation method thereof. Background Art

[0002] Affected by the current environment, air quality, and the popularity of makeup, consumers' demand for cleaning products, especially cleansing masks, is gradually increasing. At the same time, with the increase of age, the synthesis capacity of fibroblasts in the skin decreases, collagen fibers are cross-linked, and the intercellular mucopolysaccharide decreases, and the skin loses elasticity and luster. At the same time, due to factors such as fiber breakage in the dermis, fat atrophy, and reduced secretion of sweat glands and sebaceous glands, the skin is prone to a series of aging phenomena such as spots and wrinkles.

[0003] A facial mask is a product that can achieve cleansing, moisturizing, repairing and beautifying effects by applying it to the face. Applying a facial mask is the most direct way to achieve beauty and skin care, and it has the effects of whitening, moisturizing, promoting circulation, and tightening the skin. As a carrier of beauty and skin care products, applying a facial mask to the face and other parts can isolate the facial skin from the air, increase the temperature of the skin surface, speed up the blood circulation of the face, open the pores, speed up the secretion of sweat glands, promote the discharge of waste, and play a role in cleaning cells. At the same time, the beauty and skin care substances in the mask penetrate into the skin, bring more nutrients to the skin, nourish the deep cells of the skin, delay skin aging, inhibit the formation of wrinkles, and achieve a whitening effect. When the mask is applied to the face, the moisture in the mask will penetrate into the surface cells of the skin, allowing the skin to fully absorb moisture and achieve a moisturizing effect. When the mask is applied to the face, the facial cells will become larger in size after fully absorbing moisture, making the skin shiny. At the same time, the pores will shrink, which will tighten the skin moderately, produce a sense of tightness, and the skin will be tightened and contracted, wrinkles will become lighter and lighter, and the skin will become more elastic.

[0004] However, some facial masks on the market have relatively simple functions and are only effective in one aspect such as anti-aging or whitening, but their performance in many aspects is not ideal. Summary of the invention

[0005] The purpose of the present invention is to provide a collagen firming, anti-wrinkle and anti-aging facial mask and a preparation method thereof, and to obtain a facial mask product with firming, anti-wrinkle and anti-aging effects by using main ingredients such as hydrolyzed collagen, moisturizers, anti-wrinkle agents, anti-aging agents, thickeners, etc.

[0006] In order to achieve the above object, the present invention provides the following technical solutions: A collagen firming, anti-wrinkle and anti-aging facial mask comprises the following components in parts by weight: 15-25 parts of hydrolyzed collagen, 70-90 parts of deionized water, 1-3 parts of moisturizing agent, 3-6 parts of anti-wrinkle agent, 2-6 parts of anti-aging agent, 0.5-2.5 parts of thickening agent, 0.1-0.3 parts of pH adjusting agent, 0.1-0.3 parts of chelating agent, 1.5-2.5 parts of non-ionic surfactant, 0.1-0.3 parts of fragrance, 0.2-0.5 parts of emulsifier and 0.1-0.3 parts of penetrant.

[0007] Furthermore, the moisturizing agent is composed of the following components in parts by weight: 0.2-0.5 parts of methylpropanediol, 0.1-0.3 parts of erythritol, 0.3-0.6 parts of 1,2-hexanediol, 0.1-0.3 parts of betaine, 0.2-0.4 parts of butylene glycol and 0.5-1 parts of glycerol.

[0008] Furthermore, the anti-wrinkle agent is composed of the following components by weight: 4-7 parts of Chondrus crispus extract, 0.5-1.5 parts of acetyl hexapeptide-8, 0.6-1.3 parts of acetyl octapeptide-3, 0.8-1.6 parts of acetyl heptapeptide-4 and 0.5-1 parts of acetyl tetrapeptide-2.

[0009] Furthermore, the anti-aging agent is composed of the following parts by weight: 1-3 parts of peony root extract, 2-5 parts of lactobacillus / soybean fermentation product extract, 1-3 parts of ginkgo biloba leaf extract, 0.5-2.5 parts of Imperata cylindrica root extract, 0.1-0.3 parts of α-arbutin, 0.2-0.5 parts of niacinamide, 0.1-0.3 parts of 3-o-ethyl ascorbic acid, 0.2-0.4 parts of tocopherol acetate, 0.5-1.5 parts of yeast lysate and 0.3-0.5 parts of palmitoyl tripeptide-5.

[0010] Furthermore, the thickener is one or a mixture of carbomer, xanthan gum, and acrylamide / sodium acryloyldimethyl taurate copolymer; the pH adjuster is one or a mixture of tromethamine, ammonium sulfate, disodium succinate, and sodium sulfate; the chelating agent is disodium EDTA; the nonionic surfactant is one or a mixture of PEG / PPG-17 / 6 copolymer, PPG-5-cetyl alcohol polyether-20, and coconut oil grape glycoside; the fragrance is p-hydroxyacetophenone or daily fragrance; the emulsifier is polyglycerol-4 oleate; and the penetrant is isononyl isononanoate.

[0011] A method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask comprises the following steps: S1: preparing Chondrus crispus extract, Paeonia lactiflora root extract, Lactobacillus / soybean fermentation product extract, Ginkgo biloba leaf extract, and Imperata cylindrica root extract respectively; S2: Add 0.2-0.5 parts of methylpropanediol, 0.1-0.3 parts of erythritol, 0.3-0.6 parts of 1,2-hexanediol, 0.1-0.3 parts of betaine, 0.2-0.4 parts of butanediol and 0.5-1 parts of glycerol into a reaction kettle, stir and mix at a temperature of 70-80° C. and a speed of 600-700 r / min for 20-40 minutes to obtain a moisturizer; S3: adding 4-7 parts of Chondrus crispus extract, 0.5-1.5 parts of acetyl hexapeptide-8, 0.6-1.3 parts of acetyl octapeptide-3, 0.8-1.6 parts of acetyl heptapeptide-4 and 0.5-1 parts of acetyl tetrapeptide-2 into a reaction kettle, stirring and mixing at a temperature of 80-100° C. and a speed of 500-600 r / min for 30-50 minutes to obtain an anti-wrinkle agent; S4: 1-3 parts of peony root extract, 2-5 parts of lactobacillus / soybean fermentation product extract, 1-3 parts of ginkgo biloba leaf extract, 0.5-2.5 parts of Imperata cylindrica root extract, 0.1-0.3 parts of α-arbutin, 0.2-0.5 parts of niacinamide, 0.1-0.3 parts of 3-o-ethyl ascorbic acid, 0.2-0.4 parts of tocopherol acetate, 0.5-1.5 parts of yeast lysate and 0.3-0.5 parts of palmitoyl tripeptide-5 are added into a reaction kettle, and the mixture is stirred and mixed at a temperature of 95-105° C. and a speed of 450-550 r / min for 35-55 minutes to obtain an anti-aging agent; S5: Add 15-25 parts of hydrolyzed collagen, 70-90 parts of deionized water, 1-3 parts of moisturizer, 3-6 parts of anti-wrinkle agent, 2-6 parts of anti-aging agent, 0.5-2.5 parts of thickener, 0.1-0.3 parts of pH adjuster, 0.1-0.3 parts of chelating agent, 1.5-2.5 parts of non-ionic surfactant, 0.1-0.3 parts of fragrance, 0.2-0.5 parts of emulsifier and 0.1-0.3 parts of penetrant into a reactor, stir and mix at a temperature of 40-60°C and a speed of 1000-1200r / min for 45-65min, and obtain a collagen firming, anti-wrinkle and anti-aging facial mask after sterilization and cooling.

[0012] Furthermore, the preparation method of the Chondrus crispus extract in step S1 is: adding Chondrus crispus to an ethanol solution according to a solid-liquid ratio of 1g:10ml, extracting in a constant temperature shaking water bath at 30°C for 60min, transferring to a centrifuge tube for centrifugation, and collecting the supernatant to obtain the Chondrus crispus extract.

[0013] Furthermore, the preparation method of the peony root extract in step S1 is: placing the peony root powder in a Soxhlet extractor at a solid-liquid ratio of 1g:15ml, and continuously refluxing with petroleum ether at a temperature of 120°C for 2.5h to obtain the peony root extract.

[0014] Furthermore, the preparation method of the Ginkgo biloba parasitic leaf extract in step S1 is: take dried Ginkgo biloba parasitic leaves and add ethanol according to a solid-liquid ratio of 1g:20ml, reflux with water at a temperature of 90°C for 1.5 hours, extract twice continuously, collect the filtrate after filtering, and then concentrate and remove alcohol using a rotary evaporator to obtain the Ginkgo biloba parasitic leaf extract.

[0015] Furthermore, the preparation method of the Imperata root extract in step S1 is: dice the Imperata root, extract it using supercritical CO2 fluid, control the extraction pressure to 25MPa, the extraction temperature to 45°C, the static extraction time to 40min, and the dynamic extraction time to 25min.

[0016] Chondrus crispus, also known as Irish moss, is a red algae that grows on rocks along the Atlantic coast. Chondrus crispus can promote the synthesis of collagen and elastic fibers in the skin, improve skin firmness and elasticity, reduce the formation of fine lines and wrinkles, and make the skin look younger; inhibit melanin formation: some ingredients can interfere with the synthesis process of melanin, reduce the production of melanin, and help whiten the skin; rich in antioxidants, such as vitamins C and E, which help to remove free radicals and protect skin cells from oxidative damage.

[0017] Peony root extract is derived from the root of peony, a natural herbal ingredient with a long history in traditional Chinese medicine. Peony is mainly distributed in some parts of Asia and Europe, and is famous for its beautiful flowers and medicinal value. Peony root extract has also been widely used in cosmetics and personal care products due to its various bioactive ingredients. Peony root contains active ingredients such as paeoniflorin, which has a good anti-inflammatory effect and can help relieve skin inflammation, reduce symptoms such as redness, swelling and pain; Peony root extract is rich in antioxidants, which can effectively fight free radicals, prevent free radicals from damaging skin cells, and slow down the aging process of the skin; Promote blood circulation: Peony root extract can also promote skin microcirculation and improve the problem of dull complexion caused by poor blood circulation.

[0018] Lactobacillus / soy fermented product extract is a multifunctional cosmetic raw material that combines probiotic technology and natural plant ingredients. This ingredient is extracted by fermenting soybeans with lactobacillus. It not only inherits the nutrients of soybeans themselves, but also produces a variety of new substances that are beneficial to the skin through the fermentation process. Antioxidants produced during the fermentation process, such as polyphenols, can effectively resist free radicals, reduce the damage of free radicals to skin cells, delay the aging process of the skin, and reduce the occurrence of fine lines and wrinkles. By supplementing beneficial bacteria, it helps restore the healthy balance of the microbial community on the surface of the skin, inhibits the growth of harmful bacteria, and prevents the occurrence of skin problems.

[0019] Viscum album leaf extract, also known as mistletoe leaf extract, is a natural plant ingredient extracted from the leaves of mistletoe. Mistletoe is a parasitic plant that is commonly found on trees in Europe and Asia, especially on apple trees, pear trees and oak trees. Viscum album leaf extract is rich in a variety of antioxidant ingredients, such as flavonoids and polyphenols, which can effectively scavenge free radicals, reduce the damage of free radicals to skin cells, and delay the aging process of the skin. The extract can help the skin lock in moisture, improve the skin's moisture and elasticity, and make the skin look smoother and more delicate.

[0020] Imperata root extract is a natural plant ingredient extracted from the root of Imperata cylindrica. Imperata cylindrica is a perennial herb widely distributed in tropical and temperate regions of Asia, Africa and America. In traditional medicine, Imperata cylindrica root is used for a variety of purposes such as clearing away heat and detoxification, diuresis and swelling reduction. In recent years, Imperata cylindrica root extract has also been widely used in skin care products because of its various beneficial effects on the skin. Imperata cylindrica root extract has good anti-inflammatory and soothing effects, which can help relieve skin inflammation, reduce redness, swelling, itching and other discomfort symptoms, and is suitable for sensitive skin. Imperata cylindrica root extract is rich in a variety of antioxidant ingredients, such as flavonoids, polyphenols, etc., which can effectively scavenge free radicals and reduce the impact of free radicals on skin cells.

[0021] Compared with the prior art, the advantages and beneficial effects of the present invention are: The invention, under the synergistic effect of components such as Chondrus crispus extract, acetyl hexapeptide-8, acetyl octapeptide-3, acetyl heptapeptide-4, acetyl tetrapeptide-2, etc., stimulates the production of collagen and elastin in the skin, enhances the elasticity and firmness of the skin, thereby reducing the appearance of dynamic and static wrinkles; activates fibroblasts in the skin, promotes the synthesis of extracellular matrix, improves the structure and texture of the skin, and enhances the anti-wrinkle effect of the product; under the synergistic effect of peony root extract, lactobacillus / soybean fermentation product extract, α-arbutin, niacinamide, Ginkgo biloba leaf extract, 3-o-ethyl ascorbic acid, tocopherol acetate, Imperata root extract, yeast lysate, palmitoyl tripeptide-5, etc., effectively resists free radicals, reduces the damage of free radicals to skin cells, and delays the skin aging process; at the same time, supplemented with moisturizers, thickeners, pH regulators, nonionic surfactants, fragrances, etc., a collagen firming, anti-wrinkle and anti-aging facial mask with excellent effects is obtained. DETAILED DESCRIPTION

[0022] The technical solutions in the embodiments of the present invention are described clearly and completely below. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of them. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0023] Example 1 This embodiment provides a method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask, comprising the following steps: S1: adding Chondrus crispus to an ethanol solution at a solid-liquid ratio of 1 g:10 ml, extracting in a constant temperature shaking water bath at 30° C. for 60 min, transferring to a centrifuge tube, centrifuging, and collecting the supernatant to obtain a Chondrus crispus extract; The peony root powder was placed in a Soxhlet extractor at a solid-liquid ratio of 1g:15ml, and petroleum ether was used for continuous reflux at a temperature of 120°C for 2.5h to obtain a peony root extract; Take dried Ginkgo biloba parasitic leaves and add ethanol according to the solid-liquid ratio of 1g:20ml, reflux with water at a temperature of 90°C for 1.5 hours, extract twice continuously, collect the filtrate after filtration, and then concentrate and remove the alcohol with a rotary evaporator to obtain the Ginkgo biloba parasitic leaf extract; The Imperata root was diced and extracted with supercritical CO2 fluid, with the extraction pressure at 25 MPa, the extraction temperature at 45°C, the static extraction time at 40 min, and the dynamic extraction time at 25 min to obtain the Imperata root extract; S2: 0.2 g of methylpropanediol, 0.1 g of erythritol, 0.3 g of 1,2-hexanediol, 0.1 g of betaine, 0.2 g of butanediol and 0.5 g of glycerol were added into a reaction kettle, and the mixture was stirred at 70° C. and 600 r / min for 20 min to obtain a moisturizing agent; S3: 4 g of Chondrus crispus extract, 0.5 g of acetyl hexapeptide-8, 0.6 g of acetyl octapeptide-3, 0.8 g of acetyl heptapeptide-4 and 0.5 g of acetyl tetrapeptide-2 were added into a reaction kettle, and the mixture was stirred at 80° C. and 500 r / min for 30 min to obtain an anti-wrinkle agent; S4: 1 g of peony root extract, 2 g of lactobacillus / soybean fermentation product extract, 1 g of Ginkgo biloba leaf extract, 0.5 g of Imperata cylindrica root extract, 0.1 g of α-arbutin, 0.2 g of niacinamide, 0.1 g of 3-o-ethyl ascorbic acid, 0.2 g of tocopherol acetate, 0.5 g of yeast lysate and 0.3 g of palmitoyl tripeptide-5 were added to a reaction kettle, and the mixture was stirred at a temperature of 95° C. and a speed of 450 r / min for 35 min to obtain an anti-aging agent; S5: Add 15g hydrolyzed collagen, 70g deionized water, 1g moisturizer, 3g anti-wrinkle agent, 2g anti-aging agent, 0.5g carbomer, 0.1g pH adjuster ammonium sulfate, 0.1g chelating agent disodium EDTA, 1.5g non-ionic surfactant PEG / PPG-17 / 6 copolymer, 0.1g fragrance p-hydroxyacetophenone, 0.2g emulsifier polyglycerol-4 oleate, and 0.1g penetrant isononyl isononanoate into a reactor, stir and mix at a temperature of 40°C and a speed of 1000r / min for 45min, sterilize at 120°C, and cool to obtain a collagen firming, anti-wrinkle, and anti-aging facial mask.

[0024] Example 2 This embodiment provides a method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask, comprising the following steps: S1: adding Chondrus crispus to an ethanol solution at a solid-liquid ratio of 1 g:10 ml, extracting in a constant temperature shaking water bath at 30° C. for 60 min, transferring to a centrifuge tube, centrifuging, and collecting the supernatant to obtain a Chondrus crispus extract; The peony root powder was placed in a Soxhlet extractor at a solid-liquid ratio of 1g:15ml, and petroleum ether was used for continuous reflux at a temperature of 120°C for 2.5h to obtain a peony root extract; Take dried Ginkgo biloba parasitic leaves and add ethanol according to the solid-liquid ratio of 1g:20ml, reflux with water at a temperature of 90°C for 1.5 hours, extract twice continuously, collect the filtrate after filtration, and then concentrate and remove the alcohol with a rotary evaporator to obtain the Ginkgo biloba parasitic leaf extract; The Imperata root was diced and extracted with supercritical CO2 fluid, with the extraction pressure at 25 MPa, the extraction temperature at 45°C, the static extraction time at 40 min, and the dynamic extraction time at 25 min to obtain the Imperata root extract; S2: 0.5 g of methyl propanediol, 0.3 g of erythritol, 0.6 g of 1,2-hexanediol, 0.3 g of betaine, 0.4 g of butanediol and 1 g of glycerol were added into a reaction kettle, and the mixture was stirred at a temperature of 80° C. and a speed of 700 r / min for 40 min to obtain a moisturizing agent; S3: 7 g of Chondrus crispus extract, 1.5 g of acetyl hexapeptide-8, 1.3 g of acetyl octapeptide-3, 1.6 g of acetyl heptapeptide-4 and 1 g of acetyl tetrapeptide-2 were added into a reaction kettle, and stirred and mixed at a temperature of 100° C. and a speed of 600 r / min for 50 min to obtain an anti-wrinkle agent; S4: 3g of peony root extract, 5g of lactobacillus / soybean fermentation product extract, 3g of ginkgo biloba leaf extract, 2.5g of Imperata cylindrica root extract, 0.3g of α-arbutin, 0.5g of niacinamide, 0.3g of 3-o-ethyl ascorbic acid, 0.4g of tocopherol acetate, 1.5g of yeast lysate and 0.5g of palmitoyl tripeptide-5 were added to a reaction kettle, and the mixture was stirred at a temperature of 105°C and a speed of 550r / min for 55min to obtain an anti-aging agent; S5: Add 25g hydrolyzed collagen, 90g deionized water, 3g moisturizer, 6g anti-wrinkle agent, 6g anti-aging agent, 2.5g xanthan gum, 0.3g pH adjuster disodium succinate, 0.3g chelating agent disodium EDTA, 2.5g non-ionic surfactant PPG-5-cetyl alcohol polyether-20, 0.3g fragrance daily fragrance, 0.5g emulsifier polyglycerol-4 oleate, 0.3g penetrant isononyl isononanoate into a reactor, stir and mix at a temperature of 60°C and a speed of 1200r / min for 65min, sterilize at 120°C, and cool to obtain a collagen firming, anti-wrinkle and anti-aging facial mask.

[0025] Example 3 This embodiment provides a method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask, comprising the following steps: S1: adding Chondrus crispus to an ethanol solution at a solid-liquid ratio of 1 g:10 ml, extracting in a constant temperature shaking water bath at 30° C. for 60 min, transferring to a centrifuge tube, centrifuging, and collecting the supernatant to obtain a Chondrus crispus extract; The peony root powder was placed in a Soxhlet extractor at a solid-liquid ratio of 1g:15ml, and petroleum ether was used for continuous reflux at a temperature of 120°C for 2.5h to obtain a peony root extract; Take dried Ginkgo biloba parasitic leaves and add ethanol according to the solid-liquid ratio of 1g:20ml, reflux with water at a temperature of 90°C for 1.5 hours, extract twice continuously, collect the filtrate after filtration, and then concentrate and remove the alcohol with a rotary evaporator to obtain the Ginkgo biloba parasitic leaf extract; The Imperata root was diced and extracted with supercritical CO2 fluid, with the extraction pressure at 25 MPa, the extraction temperature at 45°C, the static extraction time at 40 min, and the dynamic extraction time at 25 min to obtain the Imperata root extract; S2: 0.4 g of methylpropanediol, 0.2 g of erythritol, 0.5 g of 1,2-hexanediol, 0.2 g of betaine, 0.3 g of butanediol and 0.7 g of glycerol were added into a reaction kettle, and the mixture was stirred at a temperature of 76° C. and a speed of 650 r / min for 35 min to obtain a moisturizing agent; S3: 5 g of Chondrus crispus extract, 1.2 g of acetyl hexapeptide-8, 1 g of acetyl octapeptide-3, 1.3 g of acetyl heptapeptide-4 and 0.8 g of acetyl tetrapeptide-2 were added into a reaction kettle, and stirred at a temperature of 95° C. and a speed of 550 r / min for 35 min to obtain an anti-wrinkle agent; S4: 2g of peony root extract, 4g of lactobacillus / soybean fermentation product extract, 2g of ginkgo biloba leaf extract, 2g of Imperata cylindrica root extract, 0.2g of α-arbutin, 0.4g of niacinamide, 0.2g of 3-o-ethyl ascorbic acid, 0.3g of tocopherol acetate, 1g of yeast lysate and 0.4g of palmitoyl tripeptide-5 were added to a reaction kettle, and the mixture was stirred at a temperature of 100°C and a speed of 500r / min for 50min to obtain an anti-aging agent; S5: Add 20g hydrolyzed collagen, 80g deionized water, 2g moisturizer, 5g anti-wrinkle agent, 4g anti-aging agent, 2g carbomer, 0.2g pH adjuster tromethamine, 0.2g chelating agent disodium EDTA, 2g non-ionic surfactant coconut oil base glucoside, 0.2g fragrance daily fragrance, 0.4g emulsifier polyglycerol-4 oleate, 0.2g penetrant isononyl isononanoate into a reactor, stir and mix at a temperature of 50°C and a speed of 1100r / min for 55min, sterilize at 120°C, and cool to obtain a collagen firming, anti-wrinkle and anti-aging facial mask.

[0026] Comparative Example 1 The difference between this comparative example and Example 1 is that the extract of Chondrus crispus is missing in step S1, and the other steps are the same.

[0027] Comparative Example 2 The difference between this comparative example and Example 1 is that the peony root extract is missing in step S1, and the other steps are the same.

[0028] Comparative Example 3 The difference between this comparative example and Example 1 is that the extract of Ginkgo biloba leaves is missing in step S1, and the other steps are the same.

[0029] Comparative Example 4 The difference between this comparative example and Example 1 is that step S1 lacks Imperata cylindrica root extract, and the other steps are the same.

[0030] Performance Test: Anti-aging and anti-wrinkle test: A total of 120 volunteers were selected, and the products of each embodiment and comparative example were used respectively. The test sites were the cheeks and eye corners on both sides, and the products were used twice a day after cleansing. The MicroSkinII multifunctional dermatoscope image analysis system was used to measure the changes in the average skin roughness and average wrinkle depth values ​​1 day before using the cosmetics, and 7d, 14d, 21d, and 28d after use, as shown in Table 1.

[0031]

[0032] It can be seen from the above performance test results that Examples 1-3 have good anti-aging and anti-wrinkle performance. In particular, the comprehensive performance of Example 3 is the most outstanding. However, since Comparative Examples 1-4 do not adopt the necessary technical solutions, their corresponding performance tests are significantly worse than those of the Examples. The above experimental results further prove the importance of the technical solutions defined in the present invention for its technical effects.

[0033] The above is a preferred embodiment of the present invention. It should be pointed out that for ordinary technicians in this technical field, several improvements and modifications can be made without departing from the principles of the present invention. These improvements and modifications should also be regarded as the scope of protection of the present invention.

Claims

1. A collagen firming, anti-wrinkle and anti-aging facial mask, characterized in that: The invention comprises the following components in parts by weight: 15-25 parts of hydrolyzed collagen, 70-90 parts of deionized water, 1-3 parts of moisturizing agent, 3-6 parts of anti-wrinkle agent, 2-6 parts of anti-aging agent, 0.5-2.5 parts of thickening agent, 0.1-0.3 parts of pH adjusting agent, 0.1-0.3 parts of chelating agent, 1.5-2.5 parts of nonionic surfactant, 0.1-0.3 parts of fragrance, 0.2-0.5 parts of emulsifier and 0.1-0.3 parts of penetrant.

2. The collagen firming, anti-wrinkle and anti-aging facial mask according to claim 1, characterized in that: The moisturizing agent is composed of the following components in parts by weight: 0.2-0.5 parts of methylpropanediol, 0.1-0.3 parts of erythritol, 0.3-0.6 parts of 1,2-hexanediol, 0.1-0.3 parts of betaine, 0.2-0.4 parts of butylene glycol and 0.5-1 parts of glycerol.

3. The collagen firming, anti-wrinkle and anti-aging facial mask according to claim 1, characterized in that: The anti-wrinkle agent is composed of the following components by weight: 4-7 parts of Chondrus crispus extract, 0.5-1.5 parts of acetyl hexapeptide-8, 0.6-1.3 parts of acetyl octapeptide-3, 0.8-1.6 parts of acetyl heptapeptide-4 and 0.5-1 parts of acetyl tetrapeptide-2.

4. The collagen firming, anti-wrinkle and anti-aging facial mask according to claim 1, characterized in that: The anti-aging agent is composed of the following components in parts by weight: 1-3 parts of peony root extract, 2-5 parts of lactobacillus / soybean fermentation product extract, 1-3 parts of ginkgo biloba leaf extract, 0.5-2.5 parts of Imperata cylindrica root extract, 0.1-0.3 parts of α-arbutin, 0.2-0.5 parts of niacinamide, 0.1-0.3 parts of 3-o-ethyl ascorbic acid, 0.2-0.4 parts of tocopherol acetate, 0.5-1.5 parts of yeast lysate and 0.3-0.5 parts of palmitoyl tripeptide-5.

5. The collagen firming, anti-wrinkle and anti-aging facial mask according to claim 1, characterized in that: The thickener is one of carbomer, xanthan gum, and acrylamide / sodium acryloyldimethyl taurate copolymer or a mixture thereof; the pH adjuster is one of tromethamine, ammonium sulfate, disodium succinate, and sodium sulfate or a mixture thereof; the chelating agent is disodium EDTA; the nonionic surfactant is one of PEG / PPG-17 / 6 copolymer, PPG-5-cetoeth-20, and coconut oil-based glucoside or a mixture thereof; the fragrance is p-hydroxyacetophenone or daily fragrance; the emulsifier is polyglycerol-4 oleate; and the penetrant is isononyl isononanoate.

6. A method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask, characterized in that: The steps include: S1: preparing Chondrus crispus extract, Paeonia lactiflora root extract, Lactobacillus / soybean fermentation product extract, Ginkgo biloba leaf extract, and Imperata cylindrica root extract respectively; S2: Add 0.2-0.5 parts of methylpropanediol, 0.1-0.3 parts of erythritol, 0.3-0.6 parts of 1,2-hexanediol, 0.1-0.3 parts of betaine, 0.2-0.4 parts of butanediol and 0.5-1 parts of glycerol into a reaction kettle, stir and mix at a temperature of 70-80° C. and a speed of 600-700 r / min for 20-40 minutes to obtain a moisturizer; S3: adding 4-7 parts of Chondrus crispus extract, 0.5-1.5 parts of acetyl hexapeptide-8, 0.6-1.3 parts of acetyl octapeptide-3, 0.8-1.6 parts of acetyl heptapeptide-4 and 0.5-1 parts of acetyl tetrapeptide-2 into a reaction kettle, stirring and mixing at a temperature of 80-100° C. and a speed of 500-600 r / min for 30-50 minutes to obtain an anti-wrinkle agent; S4: 1-3 parts of peony root extract, 2-5 parts of lactobacillus / soybean fermentation product extract, 1-3 parts of ginkgo biloba leaf extract, 0.5-2.5 parts of Imperata cylindrica root extract, 0.1-0.3 parts of α-arbutin, 0.2-0.5 parts of niacinamide, 0.1-0.3 parts of 3-o-ethyl ascorbic acid, 0.2-0.4 parts of tocopherol acetate, 0.5-1.5 parts of yeast lysate and 0.3-0.5 parts of palmitoyl tripeptide-5 are added into a reaction kettle, and the mixture is stirred and mixed at a temperature of 95-105° C. and a speed of 450-550 r / min for 35-55 minutes to obtain an anti-aging agent; S5: Add 15-25 parts of hydrolyzed collagen, 70-90 parts of deionized water, 1-3 parts of moisturizer, 3-6 parts of anti-wrinkle agent, 2-6 parts of anti-aging agent, 0.5-2.5 parts of thickener, 0.1-0.3 parts of pH adjuster, 0.1-0.3 parts of chelating agent, 1.5-2.5 parts of non-ionic surfactant, 0.1-0.3 parts of fragrance, 0.2-0.5 parts of emulsifier and 0.1-0.3 parts of penetrant into a reactor, stir and mix at a temperature of 40-60°C and a speed of 1000-1200r / min for 45-65min, and obtain a collagen firming, anti-wrinkle and anti-aging facial mask after sterilization and cooling.

7. The method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask according to claim 6, characterized in that: The preparation method of the Chondrus crispus extract in step S1 is as follows: adding Chondrus crispus to an ethanol solution at a solid-liquid ratio of 1 g:10 ml, extracting in a constant temperature shaking water bath at 30° C. for 60 minutes, transferring the solution to a centrifuge tube for centrifugation, and collecting the supernatant to obtain the Chondrus crispus extract.

8. The method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask according to claim 6, characterized in that: The preparation method of the peony root extract in step S1 is as follows: placing peony root powder in a Soxhlet extractor at a solid-liquid ratio of 1g:15ml, and continuously refluxing with petroleum ether at a temperature of 120°C for 2.5h to obtain the peony root extract.

9. The method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask according to claim 6, characterized in that: The preparation method of the ginkgo biloba parasitic leaf extract in step S1 is as follows: take dried ginkgo biloba parasitic leaves and add ethanol according to a solid-liquid ratio of 1g:20ml, reflux with water at a temperature of 90°C for 1.5 hours, extract twice continuously, collect the filtrate after filtering, and then concentrate and remove alcohol using a rotary evaporator to obtain the ginkgo biloba parasitic leaf extract.

10. The method for preparing a collagen firming, anti-wrinkle and anti-aging facial mask according to claim 6, characterized in that: The preparation method of the Imperata root extract in step S1 is: dice the Imperata root, use supercritical CO2 fluid extraction, control the extraction pressure to 25MPa, the extraction temperature to 45°C, the static extraction time to 40min, and the dynamic extraction time to 25min.

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