A device and method for preparing mesoporous silica material with ultra-large opening

Abstract

The present invention discloses a preparation device and method of a mesoporous silica material with a super large opening, and relates to the technical field of material synthesis. The device comprises a tank body and a shell mechanism, wherein the tank body comprises a bottom tank mechanism, a main tank mechanism and a top cover mechanism, and the tank body carries a power mechanism, wherein the bottom tank mechanism comprises a bottom tank, and a feeding auger is fixedly connected to one side of the upper part of the bottom tank, and the main tank mechanism comprises a main tank, and a discharging auger is fixedly connected to one side of the lower part of the main tank, and the bottom of the bottom tank is inwardly retracted to form an inverted truncated cone, and a drainage pipe is fixedly connected to one side of the middle part of the bottom tank, and a free end of the drainage pipe is externally connected to a water pump, and a riser mechanism is carried in the tank body, and the riser mechanism comprises an asphalt plate fixedly connected between the bottom tank and the main tank, and a preparation device and method of a mesoporous silica material with a super large opening, so that the moisture of the raw materials entering the main tank is in a suitable mixing condition, thereby improving the quality of the raw materials.

Description

Technical Field

[0001] The invention relates to the technical field of material preparation, and in particular to a device and method for preparing a mesoporous silica material with an ultra-large opening. Background Art

[0002] With the rapid development of micro-nano synthesis technology, more and more new micro-nano materials have been synthesized and have shown great application prospects in the fields of biomedicine, daily chemicals, electronic devices, energy catalysis, etc. Compared with traditional functional materials, micro-nano materials with special opening structures often show unique performance in the application process due to their unique surface topological properties. Among them, the surface opening structure that is open to the outside can directly interact with the object interface, thereby showing unique application performance, which has attracted widespread attention.

[0003] Silica materials are widely used in daily life due to their chemical stability and biological safety. For example, they are used as dispersants in food additives to improve the dispersibility of instant coffee and milk powder; in cosmetics, they are used to adjust skin feel, lubricate and moisturize; in rubber additives, they are used to improve flexibility and wear resistance, etc.

[0004] In the prior art:

[0005] 1. The currently disclosed silicon oxide materials have pore structures on the surface, but the pore diameters are relatively small, and there is no such large opening;

[0006] 2. There is no such surface morphology that has been made public.

[0007] The present invention realizes the construction of an ultra-large external opening structure, which, while retaining the functionality of the silicon oxide material itself, gives the material an ultra-large external specific surface area, greatly improving the utilization rate of the material.

[0008] The prior art does not control the moisture content of the raw materials to be mixed. Ignoring the moisture content control of the raw materials will not improve the mixing rate. Therefore, there is an urgent need for a preparation device and method for mesoporous silica materials with ultra-large openings to solve the above-mentioned problems. Summary of the invention

[0009] The purpose of the present invention is to provide a device and method for preparing a mesoporous silica material with ultra-large openings, so as to solve the problems raised in the above-mentioned background technology.

[0010] To achieve the above-mentioned purpose, the present invention provides the following technical solutions: a device for preparing a mesoporous silica material with an ultra-large opening, comprising a tank body and a shell mechanism;

[0011] The tank body comprises a bottom tank mechanism, a main tank mechanism and a top cover mechanism, and the tank body is equipped with a power mechanism;

[0012] The bottom tank mechanism comprises a bottom tank, and one side of the upper portion of the bottom tank is fixedly connected to a feeding auger;

[0013] The main tank mechanism comprises a main tank, and a discharging auger is fixedly connected to one side of the lower part of the main tank;

[0014] The bottom of the bottom tank is inwardly retracted to form an inverted truncated cone, a drainage pipe is fixedly connected to one side of the middle of the bottom tank, and a free end of the drainage pipe is externally connected to a water pump;

[0015] The tank body is provided with a riser mechanism, the riser mechanism comprises a bitumen plate fixedly connected between the bottom tank and the main tank, a tubular vertical pipe is fixedly connected through the middle of the surface of the bitumen plate, the lower end of the vertical pipe extends into the bottom tank, and the upper end of the vertical pipe extends into the main tank;

[0016] The power mechanism includes a motor, a fixed end of which is fixedly connected to the lower surface of the bottom tank, an output end of the motor passes through the bottom tank and is fixedly connected to an organic column, the organic column corresponds to a vertical pipe, and a first screw plate adapted to be inserted into the vertical pipe is fixedly wrapped around the outer side of the organic column.

[0017] As a preferred technical solution of the present invention, both sides of the lower part of the drain pipe are respectively connected with a first leg through a hinge, the end of the first leg away from the bottom tank is connected with a second leg through a torsion spring, the end of the second leg away from the first leg is connected with a third leg through a hinge, and the lower surface of the third leg is fixedly connected to the first bottom pad.

[0018] As a preferred technical solution of the present invention, the upper port of the vertical pipe expands outwardly in a trumpet shape, and a partition plate is fixedly connected to the inner side of the upper port of the vertical pipe at equal intervals.

[0019] As a preferred technical solution of the present invention, the outer side of the main tank is wrapped with a thermal component, the thermal component wraps a fixed cover connected to the thermal cover outside the main tank, thermal pipes are evenly and evenly fixedly installed between the main tank and the thermal cover, and the main tank and the thermal cover are filled with heat transfer oil; the discharge auger penetrates the thermal cover;

[0020] The upper end surface of the main tank is fixedly connected with an annular connecting ring, the inner wall of the connecting ring is evenly and evenly fixed with teeth, and the outer side of the upper end surface of the connecting ring is evenly and evenly provided with insertion holes.

[0021] A gear flush with the connecting ring is fixedly sleeved on the outer side of the upper end of the machine column;

[0022] An elastic column is fixedly connected to the lower side of the fixed end of the motor, and a second bottom pad is fixedly connected to the lower surface of the elastic column.

[0023] A stirring mechanism for stirring is arranged between the main tank and the vertical pipe, and the stirring mechanism comprises an annular ring plate, and the lower end surface of the ring plate is equidistantly and evenly connected to a first small column inserted between the connecting ring and the gear through a bearing, and a tooth column adapted to mesh with the gear is fixedly sleeved on the outer side of the first small column;

[0024] The lower end of the first small column is fixedly connected to the second small column, the outer side of the second small column is fixedly connected with the second screw plate, and the lower ends of the second small column and the second screw plate are attached to the asphalt plate;

[0025] The lower end of the remaining first small column is movably connected to the third small column through a bearing, and a shovel plate is sleeved on the outer side of the third small column. The shovel plate is adapted to fit the vertical pipe and the main tank, and the lower ends of the third small column and the shovel plate fit the asphalt plate.

[0026] As a preferred technical solution of the present invention, the top cover mechanism comprises a top cover, and the lower end surface of the top cover is evenly and evenly fixedly connected with plug posts adapted to the plug-in sockets;

[0027] A collar is fixedly connected to the middle of the upper surface of the top cover, and the upper end of the column passes through the top cover and is adapted to fit the collar;

[0028] The upper inner wall of the top cover is provided with an embedding groove adapted to fit the plug-in ring piece;

[0029] Both sides of the top cover are fixedly connected with air pipes, and the free ends of the air pipes are externally connected to a fan.

[0030] As a preferred technical solution of the present invention, the shell mechanism includes a cover shell, which is sleeved on the outside of the tank body for protection, and the outside of the cover shell is fixedly connected with a support leg.

[0031] A method for preparing a mesoporous silica material with an ultra-large opening, the steps of which are as follows:

[0032] S1: Add the raw materials to the auxiliary materials in proportion;

[0033] S2: Utilize the electric heating of the thermal components and the heat transfer of the heat transfer oil, and control the ventilation volume inside the equipment through the air pipe connected to the external fan. At the same time, the intermittent stirring of the stirring mechanism allows the air to fully enter the equipment, so that the materials are fully mixed;

[0034] S3: The materials that have been mixed once are conveyed out by the conveyor and placed in the semi-finished product area for turning and secondary mixing. The compost is turned after three to four days, and the mixing is completed when the temperature drops to 40 degrees Celsius. Finally, after further full mixing, it is transformed into products with economic benefits and environmental value.

[0035] S4: Testing the mixed bulk product;

[0036] S5: If the test results are qualified, the raw materials can be added in proportion according to the target indicators to be produced by using an automatic batching machine, and then the materials are mixed by a mixer. The mixed materials are crushed by a pulverizer and further screened by a screening machine.

[0037] S6: Based on the test results, if the product does not meet the standards, the formula will be revised or the aging time will be extended according to the indicators.

[0038] Compared with the prior art, the present invention has the following beneficial effects:

[0039] (1) A device and method for preparing a mesoporous silica material with an ultra-large opening, which adopts a high-temperature rapid mixing technology. In a closed high-temperature mixing device, by adjusting the moisture content, carbon-nitrogen ratio and other factors of the feed, and providing the appropriate temperature required for the mixing of the raw materials, the most suitable conditions are provided for the mixing of the raw materials, thereby achieving the purpose of rapid mixing.

[0040] (2) A device and method for preparing mesoporous silica materials with ultra-large openings, which generates heat through the thermal pipes of the thermal components and continuously assists in heating the raw materials inside the main tank through heat transfer oil. The heat released during the mixing process can lower the temperature inside the equipment to achieve a better mixing and synthesis effect.

[0041] (3) A device and method for preparing a mesoporous silica material with an ultra-large opening. When the raw material rises along the first screw plate, the water in the raw material can be drained away by itself, so that the water content of the raw material entering the main tank is in suitable mixing conditions, thereby improving the quality of the raw material.

[0042] (4) A device and method for preparing mesoporous silica materials with an ultra-large opening, wherein the raw materials gradually rising in the vertical pipe are evenly dispersed when passing through the partition plate by rotating the first screw plate, so that the laying of the raw materials inside the main tank is more uniform, which facilitates the regulation and control of moisture, temperature and airflow inside the equipment.

[0043] (5) A device and method for preparing a mesoporous silica material with an ultra-large opening. The raw materials in the main tank during the mixing process can use the excess water drained from the bottom tank to create a moist mixing environment, saving the energy required for the mixing equipment to create the environment and improving the energy-saving and environmental protection performance of the equipment.

[0044] (6) A device and method for preparing a mesoporous silica material with an ultra-large opening, which can fully stir and mix the waste raw materials to improve the quality of the raw material mixing. BRIEF DESCRIPTION OF THE DRAWINGS

[0045] Figure 1 It is a structural schematic diagram of the present invention;

[0046] Figure 2It is a schematic diagram of the mixing tank of the present invention;

[0047] Figure 3 This is a schematic diagram of the bottom tank mechanism of the present invention;

[0048] Figure 4 This is a schematic diagram of the pipe riser mechanism of the present invention;

[0049] Figure 5 This is a schematic diagram of the main tank mechanism of the present invention;

[0050] Figure 6 For the present invention Figure 5 A magnified schematic diagram of point A;

[0051] Figure 7 This is a schematic diagram of the position of the pipe riser mechanism of the present invention;

[0052] Figure 8 It is a schematic diagram of the position of the power mechanism of the present invention;

[0053] Fig. 9 It is a schematic diagram of the power mechanism of the present invention;

[0054] Fig.10 It is a schematic diagram of the stirring mechanism of the present invention;

[0055] Fig.11 This is a schematic diagram of the position of the stirring mechanism of the present invention;

[0056] Fig.12 For the present invention Fig.11 An enlarged schematic diagram of point B;

[0057] Fig.13 It is a schematic diagram of the top cover mechanism of the present invention;

[0058] Fig.14 It is a schematic diagram of the connection of the top cover mechanism of the present invention.

[0059] In the figure: 1. Bottom tank mechanism; 101. Bottom tank; 102. Feeding auger; 103. Drain pipe; 104. First leg; 105. Second leg; 106. Third leg; 107. First bottom pad; 2. Rising pipe mechanism; 201. Asphalt plate; 202. Vertical pipe; 203. Partition plate; 3. Main tank mechanism; 301. Main tank; 302. Discharging auger; 303. Thermal cover; 304. Thermal pipe; 305. Connecting ring; 306. Teeth; 307. Socket; 4. Power mechanism; 401. Motor; 402, machine column; 403, first screw plate; 404, gear; 405, elastic column; 406, second bottom pad; 5, stirring mechanism; 501, ring plate; 502, first small column; 503, gear column; 504, second small column; 505, second screw plate; 506, third small column; 507, shovel plate; 6, top cover mechanism; 601, top cover; 602, plug column; 603, sleeve ring; 604, embedded groove; 605, air pipe; 7, shell mechanism; 701, cover; 702, supporting leg. DETAILED DESCRIPTION

[0060] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0061] Example: See Figure 1 , Figure 2 , Figure 3 , Figure 4 , Figure 5 , Figure 7 , Figure 8 , Fig. 9 , a preparation device of a super-large opening type mesoporous silica material, comprising a mixing tank and a shell mechanism 7;

[0062] The mixing tank body comprises a bottom tank mechanism 1, a main tank mechanism 3 and a top cover mechanism 6, and the mixing tank body is equipped with a power mechanism 4;

[0063] The bottom tank mechanism 1 comprises a bottom tank 101, and a feeding auger 102 is fixedly connected to one side of the upper portion of the bottom tank 101;

[0064] The main tank mechanism 3 includes a main tank 301, and a discharging auger 302 is fixedly connected to one side of the lower part of the main tank 301;

[0065] The bottom of the bottom tank 101 is inwardly truncated to form an inverted truncated cone. A drainage pipe 103 is fixedly connected to one side of the middle of the bottom tank 101. The free end of the drainage pipe 103 is externally connected to a water pump.

[0066] The mixing tank body is provided with a riser mechanism 2, which includes a bitumen plate 201 fixedly connected between the bottom tank 101 and the main tank 301, and a tubular vertical pipe 202 is fixedly connected through the middle of the surface of the bitumen plate 201, the lower end of the vertical pipe 202 extends into the bottom tank 101, and the upper end of the vertical pipe 202 extends into the main tank 301;

[0067] The power mechanism 4 includes a motor 401, a fixed end of the motor 401 is fixedly connected to the lower surface of the bottom tank 101, an output end of the motor 401 passes through the bottom tank 101 and is fixedly connected to an organic column 402, the connection between the motor 401 and the bottom tank 101 is sealed, the machine column 402 corresponds to the vertical pipe 202, and the outer side of the machine column 402 is fixedly wrapped with a first screw plate 403 adapted to be plugged into the vertical pipe 202, and the surface of the first screw plate 403 is hollow.

[0068] See also Figure 3 The two sides of the lower part of the drain pipe 103 are respectively connected with the first leg 104 through hinges, the end of the first leg 104 away from the bottom tank 101 is connected with the second leg 105 through a torsion spring, the end of the second leg 105 away from the first leg 104 is connected with the third leg 106 through a hinge, and the lower surface of the third leg 106 is fixedly connected with the first bottom pad 107, and the first bottom pad 107 is made of rubber material.

[0069] See also Figure 4 The upper end of the vertical pipe 202 is expanded outwardly in a trumpet shape, and the inner side of the upper end of the vertical pipe 202 is evenly and evenly fixedly connected with a partition plate 203.

[0070] See also Figure 5 , Figure 6 , Figure 8 , Fig. 9 , Fig.10 , Fig.11 , Fig.12 The outer side of the main tank 301 is wrapped with a thermal component, and the thermal component wraps a thermal cover 303 fixedly connected to the outer side of the main tank 301. Thermal pipes 304 are evenly and evenly fixedly installed between the main tank 301 and the thermal cover 303. The main tank 301 and the thermal cover 303 are filled with heat transfer oil; the discharge auger 302 penetrates the thermal cover 303;

[0071] An annular connecting ring 305 is fixedly connected to the upper end surface of the main tank 301 , teeth 306 are fixedly connected to the inner wall of the connecting ring 305 at equal intervals, and insertion holes 307 are evenly and evenly opened on the outer side of the upper end surface of the connecting ring 305 .

[0072] A gear 404 flush with the ring 305 is fixedly sleeved on the outer side of the upper end of the machine column 402;

[0073] An elastic column 405 is fixedly connected to the lower side of the fixed end of the motor 401 , and a second bottom pad 406 is fixedly connected to the lower surface of the elastic column 405 . The second bottom pad 406 is made of rubber material.

[0074] A stirring mechanism 5 for stirring is arranged between the main tank 301 and the vertical pipe 202. The stirring mechanism 5 comprises an annular ring plate 501. The lower end surface of the ring plate 501 is evenly and equidistantly connected to a first small column 502 inserted between the connecting ring 305 and the gear 404 through a bearing. A tooth column 503 adapted to mesh with the tooth teeth 306 and the gear 404 is fixedly sleeved on the outer side of the first small column 502.

[0075] A second small column 504 is fixedly connected to the lower end of a first small column 502, a second screw plate 505 is fixedly wound around the outer side of the second small column 504, and the lower ends of the second small column 504 and the second screw plate 505 are attached to the asphalt plate 201;

[0076] The lower ends of the remaining first small columns 502 are movably connected to the third small columns 506 through bearings. The outer side of the third small column 506 is sleeved with a shovel plate 507. The shovel plate 507 is adapted to fit the vertical pipe 202 and the main tank 301. The lower ends of the third small column 506 and the shovel plate 507 fit the asphalt plate 201.

[0077] See also Fig.13 , Fig.14 The top cover mechanism 6 includes a top cover 601, and the lower end surface of the top cover 601 is evenly and evenly fixedly connected with plug posts 602 adapted to the plug-in sockets 307;

[0078] A collar 603 is fixedly connected to the middle of the upper surface of the top cover 601, and the upper end of the column 402 passes through the top cover 601 and is adapted to be plugged into the collar 603;

[0079] The upper inner wall of the top cover 601 is provided with an embedding groove 604 adapted to fit the plug-in ring piece 501;

[0080] Both sides of the top cover 601 are fixedly connected with air pipes 605, and the free ends of the air pipes 605 are externally connected to a fan.

[0081] See also Figure 1 The shell mechanism 7 includes a cover shell 701, which is sleeved on the outside of the mixing tank body for protection, and a support leg 702 is fixedly connected to the outside of the cover shell 701.

[0082] A method for preparing a mesoporous silica material with an ultra-large opening, the steps of which are as follows:

[0083] S1: Add the raw materials to the auxiliary materials in proportion;

[0084] S2: Using the electric heating of the thermal components and the heat transfer of the heat transfer oil, set the temperature of the equipment to 90 to 100 degrees Celsius, and control the ventilation volume inside the equipment through the air pipe connected to the fan. At the same time, the intermittent stirring of the stirring mechanism allows the air to fully enter the equipment, so that the materials are fully mixed;

[0085] S3: The materials that have been mixed once are conveyed out by the conveyor and placed in the semi-finished product area for turning and secondary mixing. The compost is turned after three to four days, and the mixing is completed when the temperature drops to 40 degrees Celsius. Finally, after further full mixing, it is transformed into products with economic benefits and environmental value.

[0086] S4: Testing the mixed bulk product;

[0087] S5: If the test results are qualified, the raw materials can be added in proportion according to the target indicators to be produced by using an automatic batching machine, and then the materials are mixed by a mixer. The mixed materials are crushed by a pulverizer and further screened by a screening machine.

[0088] S6: Based on the test results, if the product does not meet the standards, the formula will be revised or the aging time will be extended according to the indicators.

[0089] The working principle of the present invention is as follows:

[0090] The raw materials are fed into the bottom tank 101 through the feeding auger 102. At this time, the moisture content in the raw materials is relatively high. If it is not removed, the subsequent mixing process may be slowed down. Therefore, the motor 401 is started accordingly to drive the machine column 402 and the first screw plate 403 to rotate. The raw materials in the bottom tank 101 are transported to the main tank mechanism 3 through the first screw plate 403 through the rising pipe mechanism 2. In the process of the raw materials rising with the first screw plate 403, part of the moisture therein can be drained away by itself, so that the moisture content of the raw materials entering the main tank 301 is suitable for mixing conditions, thereby improving the quality of the raw materials.

[0091] Through the uniform distribution of the inner partition plate 203 at the upper end of the vertical pipe 202, the raw materials gradually rising in the vertical pipe 202 are evenly dispersed when passing through the partition plate 203 through the rotation of the first screw plate 403, so that the laying of the raw materials inside the main tank 301 is more uniform, which facilitates the adjustment and control of moisture, temperature and airflow inside the mixing equipment.

[0092] An asphalt plate 201 is arranged between the main tank 301 and the bottom tank 101, and the asphalt plate 201 can further drain out excess moisture in the raw materials, and connect the internal space of the bottom tank 101 and the internal space of the main tank 301 by gas conduction, so that the raw materials in the main tank 301 in the mixing process can use the excess moisture drained from the bottom tank 101 to create a moist mixing environment, saving the energy required for the mixing equipment to create the environment and improving the energy-saving and environmental protection performance of the equipment.

[0093] The upper part of the rotating machine column 402 is connected to the gear 404, and the rotation of the gear 404 further drives the gear column 503 meshing therewith to rotate. Through the meshing of the gear column 503 and the teeth 306, the gear column 503 itself rotates, and the ring piece 501 is driven to rotate through the first small column 502. First, the rotation of the gear column 503 causes the second screw plate 505 and the second small column 504 to rotate inside the main tank 301, and follow the ring piece 501 to revolve to stir the mixed raw materials inside the main tank 301. Secondly, the shovel plate 507 is adapted to the internal space of the main tank 301 and its unique spiral inclined plate shape can stir the raw materials inside the main tank 301 up and down when it revolves with the ring piece 501, so as to fully stir the mixed waste raw materials, make them fully mixed, and improve the mixing quality.

[0094] Through the fit between the shovel plate 507 and the main tank 301 and the vertical tube 202, the materials adhering to the surfaces of the main tank 301 and the vertical tube 202 can be scraped off during the rotation process, thereby playing a cleaning role and avoiding waste.

[0095] Through the cooperation of the power mechanism 4 and the riser mechanism 2, the raw materials with overload of water in the bottom tank 101 are drained and introduced into the main tank 301, and the raw materials are transported from the bottom to the top through the riser mechanism 2. The raw materials are introduced into the main tank 301 by gravity through the upper port of the vertical pipe 202. When the mixing space in the main tank 301 is full, excess raw materials will no longer be introduced into the main tank 301, thereby avoiding overloading of the main tank 301 and ensuring the mixing quality.

[0096] Due to the presence of the bottom motor 401, when the motor 401 is running, the tank body will vibrate, and the second bottom pad 406 under the elastic column 405 and the first bottom pad 107 under the third support leg 106 will reduce the noise generation, and the vibration of the tank body will promote the mixing of raw materials and increase the mixing speed of raw materials.

[0097] This process adopts high-temperature rapid mixing technology. In a closed high-temperature mixing equipment, by adjusting factors such as the moisture content of the feed and providing the required appropriate temperature, the most suitable conditions for mixing are provided, thereby achieving the purpose of rapid mixing and composting.

[0098] Heat is generated by the thermal pipe 304 of the thermal component and the raw materials in the main tank 301 are continuously auxiliary heated by the heat transfer oil. The heat released during the mixing process can eliminate harmful microorganisms, various pathogens and insect eggs in the raw materials, thereby achieving the purpose of harmless treatment.

[0099] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A device for preparing a mesoporous silica material with an ultra-large opening, comprising a tank body and a shell mechanism (7); The tank body comprises a bottom tank mechanism (1), a main tank mechanism (3) and a top cover mechanism (6), and the tank body is equipped with a power mechanism (4); The bottom tank mechanism (1) comprises a bottom tank (101), and one side of the upper portion of the bottom tank (101) is fixedly connected to a feeding auger (102); The main tank mechanism (3) comprises a main tank (301), and a discharge auger (302) is fixedly connected to one side of the lower portion of the main tank (301); Features: The bottom of the bottom tank (101) is inwardly retracted to form an inverted truncated cone, and a drainage pipe (103) is fixedly connected to one side of the middle of the bottom tank (101), and a free end of the drainage pipe (103) is externally connected to a water pump; The tank body carries a riser mechanism (2), the riser mechanism (2) comprising an asphalt plate (201) fixedly connected between the bottom tank (101) and the main tank (301), a tubular vertical pipe (202) fixedly connected to the middle of the surface of the asphalt plate (201), the lower end of the vertical pipe (202) extending into the bottom tank (101), and the upper end of the vertical pipe (202) extending into the main tank (301); The power mechanism (4) comprises a motor (401), the fixed end of the motor (401) is fixedly connected to the lower surface of the bottom tank (101), the output end of the motor (401) passes through the bottom tank (101) and is fixedly connected to an organic column (402), the organic column (402) is correspondingly inserted into the vertical pipe (202), and the outer side of the organic column (402) is fixedly wound with a first screw plate (403) adapted to be plugged into the vertical pipe (202); The outer side of the main tank (301) is wrapped with a thermal component, the thermal component wraps a thermal cover (303) fixedly connected to the outer side of the main tank (301), thermal pipes (304) are evenly and equidistantly fixedly installed between the main tank (301) and the thermal cover (303), and heat transfer oil is filled between the main tank (301) and the thermal cover (303); the discharge auger (302) passes through the thermal cover (303); The upper end surface of the main tank (301) is fixedly connected with an annular connecting ring (305), the inner wall of the connecting ring (305) is evenly and evenly fixedly connected with teeth (306), and the outer side of the upper end surface of the connecting ring (305) is evenly and evenly provided with insertion holes (307); A gear (404) flush with the connecting ring (305) is fixedly sleeved on the outer side of the upper end of the machine column (402); An elastic column (405) is fixedly connected to the lower side of the fixed end of the motor (401), and a second bottom pad (406) is fixedly connected to the lower surface of the elastic column (405).

2. The device for preparing a mesoporous silica material with a super large opening according to claim 1, characterized in that: The two sides of the lower part of the drainage pipe (103) are respectively connected to the first support leg (104) through a hinge, and the end of the first support leg (104) away from the bottom tank (101) is connected to the second support leg (105) through a torsion spring, and the end of the second support leg (105) away from the first support leg (104) is connected to the third support leg (106) through a hinge, and the lower surface of the third support leg (106) is fixedly connected to the first bottom pad (107).

3. The device for preparing a mesoporous silica material with a super large opening according to claim 1, characterized in that: The upper end of the vertical pipe (202) expands outwardly in a trumpet shape, and a partition plate (203) is fixedly connected to the inner side of the upper end of the vertical pipe (202) at equal intervals and uniformly.

4. The device for preparing a mesoporous silica material with a super large opening according to claim 1, characterized in that: A stirring mechanism (5) for stirring is provided between the main tank (301) and the vertical pipe (202), the stirring mechanism (5) comprising an annular ring plate (501), the lower end surface of the ring plate (501) being equidistantly and evenly connected to a first small column (502) inserted between the connecting ring (305) and the gear (404) through a bearing, and a tooth column (503) adapted to mesh with the teeth (306) and the gear (404) is fixedly sleeved on the outer side of the first small column (502); The lower end of one of the first small columns (502) is fixedly connected to a second small column (504), the outer side of the second small column (504) is fixedly connected to a second screw plate (505), and the lower ends of the second small column (504) and the second screw plate (505) are attached to the asphalt plate (201); The lower end of the remaining first small column (502) is movably connected to a third small column (506) via a bearing, and a shovel plate (507) is sleeved on the outer side of the third small column (506). The shovel plate (507) is adapted to fit the vertical pipe (202) and the main tank (301), and the lower ends of the third small column (506) and the shovel plate (507) fit the asphalt plate (201).

5. The device for preparing a mesoporous silica material with a super large opening according to claim 1, characterized in that: The top cover mechanism (6) comprises a top cover (601), and the lower end surface of the top cover (601) is evenly and equidistantly fixedly connected with plug posts (602) adapted to plug in the plug holes (307); A collar (603) is fixedly connected to the middle of the upper surface of the top cover (601); the upper end of the machine column (402) passes through the top cover (601) and is adapted to be plugged into the collar (603); The upper inner wall of the top cover (601) is provided with an embedding groove (604) adapted to fit the plug-in ring piece (501); Both sides of the top cover (601) are fixedly connected to an air pipe (605), and the free end of the air pipe (605) is externally connected to a fan.

6. The device for preparing a mesoporous silica material with a super large opening according to claim 1, characterized in that: The shell mechanism (7) comprises a cover shell (701), the cover shell (701) being sleeved on the outside of the tank body for protection, and a support leg (702) being fixedly connected to the outside of the cover shell (701).

7. A method for preparing a mesoporous silica material with ultra-large openings, using the device according to any one of claims 1 to 6, the steps of which are as follows: S1: Add the raw materials to the auxiliary materials in proportion; S2: Using the electric heating of the thermal components and the heat transfer of the heat transfer oil, set the temperature of the equipment to 90 to 100 degrees Celsius, and control the ventilation volume inside the equipment through the air pipe connected to the fan. At the same time, the intermittent stirring of the stirring mechanism allows the air to fully enter the equipment, so that the materials are fully mixed; S3: The materials that have been mixed once are conveyed out by the conveyor and placed in the semi-finished product area for turning and secondary mixing. The compost is turned after three to four days, and the mixing is completed when the temperature drops to 40 degrees Celsius. Finally, after further full mixing, it is transformed into products with economic benefits and environmental value. S4: Testing the mixed bulk product; S5: If the test results are qualified, the raw materials can be added in proportion according to the target indicators to be produced by using an automatic batching machine, and then the materials are mixed by a mixer. The mixed materials are crushed by a pulverizer and further screened by a screening machine; S6: Based on the test results, if the product does not meet the standards, the formula will be revised or the aging time will be extended according to the indicators.

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