Methanol aqueous solution supply system and method with cleaning and stirring functions

By designing a methanol aqueous solution supply system with cleaning and stirring functions, using triple mixing technology of polymerization discharge part, centrifugal part and direct stirring part, the problem of decomposition or volatility of methanol aqueous solution during long storage is solved, real-time supply and rapid mixing configuration of methanol aqueous solution are achieved.

CN119549038AInactive Publication Date: 2025-03-04SHANGHAI DIANJI UNIV
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Patent Information

Application Number
CN202411950445.6
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-12-27
Publication Date
2025-03-04
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

In the fields of chemical industry, pharmaceuticals and new energy, methanol aqueous solution will decompose or volatilize during long storage, resulting in concentration changes and affecting the progress of the reaction. Methanol has certain toxicity and flammability, and long storage time increases safety risks.

Method used

A methanol aqueous solution supply system with cleaning and stirring functions is designed, including a mixing tank, a closure assembly, a mixing assembly and an isolation assembly. Through triple mixing of the polymerization discharge part, centrifugal part and direct stirring part, real-time configuration and rapid mixing of the methanol aqueous solution are achieved.

Benefits of technology

Real-time supply of methanol aqueous solution is achieved, concentration changes and safety risks caused by early storage are avoided, and the rapid mixing and configuration capability of methanol aqueous solution is improved through triple mixing technology.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention discloses a methanol aqueous solution supply system and method with cleaning and stirring functions. The methanol aqueous solution supply system comprises a mixing tank body; the sealing assembly is arranged at the top of the mixing tank body, and the sealing assembly is used for sealed feeding of the mixing tank body; the mixing assembly is arranged in the inner cavity of the mixing tank body, the mixing assembly comprises a direct stirring part, a centrifugal part used for preliminarily mixing raw materials is arranged at the top of the direct stirring part, and a polymerization discharging part is arranged at the top of the centrifugal part and located at the bottom of the sealing assembly; the isolation assembly is arranged on the inner wall of the mixing tank body, and the isolation assembly is used for separating the mixed raw materials from the raw materials which are not uniformly mixed. According to the invention, real-time preparation of a methanol aqueous solution required by reaction is realized, real-time supply of the methanol aqueous solution is further realized, and compared with single stirring blade mixing, triple mixing of the polymerization discharging part, the centrifugal part and the direct stirring part enables methanol to be rapidly dissolved in water, and rapid mixing preparation of the methanol aqueous solution is realized.
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Description

Technical Field

[0001] The present invention relates to the technical field of methanol-water solution configuration, and in particular to a methanol-water solution supply system and method with cleaning and stirring functions. Background Art

[0002] In the fields of chemical industry, pharmaceutical industry and new energy, methanol aqueous solution is an important solvent and reaction medium, widely used in various chemical reaction processes;

[0003] Chemical reactions require methanol aqueous solutions of different concentrations. Generally, a mixing tank is used to prepare methanol aqueous solutions of various concentrations for standby use. However, during long-term storage, methanol aqueous solutions will decompose or volatilize, causing the concentration of the methanol aqueous solution of a specific concentration stored in advance to change, affecting the subsequent reaction. In addition, methanol has certain toxicity and flammability, and long-term storage will increase safety risks.

[0004] Therefore, in order to solve the problem of real-time configuration of methanol-water solution according to needs, the present invention proposes a methanol-water solution supply system and method with cleaning and stirring functions. Summary of the invention

[0005] The object of the present invention is to provide a methanol aqueous solution supply system and method with cleaning and stirring functions to solve the problems raised in the above-mentioned background technology.

[0006] To achieve the above object, the present invention provides the following technical solution: a methanol aqueous solution supply system with cleaning and stirring functions, comprising:

[0007] Mixing tank;

[0008] A closing component, which is arranged on the top of the mixing tank and is used for closed feeding of the mixing tank;

[0009] A mixing assembly, which is arranged in the inner cavity of the mixing tank body, and is used for mixing raw materials. The mixing assembly comprises a direct stirring portion, and a centrifugal portion for preliminary mixing of raw materials is arranged on the top of the direct stirring portion, and a polymerizing discharge portion is arranged on the top of the centrifugal portion and located at the bottom of the closed assembly;

[0010] The isolation component is arranged on the inner wall of the mixing tank body, and is used to separate the mixed raw materials from the unmixed raw materials.

[0011] Preferably, the closure assembly comprises:

[0012] A sealing cover, which is arranged on the top of the mixing tank;

[0013] A first feeding port, which is disposed on the top side of the sealing cover and is used for feeding methanol;

[0014] A second feeding port, the second feeding port is arranged on the top side of the sealing cover, and the second feeding port is used for feeding water;

[0015] A plurality of lifting rings are arranged around the top of the sealing cover and are used for lifting the sealing cover during maintenance.

[0016] Preferably, the direct stirring unit comprises:

[0017] An electric motor, wherein the electric motor is arranged on the top of the sealing cover;

[0018] A rotating shaft, the top end of which is fixedly connected to the output end of the motor;

[0019] A stirring blade, the stirring blade is arranged on the outer side of the bottom of the rotating shaft, and the stirring blade is used for directly stirring and mixing the methanol-water solution;

[0020] A heating component is used to accelerate the mixing of methanol and water, and the heating component is arranged on the inner wall of the mixing tank.

[0021] Preferably, the temperature raising component comprises:

[0022] A heating chamber, wherein the heating chamber is arranged on the inner wall of the mixing tank;

[0023] A plurality of flange heat source pipes, wherein the plurality of flange heat source pipes are symmetrically arranged on the top side of the mixing tank body, the flange heat source pipes are connected to the heating chamber, and the flange heat source pipes are used to introduce heat transfer oil;

[0024] A liquid discharge interface is arranged at the bottom of the mixing tank body, and is used for the outflow circulation of the heat transfer oil.

[0025] Preferably, the polymerization discharge section comprises:

[0026] A mixing plate, the top of which is interlaced with the bottoms of the first feeding port and the second feeding port, and the mixing plate is sleeved on the outside of the rotating shaft;

[0027] A circulation cavity, wherein the circulation cavity is arranged at the intersection of the first feeding port, the second feeding port and the liquid mixing disk;

[0028] A plurality of liquid outlet heads are arranged around the bottom of the liquid mixing plate, and the liquid outlet heads are used for discharging methanol and water.

[0029] Preferably, the centrifugal part comprises:

[0030] A fixing ring, wherein the fixing ring is sleeved on the outer side of the rotating shaft;

[0031] A centrifugal disc, which is sleeved on the outside of the rotating shaft and arranged at the bottom of the fixed ring, and a centrifugal cavity for raw materials to enter is opened on the top of the centrifugal disc;

[0032] A plurality of liquid discharge nozzles, which are arranged around the side of the centrifugal disc, are connected to the centrifugal cavity, and are used for centrifugal discharge of raw materials;

[0033] A guide member is arranged on the top of the centrifugal disc and is used for guiding the feed of the centrifugal chamber.

[0034] Preferably, the guide member comprises a liquid receiving ring arranged on the top of the centrifugal disc, and the inner cavity of the liquid receiving ring is communicated with the centrifugal cavity.

[0035] Preferably, the isolation assembly comprises:

[0036] An isolation plate, which is arranged on the inner wall of the mixing tank and located at the bottom of the mixing assembly;

[0037] A discharge valve, the discharge valve is connected to the bottom of the isolation plate, and the discharge valve is used to control the temporary discharge and storage of the mixed methanol-water solution;

[0038] A discharge pipe, which is arranged at the bottom of the mixing tank and is used for temporarily storing the methanol-water solution;

[0039] A clean water outlet pipe, which is arranged on the side of the discharge pipe and is used for the outflow of clean water;

[0040] The rotating part is used for opening and closing the liquid discharge valve, and the rotating part is inserted and connected to the outer side of the mixing tank body.

[0041] Preferably, the rotating part comprises:

[0042] A rotating rod, the rotating rod is inserted and connected to the side of the mixing tank body, and the end of the rotating rod is fixedly connected to the rotating opening and closing end of the liquid discharge valve;

[0043] A hand wheel is arranged at the end of the rotating rod and is located outside the mixing tank body.

[0044] A method for using a methanol-water solution supply system with cleaning and stirring functions, using the supply system described above, the method comprising the following steps:

[0045] In the first step, the equipment is powered on, and the direct stirring part in the mixing assembly starts to rotate, and the direct stirring part drives the centrifugal part to rotate in the mixing tank;

[0046] In the second step, the closed component is connected to the pressure supply pipeline of methanol and water, so that the raw material pressure flow enters the supply system and then enters the polymerization discharge part at the bottom of the closed component. The polymerization discharge part injects methanol and water into the centrifugal part. The rotating centrifugal part collides and mixes the methanol and water, and the methanol and water fly out of the centrifugal part due to the centrifugal force.

[0047] In the third step, the preliminary methanol mixed aqueous solution flying out of the centrifugal part is gathered in the inner cavity of the mixing tank body and at the top of the isolation component, and the rotating direct stirring part finally mixes the preliminary methanol mixed aqueous solution and enters the isolation component at the bottom inner cavity of the mixing tank body for temporary storage, and the final methanol mixed aqueous solution is discharged from the mixing tank body through the isolation component for use;

[0048] In the fourth step, only water is introduced into the closed component to clean the centrifugal part, polymerization discharge part, direct stirring part, isolation component and the inner wall of the mixing tank, and then discharged from the isolation component to perform self-cleaning of the system.

[0049] Technical effects and advantages of the present invention:

[0050] The present invention adds methanol and water into the sealing component at the top of the mixing tank body, and the methanol and water enter the polymerization discharge part for mixing and outputting, and then enter the centrifugal part, and the direct stirring part drives the centrifugal part to centrifugally mix the methanol and water, and the methanol and water separate from the centrifugal part again and enter the inner cavity of the mixing tank body and the top of the isolation component, and the direct stirring part performs the final mixing of the methanol and water solution, and is discharged through the isolation component. This design realizes the real-time configuration of the methanol and water solution according to the reaction needs, and then realizes the real-time supply of the methanol and water solution. Compared with the single stirring blade mixing, the triple mixing of the polymerization discharge part, the centrifugal part and the direct stirring part enables the methanol to be quickly dissolved in the water, thereby realizing the rapid mixing and configuration of the methanol and water solution. BRIEF DESCRIPTION OF THE DRAWINGS

[0051] Figure 1 It is a schematic diagram of the overall structure of the present invention.

[0052] Figure 2 It is a top view of the overall structure of the present invention.

[0053] Figure 3 It is a cross-sectional view of the present invention as a whole.

[0054] Figure 4 For the present invention Figure 3 A schematic diagram of the enlarged structure at point A in the middle.

[0055] Figure 5 This is a three-dimensional schematic diagram of the centrifugal disk structure of the present invention.

[0056] Figure 6 This is the second three-dimensional schematic diagram of the centrifugal disk structure of the present invention.

[0057] Figure 7 It is a schematic structural diagram of the liquid mixing disk of the present invention.

[0058] In the figure: 1. mixing tank body; 101. flange heat source pipe; 102. drain interface; 103. heating chamber; 104. clean water outlet pipe; 105. discharge pipe; 2. sealing cover; 201. first feeding port; 202. second feeding port; 203. lifting ring; 3. motor; 4. rotating shaft; 401. stirring blade; 5. isolation plate; 501. drain valve; 502. rotating rod; 503. hand wheel; 6. mixing plate; 601. circulation chamber; 602. liquid outlet head; 7. fixing ring; 8. centrifugal plate; 801. centrifugal chamber; 802. liquid receiving ring; 803. liquid outlet nozzle. DETAILED DESCRIPTION

[0059] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0060] Embodiment 1, the present invention provides as follows Figure 1-7 The methanol-water solution supply system shown has cleaning and stirring functions, comprising: a mixing tank 1, a sealing component, a mixing component and an isolation component;

[0061] Specifically, the closing component is arranged on the top of the mixing tank body 1, the mixing component is arranged in the inner cavity of the mixing tank body 1, and the isolation component is arranged on the inner wall of the mixing tank body 1;

[0062] It should be noted that the closing component is used for the closed feeding of the mixing tank 1, the mixing component is used for mixing the raw material methanol and water, and the isolation component is used for separating the mixed raw material from the unmixed raw material.

[0063] Specifically, the mixing component includes a direct stirring part, a centrifugal part for preliminary mixing of raw materials is arranged on the top of the direct stirring part, and a polymerization discharge part is arranged on the top of the centrifugal part and at the bottom of the closed component;

[0064] The sealing assembly includes: a sealing cover 2, a first feeding port 201, a second feeding port 202 and a plurality of lifting rings 203;

[0065] Specifically, the sealing cover 2 is arranged on the top of the mixing tank body 1, the first feeding port 201 is arranged on the top side of the sealing cover 2, the second feeding port 202 is arranged on the top side of the sealing cover 2, and a plurality of lifting rings 203 are arranged around the top of the sealing cover 2;

[0066] It should be noted that the sealing cover 2 and the mixing tank body 1 are fixed by interlacing with multiple bolts and nuts, the tops of the first feeding port 201 and the second feeding port 202 are both flange interfaces, the first feeding port 201 and the second feeding port 202 and the sealing cover 2 are fixed by welding at the interlacing point, the first feeding port 201 is used for the circulation of pressurized methanol flow, and the second feeding port 202 is used for the circulation of pressurized water flow, the amount of which flows in according to the required amount of the ratio, the lifting ring 203 and the sealing cover 2 are fixed by welding, and the lifting ring 203 is used for the inspection and lifting of the sealing cover 2;

[0067] The direct stirring part includes: a motor 3, a rotating shaft 4, a stirring blade 401 and a heating element;

[0068] Specifically, the motor 3 is arranged on the top of the sealing cover 2, the top of the rotating shaft 4 is fixedly connected to the output end of the motor 3, the stirring blade 401 is arranged on the outside of the bottom of the rotating shaft 4, and the heating element is arranged on the inner wall of the mixing tank body 1;

[0069] It should be noted that the motor 3 is fixed to the top of the sealing cover 2 by bolts, the output end of the motor 3 is connected to the rotating shaft 4 by a coupling, the stirring blade 401 is set to be U-shaped, the stirring blade 401 is welded and fixed to the rotating shaft 4, the stirring blade 401 is used for direct stirring and mixing of methanol-water solution, the heating element is used to accelerate the mixing of methanol and water, and can promote the dissolution of methanol molecules in water, and when heated, the residual methanol molecules in the mixing tank body 1 can be evaporated, and the methanol molecules evaporate from the top of the mixing tank body 1 separated from the sealing cover 2;

[0070] Specifically, the temperature-raising component includes: a heating chamber 103, a plurality of flange heat source pipes 101 and a liquid discharge interface 102;

[0071] It should be noted that the heating chamber 103 is arranged on the inner wall of the mixing tank body 1, a plurality of flange heat source pipes 101 are symmetrically arranged on the top side of the mixing tank body 1, the flange heat source pipes 101 are connected to the heating chamber 103, and the liquid discharge interface 102 is arranged at the bottom of the mixing tank body 1;

[0072] Specifically, the flange heat source pipe 101 is used for the inflow of pressurized heat exchange oil, the flange heat source pipe 101 and the mixing tank body 1 are fixed by welding, the flange heat source pipe 101 is used for the introduction of heat transfer oil, and the drain interface 102 is used for the outflow circulation of the heat transfer oil;

[0073] The polymerizing discharge section includes: a liquid mixing plate 6, a flow chamber 601 and a plurality of liquid outlet heads 602;

[0074] Specifically, the top of the mixing plate 6 is interlaced with the bottom of the first feeding port 201 and the second feeding port 202, the mixing plate 6 is sleeved on the outside of the rotating shaft 4, the flow cavity 601 is arranged at the intersection of the first feeding port 201 and the second feeding port 202 and the mixing plate 6, and a plurality of liquid outlet heads 602 are arranged around the bottom of the mixing plate 6, and the liquid outlet heads 602 are used for discharging methanol and water;

[0075] It should be noted that the first feeding port 201 and the second feeding port 202 are welded and fixed to the top of the mixing plate 6, the circulation cavity 601 is connected to the first feeding port 201 and the second feeding port 202, the liquid outlet head 602 is welded and fixed to the mixing plate 6, the circulation cavity 601 is connected to the inner cavity of the liquid outlet head 602, the circulation cavity 601 is used to discharge methanol and water out of the circulation cavity 601, and a through hole through which the rotating shaft 4 is inserted is opened in the middle of the mixing plate 6, and the cross-sectional radius of the through hole is larger than the cross-sectional radius of the rotating shaft 4;

[0076] The centrifugal part includes: a fixed ring 7, a centrifugal disc 8, a plurality of liquid outlet nozzles 803 and a guide member;

[0077] Specifically, the fixing ring 7 is sleeved on the outside of the rotating shaft 4, and the fixing ring 7 and the rotating shaft 4 are fixed by welding. The centrifugal disc 8 is sleeved on the outside of the rotating shaft 4 and arranged at the bottom of the fixing ring 7. The top of the centrifugal disc 8 is provided with a centrifugal cavity 801 for raw materials to enter, and a plurality of liquid outlet nozzles 803 are arranged around the side of the centrifugal disc 8, and a guide is arranged on the top of the centrifugal disc 8;

[0078] It should be noted that the liquid outlet nozzle 803 is connected to the centrifugal chamber 801, the liquid outlet nozzle 803 is used for centrifugal discharge of raw materials, the guide member is used for guiding the feed of the centrifugal chamber 801, the centrifugal disc 8 and the fixing ring 7 are fixed by bolts, and the guide member includes a liquid receiving ring 802 arranged on the top of the centrifugal disc 8, and the inner cavity of the liquid receiving ring 802 is connected to the centrifugal chamber 801;

[0079] Specifically, the liquid receiving ring 802 is welded and fixed to the centrifugal disk 8, and the inner side of the liquid receiving ring 802 can limit the liquid out of the liquid outlet head 602, so that the liquid out of the liquid outlet head 602 enters the centrifugal chamber 801. The centrifugal chamber is set in an annular shape to facilitate the mixing of methanol and water. The liquid outlet nozzle 803 is a columnar hole, which is used to centrifuge the mixed liquid out of the centrifugal chamber 801;

[0080] The isolation assembly includes: an isolation plate 5, a liquid discharge valve 501, a discharge pipe 105, a clean water outlet pipe 104 and a rotating part;

[0081] Specifically, the isolation plate 5 is arranged on the inner wall of the mixing tank body 1 and is located at the bottom of the mixing assembly, the drain valve 501 is inserted and connected to the bottom of the isolation plate 5, the discharge pipe 105 is arranged at the bottom of the mixing tank body 1, the clean water outlet pipe 104 is arranged on the side of the discharge pipe 105, and the rotating part is inserted and connected to the outside of the mixing tank body 1;

[0082] It should be noted that the side of the isolation plate 5 is welded and fixed to the inner wall of the mixing tank body 1, a funnel-shaped guide hole is provided on the top of the isolation plate 5, a drain valve 501 is welded and fixed to the inner wall of the guide hole, and the drain valve 501 is used to control the temporary discharge and storage of the mixed methanol aqueous solution. The isolation plate 5 divides the inner cavity of the mixing tank body 1 into two parts, the top of the isolation plate 5 is used for the configuration and mixing of the methanol aqueous solution, and the bottom space of the isolation plate 5 is used to store the prepared methanol aqueous solution. The discharge pipe 105 is used for the temporary storage and discharge of the methanol aqueous solution;

[0083] Specifically, the discharge pipe 105 is welded and fixed to the mixing tank body 1, the middle part of the discharge pipe 105 is communicated with the inner cavity of the mixing tank body 1, the clean water outlet pipe 104 is welded and fixed to the discharge pipe 105, the clean water outlet pipe 104 is used for the outflow of clean water, the outlets of the discharge pipe 105 and the clean water outlet pipe 104 are both provided with valves for controlling the outflow of liquid, and the rotating part is used for opening and closing the liquid discharge valve 501;

[0084] The rotating part includes: a rotating rod 502 and a hand wheel 503;

[0085] Specifically, the rotating rod 502 is inserted and connected to the side of the mixing tank body 1, the end of the rotating rod 502 is fixedly connected to the rotating opening and closing end of the liquid discharge valve 501, and the hand wheel 503 is arranged at the end of the rotating rod 502 and is located outside the mixing tank body 1;

[0086] It should be noted that the rotating rod 502 is welded and fixed to the rotating opening and closing end of the liquid discharge valve 501, and the rotating interlacing part of the rotating rod 502 and the mixing tank body 1 is sealed, and the storage height of the mixing tank body 1 is not allowed to exceed the rotating interlacing part of the rotating rod 502;

[0087] In actual use, methanol and water are added to the sealing component at the top of the mixing tank body 1, and the methanol and water enter the polymerization discharge part for mixing and output, and then enter the centrifugal part. The direct stirring part drives the centrifugal part to centrifugally mix the methanol and water. The methanol and water are separated from the centrifugal part again and enter the inner cavity of the mixing tank body 1 and the top of the isolation component. The direct stirring part performs the final mixing of the methanol-water solution, and the methanol-water solution is discharged through the isolation component. This design realizes the real-time configuration of the methanol-water solution according to the reaction needs without the need for advance configuration, thereby realizing the real-time supply of the methanol-water solution. Moreover, the triple mixing of the polymerization discharge part, the centrifugal part and the direct stirring part, compared with the single stirring blade mixing, the triple mixing enables the methanol to be quickly dissolved in the water, thereby realizing the rapid mixing configuration of the methanol-water solution.

[0088] Embodiment 2, a method for using a methanol aqueous solution supply system with cleaning and stirring functions,

[0089] The methanol aqueous solution supply system with cleaning and stirring functions including the first embodiment is used, and the method of use includes the following steps:

[0090] In the first step, the equipment is powered on, and the direct stirring part in the mixing assembly starts to rotate, and the direct stirring part drives the centrifugal part to rotate in the mixing tank body 1;

[0091] It should be noted that when the motor 3 is powered on and rotates, the rotating shaft 4 is driven to rotate, and at this time, the liquid discharge valve 501 is in a closed state;

[0092] In the second step, the closed component is connected to the pressure supply pipeline of methanol and water, so that the pressure flow of raw materials enters the supply system and then enters the polymerization discharge part at the bottom of the closed component. The polymerization discharge part injects methanol and water into the centrifugal part. The rotating centrifugal part collides and mixes the methanol and water, and the methanol and water fly out of the centrifugal part due to the centrifugal force.

[0093] It should be noted that the first feed port 201 and the second feed port 202 are flange-connected to the raw material supply pipeline, and methanol and water enter the mixing disk 6 through the first feed port 201 and the second feed port 202, are mixed and circulated in the circulation cavity 601 of the mixing disk 6, and enter the centrifugal cavity 801 of the centrifugal disk 8 through multiple liquid outlet heads 602, and the methanol and water are mixed again in the rotating centrifugal disk 8, and are discharged from the centrifugal disk 8 from multiple liquid outlet nozzles 803 by centrifugal force;

[0094] In the third step, the methanol preliminary mixed aqueous solution flying out of the centrifugal part is gathered in the inner cavity of the mixing tank body 1 and at the top of the isolation component, and the rotating direct stirring part finally mixes the methanol preliminary mixed aqueous solution and enters the isolation component to be temporarily stored in the bottom inner cavity of the mixing tank body 1, and can be discharged from the mixing tank body 1 through the isolation component for use;

[0095] It should be noted that the methanol preliminary mixed water solution is stirred and mixed again by the stirring blade 401 in the inner cavity of the mixing tank body 1. After the stirring is completed, the discharge valve 501 is opened, and the methanol water solution enters the inner cavity of the mixing tank body 1 located at the bottom of the isolation plate 5. The clean water outlet pipe 104 and the discharge pipe 105 are both in a closed state, the discharge pipe 105 is opened, and the clean water outlet pipe 104 is closed;

[0096] In the fourth step, only water enters the closed component to clean the centrifugal part, the polymerization discharge part, the direct stirring part, the isolation component and the inner wall of the mixing tank 1, and then discharges from the isolation component to achieve self-cleaning of the system;

[0097] Specifically, when the interior of the mixing tank body 1 is cleaned, water is introduced into the second feeding port 202, and water is introduced into the mixing disk 6 and the centrifugal disk 8. After the stirring blade 401 rotates for cleaning, the liquid release valve 501 is opened, and clean water enters the bottom inner cavity of the mixing tank body 1 for cleaning. The discharge pipe 105 is in a closed state, and the clean water outlet pipe 104 is turned from closed to open, and clean water is discharged from the mixing tank body 1.

[0098] Finally, it should be noted that the above is only a preferred embodiment of the present invention and is not intended to limit the present invention. Although the present invention has been described in detail with reference to the aforementioned embodiments, it is still possible for those skilled in the art to modify the technical solutions described in the aforementioned embodiments or to make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. A methanol-water solution supply system with cleaning and stirring functions, characterized in that: include: Mixing tank (1); A closed component, the closed component is arranged on the top of the mixing tank (1), and the closed component is used for closed feeding of the mixing tank (1); A mixing assembly, the mixing assembly being arranged in the inner cavity of the mixing tank (1), the mixing assembly being used for mixing raw materials, the mixing assembly comprising a direct stirring portion, a centrifugal portion for preliminary mixing of raw materials being arranged on the top of the direct stirring portion, and a polymerizing discharge portion being arranged on the top of the centrifugal portion and located at the bottom of the closed assembly; An isolation component is arranged on the inner wall of the mixing tank (1), and is used to separate the mixed raw materials from the unmixed raw materials.

2. A methanol-water solution supply system with cleaning and stirring functions according to claim 1, characterized in that: The closure assembly comprises: A sealing cover (2), wherein the sealing cover (2) is arranged on the top of the mixing tank body (1); A first feed port (201), the first feed port (201) being arranged on the top side of the sealing cover (2), and the first feed port (201) being used for feeding methanol; A second feeding port (202), the second feeding port (202) being arranged on the top side of the sealing cover (2), the second feeding port (202) being used for feeding water; A plurality of lifting rings (203) are arranged around the top of the sealing cover (2), and the lifting rings (203) are used for lifting the sealing cover (2) during maintenance.

3. A methanol aqueous solution supply system with cleaning and stirring functions according to claim 2, characterized in that: The direct stirring section comprises: An electric motor (3), wherein the electric motor (3) is arranged on the top of the sealing cover (2); A rotating shaft (4), the top end of which is fixedly connected to the output end of the motor (3); A stirring blade (401), the stirring blade (401) is arranged on the outer side of the bottom of the rotating shaft (4), and the stirring blade (401) is used for directly stirring and mixing the methanol-water solution; A heating element, which is used to accelerate the mixing of methanol and water, and is arranged on the inner wall of the mixing tank (1).

4. A methanol-water solution supply system with cleaning and stirring functions according to claim 3, characterized in that: The temperature raising member comprises: A heating chamber (103), wherein the heating chamber (103) is arranged on the inner wall of the mixing tank body (1); A plurality of flange heat source pipes (101), wherein the plurality of flange heat source pipes (101) are symmetrically arranged on the top side of the mixing tank body (1), the flange heat source pipes (101) are connected to the heating chamber (103), and the flange heat source pipes (101) are used to pass heat transfer oil; A liquid discharge interface (102), wherein the liquid discharge interface (102) is arranged at the bottom of the mixing tank body (1), and the liquid discharge interface (102) is used for the outflow circulation of the heat transfer oil.

5. The methanol-water solution supply system with cleaning and stirring functions according to claim 3, characterized in that: The polymerization discharge section comprises: A liquid mixing plate (6), the top of which is interlacedly connected with the bottoms of the first feeding port (201) and the second feeding port (202), and the liquid mixing plate (6) is sleeved on the outside of the rotating shaft (4); A circulation cavity (601), wherein the circulation cavity (601) is arranged at the intersection of the first feeding port (201), the second feeding port (202) and the liquid mixing disk (6); A plurality of liquid outlet heads (602) are arranged around the bottom of the liquid mixing plate (6), and the liquid outlet heads (602) are used for discharging methanol and water.

6. The methanol-water solution supply system with cleaning and stirring functions according to claim 3, characterized in that: The centrifugal part comprises: A fixing ring (7), wherein the fixing ring (7) is sleeved on the outer side of the rotating shaft (4); A centrifugal disc (8), wherein the centrifugal disc (8) is sleeved on the outside of the rotating shaft (4) and arranged at the bottom of the fixing ring (7), and a centrifugal cavity (801) for raw materials to enter is opened at the top of the centrifugal disc (8); A plurality of liquid discharge nozzles (803), wherein the plurality of liquid discharge nozzles (803) are disposed around the side of the centrifugal disc (8), the liquid discharge nozzles (803) are connected to the centrifugal chamber (801), and the liquid discharge nozzles (803) are used for centrifugal discharge of raw materials; A guide member, wherein the guide member is arranged on the top of the centrifugal disc (8), and the guide member is used for guiding the feed of the centrifugal chamber (801).

7. A methanol-water solution supply system with cleaning and stirring functions according to claim 6, characterized in that: The guide member comprises a liquid receiving ring (802) arranged on the top of the centrifugal disc (8), and the inner cavity of the liquid receiving ring (802) is connected to the centrifugal cavity (801).

8. The methanol-water solution supply system with cleaning and stirring functions according to claim 1, characterized in that: The isolation assembly comprises: An isolation plate (5), the isolation plate (5) being arranged on the inner wall of the mixing tank (1) and located at the bottom of the mixing assembly; A discharge valve (501), the discharge valve (501) is connected to the bottom of the isolation plate (5), and the discharge valve (501) is used to control the temporary discharge and storage of the mixed methanol-water solution; A discharge pipe (105), the discharge pipe (105) is arranged at the bottom of the mixing tank (1), and the discharge pipe (105) is used for temporarily storing the methanol-water solution; A clean water outlet pipe (104), the clean water outlet pipe (104) being arranged on the side of the discharge pipe (105), and the clean water outlet pipe (104) being used for the outflow of clean water; A rotating part, the rotating part is used to open and close the liquid discharge valve (501), and the rotating part is inserted and connected to the outside of the mixing tank body (1).

9. A methanol aqueous solution supply system with cleaning and stirring functions according to claim 8, characterized in that: The rotating part comprises: A rotating rod (502), the rotating rod (502) is inserted and connected to the side of the mixing tank body (1), and the end of the rotating rod (502) is fixedly connected to the rotating opening and closing end of the liquid discharge valve (501); A hand wheel (503), wherein the hand wheel (503) is arranged at the end of the rotating rod (502) and is located outside the mixing tank body (1).

10. A method for using a methanol-water solution supply system with cleaning and stirring functions, using the supply system according to any one of claims 1 to 9, characterized in that: The method of use includes the following steps: In the first step, the device is powered on, and the direct stirring part in the mixing assembly starts to rotate, and the direct stirring part drives the centrifugal part to rotate in the mixing tank (1); In the second step, the closed component is connected to the pressure supply pipeline of methanol and water, so that the raw material pressure flow enters the supply system and then enters the polymerization discharge part at the bottom of the closed component. The polymerization discharge part injects methanol and water into the centrifugal part. The rotating centrifugal part collides and mixes the methanol and water, and the methanol and water fly out of the centrifugal part due to the centrifugal force. In the third step, the methanol preliminary mixed aqueous solution flying out of the centrifugal part is gathered in the inner cavity of the mixing tank body (1) and at the top of the isolation component, and the rotating direct stirring part finally mixes the methanol preliminary mixed aqueous solution and enters the isolation component to be temporarily stored in the bottom inner cavity of the mixing tank body (1), and the methanol final mixed aqueous solution is discharged from the mixing tank body (1) through the isolation component for use; In the fourth step, only water is introduced into the closed component to clean the centrifugal part, the polymerization discharge part, the direct stirring part, the isolation component and the inner wall of the mixing tank (1), and then discharged from the isolation component to perform self-cleaning of the system.