Zirconium material reaction kettle

Abstract

The utility model discloses a zirconium material reaction kettle which comprises a kettle body, a jacket is arranged outside the kettle body, a stirring shaft is rotationally arranged between the top and the bottom of an inner cavity of the kettle body, an anchor type stirring paddle is arranged on the stirring shaft, and coil pipes are embedded outside two paddles of the anchor type stirring paddle. A cavity is formed in the stirring shaft, a first steam pipe and a first condensate pipe are installed in the stirring shaft, the top end of the first steam pipe and the bottom end of the first condensate pipe penetrate out of the top and the bottom of the stirring shaft respectively, and the bottom end of the first steam pipe is connected with the top ends of the two coil pipes through a tee joint. The top end of the first condensate pipe is connected with the bottom ends of the two coil pipes through a tee joint; the jacket mounted outside the kettle body of the zirconium material reaction kettle is matched with the coil pipe on the stirring shaft inside the kettle body to form an efficient heating system, so that steam can directly act on materials, the heat exchange area is greatly increased, the heating efficiency is improved, the materials are heated more uniformly, and the condition of local overheating or supercooling is effectively avoided.

Description

Technical Field

[0001] This utility model relates to the field of reaction vessel technology, specifically a zirconium material reaction vessel. Background Technology

[0002] In many industrial production fields such as chemical, pharmaceutical, and food industries, reaction vessels are a key reaction equipment and are widely used in various chemical reactions, material mixing, dissolution, heating and other processes. Zirconium reaction vessels are reaction vessels made using zirconium as the main material. They have excellent corrosion resistance and high temperature stability and are often used to synthesize various chemical substances, such as polymers, pharmaceutical intermediates, dyes and pesticides.

[0003] Traditional zirconium reactors typically employ jacketed heating, which involves installing a jacket around the reactor and introducing steam into the jacket to heat the materials inside. However, this heating method suffers from uneven heating, potentially leading to overheating of some materials while underheating others, thus affecting the quality and efficiency of the reaction.

[0004] Therefore, we have designed a zirconium-material reactor to address the aforementioned problems. Utility Model Content

[0005] The purpose of this invention is to address the shortcomings of existing technologies by providing a zirconium-material reactor to solve the problems mentioned in the background art.

[0006] To achieve the above objectives, this utility model provides the following technical solution: a zirconium material reactor, comprising a reactor body, a jacket installed on the outside of the reactor body, a stirring shaft rotatably mounted between the top and bottom of the inner cavity of the reactor body, an anchor-type stirring paddle mounted on the stirring shaft, and coils embedded on the outside of the two blades of the anchor-type stirring paddle, a cavity provided inside the stirring shaft and a first steam pipe and a first condensate pipe installed thereon, the top end of the first steam pipe and the bottom end of the first condensate pipe respectively passing through the top and bottom of the stirring shaft, the bottom end of the first steam pipe being connected to the top end of the two coils through a tee, the top end of the first condensate pipe being connected to the bottom end of the two coils through a tee, a shell mounted on the top of the reactor body, a motor for driving the stirring shaft to rotate being provided on the shell, a second steam pipe mounted on the top of the shell through a bracket, and a second condensate pipe mounted on the bottom of the reactor body through a bracket, the second steam pipe and the second condensate pipe being connected to the first steam pipe and the first condensate pipe respectively through rotary joints.

[0007] Preferably, a speed reducer is installed on the housing, the motor is mounted on the speed reducer, and the output shaft of the motor is connected to the input end of the speed reducer. The output shaft of the speed reducer is located inside the housing. The top of the stirring shaft penetrates through the housing. Both the stirring shaft and the output shaft of the speed reducer are equipped with sprockets. Both sprockets are located inside the housing and are connected by a chain.

[0008] Preferably, the top of the vessel is provided with a feed inlet and a manhole, the manhole is equipped with a manhole cover with an observation window, and the bottom of the vessel is provided with a discharge outlet.

[0009] Preferably, the bottom of the vessel is equipped with four support legs, which are arranged in a circular array.

[0010] Preferably, the upper part of the jacket is provided with a steam inlet, and both the steam inlet of the jacket and the second steam pipe can be connected to an external steam generator through pipes.

[0011] Preferably, the lower part of the jacket is provided with a condensate drain outlet, and bimetallic strip steam traps are installed on both the condensate drain outlet of the jacket and the second condensate pipe.

[0012] Compared with the prior art, this utility model provides a zirconium material reactor, which has the following beneficial effects:

[0013] The jacket installed on the outside of the zirconium reactor body works in conjunction with the coil on the internal stirring shaft to form a highly efficient heating system. Steam is introduced into the jacket through the steam inlet at the top to preheat the material inside the reactor as a whole. The first steam pipe in the cavity inside the stirring shaft can introduce steam into the coil embedded in the outside of the anchor-type stirring blade, so that the steam can act directly on the material, which greatly increases the heat exchange area, improves the heating efficiency, and makes the material more evenly heated, effectively avoiding local overheating or overcooling. Attached Figure Description

[0014] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0015] Figure 2 This is a schematic diagram of the bottom structure of the vessel body of this utility model;

[0016] Figure 3 This is a schematic diagram of the internal structure of the vessel body of this utility model;

[0017] Figure 4 This is a schematic diagram of the internal structure of the stirring shaft of this utility model.

[0018] Reference numerals: 1. Vessel body; 2. Jacket; 3. Stirring shaft; 4. Anchor-type stirring paddle; 5. Coil; 6. First steam pipe; 7. First condensate pipe; 8. Shell; 9. Second steam pipe; 10. Second condensate pipe; 11. Rotary joint; 12. Motor; 13. Reducer; 14. Chain; 15. Manhole cover; 16. Support leg. Detailed Implementation

[0019] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0020] Example 1: Please refer to Figures 1-4 This utility model provides a zirconium-bearing reactor, comprising a reactor body 1, which is cylindrical in shape and made of zirconium material, exhibiting good corrosion resistance and high-temperature stability. A jacket 2 is tightly fitted to the outside of the reactor body 1, used to introduce steam to heat the material inside the reactor body 1. A stirring shaft 3 is rotatably mounted between the top and bottom of the inner cavity of the reactor body 1. The upper and lower connections between the reactor body 1 and the stirring shaft 3 are sealed by shaft seals. The stirring shaft 3 is a hollow shaft structure with an internal cavity, in which a first steam pipe 6 and a first condensate pipe 7 are installed. The top end of the first steam pipe 6 and the bottom end of the first condensate pipe 7 extend from the top and bottom of the stirring shaft 3, respectively. An anchor-type stirring paddle 4 is mounted on the stirring shaft 3, and each of the two blades of the anchor-type stirring paddle 4 is inlaid with a spiral coil 5. Distributed on the blades, it can increase the contact area with the material and improve the heating efficiency. The bottom end of the first steam pipe 6 is connected to the top end of the two coils 5 through a tee. Steam can enter the two coils 5 through the first steam pipe 6. The top end of the first condensate pipe 7 is connected to the bottom end of the two coils 5 through a tee. The condensate generated in the two coils 5 can be discharged through the first condensate pipe 7. The top of the vessel body 1 is equipped with a shell 8. The top of the shell 8 is equipped with a second steam pipe 9 through a bracket. The bottom of the vessel body 1 is equipped with a second condensate pipe 10 through a bracket. The second steam pipe 9 and the second condensate pipe 10 are both connected to the first steam pipe 6 and the first condensate pipe 7 respectively through a rotary joint 11. By setting the rotary joint 11, steam and condensate can flow normally during the rotation of the stirring shaft 3.

[0021] The housing 8 is equipped with a motor 12 for driving the stirring shaft 3 to rotate. A reducer 13 is also installed on the housing 8. The motor 12 is mounted on the reducer 13, and the output shaft of the motor 12 is connected to the input end of the reducer 13. The output shaft of the reducer 13 is located inside the housing 8. The top of the stirring shaft 3 passes through the housing 8. Both the stirring shaft 3 and the output shaft of the reducer 13 are equipped with sprockets. Both sprockets are located inside the housing 8 and are connected by a chain 14. Through the transmission of the chain 14, the motor 12 can drive the stirring shaft 3 to rotate.

[0022] The top of the vessel body 1 is provided with a feed inlet and a manhole. The manhole is equipped with a manhole cover 15 with an observation window to facilitate observation of the material inside the vessel and maintenance. The bottom of the vessel body 1 is provided with a discharge outlet for discharging the reacted material. The bottom of the vessel body 1 is equipped with four support legs 16, which are arranged in a circular array to ensure the stability of the vessel body 1.

[0023] The upper part of the jacket 2 is provided with a steam inlet. Both the steam inlet of the jacket 2 and the second steam pipe 9 can be connected to an external steam generator through pipes. By starting the steam generator, steam can be provided to the reactor. The lower part of the jacket 2 is provided with a condensate drain outlet. Bimetallic strip steam traps are installed on the condensate drain outlet of the jacket 2 and the second condensate pipe 10. Condensate can be discharged in time through the bimetallic strip steam traps.

[0024] Example 2: Based on Example 1, the zirconium reactor has multiple anchor-type stirring paddles 4 installed on the stirring shaft 3. The multiple stirring paddles 4 are evenly distributed along the axial direction of the stirring shaft 3. Each stirring paddle 4 has a coil 5 embedded on its outer blade, which can further improve the stirring effect and heating uniformity of the material. The coil 5 is made of stainless steel, which improves the corrosion resistance and service life of the coil 5. The motor 12 is a variable frequency motor, which can adjust the speed of the stirring shaft 3 according to different process requirements to achieve more precise stirring control.

[0025] Example 3: Based on Example 1, a steam filter is installed on the pipe connecting the steam inlet of the jacket 2 and the second steam pipe 9 of the zirconium material reactor. This filter can remove impurities in the steam and prevent impurities from entering the coil 5 and affecting the heating effect. At the same time, a flow regulating valve is installed on the pipe connecting the steam inlet of the jacket 2 and the second steam pipe 9, which can adjust the steam flow according to the actual heating requirements.

[0026] Example 4: Based on Example 1, the zirconium reactor body 1 is equipped with a temperature sensor and a pressure sensor. The temperature sensor is used to monitor the temperature inside the reactor body 1 in real time, and the pressure sensor is used to monitor the pressure inside the reactor body 1. The sensors transmit the monitored data to the control system. When the temperature or pressure exceeds the set range, the control system can automatically adjust the steam flow or stop the operation of the motor 12 to ensure the safe operation of the reactor. Valves are installed at the inlet and outlet of the reactor body 1 to facilitate the control of material entry and exit. In addition, a heat insulation layer is provided on the outside of the reactor body 1 and the jacket 2 to reduce heat loss and improve energy utilization efficiency.

[0027] Finally, it should be noted that the above description is merely a preferred embodiment of this utility model and is not intended to limit the utility model. Although the utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of this utility model should be included within the protection scope of this utility model.

Claims

1. A zirconium-material reactor, comprising a reactor body (1), characterized in that: The vessel body (1) is fitted with a jacket (2) on its exterior. A stirring shaft (3) is rotatably mounted between the top and bottom of the inner cavity of the vessel body (1). An anchor-type stirring paddle (4) is mounted on the stirring shaft (3). The two blades of the anchor-type stirring paddle (4) are inlaid with coils (5). The stirring shaft (3) has a cavity inside and is fitted with a first steam pipe (6) and a first condensate pipe (7). The top end of the first steam pipe (6) and the bottom end of the first condensate pipe (7) pass through the top and bottom of the stirring shaft (3) respectively. The bottom end of the first steam pipe (6) is connected to the two coils through a tee. The top of (5) is connected to the bottom of the first condensate pipe (7) via a tee. The top of the vessel body (1) is equipped with a shell (8), and a motor (12) for driving the stirring shaft (3) to rotate is provided on the shell (8). The top of the shell (8) is equipped with a second steam pipe (9) via a bracket. The bottom of the vessel body (1) is equipped with a second condensate pipe (10) via a bracket. The second steam pipe (9) and the second condensate pipe (10) are both connected to the first steam pipe (6) and the first condensate pipe (7) respectively via a rotary joint (11).

2. The zirconium-material reactor according to claim 1, characterized in that: A speed reducer (13) is installed on the housing (8), and a motor (12) is installed on the speed reducer (13). The output shaft of the motor (12) is connected to the input end of the speed reducer (13). The output shaft of the speed reducer (13) is located inside the housing (8). The top of the stirring shaft (3) passes through the housing (8). Both the stirring shaft (3) and the output shaft of the speed reducer (13) are equipped with sprockets. Both sprockets are located inside the housing (8), and the two sprockets are connected by a chain (14).

3. The zirconium-material reactor according to claim 1, characterized in that: The top of the vessel body (1) is provided with a feed inlet and a manhole, and a manhole cover plate (15) with an observation window is installed on the manhole. The bottom of the vessel body (1) is provided with a discharge outlet.

4. The zirconium-material reactor according to claim 1, characterized in that: The bottom of the vessel body (1) is equipped with four support legs (16), which are arranged in a ring array.

5. A zirconium-material reactor according to claim 1, characterized in that: The upper part of the jacket (2) is provided with a steam inlet, and the steam inlet of the jacket (2) and the second steam pipe (9) can both be connected to an external steam generator through pipes.

6. A zirconium-material reactor according to claim 1, characterized in that: The lower part of the jacket (2) is provided with a condensate drain outlet, and bimetallic strip steam traps are installed on the condensate drain outlet of the jacket (2) and the second condensate pipe (10).

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