Method for producing down-converting luminescent material

A technology of luminescent materials and manufacturing methods, which is applied in the direction of luminescent materials, chemical instruments and methods, metal material coating technology, etc., can solve the problems of high synthesis cost, insufficient uniformity and dispersion of product particles, etc., and achieve low cost and high efficiency. Photoelectric conversion efficiency, method convenient and quick effect

CN107868941BInactive Publication Date: 2018-11-09HANSHAN NORMAL UNIV
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Patent Information

Authority / Receiving Office
CN · China
Current Assignee / Owner
Publication Date
2018-11-09
Estimated Expiration
Not applicable · inactive patent

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Abstract

The invention discloses a manufacturing method of a down-conversion luminescent material. The manufacturing method comprises the forming steps that 1, multi-target magnetron sputtering equipment is provided; 2, a plurality of target materials are mounted and selected according to to-be-formed rare earth doped oxide, the matrix material of the rare earth doped oxide is rare earth vanadate or rare earth niobate, the target materials comprise matrix rare earth oxide targets, vanadium oxide targets or niobium oxide targets and doped rare earth targets, wherein the matrix rare earth oxide targets,the vanadium oxide targets or the niobium oxide targets correspond to the matrix material, and the doped rare earth targets correspond to a rare earth doped material; 3, a substrate is placed on a base sheet base of a co-sputtering reaction chamber; 4, vacuumizing is conducted on the co-sputtering reaction chamber; and 5, sputtering gas is introduced, and a sputtering technology with the substratetemperature being room temperature to 400 DEG C is conducted, so that the rare earth doped oxide is formed on the surface of the substrate. According to the manufacturing method of the down-conversion luminescent material, large area growth of the down-conversion luminescent material at the low temperature can be achieved, the manufacturing method can be compatible with a microelectronic technology, the technology of the manufacturing method is simple, the cost is low, and the manufacturing method can be effectively combined with the preparation process of solar cells.
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Description

technical field

[0001] The invention relates to a manufacturing method of a nano-optoelectronic device material, in particular to a manufacturing method of a down-conversion luminescent material. Background technique

[0002] In the process of new energy research, solar energy, as a widely distributed, inexhaustible, inexhaustible and pollution-free green and clean energy, has become the first choice for the sustainable development of human society. Therefore, the research of solar cells that directly convert light energy into electrical energy has become a major subject of major investment and vigorous research and development by countries all over the world. The bandgap of single crystal silicon material at room temperature is 1.1eV, which just falls near the peak of solar radiation, and has a relatively high photoelectric energy conversion efficiency. Therefore, silicon-based solar cells have become one of the most promising materials at present and in the future. [00...

Examples

Embodiment Construction

[0028] Such as figure 1 As shown, it is a flow chart of the method of the embodiment of the present invention. In the manufacturing method of the down-conversion luminescent material in the embodiment of the present invention, the down-conversion luminescent material is composed of rare earth doped oxides formed by the following steps:

[0029] Step 1, providing multi-target magnetron sputtering equipment.

[0030] Step 2: install a plurality of targets in the co-sputtering reaction chamber of the multi-target magnetron sputtering equipment, the targets are selected according to the rare earth doped oxide to be formed, the rare earth doped oxide The matrix material is rare earth vanadate or rare earth niobate, the vanadium, niobium and rare earth in the rare earth vanadate or rare earth niobate are all metals, and the rare earth vanadate or rare earth niobate are double metal oxides. Materials include:

[0031] The host material of the rare earth doped oxide corresponds to a...