Glycerin salt separation device
Through the design of rotating shafts, stirring leaves, and automatic separation networks in glycerin distillation device, the problem of salt deposition during glycerin distillation is solved, the effective collection and equipment protection of salt is achieved, and the production efficiency and quality of glycerin are improved.
Patent Information
- Application Number
- CN202411798965.X
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-12-09
- Publication Date
- 2025-01-28
- Estimated Expiration
- Not applicable · inactive patent
AI Technical Summary
During the distillation of glycerol, salts are easily deposited on the inner wall and bottom of the distillation kettle, resulting in equipment corrosion and wear, which intensifies, affecting the service life of the distillation kettle and the production efficiency and quality of glycerol.
Design a glycerin salt division device, use rotating shaft and stirring leaves to stir in the distillation cavity, combined with the design of the collection box and connecting hole, collect the separated salt particles to Flip control to achieve effective collection and reduction of salt particles.
Effectively reduce the number of salt particles deposited in the distillation cavity during the distillation process, protect the equipment, extend its service life, and improve the production efficiency and quality of glycerin.
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Figure CN119367795A_ABST
Abstract
Description
Technical Field
[0001] The present application relates to the technical field of salt separation devices, and in particular to a glycerol salt separation device. Background Art
[0002] Glycerin distillation is a chemical process designed to separate and purify glycerin by heating it to its boiling point in a still and then condensing the vapors.
[0003] In the crude distillation process of glycerol, the common method is to introduce the raw materials into the distillation kettle and evaporate them by heating. In order to remove the liquid and impurities remaining in the distillation kettle, it is usually necessary to stop the device after each distillation cycle, drain the liquid and remove the salt and other residues deposited in the kettle by manual cleaning. This method is not only time-consuming and labor-intensive, but also the manual cleaning process may cause damage to the equipment, increasing maintenance costs.
[0004] However, in the existing glycerin distillation process, salt is easily deposited on the inner wall and bottom of the still, causing increased corrosion and wear of the equipment. This not only affects the service life of the still, but also may reduce the production efficiency and quality of glycerin. Therefore, how to reduce the salt deposited in the still during the distillation process, protect the equipment and extend its service life has become a key issue that needs to be solved urgently. Summary of the invention
[0005] In order to reduce the amount of salt deposited in the distillation kettle during the distillation process, the present application provides a glycerol salt separation device.
[0006] The present application provides a glycerol salt separation device, which adopts the following technical solution: A glycerol salt separation device, comprising A kettle body, wherein a distillation chamber is formed in the kettle body, a heating part is arranged on the kettle body, and a liquid inlet pipe, a liquid outlet pipe and a condenser are arranged on the kettle body; A rotating shaft, rotatably connected to the kettle body and located in the distillation chamber, wherein the kettle body is provided with a driving member for driving the rotating shaft to rotate; A plurality of stirring blades are evenly spaced and arranged on the outer peripheral side of the rotating shaft along the circumferential direction, and the bottom of the stirring blades is in sliding contact with the bottom wall of the distillation chamber; A collecting box is detachably arranged at the bottom of the kettle body, the collecting box is formed with a collecting groove, and the collecting box corresponds to the stirring blade one by one; The kettle body is formed with a connecting hole connecting the distillation chamber and the collecting tank; A hinge shaft, rotatably connected to the kettle body and located at the opening of the communicating hole, wherein a partition net for blocking the opening of the collecting tank is provided on the outer peripheral side of the hinge shaft; A control component is arranged on the kettle body, and when the stirring blade moves to a position close to the opening of the connecting hole, the control component controls the hinge shaft to rotate until the partition net flips over and enters the collecting tank; When the stirring blade moves to a position close to the middle of the communicating hole, the control component controls the hinge shaft to rotate to a position where the partition net flips over and blocks the opening of the communicating hole.
[0007] By adopting the above technical solution, the distillation chamber and the heating part in the kettle body heat and distill the glycerin, and the rotating shaft and the stirring blade are used to stir the glycerin in the distillation chamber to ensure that the glycerin is heated evenly. The bottom of the stirring blade is in sliding contact with the bottom of the distillation chamber, which can effectively push the bottom sediment. Through the design of the collection box and the connecting hole, the separated salt particles can be collected in the collection box, reducing the number of salt particles deposited in the distillation chamber during the distillation process. The design of the hinged shaft and the partition net can automatically flip the partition net when the stirring blade moves to the vicinity of the connecting hole, control the inflow and collection of salt particles, and at the same time block the connecting hole through the partition net, reducing the possibility that the salt particles in the collection tank will be disturbed by the glycerol and drive the distillation chamber when the next stirring blade moves to the vicinity of the connecting hole.
[0008] Optionally, the control assembly includes a control coil spring, a control rope and a control block; The control coil spring is wound around the outer peripheral side of the hinge shaft, one end of the control coil spring is clamped to the hinge shaft, and the other end is clamped to the kettle body; When the control coil spring is released, the hinge shaft is driven to rotate, driving the partition net to flip to a position to block the opening of the communication hole; The control block is slidably connected to the kettle body, and the control block is located on the peripheral wall of the distillation chamber; The control rope is slidably inserted into the kettle body, the control rope is wound around the outer peripheral side of the hinge shaft, one end of the control rope is connected to the hinge shaft, and the other end is connected to the control block; When the stirring blade slides close to the opening of the communicating hole, the stirring blade pushes the control block to slide, and at this time, the control rope pulls the hinge shaft to rotate, so that the partition net flips into the collecting tank; The kettle body is formed with receiving grooves corresponding to the control blocks one by one, and the kettle body is formed with a guiding surface for guiding the control blocks to slide into and out of the receiving grooves; When the stirring blade pushes the control block to slide into the containing groove, the stirring blade passes through the control block, and at this time the control coil spring is released.
[0009] By adopting the above technical solution, the control component realizes the automatic flipping control of the separation net by controlling the coil spring, the control rope and the control block. When the stirring blade pushes the control block to slide, the control rope pulls the hinge shaft to rotate, so that the separation net flips into the collection tank, which is convenient for the collection of salt particles. When the stirring blade is separated from the control block, the control coil spring releases energy, drives the separation net to flip back to its original position, and blocks the opening of the connecting hole. This design not only simplifies the operation process, but also improves the stability and accuracy of the salt particle collection process.
[0010] Optionally, a mounting groove is formed on the end surface of the stirring blade on the side subjected to impact, the stirring blade is rotatably connected to a connecting shaft located in the mounting groove, and a plurality of rotating blades are evenly spaced along the circumferential direction on the outer peripheral side of the connecting shaft; The stirring blade is provided with a power assembly, and during the rotation of the rotating shaft, the power assembly drives the connecting shaft to rotate; The stirring blade forms a salt collecting groove located on the groove wall at the bottom of the installation groove, and the salt collecting groove is located at a position of the installation groove away from the groove opening and away from the rotating shaft; The kettle body is formed with a discharge trough surrounding the rotating shaft and connected to the collecting tank, the connecting shaft and the stirring blade are formed with mutually connected transmission holes, one side opening of the transmission hole is connected to the discharge trough, and the other end opening is connected to the salt collecting tank.
[0011] By adopting the above technical solution, the installation groove, connecting shaft and rotating blades are arranged on the stirring blades, and the connecting shaft and the rotating blades are driven to rotate by the power assembly, thereby enhancing the stirring effect and making the glycerin heated more evenly. During the movement of the rotating blades, the salt particles floating in the glycerin can be driven into the installation groove. The design of the salt collecting tank can collect the salt particles brought into the installation groove by the rotating blades, and transport the salt to the discharge tank through the transmission hole, and then input the salt particles into the collection tank through the discharge tank, further improving the collection efficiency of the salt particles. This structure not only improves the effect of glycerin salt separation, but also simplifies the process of salt collection.
[0012] Optionally, the stirring blade is slidably connected to a blocking plate for the notch of the salt collecting tank; The stirring blade is provided with a driving assembly, and when the rotating blade moves close to the salt collecting tank, the driving assembly drives the blocking plate to open the salt collecting tank; When the rotating blade moves to a position close to the middle of the salt collecting tank, the driving assembly drives the blocking plate to block the salt collecting tank.
[0013] By adopting the above technical solution, a blocking plate is arranged on the stirring blade, and when the rotating blade approaches the salt collecting tank, the blocking plate is driven to open or block the salt collecting tank, thereby realizing precise control of the salt collecting tank. This design reduces the possibility of glycerol directly flowing into the installation tank during the stirring process. At the same time, through the automatic control of the drive component, the operation process is simplified and the salt separation efficiency is improved.
[0014] Optionally, the driving assembly includes a driving rope, a driving block and a driving spring, wherein the driving spring is installed in the stirring blade, and the driving spring drives the blocking plate to block the salt collecting tank; The driving block is slidably connected to the stirring blade and is located in the mounting groove, the driving rope is slidably passed through the stirring blade, one end of the driving rope is connected to the driving block, and the other end is connected to the blocking plate; When the rotating blade rotates close to the salt collecting tank, the rotating blade pushes the driving block to slide, and at this time the driving rope pulls the blocking plate to open the salt collecting tank; When the rotating blade passes through the middle position of the salt collecting tank, the rotating blade slides away from the driving block, and at this time, the driving spring drives the blocking plate to block the salt collecting tank.
[0015] By adopting the above technical solution, the driving assembly realizes precise control of the blocking plate through the cooperation of the driving rope, the driving block and the driving spring. When the rotating blade pushes the driving block to slide, the driving rope pulls the blocking plate to open the salt collecting tank; when the rotating blade passes the middle position of the salt collecting tank, the driving spring drives the blocking plate to block the salt collecting tank. This design not only improves the accuracy of the blocking plate control, but also ensures the stability and continuity of the salt separation process.
[0016] Optionally, the stirring blade forms a sliding groove for the sealing plate to slide, and the side wall of the sealing plate is in sliding contact with the side groove wall surrounding the sliding groove.
[0017] By adopting the above technical solution, a chute for the blocking plate to slide is provided on the stirring blade, thereby ensuring the stability of the blocking plate in the process of opening and blocking the salt collecting tank. The sliding contact between the side wall of the chute and the side wall of the blocking plate can push the salt particles deposited on the top of the blocking plate into the salt collecting tank, thereby reducing the possibility of salt particles entering the chute.
[0018] Optionally, the power assembly includes a power gear, a power column, a power shaft, a connecting gear, a power belt, a linkage chain and a linkage gear; The power column is arranged on the kettle body and is located inside the rotating shaft. The power column rotates relative to the rotating shaft. The power gear is arranged on the outer peripheral side of the power column. The power shaft is rotatably connected to the stirring blade, the connecting gear is arranged on the outer peripheral side of the power shaft, the connecting gear is meshed with the power gear, and the power belt is sleeved on the power shaft and the outer peripheral side of the connecting shaft; The linkage gear is arranged on the outer peripheral side of the connecting shaft, and the linkage belt is sleeved on the linkage gear and meshed with each other.
[0019] By adopting the above technical solution, the power assembly realizes the driving of the connecting shaft and the rotating blades through the cooperation of the power gear, power column, power shaft, connecting gear, power belt, linkage chain and linkage gear. This design not only improves the rotation efficiency of the stirring blade and the rotating blade, but also ensures the uniform heating and sufficient stirring of glycerin in the distillation chamber. At the same time, the power assembly has a compact structure and stable operation, providing reliable power support for the glycerin salt separation process.
[0020] Optionally, a plurality of water-permeable holes are evenly spaced apart on the rotating blade.
[0021] By adopting the above technical solution, water-permeable holes are formed at even intervals on the rotating blades, which can allow glycerin to pass through while limiting the passage of salt particles, making it convenient for the rotating blades to collect the salt particles in the glycerin.
[0022] Optionally, the driving member is a driving motor, and the driving motor is disposed on the outer wall of the kettle body, and the output shaft of the driving motor is connected to the rotating shaft.
[0023] By adopting the above technical solution, a driving motor is used as a driving part, and its output shaft is connected to the rotating shaft to achieve precise control of the stirring blade and the rotating blade. The driving motor has the advantages of stable operation, convenient control, and continuous power output, providing a reliable power guarantee for the glycerol salt separation process. At the same time, the setting of the driving motor also simplifies the operation process, improves the salt separation efficiency and the convenience of operation.
[0024] In summary, the present application includes at least one of the following beneficial effects: 1. The bottom of the stirring blade is in sliding contact with the bottom of the distillation chamber, which can effectively push the bottom sediment. Through the design of the collection box and the connecting hole, the separated salt particles can be collected into the collection box, reducing the number of salt particles deposited in the distillation chamber during the distillation process; 2. During the movement of the rotating blades, the salt particles floating in the glycerin can be driven into the installation tank. The design of the salt collecting tank can collect the salt particles brought into the installation tank by the rotating blades, and transport the salt to the discharge tank through the transmission hole, and then input the salt particles into the collection tank through the discharge tank, further improving the collection efficiency of the salt particles. BRIEF DESCRIPTION OF THE DRAWINGS
[0025] Figure 1It is a schematic diagram of the external structure of an embodiment of the present application; Figure 2 is a schematic diagram of the internal cross-section of the kettle body in the embodiment of the present application; Figure 3 It is a schematic diagram of the internal cross section of the kettle body in the embodiment of the present application; Figure 4 yes Figure 2 A magnified schematic diagram of part A; Figure 5 yes Figure 3 An enlarged schematic diagram of part B; Figure 6 yes Figure 2 An enlarged schematic diagram of part C of FIG. Figure 7 Schematic diagram of the overall structure of the stirring blade in the embodiment of the present application; Figure 8 yes Figure 7 An enlarged schematic diagram of the D portion; Fig. 9 yes Figure 7 Enlarged schematic diagram of part E of .
[0026] Reference numerals: 1, kettle body; 11, kettle body; 111, distillation chamber; 12, kettle cover; 13, liquid inlet pipe; 14, liquid outlet pipe; 15, condenser; 16, heating part; 17, driving motor; 18, connecting hole; 19, containing groove; 191, guide surface; 2, rotating shaft; 21, stirring blade; 211, mounting groove; 212, salt collecting groove; 213, discharging groove; 214, transmission hole; 215, blocking plate; 216, slide groove; 22, rotating groove; 3 , collecting box; 31, collecting trough; 4, hinge shaft; 41, dividing net; 5, control block; 51, control coil spring; 52, control rope; 6, connecting shaft; 61, rotating blade; 611, water permeable hole; 7, power assembly; 71, power gear; 72, power column; 73, power shaft; 74, connecting gear; 75, power belt; 76, linkage chain; 77, linkage gear; 8, driving assembly; 81, driving rope; 82, driving block; 83, driving spring. DETAILED DESCRIPTION
[0027] The following is combined with Figure 1-9 This application is described in further detail.
[0028] The embodiment of the present application discloses a glycerol salt separation device.
[0029] The inventors of the present application have found that during the crude distillation of glycerol, salts are easily deposited in the still, which not only affects the life of the still, but also may affect the production efficiency and product quality of glycerol. To this end, the present application mainly adopts the following scheme to achieve the effect of reducing the amount of salt deposited in the still during the distillation process. The present application is further described in detail below.
[0030] See also Figure 1 and Figure 2 A glycerol salt separation device provided in an embodiment of the present application includes a kettle body 1, wherein the kettle body 1 includes a kettle body 11 and a kettle cover 12, wherein a distillation chamber 111 is formed in the kettle body 11, and the kettle cover 12 is detachably fixed to the top of the kettle body 11, and is used to seal the distillation chamber 111. A liquid inlet pipe 13, a liquid outlet pipe 14 and a condenser 15 are fixedly installed on the kettle body 1, and the liquid inlet pipe 13, the liquid outlet pipe 14 and the condenser 15 are respectively connected to the distillation chamber 111. Among them, the liquid outlet pipe 14 is located near the bottom of the kettle body 11, and is used to discharge the residue in the kettle body 1; the liquid inlet pipe 13 and the condenser 15 are respectively located at the top of the kettle body 1, and the condenser 15 is connected to an external condenser. A heating part 16 is arranged outside the kettle body 1, and the heating part 16 is a heating pipe, which is arranged around the kettle body 1 and is used to heat the glycerol in the distillation chamber 111. When in use, the glycerin to be distilled is introduced into the distillation chamber 111 through the liquid inlet pipe 13, and then the glycerin is heated by the heating part 16. The steam generated when the glycerin is heated is discharged through the condenser 15, and then the steam enters the condenser for condensation.
[0031] See also Figure 3 and Figure 4 The glycerol salt separation device also includes a rotating shaft 2, a stirring blade 21, a hinge shaft 4 and a collecting box 3, wherein the rotating shaft 2 is rotatably connected to the bottom of the kettle body 1, and the rotating shaft 2 is located in the distillation chamber 111. The stirring blade 21 is installed and fixed on the outer peripheral side of the rotating shaft 2, and there are multiple stirring blades 21 and they are evenly spaced along the circumferential direction. When the rotating shaft 2 rotates, it drives the stirring blade 21 to rotate, and at this time, the bottom of the stirring blade 21 is in sliding contact with the bottom of the distillation chamber 111. The kettle body 1 is provided with a driving member, and the driving member is a driving motor 17 (the driving motor 17 is Figure 2 ), the driving motor 17 is fixed on the top of the kettle body 1, the output shaft of the driving motor 17 is rotatably connected to the kettle body 1, the end of the output shaft of the driving motor 17 is fixedly connected with a clamping block, and a clamping groove is formed on the top of the rotating shaft 2, and the clamping block is clamped into the clamping groove, so that the output shaft of the driving motor 17 and the rotating shaft 2 are linked. When the driving motor 17 is started, it drives the rotating shaft 2 to rotate, so that the stirring blade 21 stirs the glycerin in the distillation chamber 111, so that the glycerin can flow, and the uniformity of the glycerin heating is improved.
[0032] See also Figure 3 and Figure 5 The collecting box 3 is fixed to the bottom of the kettle body 1, and the collecting box 3 is a cubic structure. The collecting box 3 is formed with a collecting groove 31. The collecting boxes 3 correspond to the stirring blades 21 one by one, and the collecting boxes 3 are evenly spaced along the circumferential direction. A communicating hole 18 is formed at the bottom of the kettle body 1, and the communicating hole 18 is connected to the distillation chamber 111 and the collecting groove 31.
[0033] See also Figure 3 and Figure 4 The hinge shaft 4 is rotatably connected to the kettle body 1, and the hinge shaft 4 is located at the top opening of the communicating hole 18. There are multiple hinge shafts 4 and they correspond to the communicating holes 18 one by one. A partition net 41 is fixedly connected to the hinge shaft 4 to block the opening of the communicating hole 18. The mesh of the partition net 41 is fine, which can allow the glycerin in the collecting tank 31 to pass through while limiting the passage of salt particles.
[0034] See also Figure 3 and Figure 5 The glycerol salt separation device also includes a control component, which is arranged on the kettle body 1. When the stirring blade 21 moves to a position adjacent to the opening of the connecting hole 18, the control component controls the hinge shaft 4 to rotate, so that the partition net 41 flips into the collecting tank 31; when the stirring blade 21 moves to a position close to the middle of the connecting hole 18, the control component controls the hinge shaft 4 to rotate, so that the partition net 41 flips to a horizontal state, thereby blocking the opening of the connecting hole 18.
[0035] See also Figure 4 and Figure 6 The control assembly includes a control coil spring 51, a control rope 52 and a control block 5. The control coil spring 51 is wound around the outer peripheral side of the hinge shaft 4 and is located in the kettle body 11. One end of the control coil spring 51 is clamped and fixed on the outer peripheral side wall of the hinge shaft 4, and the other end is clamped on the kettle body 1. When the control coil spring 51 is released, the hinge shaft 4 is driven to rotate, driving the partition net 41 to flip to a horizontal state, and the position of the opening of the communication hole 18 is blocked.
[0036] See also Figure 5 and Figure 6 The control block 5 is in a T-shaped block structure, and a T-shaped control groove is formed on the wall of the distillation chamber 111. The control block 5 is slidably connected in the control groove, and part of the control block 5 protrudes into the distillation chamber 111. The control rope 52 is slidably arranged in the side wall of the kettle body 11, and the control rope 52 is wound around the outer peripheral side of the hinge shaft 4. One end of the control rope 52 is fixedly connected to the outer peripheral side wall of the hinge shaft 4, and the other end is connected and fixed to the control block 5.
[0037] When the stirring blade 21 slides close to the opening of the connecting hole 18, the stirring blade 21 pushes the control block 5 to slide. At this time, the control rope 52 pulls the hinge shaft 4 to rotate, so that the partition net 41 flips into the control groove. The kettle body 11 is formed with a receiving groove 19 corresponding to the control block 5. The receiving groove 19 is connected to the control groove, and the kettle body 11 forms a guide surface 191, and the control block 5 slides on the guide surface 191. The guide surface 191 connects the groove wall of the receiving groove 19 away from the distillation chamber 111 and the receiving groove 19, so that the guide surface 191 guides the control block 5 to slide into or out of the receiving groove 19.
[0038] The control block 5 is provided with a control surface which is inclined and is located in the distillation chamber 111; when the control block 5 slides to the guide surface 191, the stirring blade 21 slides on the control surface; then the control block 5 slides on the guide surface 191 and slides toward the receiving tank 19, until the control block 5 slides into the receiving tank 19, the stirring blade 21 separates from the control block 5, at which time the hinge shaft 4 drives the partition net 41 to flip into the collecting tank 31, and during the stirring movement of the stirring blade 21, the salt particles deposited on the bottom of the distillation chamber 111 are pushed onto the partition net 41, and then the salt particles slide along the partition net 41 into the collecting tank 31, thereby collecting the salt particles. Then, as the stirring blade 21 continues to slide, the stirring blade 21 passes through the control block 5, and then the control coil spring 51 (the control coil spring 51 is in Figure 4 The elasticity of the connecting member 12 (marked in the middle) is released, driving the hinge shaft 4 to rotate, so that the control rope 52 pulls the control block 5 from the receiving groove 19 to slide into the control groove. At this time, the partition net 41 flips to a horizontal state to block the opening of the connecting hole 18, thereby reducing the possibility that the salt particles in the collecting tank 31 are brought into the distillation chamber 111 by the disturbed glycerin when the next stirring blade 21 moves close to the opening of the connecting hole 18.
[0039] See also Figure 7 and Figure 8 , a mounting groove 211 is formed on the end surface of the side where the stirring blade 21 is impacted, and when the stirring blade 21 moves, the glycerol impacts the stirring blade 21 and enters the mounting groove 211. In the embodiment of the present application, the number of mounting grooves 211 is multiple, and in other embodiments, the number of mounting grooves 211 can also be one. The stirring blade 21 is rotatably connected to the connecting shaft 6, and the connecting shaft 6 is located in the mounting groove 211, and the connecting shaft 6 corresponds to the mounting groove 211 one by one. The outer peripheral side of the connecting shaft 6 is fixedly connected to a rotating blade 61, and the stirring blade 21 has multiple and is evenly spaced along the circumferential direction, and a plurality of water-permeable holes 611 are evenly spaced on the rotating blade 6. The stirring blade 21 is provided with a power component 7, and during the rotation of the rotating shaft 2, the power component 7 drives the connecting shaft 6 to rotate.
[0040] The power assembly 7 includes a power gear 71, a power column 72, a power shaft 73, a connecting gear 74, a power belt 75, a linkage gear 77 and a linkage chain 76. The power column 72 is fixedly connected to the kettle body 11 (the kettle body 11 is Figure 3 The power column 72 is in a "T" shape, a rotation groove 22 is formed in the rotating shaft 2, the power column 72 extends into the rotation groove 22, and the part of the power column 72 extending into the rotation groove 22 is coaxially arranged with the rotating shaft 2. When the rotating shaft 2 rotates, the power column 72 rotates relative to the rotating shaft 2.
[0041] The power gear 71 is fixedly connected to the outer peripheral side of the power column 72, and the power gear 71 is located in the rotating groove 22. The power shaft 73 is rotatably connected to the stirring blade 21, and the connecting gear 74 is fixedly connected to the outer peripheral side of the power shaft 73. The connecting gear 74 is rotatably connected to the stirring blade 21 and a part of the connecting gear 74 protrudes into the rotating groove 22, and the connecting gear 74 is combined with the power gear 71.
[0042] The power belt 75 is connected end to end and is slidably arranged in the stirring blade 21, and the power belt 75 is sleeved on the power shaft 73 and the connecting shaft 6. The linkage gear 77 is fixedly connected to the outer peripheral side of the connecting shaft 6 and is rotatably connected in the stirring blade 21. The linkage chain 76 is connected end to end and is slidably arranged in the stirring blade 21, and the linkage chain 76 is sleeved on the outer peripheral side of the linkage gear 77.
[0043] When the rotating shaft 2 rotates, the power gear 71 cooperates with the connecting gear 74 to drive the power shaft 73 to rotate, and then the power belt 75 drives the connecting shaft 6 to rotate. At the same time, the linkage chain 76 and the linkage gear 77 cooperate with each other to achieve linkage between the connecting shafts 6. When the connecting shaft 6 rotates, it drives the rotating blade 61 to rotate, so that during the rotation of the stirring blade 21, the rotating blade 61 is in contact with the distillation chamber 111 (the distillation chamber 111 is in contact with the stirring blade 21). Figure 3 While stirring the glycerin in the glycerin, the floating salt particles in the glycerin are brought into the installation tank 211, and in the process of the stirring blades collecting the salt particles, the salt particles are continuously collected and moved to the salt collecting tank 212 (the salt collecting tank 212 is in the installation tank 211) under the action of gravity. Figure 5 (marked in the middle) movement.
[0044] See also Figure 5 The stirring blade 21 is formed with a salt collecting groove 212, which is located on the bottom groove wall of the installation groove 211. The salt collecting groove 212 corresponds to the installation groove 211 one by one, and the salt collecting groove 212 is located at a position where the installation groove 211 is far away from the groove opening and far away from the rotating shaft 2. A discharge groove 213 is formed in the kettle body 11, and the discharge groove 213 is arranged around the rotating shaft 2, and the discharge groove 213 and the connecting hole 18 are connected to each other. Transmission holes 214 that are connected to each other are formed in the connecting shaft 6 and the stirring blade 21, and one side of the transmission hole 214 is connected to the salt collecting groove 212, and the other end of the transmission hole 214 is connected to the connecting hole 18. The salt particles collected in the salt collecting groove 212 enter the transmission hole 214 through the connecting hole 18, and then the salt particles in the transmission hole 214 enter the discharge groove 213 and then enter the connecting hole 18, so that the salt particles can be collected in the collecting tank 31.
[0045] See also Fig. 9The stirring blade 21 is formed with a chute 216, and the notch of the chute 216 is located on the groove wall of the salt collecting groove 212 near the notch of the installation groove 211. The stirring blade 21 is provided with a blocking plate 215, and the blocking plate 215 is slidably connected to the chute 216, and the peripheral side wall of the blocking plate 215 is in sliding contact with the peripheral side groove wall of the chute 216. When the blocking plate 215 slides into the chute 216, the stirring blade 21 pushes the salt particles on the top of the blocking plate 215 into the salt collecting groove 212. A plurality of water filtering holes are evenly spaced on the blocking plate 215 for allowing glycerin to pass through and limiting the passage of salt particles.
[0046] The stirring blade 21 is provided with a driving assembly 8, and the rotating blade 61 moves to a position close to the salt collecting tank 212 (the salt collecting tank 212 is Figure 5 When the rotating blade 61 moves to a position close to the middle of the salt collecting tank 212, the driving assembly 8 drives the blocking plate 215 to block the salt collecting tank 212.
[0047] The driving assembly 8 includes a driving rope 81, a driving block 82 and a driving spring 83. The driving spring 83 is installed in the slide groove 216. One end of the driving spring 83 abuts against the side wall of the blocking plate 215, and the other end abuts against the side wall of the slide groove 216 away from the notch. When the driving spring 83 is elastically released, the driving blocking plate 215 abuts against the salt collecting tank 212 (the salt collecting tank 212 is Figure 5 The salt collecting tank 212 is blocked on one side wall of the chute 216 (marked in the middle).
[0048] See also Figure 8 and Fig. 9 The driving block 82 is slidably connected to the side wall of the installation groove 211. When the rotating blade 61 flips into the installation groove 211, the rotating blade 61 abuts against the driving block 82 and pushes the driving block 82 to slide. The driving rope 81 is slidably arranged in the stirring blade 21. One end of the driving rope 81 is connected and fixed to the driving block 82, and the other end is connected and fixed to the blocking plate 215 away from the salt collecting tank 212 (the salt collecting tank 212 is at Figure 5 (marked in the middle) primary groove wall.
[0049] The rotating blade 61 rotates close to the salt collecting tank 212 (the salt collecting tank 212 is Figure 5During the process of rotating blade 61 first abutting driving block 82, and then when rotating blade 61 continues to rotate, driving block 82 is pushed to slide, at this time driving rope 81 pulls blocking plate 215 to slide into salt collecting tank 212 in chute 216, and driving spring 83 enters a compressed state. When rotating blade 61 moves through the middle position of salt collecting tank 212, rotating blade 61 slides on driving block 82, at this time rotating blade 61 is away from driving block 82, and then driving spring 83 is elastically released, driving blocking plate 215 to slide out of chute 216, and blocking salt collecting tank 212, reducing the possibility that salt particles in mounting groove 211 are brought out of salt collecting tank 212 by disturbed glycerol when the next rotating blade 61 moves to near the opening of connecting hole 18.
[0050] The implementation principle of a glycerol salt separation device in the embodiment of the present application is: During the glycerol distillation process, the salt in the glycerol gathers to form salt particles, and the rotating shaft 2 drives the stirring blade 21 to rotate during the glycerol distillation, thereby improving the uniformity of heat distribution in the glycerol. When the stirring blade 21 moves, the salt particles deposited at the bottom of the distillation chamber 111 are pushed into the collecting tank 31. At the same time, during the movement of the stirring blade 21, the connecting shaft 6 drives the rotating blade 61 to rotate, so that the rotating blade 61 brings the salt particles floating in the glycerol into the installation tank 211, and then pushes the salt particles into the salt collecting tank 212, thereby reducing the number of salt particles floating in the glycerol and improving the evaporation rate of the glycerol.
[0051] The above are all preferred embodiments of the present application, and the protection scope of the present application is not limited thereto. Therefore, any equivalent changes made according to the structure, shape, and principle of the present application should be included in the protection scope of the present application.
Claims
1. A glycerol salt separation device, characterized in that: include A kettle body (1), wherein a distillation chamber (111) is formed in the kettle body (1), a heating portion (16) is provided on the kettle body (1), and a liquid inlet pipe (13), a liquid outlet pipe (14) and a condenser pipe (15) are provided on the kettle body (1); a rotating shaft (2) rotatably connected to the kettle body (1) and located in the distillation chamber (111); the kettle body (1) is provided with a driving member for driving the rotating shaft (2) to rotate; A plurality of stirring blades (21) are evenly spaced and arranged on the outer peripheral side of the rotating shaft (2) along the circumferential direction, and the bottom of the stirring blades (21) is in sliding contact with the bottom wall of the distillation chamber (111); A collecting box (3) is detachably arranged at the bottom of the kettle body (1), the collecting box (3) is formed with a collecting groove (31), and the collecting box (3) corresponds one-to-one with the stirring blade (21); The kettle body (1) is formed with a communication hole (18) communicating with the distillation chamber (111) and the collecting tank (31); A hinge shaft (4) rotatably connected to the kettle body (1) and located at the opening of the communicating hole (18); a partition net (41) for sealing the opening of the collecting tank (31) is provided on the outer peripheral side of the hinge shaft (4); a control component, arranged on the kettle body (1), and when the stirring blade (21) moves to a position close to the opening of the connecting hole (18), the control component controls the hinge shaft (4) to rotate until the partition net (41) flips over into the collecting tank (31); When the stirring blade (21) moves to a position close to the middle of the communicating hole (18), the control component controls the hinge shaft (4) to rotate to a position where the partition net (41) turns over and blocks the opening of the communicating hole (18).
2. A glycerol salt separation device according to claim 1, characterized in that: The control assembly comprises a control coil spring (51), a control rope (52) and a control block (5); The control coil spring (51) is wound around the outer circumference of the hinge shaft (4), one end of the control coil spring (51) is clamped to the hinge shaft (4), and the other end is clamped to the kettle body (1); When the control coil spring (51) is released, it drives the hinge shaft (4) to rotate, driving the partition net (41) to flip to a position that blocks the opening of the communication hole (18); The control block (5) is slidably connected to the kettle body (1), and the control block (5) is located on the peripheral wall of the distillation chamber (111); The control rope (52) is slidably inserted into the kettle body (1), the control rope (52) is wound around the outer peripheral side of the hinge shaft (4), one end of the control rope (52) is connected to the hinge shaft (4), and the other end is connected to the control block (5); When the stirring blade (21) slides close to the opening of the communicating hole (18), the stirring blade (21) pushes the control block (5) to slide, and at this time the control rope (52) pulls the hinge shaft (4) to rotate, so that the partition net (41) flips over into the collecting tank (31); The kettle body (1) is formed with a receiving groove (19) corresponding one-to-one to the control block (5), and the kettle body (1) is formed with a guide surface (191) for guiding the control block (5) to slide into and out of the receiving groove (19); When the stirring blade (21) pushes the control block (5) to slide into the accommodating groove (19), the stirring blade (21) passes through the control block (5), and at this time the control coil spring (51) is released.
3. A glycerol salt separation device according to claim 1, characterized in that: A mounting groove (211) is formed on the end surface of the stirring blade (21) on the impact side, the stirring blade (21) is rotatably connected to a connecting shaft (6) located in the mounting groove (211), and a plurality of rotating blades (61) are evenly spaced along the circumferential direction on the outer peripheral side of the connecting shaft (6); The stirring blade (21) is provided with a power assembly (7), and when the rotating shaft (2) rotates, the power assembly (7) drives the connecting shaft (6) to rotate; The stirring blade (21) is formed with a salt collecting groove (212) located on the bottom groove wall of the installation groove (211), and the salt collecting groove (212) is located at a position of the installation groove (211) away from the groove opening and away from the rotating shaft (2); The kettle body (1) is formed with a discharge trough (213) surrounding the rotating shaft (2) and connected to the collecting tank (31); the connecting shaft (6) and the stirring blade (21) are formed with a transmission hole (214) that is connected to each other; a hole on one side of the transmission hole (214) is connected to the discharge trough (213), and a hole on the other end is connected to the salt collecting tank (212).
4. A glycerol salt separation device according to claim 3, characterized in that: The stirring blade (21) is slidably connected to a blocking plate (215) for a notch of the salt collecting tank (212); The stirring blade (21) is provided with a driving assembly (8), and when the rotating blade (61) moves close to the salt collecting tank (212), the driving assembly (8) drives the blocking plate (215) to open the salt collecting tank (212); When the rotating blade (61) moves to a position close to the middle of the salt collecting tank (212), the driving assembly (8) drives the blocking plate (215) to block the salt collecting tank (212).
5. A glycerol salt separation device according to claim 4, characterized in that: The driving assembly (8) comprises a driving rope (81), a driving block (82) and a driving spring (83); the driving spring (83) is installed in the stirring blade (21); the driving spring (83) drives the blocking plate (215) to block the salt collecting tank (212); The driving block (82) is slidably connected to the stirring blade (21) and is located in the mounting groove (211); the driving rope (81) is slidably inserted through the stirring blade (21); one end of the driving rope (81) is connected to the driving block (82) and the other end is connected to the blocking plate (215); When the rotating blade (61) rotates close to the salt collecting tank (212), the rotating blade (61) pushes the driving block (82) to slide, and at this time the driving rope (81) pulls the blocking plate (215) to open the salt collecting tank (212); When the rotating blade (61) passes through the middle position of the salt collecting tank (212), the rotating blade (61) slides away from the driving block (82), and at this time, the driving spring (83) drives the blocking plate (215) to block the salt collecting tank (212).
6. A glycerol salt separation device according to claim 5, characterized in that: The stirring blade (21) is formed with a sliding groove (216) for the blocking plate (215) to slide, and the side wall of the blocking plate (215) is in sliding contact with the peripheral groove wall of the sliding groove (216).
7. A glycerol salt separation device according to claim 3, characterized in that: The power assembly (7) comprises a power gear (71), a power column (72), a power shaft (73), a connecting gear (74), a power belt (75), a linkage chain (76) and a linkage gear (77); The power column (72) is arranged on the kettle body (1) and is located inside the rotating shaft (2); the power column (72) and the rotating shaft (2) rotate relative to each other; and the power gear (71) is arranged on the outer peripheral side of the power column (72); The power shaft (73) is rotatably connected to the stirring blade (21), the connecting gear (74) is arranged on the outer peripheral side of the power shaft (73), the connecting gear (74) is meshed with the power gear (71), and the power belt (75) is sleeved on the outer peripheral side of the power shaft (73) and the connecting shaft (6); The linkage gear (77) is arranged on the outer peripheral side of the connecting shaft (6), and the linkage belt is sleeved on the linkage gear (77) and meshed with each other.
8. A glycerol salt separation device according to claim 3, characterized in that: The rotating blade (61) is provided with a plurality of water-permeable holes (611) at even intervals.
9. A glycerol salt separation device according to claim 1, characterized in that: The driving member is a driving motor (17), and the driving motor (17) is arranged on the outer wall of the kettle body (1), and the output shaft of the driving motor (17) is connected to the rotating shaft (2).