Polyethylene polyamine derivative synthesis reactor
By using a stirring mechanism that combines the separator cylinder and the twisted dragon plate in the stirred tank reactor, the material can drive the solid material flow during the circulation of liquid, which solves the problem of uneven heat received by the solid-liquid mixture during the agitation process, and realizes the The uniform heating and heat transfer efficiency of the material are improved.
Patent Information
- Application Number
- CN202411746038.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-12-02
- Publication Date
- 2025-02-18
AI Technical Summary
In a stirred tank reactor, during the agitation process, solid material accumulates on the outer bottom due to centrifugal force, resulting in uneven heating of the material.
A polyethylene polyamine derivative synthesis reactor is designed, and a stirring mechanism is used to cooperate with a separator cylinder and a twisted dragon plate to enable the material to drive the flow of solid material during the circulating flow of liquid, and evenly contact the heat transferred by the heat conducting mechanism.
Through this design, solid materials are avoided to accumulate under the action of centrifugal force, uniform heating of the material is achieved, and heat transfer efficiency of the reaction process is improved.
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Figure CN119455871A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of reactors, in particular to a polyethylene polyamine derivative synthesis reactor. Background Art
[0002] At present, the synthesis of polyethylene polyamine derivatives is a chemical synthesis process with important application value. By selecting appropriate raw materials, synthesis methods and reaction conditions, polyethylene polyamine derivatives with different structures and properties can be synthesized to meet the application needs of different fields. The polyethylene polyamine derivative synthesis reactor is a key equipment for synthesizing polyethylene polyamine derivatives. Common ones include stirred tank reactors, tubular reactors, etc. The stirred tank reactor has a stirring device that can fully mix the materials and is suitable for a variety of reaction conditions. It can be operated intermittently or continuously and has high flexibility. In the synthesis of polyethylene polyamine derivatives, the stirred tank reactor can promote the reaction by controlling parameters such as stirring speed, temperature and pressure;
[0003] During the material reaction process, when the material is stirred by the stirring blade, when the material is a solid-liquid mixture, under the action of the stirring centrifugal force, the heavier solid material accumulates at the bottom of the periphery, resulting in uneven heating of the material. Summary of the invention
[0004] To achieve the above object, the present invention is implemented by the following technical scheme: a polyethylene polyamine derivative synthesis reactor, comprising:
[0005] A reaction tank, which provides a place for the synthesis reaction and is a double-layer tank body, a bracket is installed on the outside of the reaction tank, and a discharge pipe is installed at the bottom of the reaction tank;
[0006] A sealing mechanism, which is used to seal the reaction tank during operation, and the sealing mechanism is installed on the top of the reaction tank, and a motor is installed on the top of the sealing mechanism;
[0007] A stirring mechanism, which is used to stir the material and is installed inside the reaction tank;
[0008] A heat-conducting mechanism, which is used to heat the reacting material and is installed between the double-layer structure of the reaction tank;
[0009] The stirring mechanism comprises a connecting shaft, the top end of the connecting shaft is connected to the output end of the motor through a coupling, and a connecting disk is fixedly installed at the bottom end of the connecting shaft, and a stirring blade is fixedly installed at the bottom of the connecting disk, a sleeve is fixedly installed on the outer side of the connecting shaft, and connecting rings are fixedly installed at both ends of the outer side of the sleeve, and a separation cylinder is fixedly installed on the outer side of the connecting ring, and the separation cylinder cooperates with the auger plate to make the materials on both sides of the inner and outer sides of the separation cylinder circulate during the rotation process, so that the solid-liquid material can drive the solid material to flow during the circulation of the liquid, and evenly contact the heat transferred by the heat conduction mechanism, so as to avoid directly driving the material to rotate for stirring and mixing, resulting in the solid material under the action of centrifugal force. The mass of the solid material increases and accumulates at the bottom of the outer periphery of the material, resulting in uneven heating between the materials, an auger plate is fixedly installed between the separation cylinder and the sleeve, a connecting strip is fixedly installed on the outer side of the separation cylinder, and the connecting strip is evenly installed along the center position of the separation cylinder, and a brush strip is fixedly installed on the outer side of the connecting strip, and the outer side of the brush strip contacts the inner wall of the reaction tank.
[0010] Preferably, the sealing mechanism comprises a fixing ring, the inner wall of the fixing ring is fixedly connected to the top of the outer side of the reaction tank, and the top of the fixing ring is detachably installed with bolts, the top of the fixing ring is fixedly installed with a cover plate by bolts, the top of the cover plate is fixedly installed with a top cover, the top of the top cover is fixedly connected to the bottom of the motor, and the bottom of the cover plate is fixedly installed with a sealing cylinder, and the sealing cylinder cooperates with the inner disk and the outer disk to block the gas passing through the bearing by the sealing cylinder, so that the gas cannot be discharged from the reaction tank through the gap between the connecting shaft and the motor output end and the sealing mechanism, thereby avoiding the reduction of the sealing effect and preventing The high-temperature gas inside the reaction tank impacts the motor, causing the motor temperature to be too high. An inner disk is fixedly installed on the bottom of the sealing cylinder, the inner wall of the inner disk is fixedly connected to the outer side of the connecting shaft, and a bearing is fixedly installed on the outer side of the inner disk. The inner disk is rotatably installed with an outer disk through the bearing, and the outer side of the outer disk contacts the inner wall of the reaction tank. A groove disk is fixedly installed on the outer side of the sealing cylinder, and sliding grooves are evenly opened on the outer side of the groove disk, and arc sliders are slidably installed at the sliding grooves of the groove disk, and a rubber ring is fixedly installed on the outer side of the arc slider, and the outer side of the rubber ring is tightly fitted with the inner wall of the reaction tank.
[0011] The top of the connecting rod is fixedly provided with a pad, and the opposite surface of the pad is an inclined surface inclined from top to bottom to the outside, and the outer side of the inclined surface block is an inclined surface inclined from top to bottom to the outside, and the inclined surface of the inclined surface block is adapted to the upward movement of the connecting rod.
[0012] Preferably, the heat conduction mechanism comprises a liquid inlet pipe and a liquid outlet pipe, the liquid inlet pipe is fixedly mounted on the top of the outside of the reaction tank, the liquid outlet pipe is fixedly mounted on the bottom of the outside of the reaction tank, a corrugated cylinder is fixedly mounted at the center position between the double-layer structure of the reaction tank, the inner wall of the corrugated cylinder is uniformly provided with arcuate annular grooves along the axial direction, and the flow rate of hot water is limited when it reaches the convex position through the arcuate annular grooves uniformly provided on the inner wall of the corrugated cylinder during the process of passing through, and diffused to both sides, so that the hot water is uniformly diffused around the outside of the reaction tank during the process of being introduced, so that the temperature of the hot water on the same horizontal plane is kept consistent when the hot water conducts heat. , to avoid uneven heating of the reaction tank, so that it cannot transfer the same amount of heat to the material, a top ring is fixedly installed on the top of the double-layer gap of the reaction tank, a bevel ring is fixedly installed on the top of the corrugated cylinder, the bevel ring is located below the liquid inlet pipe, and the top ring is located above the liquid inlet pipe, a through groove ring is fixedly installed on the bottom of the corrugated cylinder, through grooves are evenly opened on the top of the through groove ring, a spiral plate is fixedly installed on the bottom of the through groove ring, the spiral plate is evenly installed along the center position of the through groove ring, and a bottom ring is fixedly installed on the end of the spiral plate away from the through groove ring, and the spiral plate is located above the liquid outlet pipe.
[0013] The present invention provides a polyethylene polyamine derivative synthesis reactor, which has the following beneficial effects:
[0014] 1. The polyethylene polyamine derivative synthesis reactor cooperates with the dividing cylinder and the auger plate to make the materials on both sides of the dividing cylinder circulate during the rotation, so that the solid-liquid mixed material can drive the solid material to flow during the circulation of the liquid, and evenly contact the heat transferred by the heat conduction mechanism, thereby avoiding directly driving the material to rotate for stirring and mixing, resulting in the accumulation of the solid material at the bottom of the outer periphery of the material under the action of centrifugal force, resulting in uneven heating between the materials.
[0015] Second, the polyethylene polyamine derivative synthesis reactor uses a sealing cylinder to cooperate with an inner disk and an outer disk so that the gas passing through the bearing is blocked by the sealing cylinder, making it impossible for the gas to be discharged from the reaction tank through the gap between the connecting shaft and the motor output end and the sealing mechanism, thereby avoiding a reduction in the sealing effect and preventing the high-temperature gas inside the reaction tank from impacting the motor and causing the motor temperature to be too high.
[0016] 3. The polyethylene polyamine derivative synthesis reactor, through the cooperation of the pad and the inclined block, increases the internal air pressure, so that the sliding plate is pushed up by the pressure, driving the connecting rod and the inclined block to move upward, and utilizing the opposite surface of the pad to be an inclined surface inclined from top to bottom to the outside and the outer side of the inclined surface block to be an inclined surface inclined from top to bottom to the outside, so that the pad drives the arc slider to expand, increases the contact pressure between the rubber ring and the inside of the reaction tank, and as the air pressure increases, the contact pressure is also increased, thereby improving the sealing of the equipment during the reaction.
[0017] Fourth, the polyethylene polyamine derivative synthesis reactor has arc-shaped annular grooves uniformly arranged on the inner wall of the corrugated cylinder. When the hot water passes through the process, the flow is restricted when it reaches the convex position and diffuses to both sides. In the process of hot water introduction, it is evenly diffused around the outside of the reaction tank. When the hot water conducts heat, the temperature of the hot water on the same horizontal plane remains consistent, avoiding uneven heating of the reaction tank, which makes it impossible to transfer the same amount of heat to the material. BRIEF DESCRIPTION OF THE DRAWINGS
[0018] Figure 1 This is a schematic diagram of the external structure of a polyethylene polyamine derivative synthesis reactor of the present invention;
[0019] Figure 2 This is a structural dissection diagram of a polyethylene polyamine derivative synthesis reactor of the present invention;
[0020] Figure 3 This is a schematic diagram of the stirring mechanism structure of the present invention;
[0021] Figure 4 This is a structural anatomical diagram of the stirring mechanism of the present invention;
[0022] Figure 5 It is a schematic diagram of the sealing mechanism structure of the present invention;
[0023] Figure 6 This is a structural anatomical diagram of the sealing mechanism of the present invention;
[0024] Figure 7 It is a partial structural anatomical diagram of the sealing mechanism of the present invention;
[0025] Figure 8 It is a schematic diagram of the heat conduction mechanism structure of the present invention;
[0026] Fig. 9It is a partial structural dissection diagram of the heat conduction mechanism of the present invention.
[0027] In the figure: 1, reaction tank; 2, stirring mechanism; 3, sealing mechanism; 4, heat conduction mechanism; 5, bracket; 6, discharge pipe; 7, motor; 21, separation cylinder; 22, connecting strip; 23, connecting plate; 24, stirring blade; 25, brush strip; 26, connecting shaft; 27, shaft sleeve; 28, auger plate; 29, connecting ring; 301, fixing ring; 302, cover plate; 303, bolt; 304, outer plate; 305, inner plate; 306, bearing; 307, top cover; 308, sliding plate; 309, rubber ring; 310, groove plate; 311, arc slider; 312, sealing cylinder; 313, connecting rod; 314, ramp block; 315, cushion block; 41, liquid inlet pipe; 42, liquid outlet pipe; 43, bottom ring; 44, spiral plate; 45, through-groove ring; 46, corrugated cylinder; 47, ramp ring; 48, top ring. DETAILED DESCRIPTION
[0028] The present invention is further described in detail below in conjunction with the accompanying drawings and specific embodiments. The embodiments of the present invention are provided for the purpose of illustration and description, and are not intended to be exhaustive or to limit the present invention to the disclosed forms. Many modifications and variations will be apparent to those of ordinary skill in the art. The embodiments are selected and described in order to better illustrate the principles and practical applications of the present invention, and to enable those of ordinary skill in the art to understand the present invention and thereby design various embodiments with various modifications suitable for specific uses.
[0029] The first embodiment, as Figures 1 to 4 As shown, the present invention provides a technical solution: a polyethylene polyamine derivative synthesis reactor, comprising:
[0030] A reaction tank 1, which provides a place for the synthesis reaction and is a double-layer tank body, a bracket 5 is installed on the outside of the reaction tank 1, and a discharge pipe 6 is installed at the bottom of the reaction tank 1;
[0031] A sealing mechanism 3, which is used to seal the reaction tank 1 during operation. The sealing mechanism 3 is installed on the top of the reaction tank 1, and a motor 7 is installed on the top of the sealing mechanism 3;
[0032] A stirring mechanism 2, which is used to stir the material and is installed inside the reaction tank 1;
[0033] A heat conducting mechanism 4, which is used to heat the reacting material and is installed between the double-layer structure of the reaction tank 1;
[0034] Among them, the stirring mechanism 2 includes a connecting shaft 26, the top end of the connecting shaft 26 is connected to the output end of the motor 7 through a coupling, and a connecting disk 23 is fixedly installed on the bottom end of the connecting shaft 26, and a stirring blade 24 is fixedly installed on the bottom of the connecting disk 23. A shaft sleeve 27 is fixedly installed on the outer side of the connecting shaft 26, and connecting rings 29 are fixedly installed on both ends of the outer side of the shaft sleeve 27. The connecting shaft 26 is driven to rotate by the motor 7, so that the connecting shaft 26 drives the shaft sleeve 27 and the connecting disk 23 to rotate, and the stirring blade 24 is driven by the connecting disk 23 to rotate at the bottom of the inner side of the reaction tank 1, so as to drive the materials inside the reaction tank 1 to be evenly mixed. At the same time, during the rotation of the shaft sleeve 27, the separation cylinder 21 is driven to rotate through the connecting ring 29, and during the rotation of the separation cylinder 21, the inner auger plate 28 and the outer connecting strip 22 are driven to rotate. A separation cylinder 21 is fixedly installed on the outer side of the connecting ring 29, an auger plate 28 is fixedly installed between the separation cylinder 21 and the shaft sleeve 27, a connecting strip 22 is fixedly installed on the outer side of the separation cylinder 21, the connecting strip 22 is evenly installed along the center position of the circle of the separation cylinder 21, and a brush strip 25 is fixedly installed on the outer side of the connecting strip 22. During the rotation of the auger plate 28, the spiral shape drives the material below to surge upward, and after reaching the top of the separation cylinder 21, it diffuses outward under the action of centrifugal force, and the material on the outside of the separation cylinder 21 moves up after the bottom material moves down to fill the space, so that the material inside and outside the separation cylinder 21 forms a circulating flow, and cooperates with the heat conduction mechanism 4 to heat the inner tank body of the reaction tank 1, and transfers heat to the material on the outside of the separation cylinder 21 for heating, and the outer side of the brush strip 25 contacts the inner wall of the reaction tank 1.
[0035] The second embodiment is based on the first embodiment. Figures 5 to 7As shown, the sealing mechanism 3 includes a fixing ring 301, the inner wall of the fixing ring 301 is fixedly connected to the top of the outer side of the reaction tank 1, and the top of the fixing ring 301 is detachably installed with a bolt 303, the top of the fixing ring 301 is fixedly installed with a cover plate 302 by the bolt 303, the top of the cover plate 302 is fixedly installed with a top cover 307, and the top of the top cover 307 is fixedly connected to the bottom of the motor 7. After the material is introduced into the reaction tank 1, the cover plate 302 and the fixing ring 301 are fixedly connected by the bolt 303, so that the rubber ring 30 9 and the outer disk 304 are in close contact with the inner wall of the reaction tank 1. During the heating reaction of the material inside the reaction tank 1, the pressure inside the reaction tank 1 increases. Through the cooperation between the inner disk 305 and the outer disk 304, the gas inside the reaction tank 1 passes through the bearing 306 under the blockage of the inner disk 305 and the outer disk 304 and reaches the top of the outer disk 304 and the inner disk 305. The bottom of the cover plate 302 is fixedly installed with a sealing cylinder 312, and the bottom of the sealing cylinder 312 is fixedly installed with the inner disk 305. The inner wall of the inner disk 305 is connected to the connecting shaft 26. The outer side of the inner disk 305 is fixedly connected, and the outer side of the inner disk 305 is fixedly installed with a bearing 306. The inner disk 305 is rotatably installed with the outer disk 304 through the bearing 306. The outer side of the outer disk 304 contacts the inner wall of the reaction tank 1. The outer side of the sealing cylinder 312 is fixedly installed with a groove disk 310. The outer side of the groove disk 310 is evenly provided with sliding grooves, and the sliding grooves of the groove disk 310 are slidably installed with arc sliders 311. Under the action of air pressure, the sealing cylinder 312 blocks the gas inside the reaction tank 1, so that it pushes the sliding disk 308 along the groove disk 310. The inner wall slides upward, and during the sliding process, the connecting rod 313 drives the inclined surface block 314 to move upward. The inclined surface of the inclined surface block 314 slides and fits with the inclined surface of the cushion block 315. During the upward movement of the inclined surface block 314, the cushion block 315 is pushed to make the arc slider 311 expand outward, driving the rubber ring 309 to squeeze the inner wall of the reaction tank 1, thereby increasing the contact pressure at the gap position and improving the sealing performance. The outer side of the arc slider 311 is fixedly installed with a rubber ring 309, and the outer side of the rubber ring 309 is tightly fitted with the inner wall of the reaction tank 1.
[0036] Circular holes are evenly arranged on the top of the groove plate 310, and connecting rods 313 are slidably installed at the circular holes of the groove plate 310, a sliding plate 308 is fixedly installed on the bottom end of the connecting rod 313, the outer side of the sliding plate 308 is slidably matched with the inner wall of the groove plate 310, a slope block 314 is fixedly installed on the top end of the connecting rod 313, and a cushion block 315 is fixedly installed on the opposite surface of the arc slider 311, the opposite surface of the cushion block 315 is an inclined surface inclined from top to bottom toward the outside, the outer side of the inclined surface block 314 is an inclined surface inclined from top to bottom toward the outside, and the inclined surface of the inclined surface block 314 is matched with the inclined surface of the cushion block 315.
[0037] The third embodiment is based on the first and second embodiments. Figures 8 to 9As shown, the heat conduction mechanism 4 includes a liquid inlet pipe 41 and a liquid outlet pipe 42. The liquid inlet pipe 41 is fixedly installed on the top of the outer side of the reaction tank 1, and the liquid outlet pipe 42 is fixedly installed on the bottom of the outer side of the reaction tank 1. A corrugated cylinder 46 is fixedly installed at the center position between the double-layer structures of the reaction tank 1. The inner wall of the corrugated cylinder 46 is evenly provided with arc-shaped annular grooves along the axial direction. A top ring 48 is fixedly installed on the top of the double-layer gap of the reaction tank 1. The liquid inlet pipe 41 and the liquid outlet pipe 42 are connected with the hot water pipeline, so that the hot water is introduced into the gap of the double-layer tank body of the reaction tank 1 along the liquid inlet pipe 41, and enters the inner side of the corrugated cylinder 46 by its own gravity under the restriction of the inclined ring 47 and the top ring 48. The arc-shaped annular grooves evenly provided on the inner side of the corrugated cylinder 46 along the axial direction limit the flow rate of the flowing hot water, so that it slowly passes through the corrugated cylinder On the inner side of 46, a bevel ring 47 is fixedly installed on the top of the bellows 46, the bevel ring 47 is located below the liquid inlet pipe 41, and the top ring 48 is located above the liquid inlet pipe 41. A through groove ring 45 is fixedly installed on the bottom of the bellows 46, and through grooves are evenly opened on the top of the through groove ring 45. A spiral plate 44 is fixedly installed on the bottom of the through groove ring 45. The spiral plates 44 are evenly installed along the center position of the through groove ring 45, and a bottom ring 43 is fixedly installed on one end of the spiral plate 44 away from the through groove ring 45. When hot water flows to the bottom of the bellows 46, the hot water is evenly guided by the through groove ring 45, so that the material flows evenly downward and enters the gap between the spiral plates 44. Finally, the hot water after the heat conduction is completed is led out of the reaction tank 1 through the liquid outlet pipe 42, and the spiral plate 44 is located above the liquid outlet pipe 42.
[0038] When in use, the staff introduces the materials required for the synthesis of polyethylene polyamine derivatives into the reaction tank 1, then seals the reaction tank 1 with the sealing mechanism 3, then connects the hot water pipe with the heat conducting mechanism 4, so that the hot water is introduced into the gap of the double-layer structure of the reaction tank 1 to heat the materials in the reaction tank 1, and then starts the motor 7 to drive the stirring mechanism 2 to operate to stir the materials, and cooperates with the heat conducting mechanism 4 to evenly heat the materials during the reaction process.
[0039] After the material is introduced into the reaction tank 1, the cover plate 302 and the fixing ring 301 are fixedly connected by bolts 303, so that the rubber ring 309 and the outer disk 304 are closely attached to the inner wall of the reaction tank 1. During the heating reaction of the material inside the reaction tank 1, the pressure inside the reaction tank 1 increases. Through the cooperation between the inner disk 305 and the outer disk 304, the gas inside the reaction tank 1 passes through the bearing 306 under the obstruction of the inner disk 305 and the outer disk 304, and reaches the top of the outer disk 304 and the inner disk 305. Under, in cooperation with the sealing cylinder 312 to block the internal gas of the reaction tank 1, it pushes the sliding plate 308 to slide upward along the inner wall of the groove plate 310. During the sliding process, the connecting rod 313 drives the inclined surface block 314 to move upward. The inclined surface of the inclined surface block 314 slides with the inclined surface of the cushion block 315. During the upward movement of the inclined surface block 314, the cushion block 315 is pushed to make the arc slider 311 expand outward, driving the rubber ring 309 to squeeze the inner wall of the reaction tank 1, thereby increasing the contact pressure at the gap position and improving the sealing performance.
[0040] In the process of stirring the material inside the reaction tank 1 by the stirring mechanism 2, the motor 7 drives the connecting shaft 26 to rotate, so that the connecting shaft 26 drives the sleeve 27 and the connecting plate 23 to rotate, and the connecting plate 23 drives the stirring blade 24, so that the stirring blade 24 rotates at the bottom of the inner side of the reaction tank 1, driving the material inside the reaction tank 1 to be evenly mixed. At the same time, in the process of the rotation of the sleeve 27, the connecting ring 29 drives the separation cylinder 21 to rotate. In the process of the rotation of the separation cylinder 21, the inner auger plate 28 and the outer connecting strip 22 are driven to rotate. In the process of the rotation of the auger plate 28, the spiral shape drives the material below to surge upward, and after reaching the top of the separation cylinder 21, it diffuses outward under the action of centrifugal force. After the material on the outside of the separation cylinder 21 moves up, it moves downward to fill the space, so that the materials inside and outside the separation cylinder 21 form a circulating flow, and cooperate with the heat conduction mechanism 4 to heat the inner tank body of the reaction tank 1, and transfer the heat to the material on the outside of the separation cylinder 21 for heating.
[0041] In the heat conduction mechanism 4, the liquid inlet pipe 41 and the liquid outlet pipe 42 are connected with the hot water pipeline, so that the hot water is introduced into the gap of the double-layer tank body of the reaction tank 1 along the liquid inlet pipe 41, and enters the inner side of the corrugated cylinder 46 by its own gravity under the restriction of the inclined ring 47 and the top ring 48. The arc-shaped annular grooves uniformly opened along the axial direction on the inner side of the corrugated cylinder 46 limit the flow rate of the flowing hot water, so that it slowly passes through the inner side of the corrugated cylinder 46. When the hot water flows to the bottom of the corrugated cylinder 46, the hot water is uniformly guided by the through groove ring 45, so that the material flows evenly downward and enters the gap between the spiral plates 44. Finally, the hot water after the heat conduction is discharged out of the reaction tank 1 through the liquid outlet pipe 42.
[0042] Obviously, the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field and related fields without creative work should fall within the scope of protection of the present invention. The structures, devices and operating methods not specifically described and explained in the present invention are implemented according to the conventional means in the field unless otherwise specified and limited.
Claims
1. A polyethylene polyamine derivative synthesis reactor, characterized in that: include: A reaction tank (1), which provides a place for a synthesis reaction and is a double-layer tank body, a bracket (5) is installed on the outside of the reaction tank (1), and a discharge pipe (6) is installed at the bottom of the reaction tank (1); A sealing mechanism (3), the sealing mechanism (3) being used to seal the reaction tank (1) during operation, the sealing mechanism (3) being installed on the top of the reaction tank (1), and a motor (7) being installed on the top of the sealing mechanism (3); A stirring mechanism (2), the stirring mechanism (2) is used to stir the material, and the stirring mechanism (2) is installed inside the reaction tank (1); A heat conducting mechanism (4), which is used to heat the reacting material, and is installed between the double-layer structure of the reaction tank (1); The stirring mechanism (2) comprises a connecting shaft (26), the top end of the connecting shaft (26) is connected to the output end of the motor (7) through a coupling, and the bottom end of the connecting shaft (26) is fixedly mounted with a connecting disk (23), the bottom of the connecting disk (23) is fixedly mounted with a stirring blade (24), the outer side of the connecting shaft (26) is fixedly mounted with a shaft sleeve (27), both ends of the outer side of the shaft sleeve (27) are fixedly mounted with connecting rings (29), the outer side of the connecting ring (29) is fixedly mounted with a separating cylinder (21), and a auger plate (28) is fixedly mounted between the separating cylinder (21) and the shaft sleeve (27).
2. A polyethylene polyamine derivative synthesis reactor according to claim 1, characterized in that: A connecting strip (22) is fixedly mounted on the outer side of the separation cylinder (21), the connecting strip (22) is evenly mounted along the center of the separation cylinder (21), and a brush strip (25) is fixedly mounted on the outer side of the connecting strip (22), the outer side of the brush strip (25) is in contact with the inner wall of the reaction tank (1).
3. The polyethylene polyamine derivative synthesis reactor according to claim 1, characterized in that: The sealing mechanism (3) comprises a fixing ring (301), the inner wall of the fixing ring (301) is fixedly connected to the top of the outer side of the reaction tank (1), and the top of the fixing ring (301) is detachably mounted with bolts (303), the top of the fixing ring (301) is fixedly mounted with a cover plate (302) via bolts (303), the top of the cover plate (302) is fixedly mounted with a top cover (307), and the top of the top cover (307) is fixedly connected to the bottom of the motor (7).
4. A polyethylene polyamine derivative synthesis reactor according to claim 3, characterized in that: A sealing cylinder (312) is fixedly mounted on the bottom of the cover plate (302), an inner disk (305) is fixedly mounted on the bottom of the sealing cylinder (312), an inner wall of the inner disk (305) is fixedly connected to the outer side of the connecting shaft (26), and a bearing (306) is fixedly mounted on the outer side of the inner disk (305), an outer disk (304) is rotatably mounted on the inner disk (305) via the bearing (306), and the outer side of the outer disk (304) is in contact with the inner wall of the reaction tank (1).
5. A polyethylene polyamine derivative synthesis reactor according to claim 4, characterized in that: A groove plate (310) is fixedly mounted on the outer side of the sealing cylinder (312), and sliding grooves are evenly arranged on the outer side of the groove plate (310). Arc sliding blocks (311) are slidably mounted on the sliding grooves of the groove plate (310), and a rubber ring (309) is fixedly mounted on the outer side of the arc sliding block (311), and the outer side of the rubber ring (309) is tightly fitted to the inner wall of the reaction tank (1).
6. A polyethylene polyamine derivative synthesis reactor according to claim 5, characterized in that: The top of the groove plate (310) is evenly provided with round holes, and connecting rods (313) are slidably installed at the round holes of the groove plate (310), and a sliding plate (308) is fixedly installed at the bottom end of the connecting rod (313), and the outer side of the sliding plate (308) is slidably adapted to the inner wall of the groove plate (310).
7. A polyethylene polyamine derivative synthesis reactor according to claim 6, characterized in that: A slope block (314) is fixedly mounted on the top end of the connecting rod (313), and a cushion block (315) is fixedly mounted on the opposite surface of the arc slider (311). The opposite surface of the cushion block (315) is a slope that is inclined outward from top to bottom, and the outer side of the slope block (314) is a slope that is inclined outward from top to bottom, and the slope of the slope block (314) is matched with the slope of the cushion block (315).
8. The polyethylene polyamine derivative synthesis reactor according to claim 1, characterized in that: The heat conduction mechanism (4) comprises a liquid inlet pipe (41) and a liquid outlet pipe (42); the liquid inlet pipe (41) is fixedly mounted on the top of the outside of the reaction tank (1); the liquid outlet pipe (42) is fixedly mounted on the bottom of the outside of the reaction tank (1); a corrugated cylinder (46) is fixedly mounted at the center position between the double-layer structures of the reaction tank (1); the inner wall of the corrugated cylinder (46) is uniformly provided with arc-shaped annular grooves along the axial direction; and a top ring (48) is fixedly mounted at the top of the double-layer gap of the reaction tank (1).
9. A polyethylene polyamine derivative synthesis reactor according to claim 8, characterized in that: A bevel ring (47) is fixedly mounted on the top of the bellows (46), the bevel ring (47) is located below the liquid inlet pipe (41), the top ring (48) is located above the liquid inlet pipe (41), and a through groove ring (45) is fixedly mounted on the bottom of the bellows (46), the top of the through groove ring (45) is evenly provided with through grooves.
10. A polyethylene polyamine derivative synthesis reactor according to claim 9, characterized in that: A spiral plate (44) is fixedly mounted on the bottom of the through-groove ring (45). The spiral plate (44) is evenly mounted along the center of the through-groove ring (45). A bottom ring (43) is fixedly mounted on one end of the spiral plate (44) away from the through-groove ring (45). The spiral plate (44) is located above the liquid outlet pipe (42).