Solid-liquid fusion equipment for bactericide production

Abstract

The utility model discloses solid-liquid fusion equipment for bactericide production, which relates to the technical field of chemical production equipment and comprises a base, and a fusion component for performing solid-liquid fusion on bactericide production raw materials is mounted on one side of the top of the base; a storage assembly for temporarily storing the leachate is mounted on the other side of the top of the base; the fusion assembly comprises a reaction kettle, the bottom of the reaction kettle is connected with the top of the base, and a filter screen is detachably mounted in the reaction kettle; according to the utility model, the reflux component is started to convey the leachate to the fusion area in the reaction kettle again, the circulation is repeated, and the solid raw material is continuously scoured by the liquid raw material, so that the fusion effect and the reaction effect of the solid and the liquid raw material can be improved; through cooperative use of the detection assembly, the conveying assembly and the backflow assembly, compared with manual detection, the detection device has higher stability and intelligence, the detection efficiency can be improved, and the preparation efficiency of the bactericide raw materials can be improved.

Description

Technical Field

[0001] The utility model relates to the technical field of chemical production equipment, in particular to solid-liquid fusion equipment for bactericide production. Background Art

[0002] Bactericides are also called biocides, fungicides and algaecides, and microbicides. They usually refer to chemical agents that can effectively control or kill microorganisms, bacteria, fungi and algae in water systems. Internationally, they are usually used as a general term for agents that prevent and treat various pathogenic microorganisms. Bactericides require the use of solid-liquid fusion equipment in the production process.

[0003] Taking potassium permanganate as an example of fungicide, its production process is as follows: leaching manganese-containing ore powder, dissolving manganese in manganese ore with acidic leaching agent, obtaining potassium manganate-containing leaching solution, and then a crystallization stage. During the crystallization process, the potassium manganate-containing leaching solution needs to be crystallized to crystallize into high-purity potassium permanganate crystals. Crystallization requires the control of parameters such as temperature, concentration, and stirring speed to obtain an ideal crystallization effect. The manganese-containing ore powder is solid, and the acidic leaching agent is liquid. When performing the leaching step, solid-liquid fusion equipment is required.

[0004] After manganese ore powder is mixed with acidic leaching agent, leachate will be obtained. However, existing fusion equipment mostly adopts stirring mechanism for stirring. Stirring mechanism is usually bulky and complicated, and it is not convenient to clean after production and stirring. Secondly, there is a lack of real-time monitoring function for the leachate. It is difficult to know the chemical reaction and fusion status in the reactor in real time, and the manual timed sampling and detection method is time-consuming and labor-intensive. Therefore, we need to propose a solid-liquid fusion equipment for fungicide production. Utility Model Content

[0005] The purpose of the utility model is to provide a solid-liquid fusion device for fungicide production, which has the advantages of reducing production difficulty and facilitating detection to improve the convenience of fungicide production, so as to solve the problems raised in the above-mentioned background technology.

[0006] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a solid-liquid fusion device for fungicide production, comprising a base, a fusion component for solid-liquid fusion of fungicide production raw materials is installed on one side of the top of the base;

[0007] A storage component for temporarily storing the leachate is installed on the other side of the top of the base;

[0008] The fusion assembly comprises a reaction kettle, the bottom of which is connected to the top of the base, a filter screen is detachably installed inside the reaction kettle, and the inside of the reaction kettle is divided into a fusion area and a separation area by the filter screen;

[0009] A detection component for detecting the leachate in the separation zone is installed at the bottom of the reactor, a conveying component for conveying the leachate is installed on one side of the detection component, and one end of the conveying component away from the detection component is connected to one side of the storage component;

[0010] A reflux component for circulating and flushing the solid raw materials in the fusion zone is installed on the top of the reactor, and one end of the reflux component away from the reactor is connected to the top of the storage component.

[0011] Preferably, the storage assembly comprises a storage barrel, the bottom of the storage barrel is connected to the top of the base, a liquid level detector is installed on the outside of the storage barrel, and a detection end of the liquid level detector extends to the inside of the storage barrel.

[0012] Preferably, a solid feed and a liquid feed are respectively provided at the top of the reactor, the solid feed is connected to the fusion zone, and the liquid feed is connected to the separation zone. A discharge pipe is installed at the bottom of the reactor, and the top of the discharge pipe is connected to the interior of the fusion zone.

[0013] Preferably, the detection assembly includes a drain valve, a detection tube and a detector. The drain valve is installed below the reactor and is connected to the interior of the separation zone. The detection tube is connected to the bottom of the drain valve. A first box is installed on the outside of the detector. The first box is installed on the top of the base. The detection end of the detector extends to the interior of the detection tube.

[0014] Preferably, the conveying assembly includes a first water pump, a first tube body and a second tube body, one end of the first tube body is connected to one end of the detection tube, the other end of the first tube body is connected to the pumping end of the first water pump, and the drainage end of the first water pump is connected to one end of the second tube body.

[0015] Preferably, one end of the second tube body extends to the interior of the storage barrel, and a filter cartridge is installed at one end of the second tube body and located inside the storage barrel.

[0016] Preferably, the reflux assembly includes a second water pump, a first connecting pipe and a second connecting pipe, a fixing bracket is installed on the outside of the first water pump and the second water pump, the bottom of the fixing bracket is connected to the top of the base, one end of the first connecting pipe is connected to the interior of the storage barrel, and the other end of the first connecting pipe is connected to the pumping end of the second water pump.

[0017] Preferably, one end of the second connecting pipe is connected to the drainage end of the second water pump, a joint is installed on the top of the reactor, the bottom of the joint extends to the interior of the fusion zone and is connected to the injection pipe, and the other end of the second connecting pipe is connected to an end of the joint away from the injection pipe.

[0018] Compared with the prior art, the beneficial effects of the utility model are:

[0019] 1. The utility model starts the reflux component to transport the leachate to the fusion zone in the reactor again, and repeats this cycle, continuously flushing the solid raw material with the liquid raw material, which can improve the fusion effect and reaction effect of the solid and liquid raw materials.

[0020] 2. The main structure of the reflux component in the utility model is mostly assembled by pipes, which can not only play the role of conveying raw materials, but also accelerate the mixing and fusion of raw materials during the conveying process, make rational use of kinetic energy, and have the advantages of light weight and easy disassembly and assembly, which is convenient for subsequent cleaning and maintenance.

[0021] 3. The utility model uses the detection component, the conveying component and the reflux component in coordination, which has higher stability and intelligence than manual detection, can improve the detection efficiency, and improve the preparation efficiency of the bactericide raw materials. BRIEF DESCRIPTION OF THE DRAWINGS

[0022] Figure 1 It is a structural schematic diagram of the utility model;

[0023] Figure 2 It is a schematic cross-sectional view of the storage barrel of the utility model;

[0024] Figure 3 It is a cross-sectional structural schematic diagram of the reaction kettle of the utility model;

[0025] Figure 4 It is a side structural schematic diagram of the utility model.

[0026] In the figure: 1. base; 2. reactor; 3. filter; 4. fusion zone; 5. separation zone; 6. storage barrel; 7. liquid level detector; 8. discharge pipe; 9. drain valve; 10. detection tube; 11. detector; 12. first box body; 13. first water pump; 14. first tube body; 15. second tube body; 16. filter cartridge; 17. second water pump; 18. first connecting pipe; 19. second connecting pipe; 20. fixing frame; 21. joint; 22. injection pipe; 23. second box body; 24. controller. DETAILED DESCRIPTION

[0027] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0028] See also Figure 1-4The utility model provides a technical solution: a solid-liquid fusion device for fungicide production, comprising a base 1, a fusion component for solid-liquid fusion of fungicide production raw materials is installed on one side of the top of the base 1; a storage component for temporarily storing the leaching liquid is installed on the other side of the top of the base 1; the storage component comprises a storage barrel 6, the bottom of the storage barrel 6 is connected to the top of the base 1, a liquid level detector 7 is installed outside the storage barrel 6, and the detection end of the liquid level detector 7 extends to the inside of the storage barrel 6. The storage barrel 6 is provided for temporary storage of the leaching liquid, and the liquid level detector 7 is provided for detecting the liquid level height in the storage barrel 6.

[0029] Specifically, the fusion component includes a reactor 2, the bottom of which is connected to the top of the base 1, and a filter screen 3 is detachably installed inside the reactor 2, and the interior of the reactor 2 is divided into a fusion zone 4 and a separation zone 5 by the filter screen 3; the reactor 2 is set up for reacting and fusing solid raw materials and liquid raw materials, and a solid feed and a liquid feed are respectively provided on the top of the reactor 2. The solid feed is connected to the fusion zone 4, and the solid raw material can be placed in the fusion zone 4 in the reactor 2 through the solid feed, and the liquid feed is connected to the separation zone 5, and the liquid raw material can be placed in the separation zone 5 in the reactor 2 through the liquid feed, and the solid raw material can pass through the filter screen 3 and contact with the liquid raw material, and a reaction can occur after the contact, thereby realizing the solid-liquid fusion step of fungicide production.

[0030] Among them, although the solid raw material and the liquid raw material can come into contact, the solid impurities that have not reacted and fused cannot pass through the filter 3 into the separation zone 5. A discharge pipe 8 is installed at the bottom of the reactor 2, and the top of the discharge pipe 8 is connected to the interior of the fusion zone 4. The solid impurities after the reaction and fusion can be discharged to the outside of the reactor 2 by opening the discharge pipe 8, which can facilitate the discharge of impurities.

[0031] Furthermore, a detection assembly for detecting the leachate in the separation zone 5 is installed at the bottom of the reactor 2, and the detection assembly includes a drain valve 9, a detection tube 10 and a detector 11. The drain valve 9 is installed below the reactor 2 and communicated with the interior of the separation zone 5. The detection tube 10 is connected to the bottom of the drain valve 9. A first box 12 is installed outside the detector 11. The first box 12 is installed on the top of the base 1, and the detection end of the detector 11 extends to the interior of the detection tube 10. The first box 12 is provided to protect the detector 11. By opening the drain valve 9, the leachate can enter the interior of the detection tube 10, and by starting the detector 11, the detector 11 can detect the leachate.

[0032] In addition, the detector 11 can use a conductivity meter, which refers to an instrument that measures the conductivity of an electrolyte solution by an electrochemical measurement method. Its measurement principle is to place two parallel plates in the solution to be measured, add a certain potential, usually a sine wave voltage, to both ends of the plates, and then measure the current flowing between the plates. According to Ohm's law, when the electrode constant is known and the solution resistance or conductivity is measured, the conductivity can be calculated. Conductivity is a manifestation of the electrical conductivity of an electrolyte solution. In most cases, it is proportional to the concentration of ions in the solution. Therefore, the total concentration of ions or the salt content in the solution can be determined by measuring the conductivity.

[0033] Furthermore, a conveying assembly for conveying the leachate is installed on one side of the detection assembly, and one end of the conveying assembly away from the detection assembly is connected to one side of the storage assembly; the conveying assembly includes a first water pump 13, a first tube body 14 and a second tube body 15, one end of the first tube body 14 is connected to one end of the detection tube 10, the other end of the first tube body 14 is connected to the pumping end of the first water pump 13, and the drainage end of the first water pump 13 is connected to one end of the second tube body 15. One end of the second tube body 15 extends to the inside of the storage barrel 6, and a filter cartridge 16 is installed at one end of the second tube body 15 and located inside the storage barrel 6. When it is necessary to merge the solid raw material and the liquid raw material, the first water pump 13 is started, and the first water pump 13 conveys the leachate in the reactor 2 to the storage barrel 6. By providing the filter cartridge 16, the raw materials immersed in the storage barrel 6 can be filtered to improve the quality of the leachate.

[0034] Specifically, a reflux assembly for circulating and flushing the solid raw materials in the fusion zone 4 is installed on the top of the reactor 2, and the end of the reflux assembly away from the reactor 2 is connected to the top of the storage assembly. The reflux assembly includes a second water pump 17, a first connecting pipe 18, and a second connecting pipe 19. A fixing frame 20 is installed outside the first water pump 13 and the second water pump 17. The bottom of the fixing frame 20 is connected to the top of the base 1. One end of the first connecting pipe 18 is connected to the inside of the storage barrel 6, and the other end of the first connecting pipe 18 is connected to the water pumping end of the second water pump 17. One end of the second connecting pipe 19 is connected to the drainage end of the second water pump 17. A joint 21 is installed on the top of the reactor 2. The bottom of the joint 21 extends to the inside of the fusion zone 4 and is connected to the injection pipe 22. The other end of the second connecting pipe 19 is connected to the end of the joint 21 away from the injection pipe 22.

[0035] By starting the second water pump 17, the second water pump 17 transports the raw materials in the storage barrel 6 to the second connecting pipe 19 through the first connecting pipe 18, and then the liquid raw material enters the fusion zone 4 through the joint 21 and the injection pipe 22 to flush the solid raw material powder in the fusion zone 4. The flushing method can improve the contact effect and fusion effect of the solid raw material and the liquid raw material. In this way, the traditional bulky mixing equipment can be replaced. For example, traditional mixing or stirring equipment usually adopts complex structures such as stirring rods, stirring blades, gear boxes, motors and brackets. Most of these structures are made of metal and are large in size, which is extremely inconvenient during production and installation. Therefore, the main structure of the reflux component in this embodiment is mostly assembled by pipelines, which can not only play the role of conveying raw materials, but also accelerate the mixing and fusion of raw materials during the conveying process, make rational use of kinetic energy, and have the advantages of light weight and easy disassembly and assembly, which is convenient for subsequent cleaning and maintenance.

[0036] It is worth noting that: after the solid raw material contacts the liquid raw material, it reacts and fuses. The leachate is transported to the storage barrel 6 through the first conveying component, and then the reflux component is started to transport the leachate again to the fusion zone 4 in the reactor 2. This cycle is repeated, and the solid raw material is continuously flushed by the liquid raw material, which can improve the fusion effect and reaction effect of the solid and liquid raw materials.

[0037] In addition, during the transportation of the liquid raw material, the liquid, i.e., the leachate, can be detected in real time through the detection component. A second box 23 is installed on one side of the top of the base 1, and a controller 24 is installed inside the second box 23. The controller 24 is electrically connected to the first water pump 13, the second water pump 17, the liquid level detector 7, and the detector 11 respectively.

[0038] The specific cycle process is that the liquid level in the storage tank 6 can be detected by the liquid level detector 7. After the liquid level reaches a predetermined height, the liquid level detector 7 transmits a signal to the controller 24, and the controller 24 can control the first water pump 13 to turn off and start the second water pump 17 at the same time;

[0039] The liquid in the storage tank 6 can be transported to the fusion area 4 again through the second water pump 17;

[0040] After the liquid level in the storage barrel 6 drops to a predetermined height, the first water pump 13 can be started again through the controller 24. The first water pump 13 is started again to complete the circulation work. After the detector 11 detects that the concentration of the leachate flowing through reaches the predetermined standard requirement, the detector 11 transmits a signal to the controller 24. The controller 24 controls the first water pump 13 to extract the leachate into the storage barrel 6, and then stops the operation of the first water pump 13 and the second water pump 17, thereby completing the solid-liquid fusion of the bactericide raw materials.

[0041] In this process, the coordinated use of detection components, conveying components and reflux components has higher stability and intelligence than manual detection, which can improve detection efficiency and improve the preparation efficiency of fungicide raw materials.

[0042] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A solid-liquid fusion device for producing a fungicide, comprising a base (1), characterized in that: A fusion component for solid-liquid fusion of fungicide production raw materials is installed on one side of the top of the base (1); A storage component for temporarily storing the leaching liquid is installed on the other side of the top of the base (1); The fusion assembly comprises a reaction kettle (2), the bottom of the reaction kettle (2) being connected to the top of the base (1), a filter screen (3) being detachably installed inside the reaction kettle (2), and the inside of the reaction kettle (2) being divided into a fusion zone (4) and a separation zone (5) by the filter screen (3); A detection component for detecting the leachate in the separation zone (5) is installed at the bottom of the reaction kettle (2), a conveying component for conveying the leachate is installed on one side of the detection component, and an end of the conveying component away from the detection component is connected to one side of the storage component; A reflux component for circulating and flushing the solid raw materials in the fusion zone (4) is installed on the top of the reactor (2); one end of the reflux component away from the reactor (2) is connected to the top of the storage component.

2. The solid-liquid fusion equipment for producing fungicides according to claim 1, characterized in that: The storage assembly comprises a storage barrel (6), the bottom of the storage barrel (6) being connected to the top of the base (1), a liquid level detector (7) being installed outside the storage barrel (6), and a detection end of the liquid level detector (7) extending into the interior of the storage barrel (6).

3. A solid-liquid fusion device for fungicide production according to claim 2, characterized in that: The top of the reactor (2) is provided with a solid feed point and a liquid feed point, respectively. The solid feed point is connected to the fusion zone (4), and the liquid feed point is connected to the separation zone (5). A discharge pipe (8) is installed at the bottom of the reactor (2), and the top of the discharge pipe (8) is connected to the inside of the fusion zone (4).

4. The solid-liquid fusion equipment for producing fungicides according to claim 3, characterized in that: The detection assembly comprises a drain valve (9), a detection tube (10) and a detector (11); the drain valve (9) is installed below the reaction kettle (2) and is connected to the interior of the separation zone (5); the detection tube (10) is connected to the bottom of the drain valve (9); a first box (12) is installed outside the detector (11); the first box (12) is installed on the top of the base (1); and the detection end of the detector (11) extends to the interior of the detection tube (10).

5. The solid-liquid fusion equipment for producing fungicides according to claim 4, characterized in that: The conveying assembly comprises a first water pump (13), a first tube body (14) and a second tube body (15); one end of the first tube body (14) is connected to one end of the detection tube (10); the other end of the first tube body (14) is connected to the pumping end of the first water pump (13); and the drainage end of the first water pump (13) is connected to one end of the second tube body (15).

6. The solid-liquid fusion equipment for producing fungicides according to claim 5, characterized in that: One end of the second tube body (15) extends to the interior of the storage barrel (6), and a filter cartridge (16) is installed at one end of the second tube body (15) and located inside the storage barrel (6).

7. The solid-liquid fusion equipment for producing fungicides according to claim 6, characterized in that: The reflux assembly comprises a second water pump (17), a first connecting pipe (18) and a second connecting pipe (19); a fixing frame (20) is installed outside the first water pump (13) and the second water pump (17); the bottom of the fixing frame (20) is connected to the top of the base (1); one end of the first connecting pipe (18) is connected to the inside of the storage barrel (6); and the other end of the first connecting pipe (18) is connected to the water pumping end of the second water pump (17).

8. The solid-liquid fusion equipment for producing fungicides according to claim 7, characterized in that: One end of the second connecting pipe (19) is connected to the drainage end of the second water pump (17); a joint (21) is installed on the top of the reaction kettle (2); the bottom of the joint (21) extends to the inside of the fusion zone (4) and is connected to the injection pipe (22); the other end of the second connecting pipe (19) is connected to an end of the joint (21) away from the injection pipe (22).

Images