Curing reactor capable of automatically filling products for multiphase continuous flow reaction system

Abstract

A curing reactor capable of automatically filling products and used for a multiphase continuous flow reaction system comprises a curing reactor three-dimensional synchronous belt module, and a glass discharge pipe on the curing reactor is controlled by a stepping motor to move to a specified container position; the glass reaction containers can provide the same reaction container environment and are uniformly arranged on the glass curing container mounting plate made of the bakelite material; magneons are placed in the glass reaction container, stirring is driven by matched magnetic poles and a magnetic motor on a magnetic motor mounting plate located on the lower portion of the glass reaction container, and the curing progress and the uniformity degree are accelerated. The three-dimensional synchronous belt module is controlled by a control system to move, the glass discharge pipe is driven to move above the glass reaction container, materials flow into the container and a stirring function is correspondingly started, a manual or automatic control mode is allowed to be switched, and automatic filling and stirring of the materials in the containers in the corresponding sequence are met, so that the purposes of automatically filling reaction products and automatically filling the materials in the containers in the corresponding sequence are achieved. The purpose of providing stable and same curing conditions is achieved, and continuous and efficient curing is facilitated.

Description

Technical Field

[0001] The invention relates to the field of aging reaction equipment, in particular to a aging reactor capable of automatically filling products for a multiphase continuous flow reaction system. Background Art

[0002] In order to ensure that the particle size is not too large or the particles react fully, the multiphase continuous flow reactor that produces solid particles needs to control the residence time of the particles in the reaction system. Some safe but time-consuming reactions can be placed in other reactors to continue. This type of reactor is generally called a maturation reactor; a maturation reactor refers to a secondary reaction container that provides a stable environment for continuous stirring for incomplete reaction products, which is used to fully react the products after a certain period of stirring to meet the requirements of the final product. At present, there are no maturation reactors that can automatically load products for production. Laboratory maturation reactors are generally manually loaded with materials at one time. When continuous production is carried out, it is impossible to meet the continuous filling within a certain period, and the degree of automation is far from meeting the requirements. Therefore, further research is needed on the maturation reactor that can automatically load products and is suitable for multiphase continuous flow reaction systems. Summary of the invention

[0003] In order to solve the above technical problems, the present invention proposes a aging reactor capable of automatically filling products for a multiphase continuous flow reaction system. In view of the technical deficiencies in the existing aging reactors capable of automatically filling products for production, a aging reactor is realized which is integrated with multiple reactors and automated through motor control to fill materials into each reactor one by one, thereby realizing continuous preparation of reaction products within a certain period and providing a stable and identical aging environment.

[0004] To achieve the above object, the technical solution adopted by the present invention is: A aging reactor capable of automatically loading products for a multiphase continuous flow reaction system comprises a three-dimensional synchronous belt module, an aluminum profile frame, a glass aging container mounting plate, a magnetic motor mounting plate and a bottom fixing plate. The three-dimensional synchronous belt module is mounted on the aluminum profile frame, and a driving shaft is synchronously moved to a designated container position by a stepping motor to realize multiple automatic loading of a batch of materials. The aluminum profile frame is used to form an overall frame and is placed on the bottom fixing plate. The glass aging container mounting plate is used to place materials that can be filled. A magnetic motor mounting plate is installed at the lower end of the glass aging container mounting plate. The magnetic motor mounting plate is used to place and install magnetic poles and magnetic motors, which correspond to each glass reaction container one by one to drive the rotation of the placed magnetic poles, so as to realize automatic stirring during the material aging process. The glass aging container mounting plate and the magnetic motor mounting plate are connected to each other by bolts, and finally fixed on the bottom fixing plate to realize the overall structure and operation of the device.

[0005] As a further improvement of the present invention, the three-dimensional synchronous belt module is composed of two modules along the Y-axis direction, one module along the X-axis direction and a fixed glass plate along the Z-axis, which realizes spatial movement and is installed on the aluminum profile frame through a connecting piece. The Y-axis direction module is connected by a stepper motor through an optical axis to realize the synchronous movement of the dual parallel axes controlled by the stepper motor, driving the movement of the X-axis direction module installed on the dual axes to ensure smooth operation. The X-axis direction module is controlled by a corresponding stepper motor to drive the Z-axis fixed glass plate installed on the slider to move. A glass discharge pipe for discharging reaction products is installed on the Z-axis fixed glass plate, thereby realizing full coverage movement of the glass discharge pipe on the XY plane, and the glass discharge pipe is connected to the solenoid valve on the discharge port through a silicone hose.

[0006] As a further improvement of the present invention, the glass aging container mounting plate is designed with 16 circular bottom grooves on the bakelite mounting plate for placing 16 glass reaction containers of the same specifications and a capacity of 400 mL each; 8 corresponding fixed mounting holes are also opened on the bakelite mounting plate for bolting and connecting the magnetic motor mounting plate and the bottom fixing plate.

[0007] As a further improvement of the present invention, the magnetic pole motor mounting plate is connected to the lower end magnetic motor by a stainless steel orifice plate, the magnetic pole is connected to the magnetic motor through an axis, and is located on the upper side of the stainless steel orifice plate, corresponding to the lower end of each glass reaction container, and by controlling the magnetic motor to cooperate with the magnetic pole, the magnetic particles in the glass reaction container are driven to rotate and stir the materials. The magnetic motor mounting plate is provided with 9 mounting holes by the stainless steel orifice plate, and the 4 mounting holes at the outer corners are used to pass bolts to connect to the bottom fixing plate, the mounting holes at the midpoints of the four sides are bolted to the glass ripening container mounting plate, and the middle mounting holes are bolted to support the bottom fixing plate.

[0008] As a further improvement of the present invention, the bottom fixing plate is connected and fixed to the overall upper frame and each mounting plate through a bottom aluminum plate, and is provided with a total of nine bolt rods of three types for installation, including four fastening bolts at the outer corners, which are used to pass through the mounting holes on the outer corners of the magnetic motor mounting plate and be connected to the fixed mounting holes on the outer corners of the glass ripening container mounting plate for tightening, and also include fastening bolts at the midpoints of the four sides, which are used to connect to the mounting holes at the midpoints of the four sides of the magnetic motor mounting plate through the fixed mounting holes at the midpoints of the four sides of the glass ripening container mounting plate, and also include middle fastening bolts, which are used to connect through the central mounting hole of the magnetic motor mounting plate.

[0009] Compared with the prior art, the present invention has the following significant advantages: The invention has clear structure, strong pertinence, relatively compact structure, efficient production and high automation degree.

[0010] The positioning accuracy is high and the liquid discharge efficiency is fast. The stepper motor controls the three-dimensional module to discharge the liquid quickly and accurately.

[0011] Providing the same and stable ripening environment, the magnet is driven to rotate by a separate magnetic force to achieve automatic stirring of the materials in each glass container to achieve the ripening effect.

[0012] The control has high sensitivity and strong operability. It allows switching between manual and automatic container replacement modes. It also supports time setting and capacity setting switching, allowing multiple replacement modes to coexist.

[0013] It can realize the automatic loading of a batch of materials within the production cycle, has high efficiency and high integration, and is more suitable for multiphase continuous flow reaction systems for production. BRIEF DESCRIPTION OF THE DRAWINGS

[0014] Figure 1 It is a schematic diagram of the three-dimensional structure of the present invention; Figure 2 It is a schematic diagram of the explosion of the three-dimensional structure of the present invention; Figure 3 It is a schematic diagram of the structure of the three-dimensional synchronous belt module of the present invention; Figure 4 It is a schematic diagram of the installation position structure of the aluminum profile frame and the three-dimensional synchronous belt module of the present invention; Figure 5 This is a schematic diagram of the structure of the glass ripening container mounting plate of the present invention; Figure 6 This is a schematic diagram of the planar structure of the glass ripening container mounting plate of the present invention; Figure 7 It is a structural schematic diagram of the magnetic motor mounting plate of the present invention; Figure 8 It is a schematic diagram of the plane structure of the position of the magnetic motor and the glass reaction container of the present invention; Fig. 9 It is a schematic diagram of the bottom fixing plate and the bolt structure thereon of the present invention; Fig.10 This is a diagram of the operation interface of the cooking device stirring control software of the present invention; Fig.11 This is a diagram of the operation interface of the control software for replacing the container of the ripening device of the present invention; Description of reference numerals: 1. Three-dimensional synchronous belt module; 11. Module in the Y-axis direction; 12. Module in the X-axis direction; 13. Fixed glass plate in the Z-axis; 14. Stepper motor; 15. Optical axis; 16. Glass discharge pipe; 2. Aluminum profile frame; 3. Glass aging container mounting plate; 31. Glass reaction container; 32. Bakelite mounting plate; 33. Fixed mounting hole; 34. Circular bottom groove; 4. Magnetic motor mounting plate; 41. Stainless steel orifice plate; 42. Magnetic pole; 43. Magnetic motor; 44. Mounting hole; 5. Bottom fixing plate; 51. Bottom aluminum plate; 52. Fastening bolts; 53. Fastening bolts at the midpoints of the four sides; 54. Middle fastening bolts; 6. Silicone hose. DETAILED DESCRIPTION

[0015] The present invention is further described in detail below in conjunction with the accompanying drawings and specific embodiments: See also Figure 1-11 The present invention provides a technical solution: a aging reactor capable of automatically loading products for a multiphase continuous flow reaction system, comprising the following steps: The device comprises a three-dimensional synchronous belt module 1, which is installed on an aluminum profile frame 2. The drive shaft is controlled by a motor to synchronously move to a designated container position to realize multiple automatic filling of a batch of materials. The aluminum profile frame 2 is used to form an overall frame and is placed on a bottom fixing plate 5. The glass ripening container mounting plate 3 is used to place a glass reaction container that can be filled with materials and provide a stable and identical ripening environment to realize stable ripening of materials. A magnetic motor mounting plate 4 is installed at the lower end of the glass ripening container mounting plate 3 to place and install magnetic poles and magnetic motors, which correspond to each glass reaction container one by one to drive the placed magnetic poles to rotate, thereby realizing automatic stirring during the material ripening process. The glass ripening container mounting plate 3 and the magnetic motor mounting plate 4 are connected to each other by bolts and finally fixed on the bottom fixing plate 5 to realize the overall structure and operation of the device.

[0016] The three-dimensional synchronous belt module 1 is composed of two modules 11 along the Y-axis direction, one module 12 along the X-axis direction and a fixed glass plate 13 along the Z-axis to achieve spatial movement. The whole is installed and connected to the aluminum profile frame 2 composed of multiple aluminum profiles through a connector. The Y-axis direction module 11 is connected by a stepper motor 14 through an optical axis 15, so that the stepper motor 14 controls the synchronous movement of the dual parallel axes, drives the X-axis direction module 12 installed on the dual axes to move, and ensures smooth operation.

[0017] Furthermore, the X-axis module 12 in the three-dimensional synchronous belt module 1 is controlled by the corresponding stepping motor 14, driving the Z-axis fixed glass plate 13 installed on the slider to move, and the Z-axis fixed glass plate 13 is installed with a glass discharge pipe 16 for discharging the reaction products, thereby realizing full coverage movement of the glass discharge pipe 16 on the XY plane, thereby completing the discharge of the reaction products at each designated position.

[0018] Furthermore, the glass aging container mounting plate 3 is designed with 16 circular bottom grooves 34 on the bakelite mounting plate 32, which are used to place 16 glass reaction containers 31 of the same specifications and a capacity of 400 mL, and can provide the same and stable aging environment; 8 corresponding fixed mounting holes 33 are also opened on the bakelite mounting plate 32, which are used to tighten the bolts to connect the magnetic motor mounting plate 4 and the bottom fixing plate 5.

[0019] Furthermore, the magnetic pole motor mounting plate 4 is connected to the lower end magnetic motor 43 by a stainless steel orifice plate 41, and the magnetic pole 42 is connected to the magnetic motor 43 through an axis and is located on the upper side of the stainless steel orifice plate 41, corresponding to the lower end of each glass reaction container 31. By controlling the magnetic motor 43 to cooperate with the magnetic pole 42, the magnetic particles in the glass reaction container 31 are driven to rotate and stir the materials, thereby accelerating the maturation process and uniformity during the maturation process.

[0020] Furthermore, the magnetic motor mounting plate 4 is provided with 9 mounting holes 44 by a stainless steel perforated plate 41, the 4 mounting holes 44 at the outer corners are used to pass bolts to be connected to the bottom fixing plate 5, the mounting holes 44 at the midpoints of the four sides are bolted to the glass ripening container mounting plate 3, and the middle mounting hole 44 is bolted to be supported on the bottom fixing plate 5, so that the installation is smooth and tight.

[0021] Further, the bottom fixing plate 5 is connected and fixed to the overall upper frame and each mounting plate through the bottom aluminum plate 51, and is provided with a total of nine bolt rods of three types for installation, including four fastening bolts 52 at the outer corners, which are used to pass through the mounting holes 44 on the outer corners of the magnetic motor mounting plate 4 and be connected to the fixed mounting holes 33 on the outer corners of the glass ripening container mounting plate 3 for tightening, including four-side midpoint fastening bolts 53, which are used to connect to the four-side midpoint mounting holes 44 on the four sides of the magnetic motor mounting plate 4 through the four-side midpoint fixed mounting holes 33 of the glass ripening container mounting plate 3 to form a tightening fixation, including middle fastening bolts 54, which are used to connect through the central mounting hole 44 of the magnetic motor mounting plate 5, and the installation is smooth and tight.

[0022] Furthermore, it also includes control software for controlling the magnetic motor 43 to rotate in coordination with the magnetic pole 42, thereby driving the magnets in the glass reaction container 31 to rotate. The software provides independent control to meet the characteristics of the order in which the products are loaded into each glass reaction container 31, that is, when there are more products, the stirring action in the individual glass reaction container 31 is turned on, and the stirring action is turned on by clicking the corresponding ripener stirring control software operation interface diagram from "OFF" to "ON".

[0023] Furthermore, it also includes controlling the movement of the three-dimensional synchronous belt module 1 to achieve the glass discharge pipe 16 to accurately reach the top of each glass reaction container 31 and achieve full coverage of the plane of the ripening container. The software provides two modes of "manual" and "automatic" ripening device container replacement. The "manual" mode stops the discharge of liquid by manipulating the glass discharge pipe 16 and moves it to the top of the next glass reaction container 31 to continue discharging liquid, so as to complete the position movement switching of different containers to meet different needs. The "automatic" mode provides optional "time replacement" or "capacity replacement" mode. After the set time input by the user, the glass discharge pipe 16 automatically moves to the next container and continues to discharge liquid, or after the set liquid discharge capacity meets the conditions, the glass discharge pipe 16 automatically moves to the next container position. Through the optional "manual" and "automatic" mode switching, the use of different conditions can be met.

[0024] Furthermore, it also includes a power system, a part of which is used to supply power to the stepper motor 14 on the three-dimensional synchronous belt module 1 to drive the three-dimensional module to move; and the other part is used to supply power to the magnetic motor 43.

[0025] A aging reactor capable of automatically loading products for continuous preparation, for incomplete reaction products, the specific implementation method may be: The fixed discharge port of the incomplete reaction product generated from the production reactor is set above the maturation reactor, and the outflow of the material is controlled by an electromagnetic valve (not shown) on it that automatically controls the opening and closing.

[0026] First, the silicone hose 6 connects the electromagnetic valve on the fixed discharge port and the glass discharge pipe 16 to form a discharge pipeline. Manually click "Move", and the three-dimensional synchronous belt module 1 drives the glass discharge pipe 16 on it to move to the top of the first glass reaction container 31. Click "OK" and the discharge port valve opens. At this time, the incomplete reaction products that have been completed in the reaction for a certain period of time will pass through the fixed discharge port-solenoid valve-silicone hose 6-glass discharge pipe 16, and then flow into the first glass reaction container 31. When the glass reaction container 31 receives more materials, click the stirring "OFF" button under the corresponding container to start stirring, control the magnetic motor 43 to cooperate with the magnetic pole 42 to drive the magnetic stirring, and enter the maturation process, allowing the sequential loading to correspond to the sequential stirring action to start, ensuring the same maturation environment and time, with strong reference.

[0027] After the material has been filled for a certain period of time, select the "manual" maturation device replacement setting, which means manually replacing the container, that is, click the "move" button, the glass discharge pipe 16 stops discharging, and the three-dimensional synchronous belt module 1 drives the glass discharge pipe 16 to move to the next fixed point, that is, moves to the top of the next glass reaction container 31. At this time, click the "OK" button to continue discharging liquid, and click the corresponding container stirring button to start stirring, and repeat the cycle until a batch of materials is fully filled and enters the stirring and maturation state.

[0028] After the material has been filled for a certain period of time, select the "automatic" maturation device replacement setting, which means that the container is automatically replaced. At this time, you need to choose whether to replace it according to "time" or "capacity". Replacement according to "time" means that after the set time, the first glass reaction container 31 is filled, and the material discharge is temporarily stopped, and the glass liquid discharge pipe 16 moves to the next glass reaction container 31 to continue discharging; replacement according to "capacity" means that after the set liquid discharge capacity, when the liquid discharge capacity reaches the set value, the material discharge is suspended, and the glass discharge pipe 16 moves to the next glass reaction container 31, and click the corresponding container stirring button to start stirring, and repeat until a batch of materials is fully filled and enters the stirring and maturation state.

[0029] It should be noted that the glass discharge pipe 16 can be controlled to move to the initial position by clicking the "return" button in the "manual" mode, which can be used to determine the position before the initial discharge and to return to the original position in time when a fault occurs during the process; at the same time, the ripening device replacement setting is set during the loading process of a batch of materials, allowing the "manual"-"automatic" mode to be switched at any time to adapt to different replacement needs at different times, with strong flexibility.

[0030] The same ripening environment is ensured by recording the time sequence and stirring conditions for starting stirring in each glass reaction container 31. In a production cycle, taking the product filling every 30 minutes and the ripening time of 2 hours as an example, the ripening device can realize automatic filling of materials in the production cycle while ensuring the ripening time and not changing the ripening environment, and has high efficiency and high integration.

[0031] The above description is only a preferred embodiment of the present invention and does not constitute any other form of limitation to the present invention. Any modification or equivalent change made based on the technical essence of the present invention still falls within the scope of protection required by the present invention.

Claims

1. A aging reactor capable of automatically loading products for a multiphase continuous flow reaction system, comprising a three-dimensional synchronous belt module (1), an aluminum profile frame (2), a glass aging container mounting plate (3), a magnetic motor mounting plate (4) and a bottom fixing plate (5), characterized in that: The three-dimensional synchronous belt module (1) is mounted on an aluminum profile frame (2), and a stepper motor (14) controls a driving shaft to synchronously move to a designated container position, thereby realizing multiple automatic loading of a batch of materials. The aluminum profile frame (2) is used to form an overall frame and is placed on a bottom fixing plate (5). The glass ripening container mounting plate (3) is used to place materials that can be filled. A magnetic motor mounting plate (4) is mounted at the lower end of the glass ripening container mounting plate (3). The magnetic motor mounting plate (4) is used to place mounting poles (42) and magnetic motors (43), and the magnetic poles placed corresponding to each glass reaction container (31) are driven to rotate, thereby realizing automatic stirring during the material ripening process. The glass ripening container mounting plate (3) and the magnetic motor mounting plate (4) are connected to each other by bolts and finally fixed to the bottom fixing plate (5), thereby realizing the overall structure and operation of the device.

2. The aging reactor capable of automatically loading products for a multiphase continuous flow reaction system according to claim 1, characterized in that: The three-dimensional synchronous belt module (1) is composed of two modules (11) along the Y-axis direction, one module (12) along the X-axis direction and a fixed glass plate (13) along the Z-axis, and realizes spatial movement and is installed and connected to the aluminum profile frame (2) through a connecting piece. The Y-axis direction module (11) is connected by a stepper motor (14) through an optical axis (15), and the stepper motor (14) controls the synchronous movement of the two parallel axes, driving the X-axis direction module (12) installed on the two axes to move, thereby ensuring smooth operation. The X-axis direction module (12) is controlled by a corresponding stepper motor (14) to drive the Z-axis fixed glass plate (13) installed on the slider to move. The Z-axis fixed glass plate (13) is installed with a glass discharge pipe (16) for discharging reaction products, thereby realizing full coverage movement of the glass discharge pipe (16) on the XY plane. The glass discharge pipe (16) is connected to the electromagnetic valve on the discharge port through a silicone hose (6).

3. The aging reactor capable of automatically loading products for a multiphase continuous flow reaction system according to claim 1, characterized in that: The glass ripening container mounting plate (3) is designed with 16 circular bottom recesses (34) on the bakelite mounting plate (32) for accommodating 16 glass reaction containers (31) of the same specification and each having a capacity of 400 mL; and 8 corresponding fixing mounting holes (33) are also provided on the bakelite mounting plate (32) for bolting and connecting the magnetic motor mounting plate (4) and the bottom fixing plate (5).

4. The aging reactor capable of automatically loading products for a multiphase continuous flow reaction system according to claim 1, characterized in that: The magnetic pole motor mounting plate (4) is connected to the lower end magnetic motor (43) by a stainless steel orifice plate (41); the magnetic pole (42) is connected to the magnetic motor (43) by a shaft and is located on the upper side of the stainless steel orifice plate (41) and corresponds to the lower end of each glass reaction container (31). By controlling the magnetic motor (43) to cooperate with the magnetic pole (42), the magnetic particles in the glass reaction container (31) are driven to rotate and stir the materials. The magnetic motor mounting plate (4) is provided with 9 mounting holes (44) by the stainless steel orifice plate (41); the 4 mounting holes (44) at the outer corners are used to pass bolts to connect to the bottom fixing plate (5); the mounting holes (44) at the midpoints of the four sides are bolted to the glass ripening container mounting plate (3); and the middle mounting holes (44) are bolted to support the bottom fixing plate (5).

5. The aging reactor capable of automatically loading products for a multiphase continuous flow reaction system according to claim 1, characterized in that: The bottom fixing plate (5) is connected and fixed to the overall upper frame and each mounting plate through a bottom aluminum plate (51), and is provided with a total of nine bolt rods of three types for installation, including four fastening bolts (52) at the outer corners, which are used to pass through the mounting holes (44) at the outer corners of the magnetic motor mounting plate (4) and be connected to the fixed mounting holes (33) at the outer corners of the glass ripening container mounting plate (3) for bolt tightening, and also includes fastening bolts (53) at the midpoints of four sides, which are used to connect to the mounting holes (44) at the midpoints of four sides of the magnetic motor mounting plate (4) through the fixed mounting holes (33) at the midpoints of four sides of the glass ripening container mounting plate (3), and also includes middle fastening bolts (54), which are used to connect through the central mounting hole (44) of the magnetic motor mounting plate (5).

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