Substrate material for mounting a semiconductor device, substrate for mounting a semiconductor device, semiconductor device, and method of producing the same
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example 1
An aluminum powder having an average particle diameter of 25 μm was mixed in various proportions with a silicon carbide powder consisting of a mixture of α-crystals and β-crystals and having an average particle diameter of 50 μm to prepare sample powders 1 to 9 respectively having silicon carbide contents of 5%, 10%, 20%, 30%, 40%, 50%, 60%, 70%, and 75% by weight. These sample powders each was homogenized with a kneader for 1 hour to obtain aluminum / silicon carbide starting powders.
The starting powders obtained were compacted at a pressure of 7 t / cm2 to obtain tablet test pieces having a diameter of 20 mm and a height of 30 mm. These compacts were sintered at 700° C. for 2 hours in a nitrogen atmosphere having a nitrogen concentration of 99% by volume or higher. As a results, aluminum / silicon carbide composite alloy sinters were obtained which retained the original shape of the compacted test pieces.
However, the alloy of sample 9 was not dense and had voids in a surface layer ...
example 2
An aluminum powder having an average particle diameter of 25 μm was mixed in a weight ratio of 1:1 with a silicon carbide powder consisting of a mixture of α-crystals and β-crystals and having an average particle diameter of 50 μm. This mixture was homogenized with a kneader for 1 hour to obtain an aluminum / silicon carbide starting powder. The starting powder obtained was compacted at a pressure of 7 t / cm2 to obtain tablet test pieces having a diameter of 20 mm and a height of 30 mm. These compacts were sintered in a nitrogen, hydrogen, or argon atmosphere under the conditions shown in Table 2. As a result, aluminum / silicon carbide composite alloy sinters were obtained which retained the original shape of the compacted test pieces.
Each sinter was examined for density, thermal conductivity, thermal expansion coefficient, nitrogen content, oxygen content, aluminum carbide content, and the ratio of the peak intensity for aluminum carbide (012) to that for aluminum (200) both determi...
example 3
Some of the aluminum / silicon carbide composite alloy sinters obtained as sample 6 in Example 1 were repressed at a pressure of 7 t / cm2 in a nitrogen atmosphere (sample 6-1). Part of the repressed sinters were sintered again at 700° C. for 2 hours in a nitrogen atmosphere (sample 6-2).
These sinter samples were examined for density, thermal conductivity, thermal expansion coefficient, nitrogen content, oxygen content, aluminum carbide content, and the ratio of the peak intensity for aluminum carbide (012) to that for aluminum (200) both determined by X-ray analysis with CuKα line, in the same manner as in Example 1. The results obtained are shown in Table 3. It is understood from Table 3 that repressing and resintering were effective in heightening the density and improving the thermal conductivity.
TABLE 3ThermalSinteringThermalexpansionNitrogenOxygenAl4C3Al4C3conditionsDensityconductivitycoefficientcontentcontentcontent(012) / Sample(° C. × h)(g / cm3)(W / m × K)(×10−6 ° C.)(wt %)(wt ...
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