A two-dimensional colloidal crystal-gold array/smart hydrogel composite with high diffraction intensity and a visual sensor

A two-dimensional colloid and diffraction intensity technology, applied in the field of nanomaterials, can solve the problems of low visible light diffraction intensity, low reflectivity of colloidal microspheres, sensor limitations, etc., and achieve the effect of high diffraction intensity and good sensitivity

CN105738301BActive Publication Date: 2018-09-21HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Publication Date
2018-09-21

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Abstract

The invention discloses a high-diffraction-intensity two-dimensional colloidal crystal-gold array / intelligent hydrogel composite material and a visual sensor.A preparing method of the high-diffraction-intensity two-dimensional colloidal crystal-gold array / intelligent hydrogel composite material includes the following steps that a single-layer colloidal crystal array is prepared on a substrate, the single-layer colloidal crystal array serves as a template, a gold film with the thickness of 35 nm-50 nm is deposited on the surface of the template with the physical deposition method, and therefore a two-dimensional colloidal crystal-gold array with the gold film as a shell is prepared; reaction liquid of intelligent hydrogel is injected into the two-dimensional colloidal crystal-gold array, the product is covered with a glass sheet, then photopolymerization treatment is carried out for 10-30 min, stripping and washing are carried out, and the high-diffraction-intensity two-dimensional colloidal crystal-gold array / intelligent hydrogel composite material is prepared.By means of the high-diffraction-intensity two-dimensional colloidal crystal-gold array / intelligent hydrogel composite material, intense diffraction signals can be obtained without a high reflective mirror, and the high-diffraction-intensity two-dimensional colloidal crystal-gold array / intelligent hydrogel composite material has the advantages of being sensitive, simple in preparing procedure and low in cost, and is suitable for practical industrial applications.
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Description

technical field

[0001] The present invention relates to the field of nanomaterials, in particular to a two-dimensional colloidal crystal with high diffraction intensity (for example: the colloidal crystal can be made of polystyrene (Polystyrene, PS), silicon dioxide (SiO 2 ) or polymethyl methacrylate (PMMA))-gold (chemical element symbol: Au) array / smart hydrogel composites and visualization sensors. Background technique

[0002] At present, the detection of biochemical substances mainly relies on traditional analysis methods such as Raman spectroscopy, mass spectrometry, and fluorescence methods, but these analysis methods not only require expensive equipment, but also the analysis process is relatively complicated, requiring professionally trained personnel In addition, these analytical methods cannot realize real-time online detection of biochemical substances. Therefore, how to detect biochemical substances in a simple, economical, fast and stable manner has become an u...

Examples

Embodiment 1

[0045] Such as Figure 5 As shown, a two-dimensional PS-Au array / smart hydrogel composite was prepared by the following steps:

[0046] Step a, put the glass slide into acetone, ethanol, and deionized water in turn for ultrasonic cleaning, each liquid is ultrasonically cleaned for 40 minutes, and then the cleaned glass slide is put into an oven for drying treatment, and the drying temperature is 70°C, drying time is 30 minutes; after the water on the slide is completely evaporated, place the slide in an ultraviolet ozone cleaner for 30 minutes of irradiation, so as to obtain a slide with good hydrophilicity on the surface.

[0047] Step b, take 40 microliters of polystyrene colloidal suspension (2.5wt.%) with a diameter of 350nm, and mix it with ethanol in equal volume, and then carry out ultrasonic oscillation treatment for 10min, so as to obtain polystyrene colloid with uniform composition Spherical ethanol dilution; put the glass slide treated in step a into the polystyren...