Separation devices for nanomaterial preparation

Abstract

The invention discloses a separation device for preparing nano materials, comprising a positioning frame, wherein a first material storage box is fixedly arranged at one end of the top of the positioning frame, a second material storage box is fixedly arranged at the other end of the top of the positioning frame, spiral grooves are fixedly arranged on the inner wall of the first reaction box and the inner wall of the second reaction box, spiral air guide plates are fixedly arranged at the middle position inside the first reaction box and the middle position inside the second reaction box, a first liquid feed pump is connected at one end of a third conduit, a second liquid feed pump is connected at the middle position of the top of the first reaction box, and one end of a first exhaust pipe is connected to one end of an outer wall of the second reaction box. In the invention, hot air sprayed from a hot air source and liquid mist containing nano particles are formed into a mixed gas mist, the spiral air guide plate forces the mixed gas mist to rotate, and the centrifugal force of the rotation causes the particles to enter the spiral groove, thereby strengthening the separation, and the hot air is pyrolyzed to separate the nano particles in the liquid.

Description

Technical Field

[0001] The invention relates to the field of separation devices for preparing nano materials, in particular to a separation device for preparing nano materials. Background Art

[0002] Nanomaterials refer to materials that have at least one dimension in the nanometer size (1-100nm) in three-dimensional space or are composed of nanometers as basic units, which is approximately equivalent to the scale of 10 to 1000 atoms closely arranged together. Since its size is close to the coherence length of electrons, its properties are greatly changed due to the self-organization brought about by strong coherence. In addition, its scale is close to the wavelength of light, and it has the special effect of a large surface, so its properties, such as melting point, magnetism, optics, thermal conductivity, electrical conductivity, etc., are often different from the properties of the substance in its overall state.

[0003] In response to this, Chinese Patent No. CN201921520130.2 proposes a spray thermal decomposition device, which can make the temperature inside the furnace chamber more uniform during operation, which is conducive to the full thermal decomposition of the materials contained in the slurry, avoid or reduce the generation of impurities, and improve product quality. However, in the above patents, the spray thermal decomposition device has poor separation of gas and product particles, and the production efficiency is not high, which reduces the separation efficiency of nanomaterial preparation. Therefore, a separation device for nanomaterial preparation is needed. Summary of the invention

[0004] The object of the present invention is to provide a separation device for preparing nanomaterials to solve the problems raised in the above background technology.

[0005] To achieve the above-mentioned objectives, the present invention provides the following technical solutions: a separation device for preparing nanomaterials, comprising a positioning frame, a first storage box is fixedly provided at one end of the top of the positioning frame, a second storage box is fixedly provided at the other end of the top of the positioning frame, a first reaction box is fixedly provided at the middle position of the top of the first storage box, a second reaction box is fixedly provided at the middle position of the top of the second storage box, spiral grooves are fixedly provided on the inner wall of the first reaction box and the inner wall of the second reaction box, spiral air guide plates are fixedly provided at the middle position inside the first reaction box and the middle position inside the second reaction box, a hot air source is fixedly provided at one end of one side of the top of the positioning frame, an air pump is fixedly provided at one end of the hot air source, a first conduit is fixedly provided at one end of one side of the air pump, a second conduit is fixedly provided at the other end of one side of the air pump, one end of the first conduit is connected to one end of one side of the first reaction box, and one end of the second conduit is connected to one end of one side of the second reaction box.

[0006] Furthermore, one end of the outer wall of the first reaction box is connected to a third conduit, one end of the third conduit is connected to a first liquid pump, a second liquid pump is connected to the middle position of the top of the first reaction box, one end of the second liquid pump is connected to a first exhaust pipe, one end of the first exhaust pipe is connected to one end of the outer wall of the second reaction box, a second exhaust pipe is connected to the middle position of the top of the second reaction box, and one end of the outer wall of the first conduit and one end of the outer wall of the second conduit are both fixedly provided with a one-way valve.

[0007] Furthermore, a support frame is fixedly provided at one end of the middle position of the top of the positioning frame, and the middle position of the top of the support frame is fixedly connected to the bottom end of the first liquid pump.

[0008] Furthermore, one end of the bottom of the first storage box and one end of the bottom of the second storage box are both rotatably provided with storage trays.

[0009] Furthermore, a partition plate is fixedly provided at the middle position of the two storage trays.

[0010] Furthermore, a bottom plate is fixedly provided at the bottom end of the positioning frame.

[0011] Furthermore, motors are fixedly provided at both ends of the middle position of the top of the bottom plate, and the output ends of the two motors pass through the positioning frames and are fixedly connected to the middle positions of the bottoms of the two storage trays respectively.

[0012] Furthermore, a switch panel is fixedly provided on one side of the positioning frame, and a motor switch, an air pump switch, a first liquid feed pump switch and a second liquid feed pump switch are respectively fixedly provided on the surface of the switch panel. The two motors, the air pump, the first liquid feed pump and the second liquid feed pump are respectively electrically connected to an external power supply through the motor switch, the air pump switch, the first liquid feed pump switch and the second liquid feed pump switch.

[0013] Technical effects and advantages of the present invention:

[0014] (1) The hot air sprayed by the hot air source and the liquid mist containing nanoparticles are mixed to form a mist, and the spiral air guide plate forces the mixed mist to rotate. The centrifugal force of the rotation causes the particles to enter the spiral groove, strengthen the separation, and the hot air is pyrolyzed to separate the nanoparticles in the liquid;

[0015] (2) performing pyrolysis by hot air to separate nanoparticles from the liquid material, the hot air source is transmitted through the air pump, the first conduit and the second conduit, so that the hot air flows into the first reaction box and the second reaction box, and the nanoparticles are introduced into the first reaction box through the first liquid pump and the third conduit to form a mixed gas mist, so that the reactants in the reaction box are fully mixed to increase the reaction efficiency;

[0016] (3) Excess waste gas and doped nanomaterial mist are transported by the second liquid feed pump and the first waste gas pipe and moved to the second reaction box. The mixed mist is forced to rotate by the spiral air guide plate. The centrifugal force of the rotation causes the particles to enter the spiral groove, strengthen the separation, and perform pyrolysis with hot air. The nanoparticles in the liquid are separated and fall into the second storage box, thereby avoiding material waste due to uneven separation of nanomaterials and improving the working efficiency of the separation device for nanomaterial preparation.

[0017] (4) The remaining exhaust gas is transported and treated through the second exhaust pipe, which is convenient for external treatment equipment and improves treatment efficiency;

[0018] (5) The output end of the motor fixed on the top of the bottom plate drives the storage tray to rotate, and the storage tray is separated by the middle partition plate, so that the two ends of the partition plate can be indirectly unloaded, so that the nanomaterials can be indirectly collected while continuously falling downward, avoiding the problem of accumulation of nanomaterials during storage, and improving the unloading efficiency of nanomaterials. BRIEF DESCRIPTION OF THE DRAWINGS

[0019] Figure 1 It is a schematic diagram of the overall structure of the present invention;

[0020] Figure 2 It is a schematic diagram of the structure of the present invention;

[0021] Figure 3 It is a schematic diagram of the cross-sectional structure of the inner wall of the reaction box of the present invention;

[0022] Figure 4 This is a schematic diagram of the structure of the material storage tray of the present invention;

[0023] Figure 5 It is a schematic diagram of the planar structure of the present invention.

[0024] In the figure: 1, positioning frame; 2, first storage box; 3, second storage box; 4, bottom plate; 5, support frame; 6, storage tray; 7, hot air source; 8, air pump; 9, first conduit; 10, second conduit; 11, one-way valve; 12, first reaction box; 13, second reaction box; 14, first liquid feed pump; 15, third conduit; 16, second liquid feed pump; 17, first exhaust pipe; 18, second exhaust pipe; 19, spiral groove; 20, partition plate; 21, motor; 22, spiral air guide plate. DETAILED DESCRIPTION

[0025] The present invention provides Figure 1 - Figure 5The separation device for preparing nanomaterials shown in the figure comprises a positioning frame 1, a first material storage box 2 is fixedly arranged at one end of the top of the positioning frame 1, a second material storage box 3 is fixedly arranged at the other end of the top of the positioning frame 1, a first reaction box 12 is fixedly arranged at the middle position of the top of the first material storage box 2, a second reaction box 13 is fixedly arranged at the middle position of the top of the second material storage box 3, spiral grooves 19 are fixedly arranged on the inner wall of the first reaction box 12 and the inner wall of the second reaction box 13, spiral air guide plates 22 are fixedly arranged at the middle position inside the first reaction box 12 and the middle position inside the second reaction box 13, a hot air source 7 is fixedly arranged at one end of one side of the top of the positioning frame 1, an air pump 8 is fixedly arranged at one end of the hot air source 7, a first conduit 9 is fixedly arranged at one end of one side of the air pump 8, a second conduit 10 is fixedly arranged at the other end of one side of the air pump 8, and the first conduit 9 is fixedly arranged at the second conduit 10. One end is connected with one end of one side of the first reaction box 12, one end of the second conduit 10 is connected with one end of one side of the second reaction box 13, one end of the outer wall of the first reaction box 12 is connected with a third conduit 15, one end of the third conduit 15 is connected with a first liquid pump 14, the middle position of the top of the first reaction box 12 is connected with a second liquid pump 16, one end of the second liquid pump 16 is connected with a first exhaust pipe 17, one end of the first exhaust pipe 17 is connected with one end of the outer wall of the second reaction box 13, the middle position of the top of the second reaction box 13 is connected with a second exhaust pipe 18, one end of the outer wall of the first conduit 9 and one end of the outer wall of the second conduit 10 are fixed with a one-way valve 11, one end of the middle position of the top of the positioning frame 1 is fixed with a support frame 5, and the middle position of the top of the support frame 5 is fixedly connected to the bottom end of the first liquid pump 14.

[0026] like Figure 4 As shown, a storage tray 6 is rotatably provided at one end of the bottom of the first storage box 2 and one end of the bottom of the second storage box 3 , and a partition plate 20 is fixedly provided at the middle position of the two storage trays 6 .

[0027] like Figure 1 As shown, a base plate 4 is fixedly provided at the bottom end of the positioning frame 1, and motors 21 are fixedly provided at both ends of the middle position of the top of the base plate 4, and the output ends of the two motors 21 pass through the positioning frame 1 and are fixedly connected to the middle positions of the bottoms of the two storage trays 6 respectively, and a switch panel is fixedly provided on one side of the positioning frame 1, and a motor switch, an air pump switch, a first liquid feed pump switch and a second liquid feed pump switch are fixedly provided on the surface of the switch panel respectively, and the two motors 21, the air pump 8, the first liquid feed pump 14 and the second liquid feed pump 16 are electrically connected to the external power supply through the motor switch, the air pump switch, the first liquid feed pump switch and the second liquid feed pump switch respectively.

[0028] The working principle of the present invention is as follows: Figure 1 - Figure 3 and Figure 5As shown, the hot air sprayed by the hot air source 7 and the liquid material mist containing nanoparticles form a mixed aerosol, and the spiral air guide plate 22 forces the mixed aerosol to rotate. The centrifugal force of the rotation causes the particles to enter the spiral groove 19, and the separation is enhanced. The hot air is pyrolyzed to separate the nanoparticles in the liquid material. The hot air source 7 is transmitted by the air pump 8, the first conduit 9 and the second conduit 10, so that the hot air flows into the first reaction box 12 and the second reaction box 13. The nanoparticles are introduced into the first reaction box 12 through the first liquid pump 14 and the third conduit 15 to form a mixed aerosol. The spiral air guide plate 22 forces the mixed aerosol to rotate, and the centrifugal force of the rotation causes the particles to enter the spiral groove 19. The required nanomaterials flow into the first storage box 2 at the bottom of the first reaction box 12, and the excess waste gas and the doped nanomaterial mist are moved to the second reaction box 13 through the transportation of the second liquid pump 16 and the transmission of the first waste gas pipe 17, and the mixed mist is forced to rotate by the spiral air guide plate 22. The centrifugal force of the rotation causes the particles to enter the spiral groove 19, strengthen the separation, and perform pyrolysis with hot air, so that the nanoparticles in the liquid are separated and fall into the second storage box 3. The remaining waste gas is transported and processed through the second waste gas pipe 18, thereby avoiding the waste of materials due to the uneven separation of nanomaterials and improving the working efficiency of the separation device for preparing nanomaterials.

[0029] like Figure 4 As shown, turn on the motor switch so that the output end of the motor 21 fixed on the top of the bottom plate 4 drives the storage tray 6 to rotate. The storage tray 6 is separated by the middle partition plate 20, so that the two ends of the partition plate 20 can be indirectly unloaded, so that while the nanomaterials are continuously falling downward, the materials can be indirectly collected, avoiding the problem of accumulation of the storage of nanomaterials and improving the unloading efficiency of nanomaterials.

Claims

1. A separation device for preparing nanomaterials, comprising a positioning frame (1), characterized in that: A first material storage box (2) is fixedly provided at one end of the top of the positioning frame (1), a second material storage box (3) is fixedly provided at the other end of the top of the positioning frame (1), a first reaction box (12) is fixedly provided at the middle position of the top of the first material storage box (2), a second reaction box (13) is fixedly provided at the middle position of the top of the second material storage box (3), the inner wall of the first reaction box (12) and the inner wall of the second reaction box (13) are both fixedly provided with spiral grooves (19), the middle position of the interior of the first reaction box (12) and the interior of the second reaction box (13) are fixedly provided with spiral grooves (19), and the inner wall of the first reaction box (12) and the inner wall of the second reaction box (13) are fixedly provided with spiral grooves (19). 3) A spiral air guide plate (22) is fixedly provided at the middle position of the interior, a hot air source (7) is fixedly provided at one end of the top side of the positioning frame (1), an air pump (8) is fixedly provided at one end of the hot air source (7), a first conduit (9) is fixedly provided at one end of one side of the air pump (8), a second conduit (10) is fixedly provided at the other end of one side of the air pump (8), one end of the first conduit (9) is communicated with one end of one side of the first reaction box (12), and one end of the second conduit (10) is communicated with one end of one side of the second reaction box (13); wherein, a third conduit (15) is connected to one end of the outer wall of the first reaction box (12), a first liquid feed pump (14) is connected to one end of the third conduit (15), a second liquid feed pump (16) is connected to the middle position of the top of the first reaction box (12), a first waste gas pipe (17) is connected to one end of the second liquid feed pump (16), one end of the first waste gas pipe (17) is connected to one end of the outer wall of the second reaction box (13), a second waste gas pipe (18) is connected to the middle position of the top of the second reaction box (13), and a one-way valve (11) is fixedly provided on one end of the outer wall of the first conduit (9) and one end of the outer wall of the second conduit (10); A support frame (5) is fixedly provided at one end of the middle position of the top of the positioning frame (1), and the middle position of the top of the support frame (5) is fixedly connected to the bottom end of the first liquid pump (14). One end of the bottom of the first storage box (2) and one end of the bottom of the second storage box (3) are both rotatably provided with storage trays (6), and a partition plate (20) is fixedly provided at the middle position of the two storage trays (6). A bottom plate (4) is fixedly provided at the bottom end of the positioning frame (1).

2. The separation device for preparing nanomaterials according to claim 1, characterized in that: Motors (21) are fixedly provided at both ends of the middle position of the top of the bottom plate (4), and the output ends of the two motors (21) pass through the positioning frame (1) and are respectively fixedly connected to the middle positions of the bottoms of the two storage trays (6).

3. The separation device for preparing nanomaterials according to claim 2, characterized in that: A switch panel is fixedly provided on one side of the positioning frame (1), and a motor switch, an air pump switch, a first liquid feed pump switch, and a second liquid feed pump switch are fixedly provided on the surface of the switch panel. The two motors (21), the air pump (8), the first liquid feed pump (14), and the second liquid feed pump (16) are electrically connected to an external power supply via the motor switch, the air pump switch, the first liquid feed pump switch, and the second liquid feed pump switch.

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