Moisturizing aerosol and preparation method thereof
By using specific formulas and preparation steps in moisturizing aerosols, the problem that existing moisturizing aerosols cannot penetrate deeply and regulate the skin oil balance is solved, achieving the effect of long-term moisturizing and oil balance.
Patent Information
- Application Number
- CN202410092496.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-01-23
- Publication Date
- 2025-03-04
- Estimated Expiration
- 2044-01-23
AI Technical Summary
Existing moisturizing aerosols cannot effectively penetrate deep into the skin and form a greasy feeling on the surface of the skin, which cannot effectively balance the skin's water and oil content.
Moisturizing aerosols are prepared by specific stirring and heating steps using formulas containing hyaluronic acid, glycerin, penetration enhancers, grape seed oil, walnut oil, carnauba wax, cornflower extract, cholesterol and emulsifiers.
It achieves deep penetration of moisturizers, provides long-term moisturizing effect, and at the same time adjusts the oil balance of the skin, controls excessive oil secretion, and keeps the skin soft and refreshing.
Smart Images

Figure SMS_1 
Figure SMS_2
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of aerosols, in particular to a moisturizing aerosol and a preparation method thereof. Background Art
[0002] As people's living standards improve, they pay more and more attention to the care and maintenance of their skin. Healthy skin should be smooth, moisturized and elastic, which mainly depends on the water content in the skin. In recent years, people have been working in air-conditioned rooms or dry environments for a long time, and the problem of skin dehydration has become increasingly serious, making people's skin drier and aging faster. The oil skin care of the past can no longer meet the requirements of modern people for hydrating and moisturizing cosmetics. More and more people like moisturizing aerosols that have good moisturizing properties, are also nutritious to the skin and have few side effects.
[0003] The moisturizing aerosol has a short residence time on the skin and poor penetration ability, and cannot penetrate into the deep layer of the skin. In addition, the moisturizing aerosol will form a greasy feeling on the skin surface and cannot effectively balance the water and oil content of the skin. Therefore, the present application proposes a moisturizing aerosol and a preparation method thereof. Summary of the invention
[0004] The purpose of the present invention is to solve the problem that the moisturizing aerosol in the background technology cannot penetrate into the deep layer of the skin, and to provide a moisturizing aerosol and a preparation method thereof.
[0005] In one aspect, the present invention provides a moisturizing aerosol, comprising the following raw materials in parts by weight:
[0006] 0.8-3.2 parts of hyaluronic acid, 3-7 parts of glycerin, 1-3 parts of penetration enhancer, 1-5 parts of grape seed oil, 1-3 parts of walnut oil, 0.5-1.5 parts of carnauba wax, 1.2-2.8 parts of cornflower extract, 0.2-0.8 parts of cholesterol, 1.5-4.5 parts of emulsifier, 65-98 parts of deionized water;
[0007] The penetration enhancer includes propylene glycol, almond shell powder, fruit acid, phospholipids and sodium lauryl sulfate.
[0008] Optionally, the penetration enhancer comprises the following raw materials in parts by weight: 0.5 parts of propylene glycol, 0.2 parts of almond shell powder, 0.1 parts of fruit acid, 0.1 parts of phospholipids, and 0.1 parts of sodium lauryl sulfate.
[0009] Optionally, the following raw materials are included in parts by weight: 1-3 parts of hyaluronic acid, 4-6 parts of glycerin, 2-3 parts of penetration enhancer, 2-4 parts of grape seed oil, 2-3 parts of walnut oil, 1-1.5 parts of carnauba wax, 1.5-2.5 parts of cornflower extract, 0.3-0.7 parts of cholesterol, 1.8-4.2 parts of emulsifier, and 72-90 parts of deionized water.
[0010] Optionally, the cornflower extract is prepared by a preparation method comprising the following steps:
[0011] The whole cornflower herb is ground to obtain a powder raw material, and then refluxed and leached with a 40-60% volume fraction ethanol solution for 4-6 times, each leaching time is 30-90 minutes, and then concentrated and dried to obtain the cornflower extract.
[0012] Optionally, the emulsifier is prepared by mixing glyceryl stearate and polyoxyethylene hydrogenated castor oil in a ratio of 1:1.
[0013] On the other hand, the present invention provides a method for preparing the above moisturizing aerosol, comprising the following preparation steps:
[0014] S1, preparation of penetration enhancer:
[0015] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at a speed of 200-300 rad / min at 20-30° C. for 20-40 min to obtain a mixture;
[0016] S102, adding fruit acid, phospholipids and sodium lauryl sulfate to the mixture and continuing to stir and mix for 1-2 hours to prepare a penetration enhancer for use;
[0017] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, stirring for 20-30 minutes to obtain melted oil;
[0018] S3, adding an emulsifier to the melted oil and continuing stirring for 10-20 minutes to obtain an oil mixture;
[0019] S4, heating deionized water to 80°C, then pouring the heated deionized water into the oil mixture and stirring for 30-60 minutes;
[0020] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle, and continuing to stir for 10-20 minutes;
[0021] S6, add hyaluronic acid and glycerin to the reactor and continue stirring for 20-40 minutes;
[0022] S7, the reaction kettle is cooled to 30-35°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0023] Optionally, in step S2, the heating temperature is 50-60°C.
[0024] Optionally, in S4, the deionized water is heated using a constant temperature water bath, the deionized water is added to a container, the container is placed in a water bath, and the heating temperature of 80° C. is controlled and maintained by adjusting the temperature of the water bath.
[0025] Optionally, in S6, the rotation speed of the reactor is 220-280 rad / min.
[0026] Optionally, the specific preparation steps of the almond shell powder are: putting clean and dry almond shells into the grinding chamber of a ball mill, passing the powder after 12 hours of ball milling through a 200-mesh sieve, and then putting it into a bellows to dry to obtain the almond shell powder.
[0027] Compared with the prior art, the present invention has the following beneficial technical effects:
[0028] The benefits of the above formula and the resulting moisturizer are as follows:
[0029] The present invention has good permeability through hyaluronic acid and glycerin, which can quickly penetrate into the deep layer of the skin and provide a long-lasting moisturizing effect. The permeability of grape seed oil and walnut oil also helps the moisturizer to better penetrate into the deep layer of the skin and provide a comprehensive moisturizing effect. At the same time, grape seed oil and walnut oil have the function of regulating the oil balance of the skin in the formula. They can provide sufficient moisturizing while controlling excessive oil secretion of the skin, regulating the oil balance of the skin, controlling excessive oil secretion, and keeping the skin soft and refreshing.
[0030] By adding cornflower extract rich in anti-inflammatory ingredients, it can relieve skin inflammation and sensitive reactions, reduce skin discomfort, and make the moisturizer more comfortable, gentle and non-irritating during use. It is suitable for all skin types, including sensitive skin.
[0031] By adding propylene glycol and almond shell powder and stirring and mixing, the permeability and absorption of the moisturizer can be enhanced. Propylene glycol has good permeability and can promote the moisturizer to penetrate deeper into the skin better. Almond shell powder can remove the stratum corneum, improve the skin's absorbability, and further promote the penetration and absorption of the moisturizer. It has a synergistic effect, enhancing the permeability and absorption of the moisturizer, allowing it to better penetrate deeper into the skin and provide a long-lasting moisturizing effect.
[0032] The moisturizing aerosol prepared by the present invention can enhance the permeability and absorbency of the moisturizer, allowing it to better penetrate into the deep layer of the skin, providing a lasting moisturizing effect, while controlling excessive oil secretion of the skin, regulating the oil balance of the skin, controlling excessive oil secretion, and keeping the skin soft and refreshed. DETAILED DESCRIPTION
[0033] The following describes the embodiments of the present invention by specific examples, and those skilled in the art can easily understand other advantages and effects of the present invention from the contents disclosed in this specification. The present invention can also be implemented or applied through other different specific embodiments, and the details in this specification can also be modified or changed in various ways based on different viewpoints and applications without departing from the spirit of the present invention. It should be noted that the following embodiments and features in the embodiments can be combined with each other without conflict.
[0034] In the following examples and comparative examples:
[0035] The specific preparation steps of the almond shell powder are as follows: putting clean and dry almond shells into the grinding chamber of a ball mill, passing the powder after 12 hours of ball milling through a 200-mesh sieve, and then putting the powder into a bellows to dry to obtain the almond shell powder.
[0036] The emulsifier is made by mixing glyceryl stearate and polyoxyethylene hydrogenated castor oil in a 1:1 ratio.
[0037] The cornflower extract is prepared by a preparation method comprising the following steps:
[0038] The whole cornflower herb is ground to obtain a powder raw material, and then reflux-extracted with a 50% by volume ethanol solution for 5 times, each extraction time is 60 minutes, and then concentrated and dried to obtain a cornflower extract.
[0039] Example 1
[0040] The moisturizing aerosol comprises the following raw materials in parts by weight:
[0041] Hyaluronic acid 0.8kg, glycerin 3kg, penetration enhancer 1kg, grape seed oil 1kg, walnut oil 1kg, carnauba wax 0.5kg, cornflower extract 1.2kg, cholesterol 0.2kg, emulsifier 1.5kg, deionized water 65kg;
[0042] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.2 kg of almond shell powder, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0043] Specific preparation steps of moisturizing aerosol:
[0044] S1, preparation of penetration enhancer:
[0045] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at a speed of 200 rad / min at 20° C. for 20 min to obtain a mixture;
[0046] S102, adding fruit acid, phospholipids and sodium lauryl sulfate to the mixture and continuing to stir and mix for 1 hour to prepare a penetration enhancer for use;
[0047] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 50° C., stirring for 20 minutes, to obtain melted oil;
[0048] S3, adding the emulsifier to the melted oil and continuing stirring for 10 minutes to obtain an oil mixture;
[0049] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 30 minutes;
[0050] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 10 min;
[0051] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 220 rad / min, and stirring is continued for 20 min;
[0052] S7, the reaction kettle is cooled to 30°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0053] Example 2
[0054] The moisturizing aerosol comprises the following raw materials in parts by weight:
[0055] Hyaluronic acid 1.2kg, glycerin 4kg, penetration enhancer 2kg, grape seed oil 2kg, walnut oil 2kg, carnauba wax 0.8kg, cornflower extract 1.5kg, cholesterol 0.3kg, emulsifier 2.2kg, deionized water 70kg;
[0056] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.2 kg of almond shell powder, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0057] Specific preparation steps of moisturizing aerosol:
[0058] S1, preparation of penetration enhancer:
[0059] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at a speed of 220 rad / min at 22° C. for 25 min to obtain a mixture;
[0060] S102, adding fruit acid, phospholipids and sodium lauryl sulfate to the mixture, and continuing to stir and mix for 1.5 hours to prepare a penetration enhancer for use;
[0061] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 52° C., stirring for 23 minutes, to obtain melted oil;
[0062] S3, adding the emulsifier to the melted oil and continuing stirring for 12 minutes to obtain an oil mixture;
[0063] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 40 minutes;
[0064] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 13 min;
[0065] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 240 rad / min, and stirring is continued for 28 minutes;
[0066] S7, the reaction kettle is cooled to 32°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0067] Example 3
[0068] Moisturizing aerosol, including the following raw materials by weight kg:
[0069] Hyaluronic acid 2kg, glycerin 5kg, penetration enhancer 2kg, grape seed oil 3kg, walnut oil 2kg, carnauba wax 1kg, cornflower extract 2kg, cholesterol 0.5kg, emulsifier 3kg, deionized water 81.5kg;
[0070] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.2 kg of almond shell powder, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0071] Specific preparation steps of moisturizing aerosol:
[0072] S1, preparation of penetration enhancer:
[0073] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at a speed of 250 rad / min at 25° C. for 30 minutes to obtain a mixture;
[0074] S102, adding fruit acid, phospholipids and sodium lauryl sulfate to the mixture, and continuing to stir and mix for 1.5 hours to prepare a penetration enhancer for use;
[0075] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 55° C., stirring for 25 minutes, to obtain melted oil;
[0076] S3, adding the emulsifier to the melted oil and continuing stirring for 15 minutes to obtain an oil mixture;
[0077] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 45 minutes;
[0078] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 15 min;
[0079] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 250 rad / min, and stirring is continued for 30 minutes;
[0080] S7, the reaction kettle is cooled to 32.5°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0081] Example 4
[0082] The moisturizing aerosol comprises the following raw materials in parts by weight:
[0083] Hyaluronic acid 2.8kg, glycerin 6kg, penetration enhancer 2kg, grape seed oil 4kg, walnut oil 2kg, carnauba wax 1.2kg, cornflower extract 2.4kg, cholesterol 0.6kg, emulsifier 4.0kg, deionized water 88kg;
[0084] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.2 kg of almond shell powder, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0085] Specific preparation steps of moisturizing aerosol:
[0086] S1, preparation of penetration enhancer:
[0087] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at 28° C. and a speed of 270 rad / min for 35 minutes to obtain a mixture;
[0088] S102, adding fruit acid, phospholipids and sodium lauryl sulfate to the mixture, and continuing to stir and mix for 1.8 hours to prepare a penetration enhancer for use;
[0089] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 58° C., stirring for 28 minutes, to obtain melted oil;
[0090] S3, adding the emulsifier to the melted oil and continuing stirring for 18 minutes to obtain an oil mixture;
[0091] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 50 minutes;
[0092] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 18 min;
[0093] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 270 rad / min, and stirring is continued for 35 minutes;
[0094] S7, the reaction kettle is cooled to 34°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0095] Example 5
[0096] Moisturizing aerosol, including the following raw materials by weight kg:
[0097] 3.2kg hyaluronic acid, 7kg glycerin, 3kg penetration enhancer, 5kg grape seed oil, 3kg walnut oil, 1.5kg carnauba wax, 2.8kg cornflower extract, 0.8kg cholesterol, 4.5kg emulsifier, 98kg deionized water;
[0098] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.2 kg of almond shell powder, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0099] Specific preparation steps of moisturizing aerosol:
[0100] S1, preparation of penetration enhancer:
[0101] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at 30° C. and a speed of 300 rad / min for 40 minutes to obtain a mixture;
[0102] S102, adding fruit acid, phospholipids and sodium lauryl sulfate to the mixture and continuing to stir and mix for 2 hours to prepare a penetration enhancer for use;
[0103] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 60° C., stirring for 30 minutes, to obtain melted oil;
[0104] S3, adding an emulsifier to the melted oil and continuing stirring for 20 minutes to obtain an oil mixture;
[0105] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 60 minutes;
[0106] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 20 min;
[0107] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 280 rad / min, and stirring is continued for 40 minutes;
[0108] S7, the reaction kettle is cooled to 35°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0109] Comparative Example 1
[0110] The moisturizing aerosol comprises the following raw materials in parts by weight:
[0111] Hyaluronic acid 0.8kg, glycerin 3kg, penetration enhancer 1kg, grape seed oil 1kg, walnut oil 1kg, carnauba wax 0.5kg, cornflower extract 1.2kg, cholesterol 0.2kg, emulsifier 1.5kg, deionized water 65kg;
[0112] The penetration enhancer includes the following raw materials by weight kg: 0.2 kg of almond shell powder, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0113] Specific preparation steps of moisturizing aerosol:
[0114] S1, preparing a penetration enhancer: adding almond shell powder into a blender, then adding fruit acid, phospholipids, and sodium lauryl sulfate, and continuing to stir and mix for 1 hour, stirring and mixing at 20° C. and a speed of 200 rad / min for 20 minutes to prepare a penetration enhancer for use;
[0115] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 50° C., stirring for 20 minutes, to obtain melted oil;
[0116] S3, adding the emulsifier to the melted oil and continuing stirring for 10 minutes to obtain an oil mixture;
[0117] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 30 minutes;
[0118] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 10 min;
[0119] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 220 rad / min, and stirring is continued for 20 min;
[0120] S7, the reaction kettle is cooled to 30°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0121] Comparative Example 2
[0122] The moisturizing aerosol comprises the following raw materials in parts by weight:
[0123] Hyaluronic acid 0.8kg, glycerin 3kg, penetration enhancer 1kg, grape seed oil 1kg, walnut oil 1kg, carnauba wax 0.5kg, cornflower extract 1.2kg, cholesterol 0.2kg, emulsifier 1.5kg, deionized water 65kg;
[0124] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0125] Specific preparation steps of moisturizing aerosol:
[0126] S1, preparation of penetration enhancer:
[0127] S101, adding propylene glycol into a stirrer, stirring at 20°C and a speed of 200 rad / min for 20 min, then adding fruit acid, phospholipids, and sodium lauryl sulfate, and continuing to stir and mix for 1 h to prepare a penetration enhancer for use;
[0128] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 50° C., stirring for 20 minutes, to obtain melted oil;
[0129] S3, adding the emulsifier to the melted oil and continuing stirring for 10 minutes to obtain an oil mixture;
[0130] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 30 minutes;
[0131] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 10 min;
[0132] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 220 rad / min, and stirring is continued for 20 min;
[0133] S7, the reaction kettle is cooled to 30°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0134] Comparative Example 3
[0135] The moisturizing aerosol comprises the following raw materials in parts by weight:
[0136] Hyaluronic acid 0.8kg, glycerin 3kg, penetration enhancer 1kg, grape seed oil 1kg, walnut oil 1kg, carnauba wax 0.5kg, cornflower extract 1.2kg, cholesterol 0.2kg, emulsifier 1.5kg, deionized water 65kg;
[0137] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.2 kg of almond shell powder, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0138] Specific preparation steps of moisturizing aerosol:
[0139] S1, preparation of penetration enhancer:
[0140] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at a speed of 200 rad / min at 20° C. for 20 min to obtain a mixture;
[0141] S102, adding phospholipids and sodium dodecyl sulfate to the mixture, and continuing to stir and mix for 1 hour to prepare a penetration enhancer for use;
[0142] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 50° C., stirring for 20 minutes, to obtain melted oil;
[0143] S3, adding the emulsifier to the melted oil and continuing stirring for 10 minutes to obtain an oil mixture;
[0144] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 30 minutes;
[0145] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 10 min;
[0146] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 220 rad / min, and stirring is continued for 20 min;
[0147] S7, the reaction kettle is cooled to 30°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0148] Comparative Example 4
[0149] Moisturizing aerosol, including the following raw materials by weight kg:
[0150] Hyaluronic acid 0.8kg, glycerin 3kg, penetration enhancer 1kg, grape seed oil 1kg, walnut oil 1kg, carnauba wax 0.5kg, cornflower extract 1.2kg, cholesterol 0.2kg, emulsifier 1.5kg, deionized water 65kg;
[0151] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.2 kg of almond shell powder, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0152] Specific preparation steps of moisturizing aerosol:
[0153] S1, preparation of penetration enhancer:
[0154] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at a speed of 200 rad / min at 20° C. for 20 min to obtain a mixture;
[0155] S102, adding fruit acid and sodium lauryl sulfate to the mixture, and continuing to stir and mix for 1 hour to prepare a penetration enhancer for use;
[0156] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 50° C., stirring for 20 minutes, to obtain melted oil;
[0157] S3, adding the emulsifier to the melted oil and continuing stirring for 10 minutes to obtain an oil mixture;
[0158] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 30 minutes;
[0159] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 10 min;
[0160] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 220 rad / min, and stirring is continued for 20 min;
[0161] S7, the reaction kettle is cooled to 30°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0162] Comparative Example 5
[0163] Moisturizing aerosol, including the following raw materials by weight kg:
[0164] Hyaluronic acid 0.8kg, glycerin 3kg, penetration enhancer 1kg, grape seed oil 1kg, walnut oil 1kg, carnauba wax 0.5kg, cornflower extract 1.2kg, cholesterol 0.2kg, emulsifier 1.5kg, deionized water 65kg;
[0165] The penetration enhancer includes the following raw materials by weight kg: 0.5 kg of propylene glycol, 0.2 kg of almond shell powder, 0.1 kg of fruit acid, 0.1 kg of phospholipids, and 0.1 kg of sodium lauryl sulfate.
[0166] Specific preparation steps of moisturizing aerosol:
[0167] S1, preparation of penetration enhancer:
[0168] S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at a speed of 200 rad / min at 20° C. for 20 min to obtain a mixture;
[0169] S102, adding fruit acid and phospholipid to the mixture and continuing to stir and mix for 1 hour to prepare a penetration enhancer for use;
[0170] S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, heating temperature is 50° C., stirring for 20 minutes, to obtain melted oil;
[0171] S3, adding the emulsifier to the melted oil and continuing stirring for 10 minutes to obtain an oil mixture;
[0172] S4, heating the deionized water using a constant temperature water bath, adding the deionized water into the container, placing the container in the water bath, controlling and maintaining the heating temperature of 80°C by adjusting the temperature of the water bath, and then pouring the heated deionized water into the oil and fat mixture and stirring for 30 minutes;
[0173] S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle and continuing stirring for 10 min;
[0174] S6, add hyaluronic acid and glycerin to the reactor, the speed of the reactor is 220 rad / min, and stirring is continued for 20 min;
[0175] S7, the reaction kettle is cooled to 30°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
[0176] Comparative Example 6
[0177] The only difference between this comparative example and Example 1 is that the amount of the penetration enhancer is 0.8 kg, and the preparation method is the same as that of Example 1.
[0178] Comparative Example 7
[0179] The only difference between this comparative example and Example 1 is that the amount of the penetration enhancer is 3.5 kg, and the preparation method is the same as that of Example 1.
[0180] In order to verify the technical effect of the present invention, the performance tests were carried out on the moisturizing aerosols prepared in Examples 1-5 and Comparative Examples 1-7.
[0181] Skin moisture test
[0182] Test samples: moisturizing aerosols prepared in Examples 1-5 and Comparative Examples 1-7;
[0183] Test subjects: 80 female subjects aged 27-40 years with healthy skin were randomly divided into 8 groups, 10 in each group;
[0184] Test method: Each group of subjects used the moisturizing aerosol prepared in Examples 1-5 and Comparative Examples 1-7, respectively, selected a 5 cm × 6 cm healthy skin area on the inner side of the forearm of the subject, and used a skin moisture tester (corneometer) to test the skin moisture content in the selected area before and after the treatment; then used the corresponding moisturizing aerosol in the selected area, twice a day in the morning and evening, for 7 consecutive days, tested the skin moisture content every day with a corneometer, and recorded the average value of the skin moisture content of each group;
[0185] Test results: See Table 1 for specific test results.
[0186] Table 1 Skin moisture content test data of Examples 1-5 and Comparative Examples 1-7
[0187]
[0188] By comparing Examples 1-5 and Comparative Examples 1-5 in Table 1, the penetration enhancer prepared by the present invention has excellent performance in skin moisturizing, and the moisturizing performance is better maintained. By comparing Example 1 and Comparative Examples 6-7, under the same penetration enhancer formula, the ratio of the penetration enhancer in the moisturizing aerosol prepared by the present invention is more preferred, and has obvious advantages in moisturizing effect.
[0189] Water and oil balance test
[0190] The moisturizing aerosols prepared in Examples 1-5 and the moisturizing aerosols prepared in Control Examples 1-7 were tested on test subjects respectively, and the changes in sebum content and water content before and after use proved the effectiveness of the moisturizing aerosols.
[0191] Test method: 7 females aged 22-25 were selected, all with oily or mixed skin, without any history of skin diseases or skin allergies. Each of them applied a test sample to the same part of the face. During the test, no cosmetics other than the test sample could be used.
[0192] The test was conducted using the SebumScale sebum meter and VapoMeter transepidermal moisture loss tester from the Finnish company Dilfin. The same part of the face was selected as the test site. Before use, the sebum content and moisture content of the test subjects were tested respectively. After cleansing with water, a proper amount of the product was applied to the face and massaged to promote product absorption. After 8 hours, the sebum content and moisture content of the test subjects were tested again. The test results are shown in Table 2.
[0193] Table 2 Water-oil balance test data of Examples 1-5 and Comparative Examples 1-7
[0194]
[0195] As can be seen from Table 2, the moisturizing aerosol for regulating the water-oil balance of the skin prepared in Examples 1-5 of the present invention has good oil control effect and moisturizing effect, can effectively maintain the water-oil balance, effectively reduce the greasy feeling after use, ensure the skin is refreshing, and improve the user experience. Comparing Examples 1-5 and 6-7, the raw material ratio of the present invention is more preferred. By comparing Comparative Examples 1-2 and Comparative Examples 3-5. By adding a mixture of propylene glycol and almond shell powder, the permeability and absorbency of the moisturizer can be enhanced. Propylene glycol has good permeability and can promote the moisturizer to penetrate better into the deep layer of the skin. Almond shell powder can remove the stratum corneum, improve the absorbency of the skin, and further promote the penetration and absorption of the moisturizer.
[0196] The present invention has good permeability through hyaluronic acid and glycerin, which can quickly penetrate into the deep layer of the skin and provide a long-lasting moisturizing effect. The permeability of grape seed oil and walnut oil also helps the moisturizer to better penetrate into the deep layer of the skin and provide a comprehensive moisturizing effect. At the same time, grape seed oil and walnut oil have the function of regulating the oil balance of the skin in the formula. They can provide sufficient moisturizing while controlling excessive oil secretion of the skin, regulating the oil balance of the skin, controlling excessive oil secretion, and keeping the skin soft and refreshing.
[0197] By adding cornflower extract rich in anti-inflammatory ingredients, skin inflammation and sensitive reactions can be alleviated, skin discomfort can be reduced, and the moisturizer can be made more comfortable during use, mild and non-irritating, and suitable for various skin types, including sensitive skin. By adding propylene glycol and almond shell powder, the permeability and absorptivity of the moisturizer can be enhanced. Propylene glycol has good permeability and can promote the moisturizer to penetrate into the deep layer of the skin better. Almond shell powder can remove the stratum corneum, improve the absorbability of the skin, further promote the penetration and absorption of the moisturizer, have a synergistic effect, enhance the permeability and absorptivity of the moisturizer, make it penetrate into the deep layer of the skin better, and provide a lasting moisturizing effect. The moisturizing aerosol prepared by the present invention can enhance the permeability and absorptivity of the moisturizer, make it penetrate into the deep layer of the skin better, provide a lasting moisturizing effect, and control the excessive oil secretion of the skin at the same time, adjust the oil balance of the skin, control the excessive oil secretion, and keep the skin soft and refreshing.
[0198] The above specific embodiments are only several optional embodiments of the present invention. Based on the technical solutions of the present invention and the relevant inspirations of the above embodiments, those skilled in the art can make various alternative improvements and combinations to the above specific embodiments.
Claims
1. A moisturizing aerosol, characterized in that: It includes the following raw materials in parts by weight: 0.8-3.2 parts of hyaluronic acid, 3-7 parts of glycerin, 1-3 parts of penetration enhancer, 1-5 parts of grape seed oil, 1-3 parts of walnut oil, 0.5-1.5 parts of carnauba wax, 1.2-2.8 parts of cornflower extract, 0.2-0.8 parts of cholesterol, 1.5-4.5 parts of emulsifier, 65-98 parts of deionized water; The penetration enhancer includes propylene glycol, almond shell powder, fruit acid, phospholipids, and sodium lauryl sulfate.
2. The moisturizing aerosol according to claim 1, characterized in that: The penetration enhancer comprises the following raw materials in parts by weight: 0.5 parts of propylene glycol, 0.2 parts of almond shell powder, 0.1 parts of fruit acid, 0.1 parts of phospholipids, and 0.1 parts of sodium lauryl sulfate.
3. The moisturizing aerosol according to claim 2, characterized in that: The invention comprises the following raw materials in parts by weight: 1-3 parts of hyaluronic acid, 4-6 parts of glycerin, 2-3 parts of penetration enhancer, 2-4 parts of grape seed oil, 2-3 parts of walnut oil, 1-1.5 parts of carnauba wax, 1.5-2.5 parts of cornflower extract, 0.3-0.7 parts of cholesterol, 1.8-4.2 parts of emulsifier and 72-90 parts of deionized water.
4. The moisturizing aerosol according to claim 1, characterized in that: The cornflower extract is prepared by a preparation method comprising the following steps: The whole cornflower herb is ground to obtain a powder raw material, and then reflux-extracted with a 40-60% volume fraction ethanol solution for 4-6 times, each extraction time is 30-90 minutes, and then concentrated and dried to obtain the cornflower extract.
5. The moisturizing aerosol according to claim 1, characterized in that: The emulsifier is prepared by mixing glyceryl stearate and polyoxyethylene hydrogenated castor oil in a ratio of 1:
1.
6. The method for preparing the moisturizing aerosol according to any one of claims 1 to 5, characterized in that: The method comprises the following preparation steps: S1, preparation of penetration enhancer: S101, adding propylene glycol and almond shell powder into a blender, stirring and mixing at a speed of 200-300 rad / min at 20-30° C. for 20-40 min to obtain a mixture; S102, adding fruit acid, phospholipids and sodium lauryl sulfate to the mixture and continuing to stir and mix for 1-2 hours to prepare a penetration enhancer for use; S2, adding grape seed oil, walnut oil and carnauba wax into a reaction kettle, stirring, mixing, heating and melting, stirring for 20-30 minutes to obtain melted oil; S3, adding an emulsifier to the melted oil and continuing stirring for 10-20 minutes to obtain an oil mixture; S4, heating deionized water to 80°C, then pouring the heated deionized water into the oil mixture and stirring for 30-60 minutes; S5, adding the penetration enhancer, cornflower extract and cholesterol into the reaction kettle, and continuing to stir for 10-20 minutes; S6, add hyaluronic acid and glycerin to the reactor and continue stirring for 20-40 minutes; S7, the reaction kettle is cooled to 30-35°C, the moisturizing agent in the reaction kettle is poured into a container, and the container is sealed and stored to prepare a moisturizing aerosol.
7. The method for preparing the moisturizing aerosol according to claim 6, characterized in that: In step S2, the heating temperature is 50-60°C.
8. The method for preparing the moisturizing aerosol according to claim 6, characterized in that: In S4, the deionized water is heated using a constant temperature water bath, the deionized water is added to a container, the container is placed in a water bath, and the heating temperature of 80° C. is controlled and maintained by adjusting the temperature of the water bath.
9. The method for preparing the moisturizing aerosol according to claim 6, characterized in that: In S6, the rotation speed of the reactor is 220-280 rad / min.
10. The method for preparing the moisturizing aerosol according to claim 6, characterized in that: The specific preparation steps of the almond shell powder are: putting clean and dry almond shells into the grinding chamber of a ball mill, passing the powder after 12 hours of ball milling through a 200-mesh sieve, and then putting the powder into a bellows to dry to obtain the almond shell powder.
Citation Information
Patent Citations
Neutral preservative-free exfoliating mist spray and preparation method thereof
CN108852960A
Moisturizing agent
CN110192992A