A kind of ammonium perchlorate concentration system and method

By designing an ammonium perchlorate concentration system containing magnetic power stirring components, the shortcomings of the traditional concentration device in the agitation and concentration efficiency of ammonium perchlorate liquid material are solved, and a more efficient concentration process is achieved.

CN119098083BActive Publication Date: 2025-02-07DALIAN GAOJIA CHEM
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Patent Information

Application Number
CN202411589204.3
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-11-08
Publication Date
2025-02-07
Estimated Expiration
2044-11-08

AI Technical Summary

Technical Problem

The existing ammonium perchlorate concentration device has shortcomings in terms of stirring efficiency and concentration efficiency, especially in the later concentration process of liquid materials, traditional stirring devices cannot effectively stir the liquid materials, resulting in a decrease in concentration efficiency.

Method used

An ammonium perchlorate concentration system is designed, which includes a cylinder, a liner, a stirring assembly and a drive assembly. The stirring assembly uses multiple stirring seats and a third magnetic block. Through the cooperation of the magnetic strip and the magnetic linkage, the third magnetic block can move in the radial direction of the inner liner during the stirring process, overcome centrifugal force and improve stirring efficiency.

Benefits of technology

Through the design of this system, the stirring efficiency and concentration efficiency of the ammonium perchlorate liquid material can be significantly improved, ensuring the continuity and efficiency of the concentration process.

✦ Generated by Eureka AI based on patent content.

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Abstract

This invention relates to the field of ammonium perchlorate production technology, specifically to an ammonium perchlorate concentration system and method. It includes a cylindrical body, within which an inner liner is rotatably mounted, forming an insulated cavity between the inner liner and the cylindrical body. A heating element is fixed within the insulated cavity. A stirring assembly is installed within the inner liner. A cover is fixed to the upper end of the cylindrical body, and a drive assembly for rotating the stirring assembly and the inner liner is mounted on the cover. The stirring assembly rotates in the opposite direction to the rotation of the inner liner. An inlet pipe and an air pipe are fixed to the upper end of the cover. An outlet pipe is fixed to the lower end of the cylindrical body, and an outlet hole corresponding to the outlet pipe is fixed to the lower end of the inner liner. A lower control valve is installed in the outlet hole. During the rotation of the stirring base, a third magnetic block can move radially along the inner liner, which can improve the stirring efficiency of the liquid ammonium perchlorate material, thereby improving the concentration efficiency.
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Description

Technical Field

[0001] The invention relates to the technical field of ammonium perchlorate production, and in particular to an ammonium perchlorate concentration system and method. Background Art

[0002] Ammonium perchlorate is an inorganic compound, a white crystalline powder, and is deliquescent. Ammonium perchlorate is a strong oxidant, and will explode when mixed with reducing agents, organic matter, flammable substances such as sulfur, phosphorus, or metal powder. Contact with strong acids may cause combustion and explosion. It is used to make explosives, fireworks, and as an analytical reagent.

[0003] During the ammonium perchlorate concentration process, the liquid material of ammonium perchlorate needs to be heated and stirred. Some existing concentration devices are only equipped with traditional simple stirring devices. The traditional simple stirring devices have low efficiency in stirring the liquid material of ammonium perchlorate, which leads to low concentration efficiency of the liquid material of ammonium perchlorate. In the later stage of the concentration process of the liquid material of ammonium perchlorate, ammonium perchlorate crystals are precipitated to the lower part of the concentration device. The traditional stirring device cannot effectively stir the liquid material of ammonium perchlorate at the lower part of the concentration device, and cannot continuously ensure the concentration efficiency of the ammonium perchlorate liquid. Summary of the invention

[0004] The technical problem to be solved by the present invention is to provide an ammonium perchlorate concentration system and method which can effectively stir the liquid material of ammonium perchlorate and can continuously ensure the concentration efficiency of the ammonium perchlorate liquid.

[0005] In order to achieve the above object, the technical solution provided by the present invention is:

[0006] A concentration system for ammonium perchlorate comprises a cylinder, an inner liner is rotatably arranged in the cylinder, a heat preservation chamber is formed between the inner liner and the cylinder, a heating plate is fixed in the heat preservation chamber, a stirring assembly is arranged in the inner liner, a cover is fixed at the upper end of the cylinder, the stirring assembly and the inner liner are connected with a driving assembly, the stirring assembly rotates in opposite directions to the inner liner, an inlet pipe and an air pipe are fixed at the upper end of the cover, an outlet pipe is fixed at the lower end of the cylinder, an outlet hole corresponding to the outlet pipe is fixed at the lower end of the inner liner, a lower control valve is installed in the outlet hole; the stirring assembly comprises a spline shaft concentric with the inner liner, a plurality of stirring seats are sleeved on the spline shaft, a pressing sleeve is sleeved on the spline shaft above the stirring seat, the upper end of the uppermost pressing sleeve is connected to the upper end of the spline shaft by a spring, a plurality of first Three magnetic blocks, the third magnetic block can slide on the stirring seat in the radial direction of the inner tank; a swivel is provided in the axial direction of the inner tank for sliding, the swivel is concentric with the inner tank, a vertical electric push rod is fixed on the cover body, the lower end of the electric push rod is slidably connected with the swivel, a plurality of magnetic strips are evenly distributed and slidably provided on the circumference of the lower end of the swivel, the magnetic strips can move in the radial direction of the swivel, a guide rod is fixed on the inner wall of the inner tank on one side of the magnetic strip, the guide rod is inclined downward at one end toward the center of the inner tank, a third slide groove is provided on the guide rod, the length direction of the third slide groove is parallel to the length direction of the guide rod, a guide block is fixed on the magnetic strip, the guide block is slidably engaged in the third slide groove, the magnetic pole of the magnetic strip at one end toward the center of the inner tank is the same as the magnetic pole of the third magnetic block at one end away from the center of the inner tank.

[0007] Specifically, a limit block is arranged in the inner tank below the magnetic strip, and the limit block includes a vertical portion on the upper side and a straight portion on the lower side. A guide column is fixed on the limit block, and the axial direction of the guide column is parallel to the radial direction of the inner tank. The guide column is slidably and sealedly connected to the inner tank. A vertical groove is arranged on the vertical portion of the limit block, and a protrusion is fixed on the magnetic strip, and the protrusion is slidably engaged in the vertical groove. An arc groove is arranged at the position where the vertical portion and the straight portion of the limit block are connected, and two symmetrically arranged support plates are fixed on the free end of the straight portion of the limit block, and the support plate is inclined upward at one end facing the center of the inner tank, and a straight groove is arranged on the support plate, and the length direction of the straight groove is parallel to the length direction of the support plate, and an arc groove is arranged at the connection between the straight portion and the vertical portion of the limit block. The inner groove is connected with the arc groove, the inner groove is connected with the straight groove, the inner groove and the straight groove constitute a guide groove, and the lower end of the magnetic strip is rotatably connected with a magnetic chain; the magnetic chain includes multiple first magnetic blocks, and the ends of two adjacent first magnetic blocks facing away from the inner wall of the inner tank are rotatably connected by a pin shaft, and the first magnetic block adjacent to the magnetic strip is rotatably connected to the lower end of the magnetic strip through a pin shaft, and the lower end of the magnetic chain is connected with a second magnetic block, and the second magnetic block is rotatably connected to the first magnetic block adjacent to the magnetic strip through a pin shaft, and the pin shaft of the magnetic chain part away from the magnetic strip is slidably engaged in the guide groove, and a plurality of magnetic plates are evenly distributed and fixed on the circumference of the lower end of the lowest stirring seat, and the magnetic pole at the upper end of the second magnetic block is the same as the magnetic pole at the lower end of the magnetic plate, and the magnetic pole at the upper end of the first magnetic block entering between the two support plates is the same as the magnetic pole at the lower end of the magnetic plate.

[0008] Specifically, a flat groove corresponding to the third magnetic block is formed on the stirring seat, the length direction of the flat groove is parallel to the radial direction of the inner pot, and the lower end of the third magnetic block is slidably engaged in the flat groove below it.

[0009] Specifically, the driving assembly includes a shell fixed on the outside of the cylinder, the shell is connected to the insulation chamber, a gear is rotatably arranged in the shell, a gear ring is fixed on the outside of the inner tank, the gear ring is meshed with the gear, the axle of the gear extends to the outside of the shell, a first pulley is fixed on the axle of the gear outside the shell, a bracket is fixed on the upper end of the cover body, a motor is fixed on the bracket, a second pulley is concentrically fixed on the output shaft of the motor, the second pulley is connected to the first pulley through a belt drive, the output shaft of the motor is concentric with the spline shaft, the output shaft of the motor passes through the cover body, the output shaft of the motor is rotatably connected to the cover body, and the output shaft of the motor is concentrically and fixedly connected to the spline shaft.

[0010] Specifically, a slider is fixed at the lower end of the electric push rod, and a first annular sliding groove is coaxially provided at the upper end of the rotating ring, and the slider is slidably engaged in the first sliding groove.

[0011] Specifically, an upper control valve is installed on the inlet pipe.

[0012] Specifically, a second slide groove is provided at the lower end of the rotating ring above the magnetic strip, the length direction of the second slide groove is parallel to the radial direction of the rotating ring, an upper block is fixed at the upper end of the magnetic strip, and the upper block is slidably engaged in the second slide groove.

[0013] A method for concentrating ammonium perchlorate liquid material by an ammonium perchlorate concentration system comprises the following steps:

[0014] S1, close the outlet pipe, open the inlet pipe, and add the ammonium perchlorate liquid material into the inner tank through the inlet pipe;

[0015] S2, starting the heating plate to heat the ammonium perchlorate liquid material in the inner tank, and at the same time, driving the stirring component and the inner tank to rotate;

[0016] S3. After the ammonium perchlorate liquid material is concentrated, the drive assembly is closed, and the outlet pipe is opened to discharge the concentrated ammonium perchlorate liquid material.

[0017] Compared with the prior art, the present invention has the following beneficial effects:

[0018] 1. During the rotation of the stirring seat, when the third magnetic block corresponds to the magnetic strip, since the magnetic pole of the magnetic strip facing the center of the inner tank is the same as the magnetic pole of the third magnetic block facing away from the center of the inner tank, the third magnetic block can overcome the centrifugal force and approach the center of the inner tank along the radial direction of the inner tank. When the third magnetic block is misaligned with the magnetic strip, under the action of centrifugal force, the third magnetic block moves away from the center of the inner tank along the radial direction of the inner tank. During the rotation of the stirring seat, the third magnetic block can move along the radial direction of the inner tank, which can improve the stirring efficiency of the ammonium perchlorate liquid material, thereby improving the concentration efficiency.

[0019] 2. In the later stage of the ammonium perchlorate liquid material concentration process, the liquid level of the ammonium perchlorate liquid material in the inner tank decreases, and ammonium perchlorate crystals are precipitated in the lower end of the inner tank. During the rotation of the inner tank, the support plate can stir the lower part of the ammonium perchlorate liquid material, thereby ensuring the concentration rate.

[0020] 3. Start the electric push rod, the magnetic strip moves downward, and the number of the first magnetic blocks between the two support plates connected to the limit block gradually increases, and the second magnetic block and the first magnetic block between the two support plates gradually move toward the bottom of the stirring assembly. During the rotation of the inner tank and the stirring assembly, after the second magnetic block and the first magnetic block correspond to the magnetic plate up and down, since the magnetic poles at the upper end of the second magnetic block are the same as the magnetic poles at the lower end of the magnetic plate, the magnetic poles at the upper end of the first magnetic block between the two support plates are the same as the magnetic poles at the lower end of the magnetic plate. Therefore, after the second magnetic block and the first magnetic block correspond to the magnetic plate up and down, the multiple stirring seats on the spline shaft can move upward. When the second magnetic block and the first magnetic block are misaligned with the magnetic plate, the stirring seat is restored, that is, the stirring seat can intermittently move up and down during rotation, which can further improve the stirring efficiency of the ammonium perchlorate material. BRIEF DESCRIPTION OF THE DRAWINGS

[0021] Figure 1 It is a schematic diagram of the present invention.

[0022] Figure 2 It is a cross-sectional view of the present invention.

[0023] Figure 3 for Figure 2 Magnified view of area A.

[0024] Figure 4 for Figure 2 Magnified view of area B.

[0025] Figure 5 Schematic diagram of the first magnetic block in the arc groove.

[0026] Figure 6 Schematic diagram of the connection between the swivel and the magnetic strip.

[0027] Figure 7 A schematic diagram of the stirring assembly.

[0028] Figure 8 It is a schematic diagram of a plurality of first magnetic blocks entering between two supporting plates connected to the limiting blocks.

[0029] The names of the parts in the attached figure are: 1. Cylinder; 2. Shell; 3. First pulley; 4. Belt; 5. Second pulley; 6. Bracket; 7. Motor; 8. Inlet pipe; 9. Electric push rod; 10. Upper control valve; 11. Cover; 12. Insulation chamber; 13. Heating plate; 14. Stop block; 15. Inner liner; 16. Gear ring; 17. Gear; 18. Slider; 19. First slide groove; 20. Rotating ring; 21. Outlet pipe; 2 2. Lower control valve; 23. First magnetic block; 24. Agitator seat; 25. Magnetic strip; 26. Guide column; 27. Second slide groove; 28. Guide rod; 29. ​​Third slide groove; 30. Vertical groove; 31. Press sleeve; 32. Third magnetic block; 33. Spring; 34. Spline shaft; 35. Straight groove; 36. Flat groove; 37. Magnetic plate; 38. Air pipe; 39. Second magnetic block; 40. Support plate; 41. Arc groove; 42. Inner groove. DETAILED DESCRIPTION

[0030] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.

[0031] like Figure 1-Figure 8 As shown, an ammonium perchlorate concentration system includes a cylinder 1, an inner liner 15 is rotatably arranged in the cylinder 1, a heat preservation chamber 12 is formed between the inner liner 15 and the cylinder 1, and a heating plate 13 is fixed in the heat preservation chamber 12.

[0032] A stirring assembly is arranged in the inner container 15 , a cover body 11 is fixed to the upper end of the cylinder 1 , the stirring assembly and the inner container 15 are connected to a driving assembly, and the stirring assembly and the inner container 15 rotate in opposite directions.

[0033] The upper end of the cover body 11 is fixed with an inlet pipe 8 and an air pipe 38, the lower end of the cylinder body 1 is fixed with an outlet pipe 21, the lower end of the inner liner 15 is fixed with an outlet hole corresponding to the outlet pipe 21, and the lower control valve 22 is installed in the outlet hole. The inlet pipe 8 is installed with an upper control valve 10.

[0034] The stirring assembly includes a spline shaft 34 concentric with the inner liner 15, a plurality of stirring seats 24 are sleeved on the spline shaft 34, and a press sleeve 31 is sleeved on the spline shaft 34 above the stirring seat 24. The upper end of the uppermost press sleeve 31 is connected to the upper end of the spline shaft 34 through a spring 33. A plurality of third magnetic blocks 32 are evenly distributed on the stirring seat 24, and the third magnetic block 32 can slide on the stirring seat 24 along the radial direction of the inner liner 15. Specifically, a flat groove 36 corresponding to the third magnetic block 32 is provided on the stirring seat 24, and the length direction of the flat groove 36 is parallel to the radial direction of the inner liner 15, and the lower end of the third magnetic block 32 is slidably engaged in the flat groove 36 below it.

[0035] The driving assembly includes a shell 2 fixed on the outside of the cylinder 1, the shell 2 is connected to the insulation chamber 12, a gear 17 is rotatably arranged in the shell 2, a gear ring 16 is fixed on the outside of the inner tank 15, the gear ring 16 is meshed with the gear 17, the axle of the gear 17 extends to the outside of the shell 2, and a first pulley 3 is fixed on the axle of the gear 17 on the outside of the shell 2.

[0036] A bracket 6 is fixed to the upper end of the cover body 11 , a motor 7 is fixed to the bracket 6 , a second pulley 5 is coaxially fixed to the output shaft of the motor 7 , and the second pulley 5 is connected to the first pulley 3 through a belt 4 .

[0037] The output shaft of the motor 7 is concentric with the spline shaft 34 , passes through the cover body 11 , is rotationally connected to the cover body 11 , and is concentrically fixedly connected to the spline shaft 34 .

[0038] A rotating ring 20 is slidably provided in the axial direction of the inner container 15, and the rotating ring 20 is concentric with the inner container 15. A vertical electric push rod 9 is fixed on the cover body 11, and the lower end of the electric push rod 9 is slidably connected with the rotating ring 20. Specifically, a slider 18 is fixed to the lower end of the electric push rod 9, and a first annular sliding groove 19 is concentrically provided on the upper end of the rotating ring 20, and the slider 18 is slidably engaged in the first sliding groove 19.

[0039] A plurality of magnetic strips 25 are evenly distributed and slidably arranged on the circumference of the lower end of the rotating ring 20, and the magnetic strips 25 can move in the radial direction of the rotating ring 20. Specifically, a second slide groove 27 is provided at the lower end of the rotating ring 20 above the magnetic strips 25, and the length direction of the second slide groove 27 is parallel to the radial direction of the rotating ring 20. An upper block is fixed to the upper end of the magnetic strips 25, and the upper block is slidably engaged in the second slide groove 27.

[0040] A guide rod 28 is fixed on the inner wall of the inner liner 15 on one side of the magnetic stripe 25. The guide rod 28 is inclined downward at one end toward the center of the inner liner 15. A third slide groove 29 is provided on the guide rod 28. The length direction of the third slide groove 29 is parallel to the length direction of the guide rod 28. A guide block is fixed on the magnetic stripe 25. The guide block is slidably engaged in the third slide groove 29. The magnetic pole of the end of the magnetic stripe 25 toward the center of the inner liner 15 is the same as the magnetic pole of the end of the third magnetic block 32 away from the center of the inner liner 15.

[0041] A limit block 14 is provided in the inner liner 15 below the magnetic strip 25, and the limit block 14 includes a vertical portion on the upper side and a flat portion on the lower side. A guide post 26 is fixed on the limit block 14, and the axial direction of the guide post 26 is parallel to the radial direction of the inner liner 15, and the guide post 26 is slidably and sealedly connected to the inner liner 15.

[0042] A vertical slot 30 is formed on the vertical portion of the limit block 14 , and a protrusion is fixed on the magnetic strip 25 , and the protrusion is slidably engaged in the vertical slot 30 .

[0043] An arc groove 41 is provided at the position where the vertical part and the straight part of the limit block 14 are connected. Two symmetrically arranged support plates 40 are fixed on the free end of the straight part of the limit block 14, and one end of the support plate 40 facing the center of the inner liner 15 is inclined upward, and a straight groove 35 is provided on the support plate 40, and the length direction of the straight groove 35 is parallel to the length direction of the support plate 40. An arc-shaped inner groove 42 is provided at the connection between the straight part and the vertical part of the limit block 14, and the inner groove 42 is connected to the arc groove 41, and the inner groove 42 is connected to the straight groove 35, and the inner groove 42 and the straight groove 35 constitute a guide groove.

[0044] The lower end of the magnetic strip 25 is rotatably connected with a magnetic chain. The magnetic chain includes a plurality of first magnetic blocks 23, the ends of two adjacent first magnetic blocks 23 facing away from the inner wall of the liner 15 are rotatably connected by a pin, and the first magnetic block 23 adjacent to the magnetic strip 25 is rotatably connected to the lower end of the magnetic strip 25 by a pin. The lower end of the magnetic chain is connected with a second magnetic block 39, and the second magnetic block 39 is rotatably connected to the first magnetic block 23 adjacent to the magnetic strip 25 by a pin, and the pin of the magnetic chain part away from the magnetic strip 25 is slidably engaged in the guide groove.

[0045] A plurality of magnetic plates 37 are evenly distributed and fixed on the circumference of the lower end of the lowest stirring seat 24. The magnetic pole at the upper end of the second magnetic block 39 is the same as the magnetic pole at the lower end of the magnetic plate 37. The magnetic pole at the upper end of the first magnetic block 23 entering between the two support plates 40 is the same as the magnetic pole at the lower end of the magnetic plate 37.

[0046] The upper control valve 10 is opened, and the ammonium perchlorate liquid material is added into the inner pot 15 through the inlet pipe 8. The motor 7 and the heating plate 13 are started, and the heating plate 13 heats the ammonium perchlorate liquid material in the inner pot 15, and the steam is discharged through the air pipe 38. The motor 7 drives the inner pot 15 to rotate through the first pulley 3, the second pulley 5, the belt 4, the gear 17 and the gear ring 16. At the same time, the output shaft of the motor 7 drives the stirring assembly to rotate as a whole, and the inner pot 15 rotates in the opposite direction to the stirring assembly.

[0047] During the rotation of the inner liner 15 , the swivel 20 , the magnetic strip 25 , the limit block 14 and the guide rod 28 rotate accordingly, so the stirring efficiency of the ammonium perchlorate liquid material can be improved during the rotation of the inner liner 15 .

[0048] During the rotation of the stirring assembly, the stirring seat 24 drives the multiple third magnetic blocks 32 thereon to rotate. When the third magnetic block 32 corresponds to the magnetic strip 25, since the magnetic pole of the end of the magnetic strip 25 facing the center of the inner liner 15 is the same as the magnetic pole of the end of the third magnetic block 32 away from the center of the inner liner 15, the third magnetic block 32 can overcome the centrifugal force and approach the center of the inner liner 15 along the radial direction of the inner liner 15.

[0049] When the third magnetic block 32 is misaligned with the magnetic strip 25 , under the action of centrifugal force, the third magnetic block 32 moves away from the center of the inner liner 15 along the radial direction of the inner liner 15 .

[0050] During the rotation of the stirring seat 24, the third magnetic block 32 can reciprocate along the radial direction of the inner container 15, which can improve the stirring efficiency of the ammonium perchlorate liquid material and further improve the concentration efficiency.

[0051] In the later stage of the ammonium perchlorate liquid material concentration process, the liquid level of the ammonium perchlorate liquid material in the inner liner 15 decreases, and ammonium perchlorate crystals are precipitated in the lower end of the inner liner 15. During the rotation of the inner liner 15, the support plate 40 can stir the lower part of the ammonium perchlorate liquid material, thereby ensuring the concentration rate.

[0052] In order to further improve the stirring efficiency, the electric push rod 9 is started, and the rotating ring 20 drives the magnetic strip 25 downward. When the magnetic strip 25 moves downward, the upper block at the upper end of the magnetic strip 25 moves in the second slide groove 27 under the guiding action of the third slide groove 29 on the guide rod 28 through the guide block, and the magnetic strip 25 approaches the center of the inner container 15. Since the protrusion on the magnetic strip 25 slides in the vertical groove 30 when the magnetic strip 25 moves downward, when the magnetic strip 25 approaches the center of the inner container 15, the limit block 14 also approaches the center of the inner container 15, and the guide column 26 moves relative to the inner container 15.

[0053] As the magnetic strip 25 moves downward and approaches the center of the inner container 15, under the guiding effect of the arc groove 41 on the first magnetic block 23 and the guiding effect of the guide groove on the pin shaft, the number of the first magnetic blocks 23 entering between the two support plates 40 connected to the limit block 14 gradually increases, and the second magnetic block 39 and the first magnetic block 23 between the two support plates 40 gradually move toward the bottom of the stirring assembly.

[0054] During the rotation of the inner tank 15 and the stirring assembly, after the second magnetic block 39 and the first magnetic block 23 correspond to the magnetic plate 37 up and down, since the magnetic pole at the upper end of the second magnetic block 39 is the same as the magnetic pole at the lower end of the magnetic plate 37, the magnetic pole at the upper end of the first magnetic block 23 entering between the two support plates 40 is the same as the magnetic pole at the lower end of the magnetic plate 37. Therefore, after the second magnetic block 39 and the first magnetic block 23 correspond to the magnetic plate 37 up and down, the multiple stirring seats 24 on the spline shaft 34 can move upward and compress the spring 33. When the second magnetic block 39 and the first magnetic block 23 are misaligned with the magnetic plate 37, the stirring seat 24 is restored downward, that is, the stirring seat 24 can move up and down intermittently during the rotation, which can further improve the stirring efficiency of the ammonium perchlorate material.

[0055] After the ammonium perchlorate liquid material is concentrated, the lower control valve 22 is opened, and the concentrated ammonium perchlorate liquid material is discharged through the outlet pipe 21.

[0056] A method for concentrating ammonium perchlorate liquid material by an ammonium perchlorate concentration system comprises the following steps:

[0057] S1, close the outlet pipe 21, open the inlet pipe 8, and add the ammonium perchlorate liquid material into the inner container 15 through the inlet pipe 8.

[0058] S2, start the heating plate 13 to heat the ammonium perchlorate liquid material in the inner container 15, and at the same time, drive the stirring component and the inner container 15 to rotate.

[0059] S3. After the ammonium perchlorate liquid material is concentrated, the driving assembly is closed, and the outlet pipe 21 is opened to discharge the concentrated ammonium perchlorate liquid material.

[0060] The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. Any modifications, equivalent substitutions and improvements made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. An ammonium perchlorate concentration system, comprising a cylinder (1), an inner liner (15) rotatably arranged in the cylinder (1), a heat preservation chamber (12) formed between the inner liner (15) and the cylinder (1), a heating plate (13) fixed in the heat preservation chamber (12), characterized in that: The inner container (15) is provided with a stirring assembly, the upper end of the cylinder (1) is fixed with a cover body (11), the stirring assembly and the inner container (15) are connected with a driving assembly, the stirring assembly rotates in opposite directions to the inner container (15), the upper end of the cover body (11) is fixed with an inlet pipe (8) and an air pipe (38), the lower end of the cylinder (1) is fixed with an outlet pipe (21), the lower end of the inner container (15) is fixed with an outlet hole corresponding to the outlet pipe (21), and a lower control valve (22) is installed in the outlet hole; the stirring assembly includes The inner liner (15) is provided with a spline shaft (34) concentric with the inner liner (15), and a plurality of stirring seats (24) are sleeved on the spline shaft (34), and a pressing sleeve (31) is sleeved on the spline shaft (34) above the stirring seat (24), and the upper end of the uppermost pressing sleeve (31) is connected to the upper end of the spline shaft (34) through a spring (33), and a plurality of third magnetic blocks (32) are evenly distributed on the circumference of the stirring seat (24), and the third magnetic blocks (32) can be arranged on the stirring seat (24) along the radial direction of the inner liner (15). Sliding; a rotating ring (20) is slidably arranged in the axial direction of the inner container (15), the rotating ring (20) is concentric with the inner container (15), a vertical electric push rod (9) is fixed on the cover body (11), the lower end of the electric push rod (9) is slidably connected with the rotating ring (20), a plurality of magnetic strips (25) are evenly distributed and slidably arranged on the circumference of the lower end of the rotating ring (20), the magnetic strips (25) can move in the radial direction of the rotating ring (20), and a guide is fixed on the inner wall of the inner container (15) on one side of the magnetic strip (25) A rod (28), one end of the guide rod (28) facing the center of the inner liner (15) is inclined downward, a third slide groove (29) is provided on the guide rod (28), the length direction of the third slide groove (29) is parallel to the length direction of the guide rod (28), a guide block is fixed on the magnetic strip (25), the guide block is slidably connected in the third slide groove (29), and the magnetic pole of the end of the magnetic strip (25) facing the center of the inner liner (15) is the same as the magnetic pole of the end of the third magnetic block (32) facing away from the center of the inner liner (15);A limit block (14) is provided in the inner container (15) below the magnetic strip (25), the limit block (14) comprising a vertical portion on the upper side and a straight portion on the lower side, a guide column (26) is fixed on the limit block (14), the axial direction of the guide column (26) is parallel to the radial direction of the inner container (15), the guide column (26) is slidably sealedly connected to the inner container (15), a vertical groove (30) is provided on the vertical portion of the limit block (14), a protrusion is fixed on the magnetic strip (25), and the protrusion is slidably engaged with the vertical groove (30) and the magnetic strip (25) is fixed with a protrusion. An arc groove (41) is provided in the groove (30) at the connection position between the vertical part and the flat part of the limit block (14); two symmetrically arranged support plates (40) are fixed on the free end of the flat part of the limit block (14); one end of the support plate (40) facing the center of the inner liner (15) is inclined upward; a straight groove (35) is provided on the support plate (40); the length direction of the straight groove (35) is parallel to the length direction of the support plate (40); an arc-shaped inner groove is provided at the connection position between the flat part and the vertical part of the limit block (14) (42), the inner groove (42) is connected to the arc groove (41), the inner groove (42) is connected to the straight groove (35), the inner groove (42) and the straight groove (35) constitute a guide groove, the lower end of the magnetic strip (25) is rotatably connected with a magnetic chain; the magnetic chain includes a plurality of first magnetic blocks (23), the ends of two adjacent first magnetic blocks (23) facing away from the inner wall of the inner liner (15) are rotatably connected by a pin shaft, the first magnetic block (23) adjacent to the magnetic strip (25) is rotatably connected to the lower end of the magnetic strip (25) by a pin shaft, and the lower end of the magnetic chain is connected A second magnetic block (39) is provided, and the second magnetic block (39) is rotatably connected to the first magnetic block (23) adjacent thereto via a pin shaft, and the pin shaft of the magnetic chain portion away from the magnetic strip (25) is slidably engaged in the guide groove, and a plurality of magnetic plates (37) are evenly distributed and fixed on the circumference of the lower end of the stirring seat (24) at the bottom, and the magnetic pole at the upper end of the second magnetic block (39) is the same as the magnetic pole at the lower end of the magnetic plate (37), and the magnetic pole at the upper end of the first magnetic block (23) entering between the two support plates (40) is the same as the magnetic pole at the lower end of the magnetic plate (37). ; 2. The ammonium perchlorate concentration system according to claim 1, characterized in that: The stirring seat (24) is provided with a flat groove (36) corresponding to the third magnetic block (32), the length direction of the flat groove (36) is parallel to the radial direction of the inner container (15), and the lower end of the third magnetic block (32) is slidably engaged in the flat groove (36) below it.

3. The ammonium perchlorate concentration system according to claim 1, characterized in that: The driving assembly comprises a shell (2) fixed on the outside of the cylinder (1), the shell (2) being connected to the heat preservation chamber (12), a gear (17) being rotatably arranged in the shell (2), a gear ring (16) being fixed on the outside of the inner container (15), the gear ring (16) being meshed with the gear (17), the axle of the gear (17) extending to the outside of the shell (2), a first pulley (3) being fixed on the axle of the gear (17) on the outside of the shell (2), and a gear (17) being fixed on the upper end of the cover body (11). A bracket (6) is provided, a motor (7) is fixed on the bracket (6), a second pulley (5) is coaxially fixed on the output shaft of the motor (7), the second pulley (5) is connected to the first pulley (3) through a belt (4), the output shaft of the motor (7) is concentric with the spline shaft (34), the output shaft of the motor (7) passes through the cover body (11), the output shaft of the motor (7) is rotatably connected to the cover body (11), and the output shaft of the motor (7) is coaxially and fixedly connected to the spline shaft (34).

4. The ammonium perchlorate concentration system according to claim 1, characterized in that: A slider (18) is fixed at the lower end of the electric push rod (9), and a first annular sliding groove (19) is coaxially provided at the upper end of the rotating ring (20), and the slider (18) is slidably engaged in the first sliding groove (19).

5. The ammonium perchlorate concentration system according to claim 1, characterized in that: An upper control valve (10) is installed on the inlet pipe (8).

6. The ammonium perchlorate concentration system according to claim 1, characterized in that: A second slide groove (27) is provided at the lower end of the rotating ring (20) above the magnetic strip (25), and the length direction of the second slide groove (27) is parallel to the radial direction of the rotating ring (20). An upper block is fixed at the upper end of the magnetic strip (25), and the upper block is slidably engaged in the second slide groove (27).

7. A method for using the ammonium perchlorate concentration system according to claim 1, characterized in that: The following steps are involved: S1, closing the outlet pipe (21), opening the inlet pipe (8), and adding the ammonium perchlorate liquid material into the inner container (15) through the inlet pipe (8); S2, start the heating plate (13) to heat the ammonium perchlorate liquid material in the inner container (15), and at the same time, use the driving component to rotate the stirring component and the inner container (15); S3, after the ammonium perchlorate liquid material is concentrated, close the driving component, open the outlet pipe (21) to discharge the concentrated ammonium perchlorate liquid material.

Citation Information

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