Preparation method of abalone calcium tablets using abalone shells as raw materials

Abstract

The invention discloses a method for preparing abalone calcium tablets by taking abalone shells as raw materials, which comprises the following steps: firstly, taking a proper amount of cleaned fresh abalone shells, putting the abalone shells into a 15% acetic acid solution at 60 DEG C, carrying out ultrasonic treatment for 30 minutes to remove impurities in a seaweed layer, crushing the treated abalone shells by using a high-speed crusher, and sieving by using a 200-mesh sieve to obtain abalone shell powder; 137.8 g of abalone shell powder, 0.1900 g of magnesium stearate, 78.45 g of microcrystalline cellulose, 22.38 g of polyvinylpyrrolidone K302, 11.18 g of sodium carboxymethyl starch and a proper amount of purified water are added into every 250 g of calcium tablets, and the mixture is pressed into the abalone calcium tablets through a tablet press. Wherein the mass ratio of the sodium carboxymethyl starch to the microcrystalline cellulose to the distilled water is 1: 4.5: 100; when the mass ratio of the auxiliary materials microcrystalline cellulose to polyvinylpyrrolidone to sodium carboxymethyl starch is 7: 2: 1, the abalone shell calcium tablet obtained by pressing by using a tablet press is compact in structure, not easy to loosen, relatively good in taste and relatively easy to absorb by a human body, and the calcium content in 1g of the abalone shell calcium tablet is 200mg.

Description

Technical Field

[0001] The invention relates to the technical field of agricultural product processing, in particular to a method for preparing an abalone calcium tablet using abalone shell as a raw material. Background Art

[0002] Abalone belongs to the genus Haliotis of the phylum Mollusca. my country is the world's largest abalone producer, with an annual output of more than 100,000 tons and nearly 20,000 tons of abalone shells. Abalone shells, also known as Jiukongshijueming and Haishijueming, are commonly used Chinese medicinal materials with the effects of clearing away heat, improving eyesight, calming the liver and suppressing yang. In traditional Chinese medicine, they are often used to treat headaches, dizziness, red eyes, blurred vision, amblyopia and nymphoma. Abalone shell nacre powder is homologous to pearl powder and contains the same ingredients as pearls, mainly calcium, sugars, multiple amino acids and a small amount of trace elements. The keratin contained in it has multiple amino acid components that the human body cannot produce. Nacre powder has multiple functions such as facial freckle removal, treatment of skin allergies, acne removal, and skin moisturizing. At present, there is little research and processing on the comprehensive utilization of abalone shells at home and abroad, and they are often treated as waste or low-value feed, which greatly reduces the use value of abalone shells. Therefore, the effective use of abalone shells can not only greatly reduce the waste of resources, open up the market for abalone deep-processing products, increase economic benefits, but also solve the problem of environmental pollution.

[0003] At present, there is no literature report on processing calcium tablets using abalone shell as raw material in China. Summary of the invention

[0004] 1. Technical issues to be resolved

[0005] In view of the shortcomings of the prior art, the present invention provides a method for preparing abalone calcium tablets using abalone shells as raw materials, which has the advantages of low cost and nutritional economy, and solves the problem that the abalone shell cannot be effectively synthesized.

[0006] (II) Technical solution

[0007] To achieve the purpose mentioned in the above background technology, the present invention provides the following technical scheme: a method for preparing abalone calcium tablets using abalone shell as raw material, comprising the following steps:

[0008] S1, take an appropriate amount of cleaned abalone shell, place it in acetic acid solution and ultrasonically remove impurities in the seaweed layer;

[0009] S2, the abalone shell processed by S1 is crushed and sieved to obtain abalone shell powder;

[0010] S3, adding abalone shell powder, auxiliary materials and water in different proportions, and pressing into calcium tablets.

[0011] Preferably, in step S1, the concentration of the acetic acid solution is 5% to 30%, the treatment temperature is 20° C. to 60° C., and the treatment time is 20 minutes to 50 minutes.

[0012] Preferably, in step S2, the mesh number of the crushed abalone shell is 200 meshes.

[0013] Preferably, in S3, the auxiliary materials include magnesium stearate, microcrystalline cellulose, polyvinyl pyrrolidone K30, and sodium carboxymethyl starch.

[0014] Preferably, in step S3, the tabletting step is as follows: adding 137.8 g abalone shell powder, 0.1900 g magnesium stearate, 78.45 g microcrystalline cellulose, 22.38 g polyvinyl pyrrolidone K30, 11.18 g sodium carboxymethyl starch, and an appropriate amount of purified water to every 250 g calcium tablet, and pressing the tablets into abalone calcium tablets using a tablet press.

[0015] Preferably, in step S3, when the mass ratio of sodium carboxymethyl starch, microcrystalline cellulose and distilled water is 1:4.5:100 for coating, the mass ratio of auxiliary materials microcrystalline cellulose, polyvinyl pyrrolidone and sodium carboxymethyl starch is 7:2:1.

[0016] (III) Beneficial effects

[0017] Compared with the prior art, the present invention provides a method for preparing abalone calcium tablets using abalone shell as raw material, which has the following beneficial effects:

[0018] 1. The method for preparing the abalone calcium tablet using the abalone shell as raw material is simple and easy to operate, economical and applicable, and can greatly improve the added value of the abalone shell by using the abalone shell as raw material to prepare the calcium tablet.

[0019] 2. A method for preparing abalone calcium tablets using abalone shells as raw materials. 1 g / tablet of calcium tablets prepared by the method for preparing abalone calcium tablets using abalone shells as raw materials not only contains 200 mg of calcium, but also contains 230 micrograms of iron, 72 micrograms of zinc, and 176 micrograms of copper, which are essential trace elements for the human body. DETAILED DESCRIPTION

[0020] The following will be combined with the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0021] Embodiment 1:

[0022] S1. Take an appropriate amount of cleaned abalone shells, place them in a 5% acetic acid solution at 20°C and ultrasonicate for 20 minutes to remove impurities from the seaweed layer;

[0023] S2, adopt high-speed pulverizer to carry out dry or wet grinding of the above-mentioned treated abalone shell, and obtain abalone shell powder after passing through 200 mesh sieve (if wet grinding, need to pass through 200 mesh sieve after drying);

[0024] S3, according to every 250g calcium tablet, add abalone shell powder 137.8g, magnesium stearate 0.1900g, microcrystalline cellulose 78.45g, polyvinyl pyrrolidone K3022.38g, sodium carboxymethyl starch 11.18g, and an appropriate amount of purified water, and press it into abalone calcium tablets with a tablet press. The mass ratio of sodium carboxymethyl starch, microcrystalline cellulose and distilled water is 1:4.5:100, which is a good coating ratio, and is pressed into abalone calcium tablets with a tablet press; the ratio of auxiliary materials microcrystalline cellulose, polyvinyl pyrrolidone and sodium carboxymethyl starch mass is 7:2:1.

[0025] Embodiment 2:

[0026] S1. Take an appropriate amount of cleaned abalone shells, place them in a 30% acetic acid solution at 60°C and ultrasonicate for 50 min to remove impurities from the seaweed layer;

[0027] S2, adopt high-speed pulverizer to carry out dry or wet grinding of the above-mentioned treated abalone shell, and obtain abalone shell powder after passing through 200 mesh sieve (if wet grinding, need to pass through 200 mesh sieve after drying);

[0028] S3, according to every 250g calcium tablet, add abalone shell powder 137.8g, magnesium stearate 0.1900g, microcrystalline cellulose 78.45g, polyvinyl pyrrolidone K3022.38g, sodium carboxymethyl starch 11.18g, and an appropriate amount of purified water, and press it into abalone calcium tablets with a tablet press. The mass ratio of sodium carboxymethyl starch, microcrystalline cellulose and distilled water is 1:4.5:100, which is a good coating ratio, and is pressed into abalone calcium tablets with a tablet press; the ratio of auxiliary materials microcrystalline cellulose, polyvinyl pyrrolidone and sodium carboxymethyl starch mass is 7:2:1.

[0029] Embodiment three:

[0030] S1. Take an appropriate amount of cleaned abalone shells, place them in a 20% acetic acid solution at 30°C and ultrasonicate for 30 minutes to remove impurities from the seaweed layer;

[0031] S2, adopt high-speed pulverizer to carry out dry or wet grinding of the above-mentioned treated abalone shell, and obtain abalone shell powder after passing through 200 mesh sieve (if wet grinding, need to pass through 200 mesh sieve after drying);

[0032] S3, according to every 250g calcium tablet, add abalone shell powder 137.8g, magnesium stearate 0.1900g, microcrystalline cellulose 78.45g, polyvinyl pyrrolidone K3022.38g, sodium carboxymethyl starch 11.18g, and an appropriate amount of purified water, and press it into abalone calcium tablets with a tablet press. The mass ratio of sodium carboxymethyl starch, microcrystalline cellulose and distilled water is 1:4.5:100, which is a good coating ratio, and is pressed into abalone calcium tablets with a tablet press; the ratio of auxiliary materials microcrystalline cellulose, polyvinyl pyrrolidone and sodium carboxymethyl starch mass is 7:2:1.

[0033] Best case:

[0034] S1. Take an appropriate amount of cleaned abalone shells, place them in a 15% acetic acid solution at 60°C and ultrasonicate for 30 minutes to remove impurities from the seaweed layer;

[0035] S2, adopt high-speed pulverizer to carry out dry or wet grinding of the above-mentioned treated abalone shell, and obtain abalone shell powder after passing through 200 mesh sieve (if wet grinding, need to pass through 200 mesh sieve after drying);

[0036] S3, according to every 250g calcium tablet, add abalone shell powder 137.8g, magnesium stearate 0.1900g, microcrystalline cellulose 78.45g, polyvinyl pyrrolidone K3022.38g, sodium carboxymethyl starch 11.18g, and an appropriate amount of purified water, and press it into abalone calcium tablets with a tablet press. The mass ratio of sodium carboxymethyl starch, microcrystalline cellulose and distilled water is 1:4.5:100, which is a good coating ratio, and is pressed into abalone calcium tablets with a tablet press; the ratio of auxiliary materials microcrystalline cellulose, polyvinyl pyrrolidone and sodium carboxymethyl starch mass is 7:2:1.

[0037] The beneficial effects of the present invention are:

[0038] 1. The method for preparing the abalone calcium tablet using the abalone shell as raw material is simple and easy to operate, economical and applicable, and can greatly improve the added value of the abalone shell by using the abalone shell as raw material to prepare the calcium tablet.

[0039] 2. A method for preparing abalone calcium tablets using abalone shells as raw materials. 1 g / tablet of calcium tablets prepared by the method for preparing abalone calcium tablets using abalone shells as raw materials not only contains 200 mg of calcium, but also contains 230 micrograms of iron, 72 micrograms of zinc, and 176 micrograms of copper, which are essential trace elements for the human body.

[0040] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A method for preparing abalone calcium tablets using abalone shell as raw material, characterized in that, The following steps are involved: S1, take an appropriate amount of cleaned abalone shell, place it in acetic acid solution and ultrasonically remove impurities in the seaweed layer; S2, the abalone shell processed by S1 is crushed and sieved to obtain abalone shell powder; S3, adding abalone shell powder, auxiliary materials and water in different proportions, and pressing into calcium tablets.

2. A method for preparing an abalone calcium tablet using abalone shell as raw material according to claim 1, characterized in that: In step S1, the concentration of the acetic acid solution is 5% to 30%, the treatment temperature is 20° C. to 60° C., and the treatment time is 20 minutes to 50 minutes.

3. A method for preparing an abalone calcium tablet using abalone shell as raw material according to claim 1, characterized in that, In the step S2, the abalone shells are sieved to a mesh size of 200 after being crushed.

4. A method for preparing an abalone calcium tablet using abalone shell as raw material according to claim 1, characterized in that: In S3, the auxiliary materials include magnesium stearate, microcrystalline cellulose, polyvinyl pyrrolidone K30, and sodium carboxymethyl starch.

5. A method for preparing an abalone calcium tablet using abalone shell as raw material according to claim 1, characterized in that: In step S3, the tableting step is as follows: adding 137.8 g abalone shell powder, 0.1900 g magnesium stearate, 78.45 g microcrystalline cellulose, 22.38 g polyvinyl pyrrolidone K30, 11.18 g sodium carboxymethyl starch, and an appropriate amount of purified water to every 250 g calcium tablet, and pressing the tablets into abalone calcium tablets using a tablet press.

6. A method for preparing an abalone calcium tablet using abalone shell as raw material according to claim 1, characterized in that: In the step S3, when the mass ratio of sodium carboxymethyl starch, microcrystalline cellulose and distilled water is 1:4.5:100 for coating, the mass ratio of auxiliary materials microcrystalline cellulose, polyvinyl pyrrolidone and sodium carboxymethyl starch is 7:2:1.