High-efficiency washing and caring composition capable of being quickly biodegraded and application of high-efficiency washing and caring composition

Abstract

The invention discloses an efficient washing and caring composition capable of being rapidly biodegraded and application of the efficient washing and caring composition. The washing and caring composition is mainly prepared from the following raw materials: lauroyl alanine, a soapberry peel extract and a camellia seed extract. The mode of combined fermentation of the lactobacillus and the saccharomycetes is adopted, crude fat, starch, crude protein and tea seed polysaccharide contained in the camellia seeds in the raw materials are ingeniously utilized, and nutritional conditions are provided for growth of the lactobacillus and the saccharomycetes. The color, the quality and the purity of active matters contained in the prepared washing and caring composition are better than those of the traditional extraction method. Tests prove that the cleaning composition is excellent in cleaning performance, biodegradable and beneficial to environmental protection.

Description

Technical Field

[0001] The invention relates to the field of cosmetics, and in particular to a fast biodegradable and efficient cleaning composition and application thereof. Background Art

[0002] Surfactants are widely used in industrial and agricultural production as wetting agents, emulsifiers, dispersants, bubbling agents, etc., but when the concentration in water exceeds a certain limit, it may have a significant impact on the environment, including poisoning aquatic organisms and fish, and even leading to eutrophication of water bodies. For example, when the concentration of sodium alkylbenzene sulfonate (ABS) in water reaches 10 mg / L, fish can hardly survive, and at 45 mg / L, rice growth is seriously harmed. For example, cationic surfactants have certain bactericidal capabilities and may destroy the community of microorganisms in water bodies at high concentrations. In addition, surfactants can also promote the emulsification and dispersion of insoluble organic matter such as petroleum and polychlorinated biphenyls in water bodies, increasing the difficulty of wastewater treatment. These characteristics require the use of surfactants in the environment to carefully consider their impact on the ecosystem.

[0003] The degradation process of surfactants is affected by many factors, including microorganisms, light sources, concentration, temperature, oxidants, pH value, etc. Although the complete degradation of surfactants will eventually produce inorganic substances such as carbon dioxide, ammonia, and water, it may have an impact on the environment during its degradation process. Studies have shown that the primary degradation of surfactants is the disappearance of their parent structure and the change of their properties; secondary degradation is that the degradation products no longer cause environmental pollution; and final degradation is the complete conversion of the substrate (surfactant) into inorganic substances.

[0004] In order to reduce the environmental impact of surfactants, it is essential to develop sustainable alternatives. This includes the development and use of renewable energy, the use of more environmentally friendly manufacturing processes and clean technologies, and the development of more environmentally friendly surfactants, such as biodegradable surfactants, to reduce their negative impact on the environment. Summary of the invention

[0005] The technical problem to be solved by the present invention is to provide a surfactant solution which is rapidly biodegradable and has excellent cleaning performance.

[0006] The specific technical solutions of the present invention are as follows:

[0007] A cleaning composition is characterized by being mainly composed of the following raw materials: lauroyl alanine, SAPINDUS MUKOROSSI peel extract, and CAMELLIA JAPONICA seed extract.

[0008] The lauroyl alanine used in the cleaning composition of the present invention is an amino acid surfactant with good cleaning power and mild to the human body. Suitable lauroyl alanine can be obtained from Aminiosurfact LA (from Suzhou Weimei Biotechnology Co., Ltd.).

[0009] The soapberry peel extract used in the cleaning composition of the present invention is extracted from the peel of the mature fruit of the soapberry. The peel of the soapberry contains 10%-27% triterpenoid saponins, which have the effects of clearing away heat and resolving phlegm, relieving pain and eliminating accumulation, and is also a natural non-ionic surfactant with excellent foaming and cleaning capabilities.

[0010] The camellia japonica seed extract used in the cleaning composition of the present invention is extracted from the mature fruit of camellia. Camellia seeds are mainly composed of water, crude fat, starch, crude protein, tea seed polysaccharides, polyphenols, flavonoids, 12-17% tea saponin and crude fiber, and a small amount of tannin. Tea saponin is composed of seven ligands (C 30 H6O6), four glycosides and two organic acids, a pentacyclic triterpenoid tea saponin, is also a pure natural nonionic surfactant, with hydrophilic glycosides and hydrophobic ligands in the molecule. Therefore, it has multiple surface activities such as emulsification, dispersion, wetting, decontamination, foaming, and foam stabilization, especially with strong foaming ability, and the foam produced is stable and is not affected by water hardness. In addition, it also has significant expectorant, anti-inflammatory, antitussive and analgesic effects.

[0011] The present invention also provides a method for preparing the cleaning composition, which specifically comprises the following steps:

[0012] (1) drying and crushing soapberry peel and camellia seeds to obtain plant powder; adding water to adjust the pH to 4.5-5.5; adding cellulase and stirring at a temperature of 40-45 degrees for 1-2 hours; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material;

[0013] (2) inoculating lactobacillus and yeast into the sterilized material, first fermenting at 28 degrees for 12-24 hours, then heating to 37 degrees for 24-48 hours to obtain a fermented material;

[0014] (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add glycerol aqueous solution to the extract, stir thoroughly to dissolve, then centrifuge to obtain the supernatant, then add lauroyl alanine, adjust the pH to neutral, stir to dissolve, and obtain the extract.

[0015] The present invention adopts the combined fermentation mode of lactobacillus and yeast. Lactobacillus can secrete a variety of enzymes to help yeast grow in plant culture medium, and the rich nutrition in the decomposition metabolites of yeast can be used by lactobacillus, which is helpful for the reproduction of lactobacillus under poor nutrition conditions.

[0016] The crude fat, starch, crude protein and tea seed polysaccharide contained in the camellia seeds used in the present invention provide nutritional conditions for the growth of lactobacillus and yeast.

[0017] In some embodiments, the amount of soapberry peel added in step (1) is 10-30 parts by weight, and the amount of camellia seeds added is 5-15 parts by weight.

[0018] In some embodiments, the amount of water added in step (1) is 3-5 times the weight of the plant powder.

[0019] In some embodiments, the amount of cellulase used in step (1) is 0.1-0.5% by weight of the plant powder.

[0020] In some embodiments, the inoculation amount of the lactobacillus in step (2) is 0.5% of the weight of the sterilized material; and the inoculation amount of the yeast is 1% of the weight of the sterilized material.

[0021] In some of the embodiments, the mass ratio of glycerol to water in the glycerol aqueous solution in step (3) is 1:1-2, and the added amount of the glycerol aqueous solution is 5-10 times that of the extract.

[0022] In some embodiments, the amount of lauroyl alanine added in step (3) is 5-10% by weight of the supernatant.

[0023] Another object of the present invention is to apply the above cleaning composition to cosmetics to produce a cleaning product that is rapidly biodegradable and has excellent cleaning performance.

[0024] To achieve the second purpose of the present invention, the present invention adopts the following technical scheme: the above cleaning and care composition is used to prepare cosmetics, characterized in that the cosmetics contain the above cleaning and care composition, and the usage is 1-50%.

[0025] The dosage form of the cosmetics of the present invention is not particularly limited, and may be an aqueous solution, shampoo, shower gel, dishwashing detergent, etc.

[0026] The embodiment of the present invention also provides an anti-hair loss foaming essence water, comprising the following components in percentage by mass: 20-30% of the above-mentioned washing and care composition, 1-5% of arginine, 5-10% of glycerol, 5-10% of 1,3-propylene glycol, 0.1-1% of BIOTAORIENTALIS leaf extract, 0.1-1% of ginseng root extract, 0.1-1% of Ligustrum lucidum root extract, 1-5% of cocamidopropyl betaine, 0.1-2% of capryloyl glycine, and the remainder of water.

[0027] The technical solution provided by the embodiment of the present invention has the following beneficial effects:

[0028] (1) The embodiments of the present invention provide a cleaning composition which has excellent cleaning performance, is biodegradable, and is beneficial to environmental protection.

[0029] (2) The present invention provides a method for preparing the cleaning composition, which adopts a method of combined fermentation of lactobacillus and yeast, and cleverly utilizes the crude fat, starch, crude protein, and tea seed polysaccharide contained in the camellia seeds in the raw materials to provide nutritional conditions for the growth of lactobacillus and yeast. Tests have shown that the color, quality, and purity of the active ingredients contained in the cleaning composition are better than those of the traditional extraction method.

[0030] (3) The embodiment of the present invention also provides an anti-hair loss bubble essence water, which can moisturize and nourish the hair roots while cleaning the hair, thereby achieving an anti-hair loss effect of washing and caring in one. BRIEF DESCRIPTION OF THE DRAWINGS

[0031] In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for describing the embodiments or the prior art are briefly introduced below.

[0032] Figure 1 Test 2: Foaming ability test;

[0033] Figure 2 Shows the self-assessment results of volunteers' improvement in hair loss prevention in test 4;

[0034] Figure 3 The following table shows the results of volunteers' self-evaluation of usage experience in test 4. DETAILED DESCRIPTION

[0035] The following describes the embodiments of the present invention through specific examples, and those skilled in the art can easily understand other advantages and effects of the present invention from the contents disclosed in this specification. The present invention can also be implemented or applied through other different specific embodiments, and the details in this specification can also be modified or changed in various ways based on different viewpoints and applications without departing from the spirit of the present invention.

[0036] Before further describing the specific embodiments of the present invention, it should be understood that the scope of protection of the present invention is not limited to the specific embodiments described below; it should also be understood that the terms used in the examples of the present invention are for describing specific embodiments rather than for limiting the scope of protection of the present invention.

[0037] When the embodiment gives a numerical range, it should be understood that, unless otherwise specified in the present invention, the two endpoints of each numerical range and any numerical value between the two endpoints can be selected. Unless otherwise defined, all technical and scientific terms used herein have the same meanings as those of ordinary skill in the art to which the present invention belongs.

[0038] It is worth noting that the raw materials used in the present invention are all common commercially available products, so their sources are not specifically limited.

[0039] Example 1

[0040] The preparation of a cleaning composition comprises the following steps:

[0041] (1) Weighing 10 parts of soapberry peel and 15 parts of camellia seeds by weight, drying and crushing to obtain plant powder; adding water 3 times the weight of the plant powder to adjust the pH to 5.5; adding 0.1% of cellulase by weight of the plant powder, stirring at a temperature of 45 degrees for 1 hour; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material;

[0042] (2) inoculating lactobacillus and yeast into the sterilized material, wherein the inoculation amount of lactobacillus is 0.5% of the weight of the sterilized material; the inoculation amount of yeast is 1% of the weight of the sterilized material; first fermenting at 28 degrees for 24 hours, then heating to 37 degrees for 24 hours to obtain a fermented material;

[0043] (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add a glycerol aqueous solution to the extract, wherein the mass ratio of glycerol to water in the glycerol aqueous solution is 1:2, and the amount of the glycerol aqueous solution added is 5 times that of the extract; stir thoroughly to dissolve, then centrifuge to take the supernatant, and then add lauroyl alanine in an amount of 10% of the weight of the supernatant, adjust the pH to neutral, stir to dissolve, and obtain the extract.

[0044] Example 2

[0045] The preparation of a cleaning composition comprises the following steps:

[0046] (1) Weighing 30 parts of soapberry peel and 5 parts of camellia seeds by weight, drying and crushing to obtain plant powder; adding 5 times the weight of the plant powder of water, adjusting the pH to 4.5; adding 0.5% of cellulase by weight of the plant powder, stirring at a temperature of 40 degrees for 2 hours; high temperature inactivating enzymes and sterilizing to obtain sterilized materials;

[0047] (2) inoculating lactobacillus and yeast into the sterilized material, wherein the inoculation amount of lactobacillus is 0.5% of the weight of the sterilized material; the inoculation amount of yeast is 1% of the weight of the sterilized material; first fermenting at 28 degrees for 12 hours, then raising the temperature to 37 degrees for fermentation for 48 hours to obtain a fermented material;

[0048] (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add a glycerol aqueous solution to the extract, wherein the mass ratio of glycerol to water in the glycerol aqueous solution is 1:1, and the amount of the glycerol aqueous solution added is 10 times that of the extract; stir thoroughly to dissolve, then centrifuge to take the supernatant, then add lauroyl alanine in an amount of 5% of the weight of the supernatant, adjust the pH to neutral, stir to dissolve, and obtain the extract.

[0049] Example 3

[0050] The preparation of a cleaning composition comprises the following steps:

[0051] (1) Weighing 20 parts of soapberry peel and 10 parts of camellia seeds by weight, drying and crushing to obtain plant powder; adding water 4 times the weight of the plant powder to adjust the pH to 5.0; adding 0.3% of cellulase by weight of the plant powder, stirring at a temperature of 43 degrees for 1.5 hours; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material;

[0052] (2) inoculating lactobacillus and yeast into the sterilized material, wherein the inoculation amount of lactobacillus is 0.5% of the weight of the sterilized material; the inoculation amount of yeast is 1% of the weight of the sterilized material; first fermenting at 28 degrees for 16 hours, then raising the temperature to 37 degrees for fermentation for 36 hours to obtain a fermented material;

[0053] (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add a glycerol aqueous solution to the extract, wherein the mass ratio of glycerol to water in the glycerol aqueous solution is 1:1.5, and the amount of the glycerol aqueous solution added is 8 times that of the extract; stir thoroughly to dissolve, then centrifuge to take the supernatant, then add lauroyl alanine in an amount of 8% of the weight of the supernatant, adjust the pH to neutral, stir to dissolve, and obtain the extract.

[0054] Comparative Example 1

[0055] In this comparative example, the cleaning composition was prepared by alcohol extraction.

[0056] The preparation of a cleaning composition comprises the following steps:

[0057] (1) Weighing 20 parts of soapberry peel and 10 parts of camellia seeds by weight, drying and crushing to obtain plant powder; adding water 4 times the weight of the plant powder to adjust the pH to 5.0; adding 0.3% of cellulase by weight of the plant powder, stirring at a temperature of 43 degrees for 1.5 hours; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material;

[0058] (2) Add 30 parts by weight of 1,3-propylene glycol to the sterilized material, heat to 65° C., and stir for 4 hours; then centrifuge to obtain the supernatant, and then add lauroyl alanine in an amount of 8% by weight of the supernatant, adjust the pH to neutral, and stir to dissolve.

[0059] Comparative Example 2

[0060] In this comparative example, the cleaning composition was prepared by water extraction.

[0061] The preparation of a cleaning composition comprises the following steps:

[0062] (1) Weighing 20 parts of soapberry peel and 10 parts of camellia seeds by weight, drying and crushing to obtain plant powder; adding water 4 times the weight of the plant powder to adjust the pH to 5.0; adding 0.3% of cellulase by weight of the plant powder, stirring at a temperature of 43 degrees for 1.5 hours; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material;

[0063] (2) Heat the sterilized material to boiling and keep it at a slight boil for 2-3 hours, separate the decoction, decoct the residue again according to the method, and mix the two decoctions; then centrifuge to obtain the supernatant, and then add lauroyl alanine in an amount of 8% by weight of the supernatant, adjust the pH to neutral, and stir to dissolve.

[0064] Comparative Example 3

[0065] The preparation of a cleaning composition comprises the following steps:

[0066] (1) Weighing 30 parts of soapberry peel by weight, drying, and crushing to obtain plant powder; adding water 4 times the weight of the plant powder to adjust the pH to 5.0; adding 0.3% of cellulase by weight of the plant powder, stirring at a temperature of 43 degrees for 1.5 hours; high temperature inactivating the enzyme and sterilizing to obtain a sterilized material;

[0067] (2) inoculating lactobacillus and yeast into the sterilized material, wherein the inoculation amount of lactobacillus is 0.5% of the weight of the sterilized material; the inoculation amount of yeast is 1% of the weight of the sterilized material; first fermenting at 28 degrees for 16 hours, then raising the temperature to 37 degrees for fermentation for 36 hours to obtain a fermented material;

[0068] (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add a glycerol aqueous solution to the extract, wherein the mass ratio of glycerol to water in the glycerol aqueous solution is 1:1.5, and the amount of the glycerol aqueous solution added is 8 times that of the extract; stir thoroughly to dissolve, then centrifuge to take the supernatant, then add lauroyl alanine in an amount of 8% of the weight of the supernatant, adjust the pH to neutral, stir to dissolve, and obtain the extract.

[0069] Comparative Example 4

[0070] The preparation of a cleaning composition comprises the following steps:

[0071] (1) Weighing 30 parts of camellia seeds by weight, drying them, and crushing them to obtain plant powder; adding water 4 times the weight of the plant powder to adjust the pH to 5.0; adding 0.3% of cellulase by weight of the plant powder, stirring at a temperature of 43 degrees for 1.5 hours; inactivating the enzyme and sterilizing them at high temperature to obtain a sterilized material;

[0072] (2) inoculating lactobacillus and yeast into the sterilized material, wherein the inoculation amount of lactobacillus is 0.5% of the weight of the sterilized material; the inoculation amount of yeast is 1% of the weight of the sterilized material; first fermenting at 28 degrees for 16 hours, then raising the temperature to 37 degrees for fermentation for 36 hours to obtain a fermented material;

[0073] (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add a glycerol aqueous solution to the extract, wherein the mass ratio of glycerol to water in the glycerol aqueous solution is 1:1.5, and the amount of the glycerol aqueous solution added is 8 times that of the extract; stir thoroughly to dissolve, then centrifuge to take the supernatant, then add lauroyl alanine in an amount of 8% of the weight of the supernatant, adjust the pH to neutral, stir to dissolve, and obtain the extract.

[0074] Comparative Example 5

[0075] The preparation of a cleaning composition comprises the following steps:

[0076] (1) Weighing 20 parts of soapberry peel and 10 parts of camellia seeds by weight, drying and crushing to obtain plant powder; adding water 4 times the weight of the plant powder to adjust the pH to 5.0; adding 0.3% of cellulase by weight of the plant powder, stirring at a temperature of 43 degrees for 1.5 hours; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material;

[0077] (2) inoculating lactobacillus and yeast into the sterilized material, wherein the inoculation amount of lactobacillus is 0.5% of the weight of the sterilized material; the inoculation amount of yeast is 1% of the weight of the sterilized material; first fermenting at 28 degrees for 16 hours, then raising the temperature to 37 degrees for fermentation for 36 hours to obtain a fermented material;

[0078] (3) Centrifuging the fermented material and taking the supernatant; mixing the supernatant and n-butanol evenly and taking the n-butanol layer solution; then rotary evaporating to obtain an extract; adding a glycerol aqueous solution to the extract, wherein the mass ratio of glycerol to water in the glycerol aqueous solution is 1:1.5, and the amount of the glycerol aqueous solution added is 8 times that of the extract; stirring thoroughly to dissolve, and then centrifuging to obtain the supernatant.

[0079] Comparative Example 6

[0080] The preparation of a cleaning composition comprises the following steps:

[0081] (1) Weighing 20 parts of soapberry peel and 10 parts of camellia seeds by weight, drying and crushing to obtain plant powder; adding water 4 times the weight of the plant powder to adjust the pH to 5.0; adding 0.3% of cellulase by weight of the plant powder, stirring at a temperature of 43 degrees for 1.5 hours; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material;

[0082] (2) inoculating lactobacillus into the sterilized material, wherein the inoculation amount of lactobacillus is 0.5% of the weight of the sterilized material; first fermenting at 28 degrees for 16 hours, then raising the temperature to 37 degrees for 36 hours to obtain a fermented material;

[0083] (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add a glycerol aqueous solution to the extract, wherein the mass ratio of glycerol to water in the glycerol aqueous solution is 1:1.5, and the amount of the glycerol aqueous solution added is 8 times that of the extract; stir thoroughly to dissolve, then centrifuge to take the supernatant, then add lauroyl alanine in an amount of 8% of the weight of the supernatant, adjust the pH to neutral, stir to dissolve, and obtain the extract.

[0084] Comparative Example 7

[0085] The preparation of a cleaning composition comprises the following steps:

[0086] (1) Weighing 20 parts of soapberry peel and 10 parts of camellia seeds by weight, drying and crushing to obtain plant powder; adding water 4 times the weight of the plant powder to adjust the pH to 5.0; adding 0.3% of cellulase by weight of the plant powder, stirring at a temperature of 43 degrees for 1.5 hours; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material;

[0087] (2) inoculating yeast into the sterilized material, wherein the inoculation amount of the yeast is 1% of the weight of the sterilized material; first fermenting at 28 degrees for 16 hours, then raising the temperature to 37 degrees for 36 hours to obtain a fermented material;

[0088] (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add a glycerol aqueous solution to the extract, wherein the mass ratio of glycerol to water in the glycerol aqueous solution is 1:1.5, and the amount of the glycerol aqueous solution added is 8 times that of the extract; stir thoroughly to dissolve, then centrifuge to take the supernatant, then add lauroyl alanine in an amount of 8% of the weight of the supernatant, adjust the pH to neutral, stir to dissolve, and obtain the extract.

[0089] Test Trial 1:

[0090] The total saponin content test was used to evaluate the effects of conventional extraction process and biological fermentation process on the effective matter content. The total saponin content test method was specifically determined by referring to the literature "Xu Jinghui, et al. Extraction of total saponins and polysaccharides from ginseng and rose schisandra powder and study on their in vitro activity [J / OL]. Feed Research, 2024, (14): 1-6." The test results are shown in Table 1.

[0091] Table 1 Appearance and total saponin content of each test group

[0092]

[0093] As can be seen from Table 1, the total saponin content extracted by the biological fermentation process in Examples 1-3 and Comparative Examples 3-7 of the present invention is higher than 14 mg / g, far exceeding the total saponin content in the cleaning composition prepared by the traditional extraction process. In Comparative Examples 6-7, which adopt single yeast or lactobacillus inoculation and fermentation, the total saponin content in the cleaning composition prepared is less than the total saponin content in the cleaning composition prepared by the combined fermentation of lactobacillus and yeast.

[0094] Test Trial 2:

[0095] The cleaning compositions prepared in Examples 1-3 were diluted with water to a 15% aqueous solution, and then a proper amount of the composition was taken and rubbed in the center of the palm for 15 circles to generate foam, and then the size and shape of the foam were compared to evaluate the foaming ability of the cleaning compositions prepared in the examples of the present invention.

[0096] Depend on Figure 1 It can be seen that the cleaning compositions prepared in Examples 1-3 of the present invention foam quickly and have rich and dense foam.

[0097] Test experiment 3:

[0098] The rapid biodegradability of the cleaning composition prepared in Example 3 of the present invention was evaluated by manometric respirometry test, using activated sludge as inoculum and sodium benzoate as reference, stirring continuously for 28 days at a temperature of 22±1°C in the dark. The oxygen consumed by the inoculum during biodegradation of the test sample was corrected by the oxygen consumption of the blank control group of the inoculum in a parallel test, and the biodegradation rate of the test sample was expressed as a percentage of ThOD. Specific reference: Chemical Testing Methods Editorial Committee of the Chemical Registration Center of the Ministry of Environmental Protection. Chemical Testing Methods Degradation and Accumulation Volume, 301F Manometric Respirometry Test [M]. Second Edition. Beijing: China Environment Press, 2013: 56-61.

[0099] Test results: In the control group, the biodegradation rate of the reference material on the 14th day was 73.1%, which was greater than 60%. The biodegradation rate of the toxicity control group on the 14th day was 81.7%, which was greater than 25%, indicating that the test sample had no toxicity or inhibitory effect on the inoculum. The 10-day observation period for the test sample started on the 2nd day and ended on the 12th day. The average biodegradation rate (in terms of ThOD NO3- The total weight of the cleaning composition is 87.9%, which is greater than 60%, reaching the passing level of rapid biodegradation. Therefore, under the test conditions, the cleaning composition prepared in the embodiment of the present invention has rapid biodegradability.

[0100] Example 4

[0101] An anti-hair loss foaming essence water comprises the following components in percentage by weight: 20% of the washing and conditioning composition prepared in Example 1, 5% of arginine, 5% of glycerol, 10% of 1,3-propylene glycol, 0.1% of BIOTA ORIENTALIS leaf extract, 1% of PANAX GINSENG root extract, 0.1% of LIGUSTICUM CHUANXIONG root extract, 1% of LIGUSTRUM LUCIDUM fruit extract, 1% of cocamidopropyl betaine, 2% of capryloyl glycine, and the balance of water.

[0102] Example 5

[0103] A hair loss prevention foaming essence water comprises the following components in percentage by weight: 30% of the washing and conditioning composition prepared in Example 2, 1% of arginine, 10% of glycerol, 5% of 1,3-propylene glycol, 1% of BIOTA ORIENTALIS leaf extract, 0.1% of ginseng root extract, 1% of LIGUSTICUM CHUANXIONG root extract, 0.1% of LIGUSTRUM LUCIDUM fruit extract, 5% of cocamidopropyl betaine, 0.1% of capryloyl glycine, and the balance of water.

[0104] Test Trial 4:

[0105] 60 volunteers with hair loss problems, regardless of gender, aged 35-55 years old, were recruited and randomly divided into 2 groups, 30 in each group, the first group tested the anti-hair loss bubble essence water prepared in Example 5, and the second group tested a commercially available brand of anti-hair loss and hair growth shampoo.

[0106] How to use: Soak your hair with warm water at 35-40℃. Take an appropriate amount of shampoo, rub it with your palms to make bubbles, then apply it to your hair and rub it gently for 3-5 minutes to make sure the shampoo covers your scalp evenly. Then rinse your hair and scalp with running warm water and dry your hair with a towel. Wash once every night for 8 weeks. Conduct a follow-up visit in the 8th week to collect the volunteers' self-evaluation results and calculate the average score of each group.

[0107] Volunteers' self-assessment criteria for improving their hair loss prevention: 0 points for no improvement in hair loss problem; 3 points for a certain improvement; 5 points for a significant improvement.

[0108] Volunteers' self-evaluation criteria: Volunteers rate the product on a scale of 1-5, with two dimensions for self-evaluation. The first dimension is cleaning power: whether the foam is dense during cleaning, whether it can be rinsed off quickly with water, and whether there is a feeling of incomplete cleaning; the second dimension is mildness: whether the scalp is irritated and causes discomfort during cleaning, and whether there are problems such as itching and redness after cleaning.

[0109] Depend on Figure 2 Volunteers' self-assessment results on hair loss prevention and improvement, Figure 3 The self-evaluation results of the volunteers show that the anti-hair loss effect and the feeling of use of the anti-hair loss bubble essence water prepared in the embodiment of the present invention are better than those of commercially available products, and an excellent technical effect has been achieved.

[0110] Finally, it should be noted that the above content is only used to illustrate the technical solution of the present invention, rather than to limit the scope of protection of the present invention. Any simple modification or equivalent substitution made by any technician familiar with the technical field within the technical scope disclosed by the present invention does not deviate from the essence and scope of the technical solution of the present invention.

Claims

1. A cleaning composition, characterized in that: It is mainly composed of the following raw materials: lauroyl alanine, soapberry (SAPINDUS MUKOROSSI) peel extract, camellia (CAMELLIA JAPONICA) seed extract.

2. The cleaning composition according to claim 1, characterized in that The preparation method thereof comprises the following steps: (1) drying and crushing soapberry peel and camellia seeds to obtain plant powder; adding water to adjust the pH to 4.5-5.5; adding cellulase and stirring at a temperature of 40-45 degrees for 1-2 hours; inactivating the enzyme and sterilizing at high temperature to obtain a sterilized material; (2) inoculating lactobacillus and yeast into the sterilized material, first fermenting at 28 degrees for 12-24 hours, then heating to 37 degrees for 24-48 hours to obtain a fermented material; (3) Centrifuge the fermented material and take the supernatant; mix the supernatant and n-butanol evenly and take the n-butanol layer solution; then rotary evaporate to obtain an extract; add glycerol aqueous solution to the extract, stir thoroughly to dissolve, then centrifuge to obtain the supernatant, then add lauroyl alanine, adjust the pH to neutral, stir to dissolve, and obtain the extract.

3. The cleaning composition according to claim 2, characterized in that In step (1), the added amount of soapberry peel is 10-30 parts by weight, and the added amount of camellia seed is 5-15 parts by weight.

4. The cleaning composition according to claim 2, characterized in that The amount of water added in step (1) is 3-5 times the weight of the plant powder.

5. The cleaning composition according to claim 2, characterized in that: The amount of the cellulase used in step (1) is 0.1-0.5% of the weight of the plant powder.

6. The cleaning composition according to claim 2, characterized in that: The inoculation amount of the lactobacillus in step (2) is 0.5% of the weight of the sterilized material; the inoculation amount of the yeast is 1% of the weight of the sterilized material.

7. The cleaning composition according to claim 2, characterized in that The mass ratio of glycerol to water in the glycerol aqueous solution in step (3) is 1:1-2, and the added amount of the glycerol aqueous solution is 5-10 times that of the extract.

8. The cleaning composition according to claim 2, characterized in that: The amount of lauroyl alanine added in step (3) is 5-10% of the weight of the supernatant.

9. Use of the cleaning composition according to any one of claims 1 to 8 in the preparation of cosmetics.

10. An anti-hair loss bubble essence water, characterized in that: The invention comprises the following components in percentage by weight: 20-30% of the cleaning composition according to any one of claims 1 to 8, 1-5% of arginine, 5-10% of glycerol, 5-10% of 1,3-propylene glycol, 0.1-1% of BIOTA ORIENTALIS leaf extract, 0.1-1% of PANAX GINSENG root extract, 0.1-1% of LIGUSTICUM CHUANXIONG root extract, 0.1-1% of LIGUSTRUM LUCIDUM fruit extract, 1-5% of cocamidopropyl betaine, 0.1-2% of capryloyl glycine, and the balance of water.

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