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77results about How to "Loose internal structure" patented technology

Selective-oxidized chitosan and heterogeneous preparation method thereof

InactiveCN107474161AHigh oxidation selectivityMild reaction conditionsSolubilityReaction rate
The invention discloses a selective-oxidized chitosan and a heterogeneous preparation method thereof. The method is characterized in that according to preparation of the oxidized chitosan, macromolecular chitosan is dissolved in an ionic liquid, the chitosan is precipitated from the ionic liquid by adding absolute ethyl alcohol, and porous chitosan is obtained after the ionic liquid in a precipitation is fully replaced through absolute ethyl alcohol dipping and ultrasonic oscillation; the porous chitosan is moistened and expanded in the ionic liquid to form a semisolid gel with certain viscosity, and then partial or all hydroxyls at C6 position in pyranose rings of the chitosan are selectively oxidized into carboxyls in an ionic liquid medium to obtain the selective-oxidized chitosan with adoption of a concentrated nitric acid-concentrated phosphoric acid-sodium nitrite system. According to the method, operation is simple and convenient, the oxidation reaction rate is high, the oxidation degree of the chitosan is easily controlled, oxidation products are easy to separate, the yield of the products is high, the prepared carboxyl chitosan has good antibacterial activity and water solubility, and the ionic liquid can be recycled for cyclic utilization, which is environmentally friendly.
Owner:TAIHE KERUNGE GARMENT CO LTD

Method for preparing iron-based magnetic activated carbon by catalytic activation of radix puerariae waste residue with compound enzyme

The invention provides a method for preparing iron-based magnetic activated carbon from by catalytic activation of radix puerariae waste residue with compound enzyme, and belongs to the technical field of activated carbon. The method comprises the steps of by taking the radix puerariae waste residue as the raw material, carrying out raw material pretreatment, preparing a radix puerariae activated substrate through catalytic activation with compound enzymes (cellulase, ligninase and pectinase), and preparing the magnetic activated carbon by doping iron, thereby obtaining the product. The method provided by the invention has the characteristics of wide raw material source, low waste material utilization cost, few production steps and low process energy consumption and no secondary pollution, and is beneficial to environment protection; the activated carbon product are excellent in adsorptive property and the magnetic properties and wide in application, and secondary pollution caused by difficult activated carbon recovery is not generated, etc. The method can be widely applied to preparation of the magnetic activated carbon by using the radix puerariae residue solid wastes as raw materials and doping iron; the activated carbon prepared by the method can be widely applied to the fields of waste water treatment, oil fume desorption and odor adsorption in food preservation and the like.
Owner:CHONGQING TECH & BUSINESS UNIV

Radix angelicae sinensis traditional Chinese medicine decoction pieces and preparation method thereof

The invention relates to the technical field of traditional Chinese medicine decoction pieces, in particular to radix angelicae sinensis traditional Chinese medicine decoction pieces and a preparationmethod thereof. The preparation method comprises the following steps of A, material selection and washing; B, infiltration; C, slicing and steaming; D, vacuum freeze drying and smashing; E, encapsulation; F, drying and tabletting. The preparation method is simple in process, the operation is easy to control, the production efficiency is high, and the cost is low; through encapsulation, active functional ingredients in radix angelicae sinensis are effectively protected, the water content is equal to or lower than 4.5%, the ligustilide content is 57.83%-58.64%, the ferulic acid content is 0.061-0.073%, the radix angelicae sinensis traditional Chinese medicine decoction pieces prepared by using the method are easy to dissolve and easy to digest and absorb, the dissolution rate is 97.25-98.88%, and bacteria are not easy to breed. The content of aflatoxin B1 is 1.6-2.3 microgram/kg, the shelf life is long, the quality is stable and the preparation method can be used for massive industrialproduction.
Owner:广东元德中药饮片有限公司

Method for preparing chitosan modified carboxylation cotton fabric in ionic liquid medium

The invention discloses a method for preparing a chitosan modified carboxylation cotton fabric in an ionic liquid medium. The method is characterized by comprising the following steps: firstly, dissolving low-crystallization chitosan into an ionic liquid, carrying out selective oxidation on a cotton fabric after desizing and boiling in isopropanol in a concentrated nitric acid / strong phosphoric acid-sodium nitrite system, further stirring a carboxylation cotton fabric and chitosan in the ionic liquid medium at 30-40 DEG C to implement an amide chemical reaction, removing the ionic liquid, carrying out vacuum drying and water washing, thereby obtaining the chitosan modified carboxylation cotton fabric. The method disclosed by the invention is simple and feasible, rapid in amide reaction, high in grafting rate, possible in ionic liquid recycling and green and environmentally friendly, the prepared chitosan amide modified cotton fabric has a long-lasting and efficient antibacterial capability, is affiliative to human bodies, is safe and sanitary and good in wearing comfort, overcomes adverse influence caused by chemical cross-linking agents and acid solutions upon excellent propertiesof cotton fabrics and human health in conventional chitosan modification, and has wide practical application prospects.
Owner:SHAOXING MAIBAO TECH CO LTD

Macromolecular sound absorption composition board and preparation method thereof

ActiveCN108481861AEnhance weakening effectStrong abatement abilitySynthetic resin layered productsWood layered productsFiberPolyvinyl chloride
The invention discloses a macromolecular sound absorption composition board which comprises a macromolecular foaming layer, mixed aerogel layers and reinforcing layers, wherein two sides of the macromolecular foaming layer are respectively provided with the mixed aerogel layers and the reinforcing layers. The macromolecular sound absorption composition board is characterized in that the macromolecular foaming layer contains the following components in parts by weight: 80-100 parts of polyvinyl chloride, 15-25 parts of porous ceramic particles, 8-15 parts of a foaming agent, 20-25 parts of a flame retardant, 2-3 parts of acrosslinking agent, 15-25 parts of EVA particles, 40-60 parts of spay fusing fiber, 2-5 parts of a gas forming admixture, and 15-20 parts of magnesium chloride. The macromolecular sound absorption composition board has the advantages that because the porous ceramic particles, the EVA particles, the spay fusing fiber and the like are added, the sound absorption capacityis greatly improved, the diameter of the spay fusing fiber can reach micro order, and the induction strength to low-frequency low-strength sound wave is relatively strong; because the mixed aerogel layers are small in density and more in gaps, vibration is easy to generate to convert the energy of sound wave to mechanical energy or to internal energy to be dissipated. Therefore, the macromolecular sound absorption composition board not only is strong in high frequency sound wave reduction capacity, but also is stronger in low frequency sound wave reduction capacity compared with that of general absorber materials.
Owner:兴仁县详务新型节能建材有限公司

Treatment agent for formaldehyde wastewater

The invention discloses a treatment agent for formaldehyde wastewater and belongs to the field of wastewater treatment. According to the treatment agent for formaldehyde wastewater, coconut shell granules are obtained through subjecting coconut shells to crushing and alkali dipping and then are subjected to liquid-nitrogen freezing and pyrolyzing, so that the porosity among the coconut shell granules is improved, and the adsorption capacity is also improved; thiourea added can be combined with formaldehyde as a nucleophilic reagent, and a produced combination can be adsorbed by a diatomite ingredient of the treatment agent, so as to achieve the effect of stably removing the formaldehyde; diatomite is modified with acrylic acid and citric acid containing three -COOH, so that the uniformityof air hole distribution is improved, and the formaldehyde can be adsorbed thoroughly; and abietate added has tackifying and film forming properties and high stability, has certain plasticity and hasgood wettability to the surface of an adherend, so that the treatment agent durably maintains formaldehyde combining and adsorbing stability. According to the treatment agent, the problem that formaldehyde wastewater treatment agents frequently used at present are poor in effect and stability during formaldehyde treatment is solved.
Owner:张芸

Plasticized polymer ionic liquid film and method for selective separation of chromium (VI) through same

The invention discloses a plasticized polymer ionic liquid film and a method for selective separation of chromium (VI) through the same. The method comprises the steps that 1.5-2.5% of fatty amine and3.0-3.5% of polyvinyl chloride are taken as reaction raw materials to be subjected to reactive blending in 91.5-93.0% of an organic solvent, then 1.0-4.0% of a plasticizer is added, the solvent is removed through volatilization, the plasticized polymer ionic liquid film is prepared through acidification transformation, and selective separation of the chromium (VI) in chromium (VI) feed liquid isconducted through the plasticized polymer ionic liquid film under synchronous conducting of extraction and reverse extraction. A film preparation technology is simple, the using amount of a reagent issmall, and selectivity to the chromium (VI) is high; energy consumption is low in the extraction process, and secondary pollution is avoided; a film phase is not prone to leakage, a liquid film is stable in property, and the plasticized polymer ionic liquid film has the ability of continuous and repeated application; and the plasticized polymer ionic liquid film and the method can be applied to industrial application of selective removal of the chromium (VI) in the chromium-containing wastewater.
Owner:XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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