Nucleation device for preparing lithium iron phosphate by high-temperature solid-phase method
By designing a gas discharge device in the nucleation device for preparing lithium iron phosphate in a high-temperature solid phase method, the fan and filter are used to discharge hot gas and reduce their temperature, the problem of room temperature increase caused by the release of hot gas when lithium iron phosphate is removed is solved, and the room temperature rise is improved Safety of the work environment.
Patent Information
- Application Number
- CN202411256543.X
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-09
- Publication Date
- 2025-01-07
AI Technical Summary
When preparing a nucleation device for lithium iron phosphate using high-temperature solid phase method, a large amount of hot air will be released when the lithium iron phosphate is taken out, causing a significant increase in the indoor temperature and affecting the safety of the working environment.
A nucleation device including an air outlet device is designed, which discharges hot air through a fan blowing air, uses the first and second filters to prevent lithium iron phosphate from entering the pipeline, and reduces the hot air temperature through a heat dissipation ring to avoid an increase in the indoor temperature. .
It effectively avoids a significant increase in indoor temperature, improves the safety of the working environment, and facilitates the maintenance and cleaning of the device.
Smart Images
Figure CN119268351A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of preparing lithium iron phosphate, and in particular to a nucleation device for preparing lithium iron phosphate by a high-temperature solid phase method. Background Art
[0002] A nucleation device is a device used to form lithium iron phosphate from raw materials at high temperature in the preparation of lithium iron phosphate by a high-temperature solid-phase method. When using the nucleation device, the raw materials for preparing lithium iron phosphate by a high-temperature fixed method are pretreated and placed inside a preparation furnace. The preparation furnace is heated to a certain degree and then heated inside the preparation furnace for a period of time to allow the raw materials to react into lithium iron phosphate.
[0003] The inventors have discovered in their daily work that the nucleation device still has at least the following problems: when using the nucleation device, the raw materials for preparing lithium iron phosphate by the high-temperature fixation method are pre-treated and placed inside a preparation furnace. After being heated to a certain degree by the preparation furnace, they are heated inside the preparation furnace for a period of time so that the raw materials react to form lithium iron phosphate. However, in actual use, when the lithium iron phosphate is taken out of the preparation furnace, a large amount of heat is released into the room, causing the temperature in the room to rise significantly, which affects the safety of the working environment to a certain extent. Summary of the invention
[0004] The purpose of the present invention is to solve the shortcomings of the prior art and to propose a nucleation device for preparing lithium iron phosphate by a high-temperature solid phase method.
[0005] In order to achieve the above-mentioned purpose, the present invention adopts the following technical scheme: a nucleation device for preparing lithium iron phosphate by a high-temperature solid phase method, comprising a preparation furnace, a feed port is arranged at the top of the preparation furnace, a discharge pipe is arranged at the bottom of the preparation furnace, a solenoid valve is arranged inside the discharge pipe, a support ring is fixedly connected to the surface of the preparation furnace, and a support leg is evenly fixedly connected to the bottom of the support ring, an air outlet device is arranged on the surface of the discharge pipe, and a connecting device is arranged on the surface of the preparation furnace, the air outlet device comprises a first connecting pipe and a second connecting pipe, the first connecting pipe is fixedly connected to one end of the discharge pipe, the first connecting pipe and the inside of the discharge pipe are connected together, the side of the discharge pipe away from the first connecting pipe is fixedly connected to the second connecting pipe, the second connecting pipe and the inside of the discharge pipe are connected together, the first connecting pipe is fixedly connected to the inside of the end close to the discharge pipe of the first connecting pipe, the second connecting pipe is fixedly connected to the inside of the discharge pipe, the first filter is fixedly connected to the inner wall of the end close to the discharge pipe of the second connecting pipe, a fan is arranged at the end of the first connecting pipe away from the discharge pipe, and a heat dissipation ring is evenly fixedly connected to the surface of the second connecting pipe.
[0006] The effect achieved by the above-mentioned components is: when using the air outlet device, air is blown into the interior of the first connecting pipe through the fan, and then the hot air generated inside the preparation furnace can be blown out to the outside through the second connecting pipe. The function of the first filter is to prevent lithium iron phosphate from entering the interior of the first connecting pipe, and the function of the second filter is to prevent lithium iron phosphate from entering the interior of the second connecting pipe. When the hot air passes through the second connecting pipe, because the heat dissipation ring is arranged on the surface of the second connecting pipe arranged outdoors, the temperature of the hot air can be reduced to a certain extent through the heat dissipation ring, which can avoid a significant increase in the temperature of the indoor environment to a certain extent.
[0007] Preferably, the inner wall of the first connecting tube is fixedly connected to a connecting box, the inner wall of the connecting box and the first connecting tube are communicated together, the bottom of the connecting box is slidably connected to a baffle, the bottom of the baffle is fixedly connected to a sliding plate, both sides of the connecting box are provided with sliding grooves, the inner wall of the sliding groove is slidably connected to a sliding block, the side of the sliding block away from the sliding groove is fixedly connected to one side of the sliding plate, a rectangular groove is provided on one side of the sliding plate, the top of the connecting box is provided with a connecting groove, the inner wall of the connecting groove is slidably connected to a clamping plate, and the clamping plate One end away from the connecting groove is slidably connected to the inner wall of the rectangular groove, one side of the inner wall of the connecting groove is fixedly connected with a first spring, one end of the first spring away from the connecting box is fixedly connected to the side of the positioning plate, the side of the positioning plate away from the connecting groove is fixedly connected to the limiting plate, an L-shaped plate is slidingly sleeved on the surface of the limiting plate, one end of the L-shaped plate away from the limiting plate is slidably connected to the inner wall of the sliding groove, a side of the L-shaped plate close to the limiting plate is fixedly connected with a second spring, and one end of the second spring away from the L-shaped plate is fixedly connected to the side of the positioning plate away from the connecting groove.
[0008] The effect achieved by the above-mentioned components is as follows: when the air outlet device is not in use, the baffle is slid to the inside of the connecting box, and then the locking plate is manually controlled to slide on the inner wall of the connecting groove, and then the end of the locking plate away from the connecting groove is slid to the inside of the rectangular groove, and the locking plate is pulled toward the direction close to the connecting box by the first spring, so that the baffle can be well restricted to the inside of the connecting box, which can to a certain extent prevent the hot air from being away from the end of the first connecting pipe away from the discharge pipe away from the preparation furnace. When the air outlet device is used, the baffle is manually controlled to slide out of the connecting box, and at this time the sliding block slides to the bottom of the slide groove, and then the L-shaped plate is controlled to be inserted into the inside of the slide groove, and the L-shaped plate is pulled toward the direction close to the locking plate by the second spring, and then the L-shaped plate is well restricted to the top of the sliding plate, so that the baffle can be kept away from the inside of the connecting box, so that the wind blown out by the fan can pass through the first connecting pipe well.
[0009] Preferably, the fan is slidably connected to the inner wall of the first connecting tube away from the discharge pipe, the fan is fixedly connected to a connecting rod on the side away from the first connecting tube, the connecting rod is fixedly connected to a rectangular bar on the end away from the fan, a retaining groove is provided on the side of the rectangular bar close to the connecting rod, a circular ring is rotatably provided on the inner wall of the retaining groove, a first threaded groove is provided on the inner wall of the circular ring, a second threaded groove is provided on the surface of the end of the first connecting tube away from the discharge pipe, and the circular ring is threadedly sleeved on the surface of the first connecting tube away from the discharge pipe.
[0010] The effect achieved by the above components is: slide the fan to the inner wall of the end of the first connecting pipe away from the discharge pipe, and then manually control the ring to rotate on the inner wall of the positioning groove, so that the ring thread can be well sleeved on the surface of the end of the first connecting pipe away from the discharge pipe. In this way, the fan can be well set inside the first connecting pipe. The reverse operation can remove the fan, which is convenient for maintenance of the fan.
[0011] Preferably, an extension tube is provided at the end of the second connecting tube away from the discharge tube, and a retaining ring is fixedly connected to the surface of the extension tube, and the end of the second connecting tube away from the discharge tube is fixedly connected to the connecting ring, the connecting ring is slidably sleeved on the surface of one end of the extension tube, and a rotating groove is clamped on the surface of the connecting ring, and a moving ring is slidably connected to the inner wall of the rotating groove, the moving ring is slidably sleeved on the surface of the connecting ring, and a limiting groove is provided on the surface of the moving ring, and a retaining strip is slidably connected to the inner wall of the limiting groove, and a side of the retaining strip close to the moving ring is arranged on the side of the retaining ring close to the extension tube, and a round rod is slidably inserted through the top of the retaining strip, and the bottom of the round rod is fixedly connected to the surface of the moving ring, and a third spring is sleeved on the surface of the round rod, and one end of the third spring is fixedly connected to the surface of the moving ring, and one end of the third spring close to the round rod is fixedly connected to the bottom of the retaining strip.
[0012] The effect achieved by the above-mentioned components is: manually slide the extension tube to the inner wall of the connecting ring, and then manually control the moving ring to slide on the inner wall of the limiting groove, so that the moving ring is close to the extension tube, and then the locking bar is passed through the limiting groove and arranged on the side of the locking ring close to the extension tube, and the locking bar is pulled in the direction close to the moving ring by the third spring, so that the locking bar can be well restricted to one side of the locking ring, and then the extension tube can be well set at the end of the second connecting tube away from the discharge pipe, so that the length of the second connecting tube can be lengthened to a certain extent, which makes it easier to pass the hot air to the outdoors.
[0013] Preferably, the connecting device includes a first connecting tube and a second connecting tube, the first connecting tube is arranged on the top of the second connecting tube, a circular groove is opened on the top of the second connecting tube, a fixing ring is slidably connected to the inner wall of the circular groove, and the top of the fixing ring is fixedly connected to the bottom of the first connecting tube.
[0014] The effect achieved by the above-mentioned components is: when using the connecting device, slide the fixing ring into the inside of the circular groove, so that the first connecting tube can be set on the top of the second connecting tube. The reverse operation can disassemble the preparation furnace into the first connecting tube and the second connecting tube, which is convenient for cleaning the lithium iron phosphate or other substances that may remain inside the preparation furnace, which can avoid such substances from affecting subsequent experiments to a certain extent.
[0015] Preferably, a cylinder is fixedly connected to the surface of the second connecting cylinder, and the cylinder is slidably sleeved on the surface of the first connecting cylinder close to the second connecting cylinder.
[0016] The effect achieved by the above components is: the first connecting cylinder is slid into the interior of the cylinder, so that the connection between the first connecting cylinder and the second connecting cylinder can be made tighter.
[0017] Preferably, a positioning groove is provided at the top of the second connecting tube, a rotating ring is rotatably provided on the inner wall of the positioning groove, a semicircular plate is fixedly connected to the inner wall of the rotating ring, a semicircular groove is provided at the bottom of the surface of the first connecting tube, the inner wall of the semicircular groove and the semicircular plate are slidingly connected, a fixing groove is provided on the side of the surface of the first connecting tube away from the semicircular groove, the tops of the semicircular grooves of the fixing groove are arranged together, and the inner wall of the fixing groove is rotatably sleeved on the surface of the semicircular plate.
[0018] The effect achieved by the above components is: when the first connecting tube is slid into the inside of the cylinder, the semicircular plate slides inside the semicircular groove; when the first connecting tube is completely slid into the inside of the cylinder, the rotating ring is manually controlled to rotate inside the positioning groove, and then the semicircular plate is slid into the inside of the fixed groove, so that the first connecting tube can be well restricted inside the cylinder, and then the first connecting tube and the second connecting tube can be well connected together.
[0019] Preferably, a fixing rod is inserted and slidably penetrated through the bottom of the rotating ring, a rectangular plate is slidably sleeved on the surface of the fixing rod, one side of the rectangular plate is fixedly connected to the surface of the first connecting tube close to the fixing groove, a fourth spring is sleeved on the surface of the fixing rod, one end of the fourth spring is fixedly connected to the bottom of the fixing rod, one end of the fourth spring close to the fixing rod is fixedly connected to the bottom of the rotating ring, a heat preservation belt is provided on the surface of the rotating ring, and the heat preservation belt is provided at the connection between the first connecting tube and the second connecting tube.
[0020] The effect achieved by the above-mentioned components is: the fixing rod is passed through the rotating ring and then through the rectangular plate, and then the fixing rod is pulled in the direction close to the rotating ring through the fourth spring, so that the fixing rod is well restricted inside the rectangular plate, so that the rotating ring can be well fixed inside the positioning groove and then the insulation belt is wrapped around the connection between the first connecting tube and the second connecting tube, which can achieve a certain sealing and insulation effect.
[0021] In the present invention, an air outlet device is provided. When the air outlet device is used, air is blown into the interior of the first connecting pipe by a fan, and then the hot air generated inside the preparation furnace can be blown to the outside through the second connecting pipe. The function of the first filter is to prevent lithium iron phosphate from entering the interior of the first connecting pipe, and the function of the second filter is to prevent lithium iron phosphate from entering the interior of the second connecting pipe. When the hot air passes through the second connecting pipe, because the heat dissipation ring is provided on the surface of the second connecting pipe provided outdoors, the temperature of the hot air can be reduced to a certain extent through the heat dissipation ring, which can avoid a significant increase in the temperature of the indoor environment to a certain extent. BRIEF DESCRIPTION OF THE DRAWINGS
[0022] Figure 1 A schematic diagram of the three-dimensional structure of a nucleation device for preparing lithium iron phosphate by a high-temperature solid phase method proposed by the present invention; Figure 2 A schematic diagram of the three-dimensional structure of a novel heat dissipation ring proposed by the present invention; Figure 3 A schematic diagram of the three-dimensional structure of a novel L-shaped plate proposed in the present invention; Figure 4 A schematic diagram of the three-dimensional structure of a novel circular ring proposed by the present invention; Figure 5 A schematic diagram of the three-dimensional structure of a novel mobile ring proposed in the present invention; Figure 6 A schematic diagram of the three-dimensional structure of a novel rotating ring proposed by the present invention; Figure 7 A schematic diagram of the three-dimensional structure of a novel fixing rod proposed by the present invention; Figure 8 The present invention provides a three-dimensional structural schematic diagram of a novel thermal insulation belt.
[0023] Legend: 1. Preparation furnace; 2. Feed inlet; 3. Discharge pipe; 4. Solenoid valve; 5. Support ring; 6. Support leg; 7. Exhaust device; 701. First connecting pipe; 702. Second connecting pipe; 703. Fan; 704. First filter; 705. Second filter; 706. Heat dissipation ring; 707. Connecting box; 708. Baffle; 709. Sliding plate; 710. Slide; 711. Sliding block; 712. Rectangular groove; 713. Connecting groove; 714. Positioning plate; 715. First spring; 716. L-shaped plate; 717. Second spring; 718. Connecting rod; 719. Rectangular bar; 720. Positioning groove; 721. Ring; 722. First thread groove; 723. Second thread groove; 724. Extension tube; 725. Connecting ring; 726. Rotating groove; 727. Moving ring; 728. Limiting groove; 729. Positioning strip; 730. Round rod; 731. Third spring; 732. Positioning ring; 733. Positioning plate; 8. Connecting device; 801. First connecting cylinder; 802. Second connecting cylinder; 803. Round groove; 804. Fixed ring; 805. Cylinder; 806. Positioning groove; 807. Rotating ring; 808. Semicircular plate; 809. Semicircular groove; 810. Fixed groove; 811. Fixed rod; 812. Fourth spring; 813. Rectangular plate; 814. Insulation belt. DETAILED DESCRIPTION
[0024] Embodiment 1, as Figure 1-8 As shown, a nucleation device for preparing lithium iron phosphate by a high-temperature solid phase method, a feed port 2 is arranged on the top of a preparation furnace 1, a discharge pipe 3 is arranged on the bottom of the preparation furnace 1, a solenoid valve 4 is arranged inside the discharge pipe 3, a support ring 5 is fixedly connected to the surface of the preparation furnace 1, a support leg 6 is evenly fixedly connected to the bottom of the support ring 5, a gas outlet device 7 is arranged on the surface of the discharge pipe 3, and a connecting device 8 is arranged on the surface of the preparation furnace 1. When the nucleation device is used, the raw materials for preparing lithium iron phosphate by a high-temperature fixed method are pretreated and placed inside the preparation furnace 1. The preparation furnace 1 is heated to a certain degree and then heated inside the preparation furnace 1 for a period of time, so that the raw materials react to form lithium iron phosphate.
[0025] Reference Figures 2 to 5The air outlet device 7 includes a first connecting pipe 701 and a second connecting pipe 702. The first connecting pipe 701 is fixedly connected to one end of the discharge pipe 3. The first connecting pipe 701 and the interior of the discharge pipe 3 are connected together. The side of the discharge pipe 3 away from the first connecting pipe 701 is fixedly connected with the second connecting pipe 702. The second connecting pipe 702 and the interior of the discharge pipe 3 are connected together. The first connecting pipe 701 is fixedly connected to the end of the discharge pipe 3. The first filter screen 704 is fixedly connected to the inner wall of the end of the second connecting pipe 702 close to the discharge pipe 3. A fan 703 is arranged at the end of the first connecting pipe 701 away from the discharge pipe 3. A heat dissipation ring 706 is evenly fixedly connected to the surface of the second connecting pipe 702. When the device 7 is installed, air is blown into the first connecting pipe 701 through the fan 703, and then the hot air generated in the preparation furnace 1 can be blown out to the outside through the second connecting pipe 702. The function of the first filter 704 is to prevent lithium iron phosphate from entering the first connecting pipe 701, and the function of the second filter 705 is to prevent lithium iron phosphate from entering the second connecting pipe 702. When the hot air passes through the second connecting pipe 702, because the heat dissipation ring 706 is arranged on the surface of the second connecting pipe 702 arranged outdoors, the heat dissipation ring 706 can reduce the temperature of the hot air to a certain extent, which can avoid a significant increase in the temperature of the indoor environment to a certain extent. The inner wall of the first connecting pipe 701 is fixedly connected to a connecting box 707, and the connecting box 707 is fixedly connected to the inner wall of the first connecting pipe 701. The inner wall of the box 707 is connected to the first connecting pipe 701, and the bottom of the connecting box 707 is slidably connected with a baffle 708, and the bottom of the baffle 708 is fixedly connected with a sliding plate 709. Both sides of the connecting box 707 are provided with sliding grooves 710, and the inner wall of the sliding groove 710 is slidably connected with a sliding block 711. The side of the sliding block 711 away from the sliding groove 710 is fixedly connected to one side of the sliding plate 709, and a rectangular groove 712 is provided on one side of the sliding plate 709. A connecting groove 713 is provided on the top of the connecting box 707, and a locking plate 714 is slidably connected to the inner wall of the connecting groove 713. The end of the locking plate 714 away from the connecting groove 713 is slidably connected to the inner wall of the rectangular groove 712, and one side of the inner wall of the connecting groove 713 is fixedly connected with a first spring The first spring 715 is fixedly connected to one end of the connection box 707 and the side of the positioning plate 714, and the side of the positioning plate 714 away from the connection groove 713 is fixedly connected to the limiting plate 733. The surface of the limiting plate 733 is slidingly sleeved with an L-shaped plate 716, and the end of the L-shaped plate 716 away from the limiting plate 733 is slidingly connected to the inner wall of the slide groove 710. The side of the L-shaped plate 716 close to the limiting plate 733 is fixedly connected to the second spring 717, and the end of the second spring 717 away from the L-shaped plate 716 is fixedly connected to the side of the positioning plate 714 away from the connection groove 713. When the air outlet device 7 is not in use, the baffle 708 is slid into the interior of the connection box 707, and then the positioning plate 714 is manually controlled to slide on the inner wall of the connection groove 713.Then, the end of the locking plate 714 away from the connecting groove 713 is slid into the inside of the rectangular groove 712, and the locking plate 714 is pulled in the direction close to the connecting box 707 by the first spring 715. In this way, the baffle 708 can be well restricted in the inside of the connecting box 707. In this way, it can prevent the hot air from being away from the end of the first connecting pipe 701 away from the discharge pipe 3 away from the preparation furnace 1 to a certain extent. When using the gas outlet device 7, the baffle 708 is manually controlled to slide out of the connecting box 707. At this time, the sliding block 711 slides to the bottom of the slide groove 710, and then the L-shaped plate 716 is controlled to be inserted into the inside of the slide groove 710, and the L-shaped plate 716 is pulled in the direction close to the locking plate 714 by the second spring 717, thereby well restricting the L-shaped plate 716 to the sliding plate 709. The top of the device can make the baffle 708 away from the interior of the connecting box 707, so that the wind blown by the fan 703 can pass through the first connecting pipe 701 well. The fan 703 is slidably connected to the inner wall of the first connecting pipe 701 away from the end of the discharge pipe 3. The side of the fan 703 away from the first connecting pipe 701 is fixedly connected with a connecting rod 718, and the end of the connecting rod 718 away from the fan 703 is fixedly connected with a rectangular bar 719. A clamping groove 720 is provided on the side of the rectangular bar 719 close to the connecting rod 718. A circular ring 721 is rotatably provided on the inner wall of the clamping groove 720. A first threaded groove 722 is provided on the inner wall of the circular ring 721. A second threaded groove 723 is provided on the surface of the end of the first connecting pipe 701 away from the discharge pipe 3. The circular ring 721 is threadedly sleeved on On the surface of the end of the first connecting tube 701 away from the discharge pipe 3, the fan 703 is slid to the inner wall of the end of the first connecting tube 701 away from the discharge pipe 3, and then the ring 721 is manually controlled to rotate on the inner wall of the positioning groove 720, so that the ring 721 can be well threaded on the surface of the end of the first connecting tube 701 away from the discharge pipe 3. In this way, the fan 703 can be well set inside the first connecting tube 701, and the fan 703 can be disassembled by reverse operation, so as to facilitate the maintenance of the fan 703. An extension tube 724 is provided at the end of the second connecting tube 702 away from the discharge pipe 3, and a positioning ring 732 is fixedly connected to the surface of the extension tube 724, and a connecting ring 725 is fixedly connected to the end of the second connecting tube 702 away from the discharge pipe 3. The ring 725 is slidably sleeved on the surface of one end of the extension tube 724, and a rotating groove 726 is clamped on the surface of the connecting ring 725. A moving ring 727 is slidably connected to the inner wall of the rotating groove 726. The moving ring 727 is slidably sleeved on the surface of the connecting ring 725. A limiting groove 728 is provided on the surface of the moving ring 727. A positioning strip 729 is slidably connected to the inner wall of the limiting groove 728. The side of the positioning strip 729 close to the moving ring 727 is arranged on the side of the positioning ring 732 close to the extension tube 724. A round rod 730 is inserted and slidably penetrated at the top of the positioning strip 729. The bottom of the round rod 730 is fixedly connected to the surface of the moving ring 727. A third spring 731 is sleeved on the surface of the round rod 730. One end of the third spring 731 is fixedly connected to the surface of the moving ring 727.The end of the third spring 731 close to the round rod 730 is fixedly connected to the bottom of the positioning strip 729, and the extension tube 724 is manually slid to the inner wall of the connecting ring 725, and then the moving ring 727 is manually controlled to slide on the inner wall of the limiting groove 728, so that the moving ring 727 is close to the extension tube 724, and then the positioning strip 729 is passed through the limiting groove 728 and arranged on the side of the positioning ring 732 close to the extension tube 724, and the positioning strip 729 is pulled in the direction close to the moving ring 727 by the third spring 731, so that the positioning strip 729 can be well restricted to one side of the positioning ring 732, and then the extension tube 724 can be well arranged at the end of the second connecting tube 702 away from the discharge pipe 3, so that the length of the second connecting tube 702 can be lengthened to a certain extent, which is convenient for passing the hot air to the outside.
[0026] Reference Figures 6 to 8The connecting device 8 includes a first connecting tube 801 and a second connecting tube 802. The first connecting tube 801 is arranged on the top of the second connecting tube 802. A circular groove 803 is opened on the top of the second connecting tube 802. A fixing ring 804 is slidably connected to the inner wall of the circular groove 803. The top of the fixing ring 804 is fixedly connected to the bottom of the first connecting tube 801. When using the connecting device 8, slide the fixing ring 804 into the inside of the circular groove 803, so that the first connecting tube 801 can be arranged on the top of the second connecting tube 802. The reverse operation can disassemble the preparation furnace 1 into the first connecting tube 801 and the second connecting tube 802, which is convenient for cleaning the lithium iron phosphate or other substances that may remain in the preparation furnace 1, which can avoid to a certain extent. In order to prevent such substances from affecting subsequent experiments, a cylinder 805 is fixedly connected to the surface of the second connecting cylinder 802, and the cylinder 805 is slidably sleeved on the surface of the first connecting cylinder 801 close to the second connecting cylinder 802. The first connecting cylinder 801 is slid into the inside of the cylinder 805, so that the connection between the first connecting cylinder 801 and the second connecting cylinder 802 can be tighter. A positioning groove 806 is provided on the top of the second connecting cylinder 802, and a rotating ring 807 is rotatably provided on the inner wall of the positioning groove 806. A semicircular plate 808 is fixedly connected to the inner wall of the rotating ring 807. A semicircular groove 809 is provided on the bottom of the surface of the first connecting cylinder 801. The inner wall of the semicircular groove 809 is slidably connected to the semicircular plate 808. The surface of the first connecting cylinder 801 is away from the semicircular groove 809. A fixing groove 810 is provided on one side, and the top of the semicircular groove 809 of the fixing groove 810 is set together. The inner wall of the fixing groove 810 is rotatably sleeved on the surface of the semicircular plate 808. When the first connecting cylinder 801 is slid into the cylinder 805, the semicircular plate 808 slides inside the semicircular groove 809. When the first connecting cylinder 801 completely slides into the cylinder 805, the rotating ring 807 is manually controlled to rotate inside the positioning groove 806, and then the semicircular plate 808 slides into the fixing groove 810. In this way, the first connecting cylinder 801 can be well restricted inside the cylinder 805, and then the first connecting cylinder 801 and the second connecting cylinder 802 can be well connected together. The bottom of the rotating ring 807 is slidably penetrated and is provided with a fixing rod 8 11. A rectangular plate 813 is slidably sleeved on the surface of the fixed rod 811. One side of the rectangular plate 813 is fixedly connected to the surface of the first connecting tube 801 near the fixed groove 810. A fourth spring 812 is sleeved on the surface of the fixed rod 811. One end of the fourth spring 812 is fixedly connected to the bottom of the fixed rod 811. One end of the fourth spring 812 near the fixed rod 811 is fixedly connected to the bottom of the rotating ring 807. A heat preservation belt 814 is provided on the surface of the rotating ring 807. The heat preservation belt 814 is provided at the connection between the first connecting tube 801 and the second connecting tube 802. The fixed rod 811 is passed through the rotating ring 807 and then through the rectangular plate 813, and then the fixed rod 811 is pulled toward the direction close to the rotating ring 807 through the fourth spring 812.Then the fixing rod 811 is well restricted inside the rectangular plate 813, so that the rotating ring 807 can be well fixed inside the positioning groove 806, and then the insulation belt 814 is wrapped around the connection between the first connecting tube 801 and the second connecting tube 802, which can achieve a certain sealing and insulation effect.
[0027] Working principle: when using the nucleation device, the raw materials for preparing lithium iron phosphate by the high-temperature fixing method are pretreated and placed inside the preparation furnace 1. After being heated to a certain degree, the raw materials are heated inside the preparation furnace 1 for a period of time to react into lithium iron phosphate. When using the gas outlet device 7, the fan 703 is slid to the inner wall of the end of the first connecting tube 701 away from the discharge pipe 3, and then the ring 721 is manually controlled to rotate on the inner wall of the positioning groove 720, so that the ring 721 can be well threaded on the surface of the end of the first connecting tube 701 away from the discharge pipe 3, so that the fan 703 can be well set inside the first connecting tube 701, and the reverse operation can remove the fan 703, which is convenient for the fan. 703 is maintained, the baffle plate 708 is manually controlled to slide out of the connection box 707, at this time the sliding block 711 slides to the bottom of the slide slot 710, and then the L-shaped plate 716 is controlled to be inserted into the inside of the slide slot 710, and the L-shaped plate 716 is pulled toward the direction close to the positioning plate 714 by the second spring 717, and then the L-shaped plate 716 is well restricted to the top of the sliding plate 709, so that the baffle plate 708 can be kept away from the inside of the connection box 707, so that the wind blown by the fan 703 can pass through the first connecting pipe 701 well, and then the extension pipe 724 is manually slid to the inner wall of the connecting ring 725, and then the moving ring 727 is manually controlled to slide on the inner wall of the limiting groove 728, so that the moving ring 727 is close to the extension pipe 724, and then the positioning bar After passing through the limiting groove 728, 729 is arranged on the side of the locking ring 732 close to the extension tube 724, and the locking strip 729 is pulled in the direction close to the movable ring 727 by the third spring 731, so that the locking strip 729 can be well limited to one side of the locking ring 732, and then the extension tube 724 can be well arranged at the end of the second connecting tube 702 away from the discharge pipe 3, so that the length of the second connecting tube 702 can be lengthened to a certain extent, which makes it easier to pass the hot air to the outside, and blow air into the inside of the first connecting tube 701 through the fan 703, and then the hot air generated in the preparation furnace 1 can be blown out of the outside through the second connecting tube 702, and the function of the first filter 704 is to prevent lithium iron phosphate from entering the inside of the first connecting tube 701 The function of the second filter 705 is to prevent lithium iron phosphate from entering the second connecting pipe 702. When the hot air passes through the second connecting pipe 702, because the heat dissipation ring 706 is arranged on the surface of the second connecting pipe 702 arranged on the outdoor part, the temperature of the hot air can be reduced to a certain extent through the heat dissipation ring 706, which can avoid a significant increase in the temperature of the indoor environment to a certain extent. When the air outlet device 7 is not used, the baffle 708 is slid into the inside of the connecting box 707, and then the positioning plate 714 is manually controlled to slide on the inner wall of the connecting groove 713, and then the end of the positioning plate 714 away from the connecting groove 713 is slid into the inside of the rectangular groove 712, and the positioning plate 714 is pulled toward the direction close to the connecting box 707 by the first spring 715.In this way, the baffle plate 708 can be well restricted inside the connecting box 707, which can prevent the hot air from being away from the end of the first connecting tube 701 away from the discharge tube 3 and away from the preparation furnace 1 to a certain extent. When using the connecting device 8, the fixing ring 804 is slid into the inside of the circular groove 803, so that the first connecting tube 801 can be set on the top of the second connecting tube 802. In the process of sliding the first connecting tube 801 into the cylinder 805, the semicircular plate 808 slides inside the semicircular groove 809. After the first connecting tube 801 completely slides into the cylinder 805, the rotating ring 807 is manually controlled to rotate inside the positioning groove 806, and then the semicircular plate 808 is slid into the inside of the fixing groove 810. In this way, the first connecting tube 801 can be well restricted inside the cylinder 805, thereby well restricting the first connecting tube 801. The connecting tube 801 and the second connecting tube 802 are connected together, and then the fixing rod 811 is passed through the rotating ring 807 and then through the rectangular plate 813, and then the fixing rod 811 is pulled toward the rotating ring 807 by the fourth spring 812, so that the fixing rod 811 is well restricted inside the rectangular plate 813, so that the rotating ring 807 can be well fixed inside the positioning groove 806, and then the insulation belt 814 is wrapped around the connection between the first connecting tube 801 and the second connecting tube 802, so that a certain sealing and insulation effect can be achieved, and the reverse operation can disassemble the preparation furnace 1 into the first connecting tube 801 and the second connecting tube 802, so that it is convenient to clean the lithium iron phosphate or other substances that may remain inside the preparation furnace 1, so as to avoid such substances from affecting subsequent experiments to a certain extent.
Claims
1. A nucleation device for preparing lithium iron phosphate by a high temperature solid phase method, characterized in that: It includes a preparation furnace, wherein a feed port is provided at the top of the preparation furnace, a discharge pipe is provided at the bottom of the preparation furnace, a solenoid valve is provided inside the discharge pipe, a support ring is fixedly connected to the surface of the preparation furnace, a support leg is evenly fixedly connected to the bottom of the support ring, an air outlet device is provided on the surface of the discharge pipe, and a connecting device is provided on the surface of the preparation furnace, the air outlet device includes a first connecting pipe and a second connecting pipe, the first connecting pipe is fixedly connected to one end of the discharge pipe, the first connecting pipe and the interior of the discharge pipe are communicated together, the side of the discharge pipe away from the first connecting pipe is fixedly connected to the second connecting pipe, the second connecting pipe and the interior of the discharge pipe are communicated together, the first connecting pipe is fixedly connected to the interior of the end close to the discharge pipe of the first connecting pipe, the second connecting pipe is fixedly connected to the inner wall of the end close to the discharge pipe of the second connecting pipe, a fan is provided at one end of the first connecting pipe away from the discharge pipe, and a heat dissipation ring is evenly fixedly connected to the surface of the second connecting pipe.
2. The nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 1, characterized in that: The inner wall of the first connecting tube is fixedly connected to a connecting box, the inner wall of the connecting box and the first connecting tube are communicated together, the bottom of the connecting box is slidably connected to a baffle, the bottom of the baffle is fixedly connected to a sliding plate, both sides of the connecting box are provided with sliding grooves, the inner wall of the sliding groove is slidably connected to a sliding block, the side of the sliding block away from the sliding groove is fixedly connected to one side of the sliding plate, a rectangular groove is provided on one side of the sliding plate, the top of the connecting box is provided with a connecting groove, the inner wall of the connecting groove is slidably connected to a clamping plate, the clamping plate is away from One end of the connecting groove is slidably connected to the inner wall of the rectangular groove, one side of the inner wall of the connecting groove is fixedly connected with a first spring, one end of the first spring away from the connecting box is fixedly connected to the side of the positioning plate, the side of the positioning plate away from the connecting groove is fixedly connected to the limiting plate, an L-shaped plate is slidingly sleeved on the surface of the limiting plate, one end of the L-shaped plate away from the limiting plate is slidably connected to the inner wall of the slide groove, a side of the L-shaped plate close to the limiting plate is fixedly connected with a second spring, and one end of the second spring away from the L-shaped plate is fixedly connected to the side of the positioning plate away from the connecting groove.
3. The nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 1, characterized in that: The fan is slidably connected to the inner wall of the first connecting tube away from the discharge tube, the fan is fixedly connected to a connecting rod on one side away from the first connecting tube, the connecting rod is fixedly connected to a rectangular bar on one end away from the fan, a retaining groove is provided on the side of the rectangular bar close to the connecting rod, a circular ring is rotatably provided on the inner wall of the retaining groove, a first thread groove is provided on the inner wall of the circular ring, a second thread groove is provided on the surface of the end of the first connecting tube away from the discharge tube, and the circular ring is threadedly sleeved on the surface of the end of the first connecting tube away from the discharge tube.
4. The nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 1, characterized in that: An extension tube is provided at the end of the second connecting tube away from the discharge tube, and a retaining ring is fixedly connected to the surface of the extension tube, and the end of the second connecting tube away from the discharge tube is fixedly connected to the connecting ring, the connecting ring is slidably sleeved on the surface of one end of the extension tube, and a rotating groove is clamped on the surface of the connecting ring, and a moving ring is slidably connected to the inner wall of the rotating groove, and the moving ring is slidably sleeved on the surface of the connecting ring, and a limiting groove is provided on the surface of the moving ring, and a retaining strip is slidably connected to the inner wall of the limiting groove, and a side of the retaining strip close to the moving ring is provided on the side of the retaining ring close to the extension tube, and a round rod is slidably inserted through the top of the retaining strip, and the bottom of the round rod is fixedly connected to the surface of the moving ring, and a third spring is sleeved on the surface of the round rod, and one end of the third spring is fixedly connected to the surface of the moving ring, and one end of the third spring close to the round rod is fixedly connected to the bottom of the retaining strip.
5. The nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 1, characterized in that: The connecting device includes a first connecting tube and a second connecting tube. The first connecting tube is arranged on the top of the second connecting tube. A circular groove is opened on the top of the second connecting tube. A fixing ring is slidably connected to the inner wall of the circular groove. The top of the fixing ring is fixedly connected to the bottom of the first connecting tube.
6. The nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 5, characterized in that: A cylinder is fixedly connected to the surface of the second connecting cylinder, and the cylinder is slidably sleeved on the surface of the first connecting cylinder close to the second connecting cylinder.
7. The nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 5, characterized in that: A positioning groove is provided on the top of the second connecting tube, and a rotating ring is rotatably provided on the inner wall of the positioning groove, and a semicircular plate is fixedly connected to the inner wall of the rotating ring. A semicircular groove is provided on the bottom of the surface of the first connecting tube, and the inner wall of the semicircular groove is slidably connected to the semicircular plate. A fixing groove is provided on the side of the surface of the first connecting tube away from the semicircular groove, and the tops of the semicircular grooves of the fixing groove are arranged together, and the inner wall of the fixing groove is rotatably sleeved on the surface of the semicircular plate.
8. The nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 7, characterized in that: A fixing rod is inserted and slidably penetrated through the bottom of the rotating ring, a rectangular plate is slidably sleeved on the surface of the fixing rod, and one side of the rectangular plate is fixedly connected to the surface of the first connecting tube close to the fixing groove.
9. A nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 8, characterized in that: A fourth spring is sleeved on the surface of the fixed rod, one end of the fourth spring is fixedly connected to the bottom of the fixed rod, and one end of the fourth spring close to the fixed rod is fixedly connected to the bottom of the rotating ring.
10. A nucleation device for preparing lithium iron phosphate by a high temperature solid phase method according to claim 9, characterized in that: The surface of the rotating ring is provided with a heat preservation belt, and the heat preservation belt is provided at the connection between the first connecting tube and the second connecting tube.