Unmanned preparation system, method, equipment and medium of high-flux molecular sieve

Abstract

The invention discloses an unmanned preparation system, method and equipment for a high-flux molecular sieve and a medium, and the system comprises a gel preparation module which is used for executing gel preparation operation; the hydrothermal crystallization module is used for executing hydrothermal crystallization operation; the centrifugal curing module is used for executing centrifugal curing operation; the central control module is used for performing instruction control, working parameter setting and state data display on the gel preparation module, the hydrothermal crystallization module and the centrifugal curing module; the composite robot module is used for transferring a molecular sieve synthetic material among the gel preparation module, the hydrothermal crystallization module and the centrifugal curing module; according to the invention, unmanned automatic operation of the whole molecular sieve preparation process based on the hydrothermal synthesis process can be realized, accurate execution of the process flow is realized through logic cooperation among automation equipment, working parameters and a formula of each process link are independently adjustable, the working state and the station condition of each link can be monitored and displayed in real time, and the working efficiency is improved. And the preparation precision, quality and efficiency of the molecular sieve material are improved.

Description

Technical Field

[0001] The present invention relates to the technical field of molecular sieve preparation, and in particular to an unmanned preparation system, method, equipment and medium for high-throughput molecular sieve. Background Art

[0002] Molecular sieve is a synthetic aluminosilicate, a water and acid crystal with a porous skeleton. Due to its unique microporous structure and ionic adsorption characteristics, it is widely used in petrochemical, natural gas, refrigeration, food and other fields. The preparation process of molecular sieve involves a complex synthesis process, which needs to be carried out under conditions such as high temperature and high pressure.

[0003] The existing artificial preparation scheme of molecular sieves usually includes the steps of raw material selection, mixing, molding, crystallization, etc. The raw materials are generally silicon source, aluminum source, template agent and alkali source, etc. After mixing in a specific ratio, crystallization reaction is carried out under suitable conditions to form molecular sieve crystals with regular pore structure. The crystallized product needs to be washed, dried and calcined to obtain the final molecular sieve product.

[0004] Although molecular sieves have broad application prospects in many fields, a series of technical and process challenges may be encountered in the process of artificial preparation of molecular sieves, which may affect the quality and performance of the final product, as follows: (1) Raw material selection and ratio issues: The preparation of molecular sieves requires specific raw materials, such as silicon source, aluminum source, template and alkali source. The quality and ratio of these raw materials directly affect the structure and performance of the final product. If the raw material quality does not meet the standards or the manual operation leads to inaccurate and unreasonable ratios, it may lead to incomplete crystallization, structural defects or performance degradation.

[0005] (2) Problems in controlling synthesis conditions: The synthesis process of molecular sieves needs to be carried out under specific conditions such as temperature, pressure and pH value. However, in actual operation, these conditions may be difficult to accurately control due to equipment limitations, manual operation errors or environmental factors, which may ultimately lead to slow crystallization rate, uneven structure or substandard product performance.

[0006] (3) Crystallization process control issues: Crystallization is a key step in the preparation of molecular sieves, involving complex chemical reactions and phase change processes. During this operation, the control of crystallization time, the fluctuation of crystallization temperature, and the uniformity of stirring and mixing may affect the growth of crystals and the structure of the final product. If precise control effects cannot be achieved, it may lead to inconsistent crystal size, irregular pore structure or low product purity.

[0007] (4) Environmental and safety issues: The preparation process of molecular sieves may produce pollutants such as wastewater, waste gas and solid waste. Improper treatment of these pollutants may cause harm to the environment. At the same time, some raw materials and reaction conditions may be dangerous, which may easily cause environmental pollution and pose health risks to operators.

[0008] (5) Cost and efficiency issues: The preparation process of molecular sieves involves complex processes and expensive raw materials, resulting in high preparation costs. At the same time, preparation efficiency may be affected by many factors, such as equipment performance, manual operation proficiency and raw material utilization. This will undoubtedly increase production costs and reduce market competitiveness. Summary of the invention

[0009] The object of the present invention is to provide an unmanned preparation system, method, equipment and medium for high-throughput molecular sieves, thereby solving all or one of the above-mentioned problems existing in the prior art.

[0010] In order to solve the above technical problems, the specific technical solutions of the present invention are as follows: In one aspect, the present invention provides an unmanned preparation system for high-throughput molecular sieves, comprising: A gel preparation module is used to perform a gel preparation operation, wherein the gel preparation operation includes: heating and uniformly stirring the molecular sieve synthesis material; during the heating and uniformly stirring, adding a reaction liquid to the molecular sieve synthesis material, and performing a pH test on the molecular sieve synthesis material after adding the reaction liquid; A hydrothermal crystallization module, used to perform a hydrothermal crystallization operation, wherein the hydrothermal crystallization operation comprises: subjecting the molecular sieve synthesis material after the pH test to a hydrothermal crystallization reaction based on heating and stirring; A centrifugal solidification module is used to perform a centrifugal solidification operation, wherein the centrifugal solidification operation includes: performing a finished product preparation process on the molecular sieve synthesis material after the hydrothermal crystallization reaction according to the number of cycles; the finished product preparation process includes: performing a centrifugal balancing process on the molecular sieve synthesis material after the hydrothermal crystallization reaction, performing a centrifugal treatment on the balanced molecular sieve synthesis material after the centrifugal balancing process, performing a waste liquid absorption process on the molecular sieve synthesis material after the centrifugal treatment, and drying the product after the waste liquid absorption process to obtain a finished molecular sieve; A central control module, used for command control, working parameter setting and status data display of the gel preparation module, the hydrothermal crystallization module and the centrifugal curing module; The composite robot module is used to transfer the molecular sieve synthesis material between the gel preparation module, the hydrothermal crystallization module and the centrifugal solidification module.

[0011] As an improved solution, the composite robot module is also used to store the molecular sieve synthesis material using a reaction liner; The composite robot module is also used to store a plurality of the reaction liners using a liner fixture; The reaction liner is provided with a QR code storing the reaction liner information.

[0012] As an improved solution, the gel preparation module is also used to scan the reaction liner containing the molecular sieve synthesis material before performing the gel preparation operation; The hydrothermal crystallization module is also used to scan the reaction liner containing the molecular sieve synthesis material before performing the hydrothermal crystallization operation; The centrifugal solidification module is also used to scan the reaction liner containing the molecular sieve synthesis material before performing the centrifugal solidification operation.

[0013] As an improved solution, the gel preparation module includes: a liquid aspiration unit for gel preparation, a pH testing unit for gel preparation, and a cleaning unit for gel preparation; The liquid aspiration unit for preparing the gel is used to aspirate the liquid to be added as the reaction liquid during the heating and uniform stirring, and to add the aspirated liquid to be added into the reaction liner containing the molecular sieve synthesis material; The pH test unit for gel preparation is used to perform pH calibration using a standard solution, and to test and record the pH value of the molecular sieve synthesis material in the reaction liner after the pH calibration; The gel preparation cleaning unit is used to clean the liquid injection pipette of the gel preparation liquid pipetting unit and the sensor of the gel preparation pH testing unit.

[0014] As an improved solution, the centrifugal solidification module includes: a centrifugal unit, a centrifugal solidification transport unit and a centrifugal solidification liquid adding unit; The centrifugal balancing process is achieved by the cooperation of the centrifugal solidification transport unit and the centrifugal solidification liquid adding unit, and includes: The centrifugal solidification transport unit is used to place the reaction liner containing the molecular sieve synthesis material after the hydrothermal crystallization reaction into the centrifugal unit; when there is a vacancy in the centrifugal unit, the centrifugal solidification transport unit adds an empty liner to the vacancy in the centrifugal unit, and controls the empty liner to be symmetrically placed with the reaction liner; The liquid adding unit for centrifugal solidification is used to add liquid to balance the solution in the reaction lining according to the liquid level value of the molecular sieve synthesis material in the reaction lining, and control the liquid level in the reaction lining in the centrifugal unit to be consistent.

[0015] As an improved solution, the central control module is also used to set a functional operation interface including a gel preparation station control page, a hydrothermal crystallization station control page, a centrifugal solidification station control page and a working status page; The central control module is further used to respectively set the working parameters of the gel preparation module, the hydrothermal crystallization module and the centrifugal curing module through the gel preparation station control page, the hydrothermal crystallization station control page and the centrifugal curing station control page; The central control module is also used to display the status parameters of the gel preparation module, the hydrothermal crystallization module and the centrifugal curing module through the working status page.

[0016] As an improved solution, the composite robot module includes: a plurality of AGV composite robots; Each of the AGV compound robots is equipped with a multi-axis manipulator, and the multi-axis manipulator is equipped with a visual guidance system and an electric gripper.

[0017] On the other hand, the present invention also provides an unmanned preparation method of a high-throughput molecular sieve, comprising the following steps: Gel preparation steps: The molecular sieve synthesis material is heated and stirred at a uniform speed; during the heating and stirring, a reaction liquid is added to the molecular sieve synthesis material, and after the reaction liquid is added, a pH test of the molecular sieve synthesis material is performed; Hydrothermal crystallization steps: The molecular sieve synthesis material after the pH test is subjected to a hydrothermal crystallization reaction based on heating and stirring; Centrifugal solidification steps: The molecular sieve synthesis material after the hydrothermal crystallization reaction is subjected to a finished product preparation process according to the number of cycles; the finished product preparation process comprises: performing a centrifugal balancing process on the molecular sieve synthesis material after the hydrothermal crystallization reaction, performing a centrifugal treatment on the balanced molecular sieve synthesis material after the centrifugal balancing process, performing a waste liquid absorption process on the molecular sieve synthesis material after the centrifugal treatment, and drying the product after the waste liquid absorption process to obtain a finished molecular sieve; Status display steps: Displaying the status data of the gel preparation step, the hydrothermal crystallization step, and the centrifugal solidification step; A composite robot module is used to transfer the molecular sieve synthesis material between the gel preparation step, the hydrothermal crystallization step and the centrifugal solidification step.

[0018] On the other hand, the present invention also provides a computer-readable storage medium having a computer program stored thereon, and when the computer program is executed by a processor, the steps of the unmanned preparation method of the high-throughput molecular sieve are implemented.

[0019] On the other hand, the present invention further provides a computer device, comprising a processor, a communication interface, a memory and a communication bus, wherein the processor, the communication interface and the memory communicate with each other via the communication bus; wherein: The memory is used to store computer programs; The processor is used to execute the steps of the unmanned preparation method of the high-throughput molecular sieve by running the program stored in the memory.

[0020] The beneficial effects of the technical solution of the present invention are: 1. The unmanned preparation system of the high-throughput molecular sieve described in the present invention can realize unmanned automatic operation of the entire process of molecular sieve preparation based on the hydrothermal synthesis process through the mutual cooperation of system modules. The entire process does not require human participation, and the precise execution of the process flow is achieved through the logical cooperation between automated equipment. The working parameters and formula of each process link are independently adjustable, and the working status and workstation conditions of each link can be monitored and displayed in real time. Finally, the molecular sieve material is synthesized in a multi-channel parallel manner, which improves the preparation accuracy, quality and efficiency of the molecular sieve material, makes up for the defects of the existing technology, and has extremely high application value.

[0021] 2. The unmanned preparation method of the high-throughput molecular sieve described in the present invention can call the system modules in an orderly manner, thereby realizing the system logic of the unmanned preparation system of the high-throughput molecular sieve described in the present invention.

[0022] 3. The computer-readable storage medium described in the present invention can realize the cooperation of the guidance system module, thereby realizing the unmanned preparation method of the high-throughput molecular sieve described in the present invention, and the computer-readable storage medium described in the present invention also effectively improves the operability of the unmanned preparation method of the high-throughput molecular sieve.

[0023] 4. The computer device described in the present invention can store and execute the computer-readable storage medium, thereby realizing the unmanned preparation method of the high-throughput molecular sieve described in the present invention. BRIEF DESCRIPTION OF THE DRAWINGS

[0024] In order to more clearly illustrate the specific implementation methods of the present invention or the technical solutions in the prior art, the drawings required for use in the specific implementation methods or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are some implementation methods of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative work.

[0025] Figure 1 Schematic diagram of the architecture of the unmanned preparation system of high-throughput molecular sieve according to Example 1 of the present invention; Figure 2 It is a schematic diagram of the actual architecture of the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Figure 3 It is a schematic diagram of the three-dimensional structure of the lining fixture in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Figure 4 1 is a schematic diagram of the top view of the gel preparation module in the unmanned preparation system for high-throughput molecular sieves according to Example 1 of the present invention; Figure 5 is a schematic diagram of the top view of the first workbench in the gel preparation module in the unmanned preparation system for high-throughput molecular sieves described in Example 1 of the present invention; Figure 6 It is a schematic diagram of the three-dimensional structure of the first twin module in the gel preparation module in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Figure 7 It is a schematic diagram of the three-dimensional structure of the heating unit for gel preparation in the gel preparation module in the unmanned preparation system for high-throughput molecular sieves described in Example 1 of the present invention; Figure 8 1 is a schematic diagram of the top view of the hydrothermal crystallization module in the unmanned preparation system of the high-throughput molecular sieve according to Example 1 of the present invention; Fig. 9 is a front view structural schematic diagram of the hydrothermal crystallization module in the unmanned preparation system of the high-throughput molecular sieve according to Example 1 of the present invention; Fig.10 It is a schematic diagram of the three-dimensional structure of the hydrothermal crystallization reaction unit in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Fig.11 It is a schematic diagram of the three-dimensional structure of the ceiling rail in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Fig.12 1 is a schematic diagram of the top view of the centrifugal solidification module in the unmanned preparation system of the high-throughput molecular sieve according to Example 1 of the present invention; Fig.13It is a schematic diagram of the three-dimensional structure of the centrifugal solidification module in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Fig.14 It is a schematic diagram of the three-dimensional structure at the third workbench in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Fig.15 3. It is a schematic diagram of the three-dimensional structure of the ground rail in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Fig.16 It is a schematic diagram of the three-dimensional structure of the AGV composite robot in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Fig.17 It is a schematic diagram of the main interface of the central control module in the unmanned preparation system of the high-throughput molecular sieve described in Example 1 of the present invention; Fig.18 It is a schematic diagram of the main interface of the central control module at another position in the unmanned preparation system of the high-throughput molecular sieve according to Example 1 of the present invention; Fig.19 1 is a schematic diagram of the process of the unmanned preparation method of the high-throughput molecular sieve according to Example 2 of the present invention; Fig. 20 is a schematic diagram of the structure of the computer device described in Example 4 of the present invention; The symbols in the accompanying drawings are explained as follows: 1. First workbench; 2. First transparent protective cover; 3. Temporary storage table for gel preparation; 4. First X-axis linear module; 5. Y-axis linear module; 6. pH test unit for gel preparation; 7. Liquid aspiration unit for gel preparation; 8. Handling unit for gel preparation; 9. Second X-axis linear module; 10. Lifting cylinder; 11. Heating lifting bracket; 12. Solution box assembly; 13. Heating unit for gel preparation; 14. Plunger pump; 15. Lining to be processed; 16. Tray; 17. Lining slot tray; 18. Lining sensor; 19. Rotating downward pressure cylinder; 20. Stirring unit for gel preparation; 55. Mounting parts; 21. Temporary storage table for hydrothermal crystallization; 22. Transport unit for hydrothermal crystallization; 23. Reaction unit for hydrothermal crystallization; 24. Second workbench; 25. Equipment frame; 26. Reactor pressing mechanism; 27. Reactor telescopic mechanism; 28. Reactor mechanism; 29. ​​Fourth X-axis linear module; 30. Equipment fence; 31. Display touch screen operation interface; 32. Material discharge entrance; 33. Safety grating; 34. Personnel entrance and exit door; 35. Temporary storage table for centrifugal curing; 36. Temporary storage table for finished product unloading; 37. Transport unit for centrifugal curing; 38. Third workbench; 39. Second twin module; 40. Liquid adding unit for centrifugal curing; 41. Waste liquid suction mechanism; 42. Centrifuge; 43. Drying treatment unit; 44. Ultrasonic cleaning unit; 45. Stirring unit for centrifugal curing; 46. Lining bracket; 47. Ground rail; 48. Second transparent protective cover; 49. AGV composite robot; 50. Six-axis manipulator for robot; 51. Visual camera; 52. Electric gripper; 53. Automatic wireless charging station; 54. AGV track; 1501, processor; 1502, communication interface; 1503, memory; 1504, communication bus. DETAILED DESCRIPTION

[0026] The preferred embodiments of the present invention are described in detail below in conjunction with the accompanying drawings so that the advantages and features of the present invention can be more easily understood by those skilled in the art, thereby making a clearer and more definite definition of the protection scope of the present invention.

[0027] In the description of the present invention, it should be noted that the embodiments described in the present invention are only part of the embodiments of the present invention, rather than all of the embodiments; based on the embodiments in the present invention, all other embodiments obtained by ordinary technicians in the field without making creative work are within the scope of protection of the present invention.

[0028] The terms "first", "second", etc. in the specification and claims of this article and the above-mentioned drawings are used to distinguish similar objects, and are not necessarily used to describe a specific order or sequence. It should be understood that the data used in this way can be interchanged where appropriate, so that the embodiments of this article described here can be implemented in an order other than those illustrated or described here. In addition, the terms "including" and "having" and any variations thereof are intended to cover non-exclusive inclusions, for example, a process, method, device, product or equipment that includes a series of steps or units is not necessarily limited to those steps or units clearly listed, but may include other steps or units that are not clearly listed or inherent to these processes, methods, products or equipment.

[0029] Example 1: This example provides an unmanned preparation system for high-throughput molecular sieves, such as Figure 1 to Figure 18 As shown, it includes: gel preparation module, hydrothermal crystallization module, centrifugal curing module, central control module and composite robot module. The functional logic and architecture description of the above modules are as follows: Gel Preparation Module: The module is composed of a gel preparation temporary storage table 3, a gel preparation transport unit 8, a gel preparation code scanning unit, a gel preparation heating unit 13, a gel preparation stirring unit 20, a gel preparation liquid absorption unit 7, a gel preparation pH testing unit 6 and a gel preparation cleaning unit; wherein, the gel preparation transport unit 8 adopts a four-axis robot; the gel preparation code scanning unit is installed on the four-axis robot; the gel preparation liquid absorption unit 7 adopts 8 groups of liquid injection pipettes driven by 8 groups of plunger pumps 14 respectively and a first solution box for storing liquid to be added; the gel preparation pH testing unit 6 adopts eight groups of pH value test sensors and a second solution box for storing standard solution; the first solution box and the second solution box are adjacent to each other to form a whole solution box assembly 12.

[0030] Specifically, Figure 4~Figure 7 As shown, the gel preparation module is an integrated module, which is equipped with a first workbench 1 for carrying the above-mentioned units. The above-mentioned units are all installed in the first workbench 1 and are covered by a first transparent protective cover 2 on the first workbench 1. The gel preparation temporary storage table 3 is arranged outside the first workbench 1; a first twin module is arranged on the first workbench 1, and the first twin module is composed of a first X-axis linear module 4 and two Y-axis linear modules 5 slidably installed on the first X-axis linear module 4; a pH test unit 6 for gel preparation is arranged on the Y-axis linear module 5 at one end, and a liquid suction unit 7 for gel preparation and a handling unit 8 for gel preparation are arranged on the Y-axis linear module 5 at the other end; a second X-axis linear module 9 is arranged on one side of the first twin module, which is lower than the first twin module, and a lifting cylinder 10 arranged parallel to the Y-axis direction is arranged on the second X-axis linear module 9, and the piston of the lifting cylinder 10 A heating lifting bracket 11 is installed at the end of the rod; the gel preparation temporary storage table 3 and the solution box assembly 12 are respectively arranged on both sides of the second X-axis linear module 9, and the gel preparation heating unit 13 is arranged on the heating lifting bracket 11; the gel preparation stirring unit 20 is fixed on the first workbench 1 and is located above the gel preparation heating unit 13; the gel preparation cleaning unit can be arranged at a position close to the first twin module; through the design of the first twin module, the gel preparation pH test unit 6, the gel preparation liquid absorption unit 7 and the gel preparation conveying unit 8 can be driven to move freely and flexibly in the X-axis direction and the Y-axis direction, achieving a precise and stable control effect, ensuring the position accuracy and the subsequent high customization flexibility; the second X-axis linear module 9 and the lifting cylinder 10 can control the gel preparation heating unit 13 and the gel preparation stirring unit 20 to align; in this embodiment, Figure 3As shown, the material to be processed is 24 liners 15 to be processed (i.e., reaction liners), and each of the liners 15 to be processed contains reaction materials for synthesizing molecular sieves; the liners 15 to be processed are stored by a liner jig, and the liners 15 to be processed are provided with a two-dimensional code storing independent number information; the liner jig is composed of a tray 16 and a liner slot tray 17 arranged on the tray 16, and the liner slot tray 17 is provided with 24 liner slots, distributed in 3*8, and a gap is provided between the liner slot tray 17 and the tray 16, and both sides of the liner slot tray 17 are installed on the tray 16 by mounting parts 55, and the upper surface of the tray 16 is provided with an independent The lining sensor 18 detects the lining one by one and monitors the online status of the lining in real time; in addition, a rotating downward pressure cylinder 19 is added between the two sides of the lining slot disk 17 and the mounting part 55 to lock the lining slot disk 17 to ensure the stability and parallelism of the lining; in addition, in order to achieve higher operating efficiency, the heating unit 13 for gel preparation has 24 heating slots corresponding to and arranged in the same manner as the lining jig, and the stirring unit 20 for gel preparation has 24 stirring heads corresponding to and arranged in the same manner as the lining jig; the 8 groups of liquid injection pipettes of the liquid pipetting unit 7 for gel preparation are arranged side by side, which is the same as the arrangement of 8 liners in one column of the lining jig.

[0031] Specifically, the operation logic of the gel preparation module is as follows: (1) The composite robot module places the lining jig to be processed into the gel preparation temporary storage table 3; (2) The four-axis manipulator, under the mobile control of the first twin modules, controls the scanning unit for gel preparation to scan the liner in the liner fixture, and then the four-axis manipulator moves the liner into the heating unit for gel preparation 13 for heating treatment; (3) The heating unit 13 for gel preparation, driven by the second X-axis linear module 9, supports the scanned liner and moves to the bottom of the stirring unit 20 for gel preparation. At this time, the heating unit 13 for gel preparation moves upward under the drive of the lifting cylinder 10, so that the stirring end of the stirring unit 20 for gel preparation penetrates into the liner to stir the reaction materials in the multiple groups of liners at a uniform speed. (4) The gel preparation liquid suction unit 7, under the control of the movement of the first twin module, controls its eight groups of liquid injection pipettes to suck a fixed amount of liquid to be added from the first solution box, and the gel preparation liquid suction unit 7 moves to the gel preparation stirring unit 20, and adds the liquid to be added to the solution in the inner liner being stirred; after adding the liquid, it returns to the gel preparation cleaning unit; the gel preparation cleaning unit cleans the liquid injection pipette, and the gel preparation liquid suction unit 7 is reset after its liquid injection pipette is cleaned; (5) The pH test unit 6 for gel preparation extends its sensor into the second solution box and performs pH calibration using a standard solution; after calibration, the heating unit 13 for gel preparation, which is waiting for stirring to be completed, moves the liner to the vicinity of the second solution box under the drive of the second X-axis linear module 9; then the pH test unit 6 for gel preparation extends its sensor into the liner to measure the corresponding pH value and record it; after recording, the pH test unit moves its sensor to the cleaning unit for gel preparation; the cleaning unit for gel preparation cleans the sensor; (6) After completing the above process, the heating unit 13 for gel preparation is driven by the second X-axis linear module 9 to move the liner to the starting point. At this time, the liner in the heating unit 13 for gel preparation is moved into the liner jig on the gel preparation temporary storage table 3 by the four-axis manipulator; then the composite robot module moves the liner jig to the next process point.

[0032] Hydrothermal crystallization module: The module is composed of a hydrothermal crystallization temporary storage table 21, a hydrothermal crystallization code scanning unit, a hydrothermal crystallization transport unit 22 and a hydrothermal crystallization reaction unit 23; wherein, the hydrothermal crystallization transport unit 22 adopts a six-axis robot, and the hydrothermal crystallization code scanning unit is installed on the six-axis robot; the hydrothermal crystallization reaction unit 23 is composed of a reactor mechanism 28, a reactor telescopic mechanism 27 and a reactor pressing mechanism 26.

[0033] Specifically, Figure 8~Figure 11As shown, the reaction unit 23 for hydrothermal crystallization is an integrated device, which is also provided with a second workbench 24, on which a reactor mechanism 28, a reactor telescopic mechanism 27 and a reactor pressing mechanism 26 are respectively arranged, and the hydrothermal crystallization temporary storage table 21 is arranged outside the second workbench 24; an equipment frame 25 is provided on the second workbench 24, and the reactor pressing mechanism 26 can be lifted and lowered in the equipment frame 25 and is located at the top of the equipment frame 25; a feeding port is provided on the equipment frame 25 corresponding to the feeding position of the reactor mechanism 28, the reactor telescopic mechanism 27 adopts a third X-axis linear module, and the third X-axis linear module is arranged corresponding to the feeding port, the reactor mechanism 28 is arranged on the third X-axis linear module and is located below the reactor pressing mechanism 26, and the reactor pressing mechanism 26 is translated along the X-axis direction under the drive of the third X-axis linear module; in addition, a ceiling rail is set at the position above the third X-axis linear module, and the ceiling rail is the fourth X-axis linear module. 29, a six-axis manipulator is arranged on the overhead rail, and a fourth X-axis linear module 29 is arranged perpendicular to the third X-axis linear module in the horizontal direction; in this embodiment, three hydrothermal crystallization reaction units 23 can be arranged under one overhead rail to complete the high-throughput crystallization task; in order to ensure the safety of the entire operation, an equipment fence 30 is arranged between the hydrothermal crystallization module and the moving area of ​​the composite robot module. The equipment fence 30 is constructed with a profile acrylic cover plate, and a display touch screen operation interface 31 is also embedded on the equipment fence 30 to facilitate manual operation; a material discharge entrance 32 for avoiding the manipulator of the composite robot module is opened on the equipment fence 30, and a safety grating 33 is installed at the material discharge entrance 32, thereby restricting the equipment from starting under unsafe conditions; a personnel passage entrance is also opened on the equipment fence 30, and a personnel access door 34 is installed at the personnel passage entrance, and a safety door lock is provided on the personnel access door 34 to ensure that the equipment cannot be started after the personnel enter the area, thereby protecting the safety of the personnel.

[0034] Specifically, the operating logic of the hydrothermal crystallization module is as follows: (1) The composite robot module places the lining fixture processed by the gel preparation module into the hydrothermal crystallization temporary storage table 21; (2) The hydrothermal crystallization transport unit 22, driven by the overhead rail, scans the lining in the lining fixture on the hydrothermal crystallization temporary storage table 21 and then transports it into the reactor mechanism 28 of the hydrothermal crystallization reaction unit 23; (3) The reactor telescopic mechanism 27 moves the reactor mechanism 28 to the inside of the machine; then the reactor pressing mechanism 26 presses down and seals the reactor mechanism 28 through the gas-liquid booster cylinder; after the sealing is completed, the reactor mechanism 28 starts heating and stirs the solution in the lining until the reaction is completed; after completion, the reactor telescopic mechanism 27 moves the reactor mechanism 28 to the outside of the machine; (4) After completing the above process, the hydrothermal crystallization transport unit 22 moves the lining of the reactor mechanism 28 to the lining fixture of the temporary storage table; then the composite robot module transports the lining fixture to the next process point.

[0035] Centrifugal curing module: This module is composed of a temporary storage table 35 for centrifugal curing, a temporary storage table 36 for finished product unloading, a conveying unit 37 for centrifugal curing, a code scanning unit for centrifugal curing, a centrifugal unit, a liquid level detection unit, a liquid adding unit 40 for centrifugal curing, a stirring unit 45 for centrifugal curing, an ultrasonic cleaning unit 44, a waste liquid suction unit and a drying treatment unit 43; wherein, the conveying unit 37 for centrifugal curing adopts a six-axis manipulator, and the code scanning unit for centrifugal curing is installed on the conveying unit 37 for centrifugal curing; the centrifugal unit adopts a centrifuge 42; the ultrasonic cleaning unit 44 adopts an ultrasonic cleaning machine; the liquid level detection unit adopts an inner lining liquid level sensor; the liquid adding unit 40 for centrifugal curing is provided with a liquid adding head; the waste liquid suction unit adopts a waste liquid suction mechanism 41 and a waste liquid collection container.

[0036] Specifically, Figure 12~Figure 15 As shown, a third workbench 38 is also provided in the centrifugal curing transport unit 37, on which a second twin module 39 is provided, and a liquid adding unit 40 for centrifugal curing and a waste liquid suction mechanism 41 are respectively installed on the two Y-axis linear modules 5 of the second twin module 39; a centrifuge 42 is arranged on one side of the second twin module 39 and close to the waste liquid suction mechanism 41; a drying treatment unit 43 is arranged on one side of the centrifuge 42; an ultrasonic cleaning unit 44 is arranged between the drying treatment unit 43 and the centrifuge 42; a stirring unit 45 for centrifugal curing is installed on the third workbench 38 in a liftable manner and is located above the centrifuge 42; a liner bracket 46 for placing an empty liner is also provided on the third workbench 38; a ground rail 47 is arranged on one side of the third workbench 38 close to the drying treatment unit 43, and the ground rail 47 is also an X-axis linear module. , an X-axis linear module is arranged parallel to the second twin module 39, and a six-axis manipulator is installed on the ground rail 47, and is driven by its X-axis linear module to perform a translational movement; a temporary storage table 35 for centrifugal curing and a temporary storage table 36 for finished product unloading are respectively arranged outside the third workbench 38; in order to ensure stability, the bracket of the ground rail 47 is composed of thickened steel plates welded together, and is connected to the ground through eight sets of connecting feet to enhance the balance of the manipulator's movement; in this embodiment, the twin modules, the ceiling rail and the ground rail 47 all adopt a double guide rail design, thereby ensuring smooth and precise movement; in addition, in order to improve operational safety, a second transparent protective cover 48 is provided on the entire third workbench 38; along the outer periphery of the front surface of the third workbench 38, an equipment fence 30 surrounding the entire ground rail 47 is provided, and the structural design of this equipment fence 30 is the same as the equipment fence 30 of the hydrothermal crystallization module.

[0037] Specifically, the operation logic of the centrifugal curing module is as follows: (1) The composite robot module places the lining fixture processed by the hydrothermal crystallization module into a temporary storage table 35 for centrifugal curing; (2) The centrifugal solidification transport unit 37, under the control of the movement of the ground rail 47, uses the centrifugal solidification scanning unit to scan the liner in the liner fixture of the centrifugal solidification temporary storage table 35; after scanning, the liner is moved into the centrifugal unit, and the balance of the liner in the centrifugal unit is judged. If there is a vacancy in the centrifugal unit, the empty liner on the liner bracket 46 is grabbed and added to the vacancy in the centrifuge 42, thereby maintaining the symmetrical placement of the liner 15 to be processed in the centrifuge 42, maintaining the balance of the number of liners, and ensuring the centrifugal effect; (3) A liquid adding unit 40 for centrifugal solidification detects the liquid level value of the inner liner 15 to be treated in the centrifugal unit through a liquid level detection unit. The liquid adding unit 40 for centrifugal solidification controls the liquid adding head to add liquid to the inner liner according to the height value to make the liquid level in the inner liner of the centrifugal unit consistent, thereby ensuring the balance of the centrifugal unit; (4) The stirring unit 45 for centrifugal curing, after the above-mentioned balancing operation, moves its stirring head to the inner liner in the centrifugal unit for stirring; after stirring, the stirring unit 45 for centrifugal curing moves to the ultrasonic cleaning unit 44 for cleaning the stirring head; at this time, the centrifugal unit simultaneously centrifuges the inner liner after stirring; (5) a waste liquid suction unit, which moves to the inner liner of the centrifugal unit to suck the supernatant into the waste liquid collection container after the centrifugal treatment is completed and the centrifugal unit stops rotating, thereby completing one centrifugal operation; (6) The liquid adding unit 40 for centrifugal solidification, after the above-mentioned centrifugal operation, cooperates with the liquid level detection unit to add liquid to the liner for leveling, and then the stirring unit 45 for centrifugal solidification, the centrifugal unit and the waste liquid suction unit perform the same stirring, centrifugal and supernatant suction operations again; in this module, "liquid adding and leveling → stirring → ultrasonic cleaning → centrifugation → supernatant suction" is executed cyclically according to the preset number of cycles; (7) After the above-mentioned cycle operation is completed, the liquid adding unit 40 for centrifugal solidification sucks the semi-finished product in the liner into the material tray of the drying processing unit 43 through its liquid adding head; at this time, the drying processing unit 43 heats and dries the semi-finished product put in; (8) After the drying unit 43 completes the drying process for a preset time and temperature, the centrifugal solidification transport unit 37 grabs the material tray of the drying unit 43 and places it in the finished product unloading temporary storage table 36.

[0038] Composite robot module: The module, such as Fig.16As shown, it is mainly used to autonomously complete the transfer of samples (i.e., linings and lining fixtures) between the above modules and the corresponding physical operations of each module according to the experimental process; the composite machine module is composed of multiple AGV composite robots 49; the AGV composite robot 49 is equipped with a robot six-axis manipulator 50, the six-axis manipulator has a load of 12 kg and an arm span of 1300 mm; the end of the six-axis manipulator is equipped with a visual camera 51 (i.e., a visual guidance system) and an electric gripper 52, the visual camera 51 is used to realize the moving coordinate guidance of the six-axis manipulator through target detection technology, The electric gripper 52 is used to grasp the lining fixture; the moving wheels of the AGV compound robot 49 adopt Mecanum wheels; in addition, in order to achieve stable operation of the composite machine module, an AGV ground rail 54 that supports the movement of the AGV compound robot 49 is provided between the above-mentioned modules, and in this system, an automatic wireless charging station 53 for the AGV compound robot 49 is provided; when the AGV compound robot 49 is in a low-battery state, it is automatically recorded and reported, and the AGV compound robot 49 is set to return to the automatic wireless charging station 53 for automatic charging after completing the task first.

[0039] Central control module: This module is mainly for back-end management personnel, and is mainly used to realize the data status display and command interaction between the above modules, to pre-set the experimental process and module working parameters, and to control and intervene in the module operation in the experimental process; this module mainly controls and displays the status of the above modules through the preset function control logic and the corresponding function operation interface, as follows: A. Functional control logic, including: (1) Workstation operation control, including: working status, current work order, detailed information collection and real-time chart generation for the gel preparation station, hydrothermal crystallization station and centrifugal curing station respectively; at the same time, it also supports integrated statistics of the working status of the gel preparation station, hydrothermal crystallization station and centrifugal curing station and the information overview of the three stations.

[0040] (2) Recipe management, including: customizing the order of liquid collection based on the liquid collection area, customizing the dosage of liquid collection based on the upper and lower limits of liquid collection, setting the pipetting volume of each station, setting the temperature of the temperature control module of each station, setting the stirring rate of the stirring module of each station, setting the pressure of the pressure control module of each station, maintaining different liquid collection sequences and different liquid collection volumes as different recipes, supporting recipe modification, deletion and copying, and supporting batch modification of specific parameters.

[0041] (3) Single module management, including: (3.1) Gel preparation module management: pipetting volume setting, pH value setting of pH test gun, stirring rate setting of stirring module, heating temperature setting of heating module; (3.2) Gel preparation area management: separate setting of the location, numbering, and coordinates of the liquid addition area, reagent storage area, and stirring area; (3.3) Crystal heating module management: reactor position, number, coordinate setting; lining number setting; heating module heating temperature, manual cut-off setting; heating sensor acquisition temperature, over-temperature limit setting; pressure sensor automatic pressure relief setting; stirring rate setting of each reactor stirring module; (3.4) Management of solidification and separation module: setting of position number, rotation speed, and number of cycles of centrifuge 42; setting of injection volume of the pipette head; setting of heating temperature of the heating module.

[0042] (4) Report management: historical test data query and statistical analysis.

[0043] (5) Log management: Record the time point of each action, exception, and other operations of each module, and store it locally in TXT text format.

[0044] (6) Data management: set data retention period and clean up expired data; extract commonly used data; support data conversion and classification.

[0045] B. Functional operation interface, including: (1) Login page: Users need to enter their username and password to log in, where they can set their permissions. Administrator users can use all pages of the system, while operator users can only use related operation pages.

[0046] (2) Main interface: Figure 17-18 As shown, the interface displays a menu bar and a central control console; the menu positions in the menu bar include home page, automatic test, single station control, working status, system configuration and historical data; the central control console displays the acupoint utilization rate of gel preparation, hydrothermal crystallization and centrifugal solidification, the specific acupoint status of these three functional steps, and the current operating parameters and temperature change curves of the acupoints.

[0047] (2) Automatic test: Click the automatic test button on the menu bar to jump to the automatic test interface. In this interface, you can set the operating parameters of the three functional steps mentioned above, select the maintained recipe, and quickly fill in the test parameters of the three stations. It also supports starting the test after manual adjustment.

[0048] (3) System configuration: Click System Configuration on the menu bar to jump to the system configuration interface. In this interface, recipe management is supported, that is, configuring the three-station parameters required for the test, and custom naming is supported. After the recipe is pre-configured, it can be directly selected in the automatic test page and the test can be quickly started, such as: setting the stirring time, heating temperature, stirring rate and other general parameters of the gel preparation module, configuring the solution name, selecting the corresponding slot, setting the aspiration volume of each of the 8 pipettes, etc. In addition, the system configuration interface also supports user management, supports configuring the user's login name and password, and setting the corresponding user's page usage permissions.

[0049] (4) Single station control: Click the single station control in the menu bar to jump to the single station control interface. Select any of the three operation stations to make relevant settings, including: gel preparation station control page, hydrothermal crystallization station control page and centrifugal curing station control page, as follows: (4.1) Gel preparation station control page: This page supports manual single-step completion of pH calibration, pH measurement, and pipetting, and can also complete continuous pipetting according to the recipe; (4.2) Hydrothermal crystallization station control page: This page supports the individual control of the stirring rate and temperature of each acupoint. The control can be completed by setting the relevant parameters. In addition, it also supports the pulling, pushing, locking, opening and closing of a single group of reactors; (4.3) Centrifugal curing station control page: This page supports temperature control of the heating plate, which can be controlled by setting relevant parameters; it also supports the setting of finished product aspiration, waste aspiration, adding clean water, cleaning time and centrifugation time of centrifuge 42.

[0050] (5) Working status: Click the working status in the menu bar to jump to the working status interface. In this interface, the status of the three operating stations is displayed separately, as follows: (5.1) Gel preparation station status: digital and graphical display of the heating plate temperature, stirring rate, pH value of the test group and temperature change curve in the gel preparation module; (5.2) Hydrothermal crystallization station status: The current rotation speed and temperature of each acupoint in the hydrothermal crystallization module are displayed digitally and graphically, with the horizontal axis representing the reaction group acupoint number and the vertical axis representing the reaction group number; (5.3) Centrifugal curing station status: The real-time temperature of the heating plate in the centrifugal curing module and the real-time speed of the centrifuge 42 are displayed digitally and graphically. At the same time, the temperature change curve of the heating plate is fitted according to the real-time temperature record of the heating plate, and the speed change curve of the centrifuge 42 is fitted according to the real-time speed of the centrifuge 42.

[0051] (6) Historical data: Click on the historical data button in the menu bar to jump to the historical data interface. In this interface, a data search box is provided. Enter the time or test number in the data search box to query the temperature collection data corresponding to the hydrothermal crystallization stage.

[0052] It should be noted that the above examples are only for explaining the present invention and cannot limit the protection scope of the present invention.

[0053] Example 2, based on the same inventive concept as the unmanned preparation system for high-throughput molecular sieves described in Example 1, this example provides an unmanned preparation method for high-throughput molecular sieves, such as Fig.19 As shown, the following steps are included: S100, gel preparation steps: The molecular sieve synthesis material is heated and stirred at a uniform speed; during the heating and stirring, a reaction liquid is added to the molecular sieve synthesis material, and after the reaction liquid is added, a pH test of the molecular sieve synthesis material is performed; S200, hydrothermal crystallization step: The molecular sieve synthesis material after the pH test is subjected to a hydrothermal crystallization reaction based on heating and stirring; S300, centrifugal curing step: The molecular sieve synthesis material after the hydrothermal crystallization reaction is subjected to a finished product preparation process according to the number of cycles; the finished product preparation process comprises: performing a centrifugal balancing process on the molecular sieve synthesis material after the hydrothermal crystallization reaction, performing a centrifugal treatment on the balanced molecular sieve synthesis material after the centrifugal balancing process, performing a waste liquid absorption process on the molecular sieve synthesis material after the centrifugal treatment, and drying the product after the waste liquid absorption process to obtain a finished molecular sieve; S400, status display steps: Displaying the status data of the gel preparation step, the hydrothermal crystallization step, and the centrifugal solidification step; S500, a composite robot module is used to transfer the molecular sieve synthesis material between the gel preparation step, the hydrothermal crystallization step and the centrifugal solidification step.

[0054] Embodiment 3: This embodiment provides a computer-readable storage medium, including: The storage medium is used to store computer software instructions used to implement the unmanned preparation method for high-throughput molecular sieves described in the above-mentioned Example 2, which includes instructions for executing the above-mentioned program set for the unmanned preparation method for high-throughput molecular sieves; specifically, the executable program can be built into the unmanned preparation system for high-throughput molecular sieves described in Example 1, so that the unmanned preparation system for high-throughput molecular sieves can implement the unmanned preparation method for high-throughput molecular sieves described in Example 2 by executing the built-in executable program.

[0055] In addition, the computer-readable storage medium of this embodiment may adopt any combination of one or more computer-readable storage media, wherein the computer-readable storage medium includes electrical, optical, electromagnetic, infrared or semiconductor systems, devices or components, or any combination thereof.

[0056] Embodiment 4, this embodiment provides an electronic device, such as Fig. 20 As shown, the electronic device may include: a processor 1501 , a communication interface 1502 , a memory 1503 and a communication bus 1504 , wherein the processor 1501 , the communication interface 1502 , and the memory 1503 communicate with each other via the communication bus 1504 .

[0057] Memory 1503, used for storing computer programs; The processor 1501 is used to implement the steps of the unmanned preparation method of high-throughput molecular sieve described in the above embodiment 1 when executing the computer program stored in the memory 1503.

[0058] As an embodiment of the present invention, the communication bus mentioned in the above terminal can be a Peripheral Component Interconnect (PCI) bus or an Extended Industry Standard Architecture (EISA) bus. The communication bus can be divided into an address bus, a data bus, a control bus, etc. For ease of representation, Fig. 20 Only one thick line is used in the diagram, but this does not mean that there is only one bus or only one type of bus.

[0059] As an implementation mode of the present invention, the communication interface is used for communication between the above-mentioned terminal and other devices.

[0060] As an embodiment of the present invention, the memory may include a random access memory (RAM) or a non-volatile memory, such as at least one disk memory. Optionally, the memory may also be at least one storage device located away from the aforementioned processor.

[0061] As an embodiment of the present invention, the above-mentioned processor can be a general-purpose processor, including a central processing unit (CPU), a network processor (NP), etc.; it can also be a digital signal processor (DSP), an application specific integrated circuit (ASIC), a field programmable gate array (FPGA) or other programmable logic devices, discrete gates or transistor logic devices, discrete hardware components.

[0062] Different from the prior art, the unmanned preparation system, method, equipment and medium of a high-throughput molecular sieve of the present application can realize unmanned automatic operation of the entire process of molecular sieve preparation based on the hydrothermal synthesis process. The entire process does not require human participation, and the precise execution of the process flow is achieved through the logical coordination between automated equipment. The working parameters and formula of each process link are independently adjustable, and the working status and workstation conditions of each link can be monitored and displayed in real time. Finally, the molecular sieve material is synthesized in a multi-channel parallel manner, which improves the preparation accuracy, quality and efficiency of the molecular sieve material, makes up for the defects of the prior art, and has extremely high application value.

[0063] It should be understood that in the various embodiments of this document, the size of the serial numbers of the above-mentioned processes does not mean the order of execution. The execution order of each process should be determined by its function and internal logic, and should not constitute any limitation on the implementation process of the embodiments of this document.

[0064] It should also be understood that in the embodiments of this article, the term "and / or" is only a description of the association relationship of the associated objects, indicating that three relationships may exist. For example, A and / or B can represent: A exists alone, A and B exist at the same time, and B exists alone. In addition, the character " / " in this article generally indicates that the associated objects before and after are in an "or" relationship.

[0065] Those of ordinary skill in the art will appreciate that the units and algorithm steps of each example described in conjunction with the embodiments disclosed herein can be implemented in electronic hardware, computer software, or a combination of the two. In order to clearly illustrate the interchangeability of hardware and software, the composition and steps of each example have been generally described in terms of function in the above description. Whether these functions are performed in hardware or software depends on the specific application and design constraints of the technical solution. Professional and technical personnel can use different methods to implement the described functions for each specific application, but such implementation should not be considered to be beyond the scope of this article.

[0066] Those skilled in the art can clearly understand that, for the convenience and brevity of description, the specific logical process of the method described above can refer to the corresponding working processes of the systems, devices and units in the aforementioned method embodiments, and will not be repeated here.

[0067] In the several embodiments provided herein, it should be understood that the disclosed systems, devices and methods can be implemented in other ways. For example, the device embodiments described above are only schematic, for example, the division of the units is only a logical function division, and there may be other division methods in actual implementation, such as multiple units or components can be combined or integrated into another system, or some features can be ignored or not executed. In addition, the mutual coupling or direct coupling or communication connection shown or discussed can be an indirect coupling or communication connection through some interfaces, devices or units, or can be electrical, mechanical or other forms of connection.

[0068] The units described as separate components may or may not be physically separated, and the components shown as units may or may not be physical units, that is, they may be located in one place or distributed on multiple network units. Some or all of the units may be selected according to actual needs to achieve the purpose of the embodiments of this article.

[0069] In addition, each functional unit in each embodiment of this invention may be integrated into one processing unit, or each unit may exist physically separately, or two or more units may be integrated into one unit. The above integrated unit may be implemented in the form of hardware or in the form of software functional unit.

[0070] If the integrated unit is implemented in the form of a software functional unit and sold or used as an independent product, it can be stored in a computer-readable storage medium. Based on this understanding, the technical solution of this article is essentially or the part that contributes to the prior art, or all or part of the technical solution can be embodied in the form of a software product, and the computer software product is stored in a storage medium, including a number of instructions to enable a computer device (which can be a personal computer, a server, or a network device, etc.) to perform all or part of the steps of the method described in each embodiment of this article. The aforementioned storage medium includes: U disk, mobile hard disk, read-only memory (ROM, Read-Only Memory), random access memory (RAM, Random Access Memory), disk or optical disk and other media that can store program codes.

[0071] The above descriptions are merely embodiments of the present invention and are not intended to limit the patent scope of the present invention. Any equivalent structure or equivalent process transformation made using the contents of the present invention specification and drawings, or directly or indirectly applied in other related technical fields, are also included in the patent protection scope of the present invention.

Claims

1. An unmanned preparation system for high-throughput molecular sieves, characterized in that: include: A gel preparation module is used to perform a gel preparation operation, wherein the gel preparation operation includes: heating and uniformly stirring the molecular sieve synthesis material; during the heating and uniformly stirring, adding a reaction liquid to the molecular sieve synthesis material, and performing a pH test on the molecular sieve synthesis material after adding the reaction liquid; A hydrothermal crystallization module, used to perform a hydrothermal crystallization operation, wherein the hydrothermal crystallization operation comprises: subjecting the molecular sieve synthesis material after the pH test to a hydrothermal crystallization reaction based on heating and stirring; A centrifugal solidification module is used to perform a centrifugal solidification operation, wherein the centrifugal solidification operation includes: performing a finished product preparation process on the molecular sieve synthesis material after the hydrothermal crystallization reaction according to the number of cycles; the finished product preparation process includes: performing a centrifugal balancing process on the molecular sieve synthesis material after the hydrothermal crystallization reaction, performing a centrifugal treatment on the balanced molecular sieve synthesis material after the centrifugal balancing process, performing a waste liquid absorption process on the molecular sieve synthesis material after the centrifugal treatment, and drying the product after the waste liquid absorption process to obtain a finished molecular sieve; A central control module, used for command control, working parameter setting and status data display of the gel preparation module, the hydrothermal crystallization module and the centrifugal curing module; The composite robot module is used to transfer the molecular sieve synthesis material between the gel preparation module, the hydrothermal crystallization module and the centrifugal solidification module.

2. The unmanned preparation system for high-throughput molecular sieve according to claim 1, characterized in that: The composite robot module is also used to store the molecular sieve synthesis material using a reaction liner; The composite robot module is also used to store a plurality of the reaction liners using a liner fixture; The reaction liner is provided with a QR code storing the reaction liner information.

3. The unmanned preparation system for high-throughput molecular sieve according to claim 2, characterized in that: The gel preparation module is also used to scan the reaction liner containing the molecular sieve synthesis material before performing the gel preparation operation; The hydrothermal crystallization module is also used to scan the reaction liner containing the molecular sieve synthesis material before performing the hydrothermal crystallization operation; The centrifugal solidification module is also used to scan the reaction liner containing the molecular sieve synthesis material before performing the centrifugal solidification operation.

4. The unmanned preparation system for high-throughput molecular sieve according to claim 2, characterized in that: The gel preparation module comprises: a liquid aspiration unit for gel preparation, a pH testing unit for gel preparation, and a cleaning unit for gel preparation; The liquid aspiration unit for preparing the gel is used to aspirate the liquid to be added as the reaction liquid during the heating and uniform stirring, and to add the aspirated liquid to be added into the reaction liner containing the molecular sieve synthesis material; The pH test unit for gel preparation is used to perform pH calibration using a standard solution, and to test and record the pH value of the molecular sieve synthesis material in the reaction liner after the pH calibration; The gel preparation cleaning unit is used to clean the liquid injection pipette of the gel preparation liquid aspiration unit and the sensor of the gel preparation pH testing unit.

5. The unmanned preparation system for high-throughput molecular sieve according to claim 2, characterized in that: The centrifugal curing module comprises: a centrifugal unit, a centrifugal curing transport unit and a centrifugal curing liquid adding unit; The centrifugal balancing process is achieved by the cooperation of the centrifugal solidification transport unit and the centrifugal solidification liquid adding unit, and includes: The centrifugal solidification transport unit is used to place the reaction liner containing the molecular sieve synthesis material after the hydrothermal crystallization reaction into the centrifugal unit; when there is a vacancy in the centrifugal unit, the centrifugal solidification transport unit adds an empty liner to the vacancy in the centrifugal unit, and controls the empty liner to be symmetrically placed with the reaction liner; The liquid adding unit for centrifugal solidification is used to add liquid to balance the solution in the reaction lining according to the liquid level value of the molecular sieve synthesis material in the reaction lining, and control the liquid level in the reaction lining in the centrifugal unit to be consistent.

6. The unmanned preparation system for high-throughput molecular sieve according to claim 1, characterized in that: The central control module is also used to set a functional operation interface including a gel preparation station control page, a hydrothermal crystallization station control page, a centrifugal curing station control page and a working status page; The central control module is further used to respectively set the working parameters of the gel preparation module, the hydrothermal crystallization module and the centrifugal curing module through the gel preparation station control page, the hydrothermal crystallization station control page and the centrifugal curing station control page; The central control module is also used to display the status parameters of the gel preparation module, the hydrothermal crystallization module and the centrifugal curing module through the working status page.

7. The unmanned preparation system for high-throughput molecular sieve according to claim 2, characterized in that: The composite robot module includes: a plurality of AGV composite robots; Each of the AGV compound robots is equipped with a multi-axis manipulator, and the multi-axis manipulator is equipped with a visual guidance system and an electric gripper.

8. An unmanned preparation method for high-throughput molecular sieves, characterized in that: The following steps are involved: Gel preparation steps: The molecular sieve synthesis material is heated and stirred at a uniform speed; during the heating and stirring, a reaction liquid is added to the molecular sieve synthesis material, and after the reaction liquid is added, a pH test of the molecular sieve synthesis material is performed; Hydrothermal crystallization steps: The molecular sieve synthesis material after the pH test is subjected to a hydrothermal crystallization reaction based on heating and stirring; Centrifugal solidification steps: The molecular sieve synthesis material after the hydrothermal crystallization reaction is subjected to a finished product preparation process according to the number of cycles; The finished product preparation process comprises: performing centrifugal balancing treatment on the molecular sieve synthesis material after the hydrothermal crystallization reaction, centrifuging the balanced molecular sieve synthesis material after the centrifugal balancing treatment, absorbing waste liquid from the molecular sieve synthesis material after the centrifugal treatment, and drying the product after the waste liquid absorption treatment to obtain a finished molecular sieve; Status display steps: Displaying the status data of the gel preparation step, the hydrothermal crystallization step, and the centrifugal solidification step; A composite robot module is used to transfer the molecular sieve synthesis material between the gel preparation step, the hydrothermal crystallization step and the centrifugal solidification step.

9. A computer-readable storage medium, characterized in that: The computer-readable storage medium stores a computer program, and when the computer program is executed by a processor, the steps of the unmanned preparation method of the high-throughput molecular sieve described in claim 8 are implemented.

10. A computer device, characterized in that: It includes a processor, a communication interface, a memory and a communication bus, wherein the processor, the communication interface and the memory communicate with each other through the communication bus; wherein: The memory is used to store computer programs; The processor is used to execute the steps of the unmanned preparation method of high-throughput molecular sieve described in claim 8 by running the program stored in the memory.

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