The invention provides a C60 / CNT composite photocatalytic material as well as a preparation method and application thereof, and belongs to the technical field of photocatalytic materials. The C60 / CNT composite photocatalytic material is prepared from C60 and a
carbon nanotube, the
mass ratio of the C60 to the carbon
nano tube is 0.002 to 0.1; wherein the C60 is coated on the surface of the carbon
nano tube or doped in gaps of the carbon
nano tube. The preparation method of the composite photocatalytic material is simple and rapid, and the obtained C60 / CNT composite photocatalytic material has wide application prospects in the fields of adsorption and
photocatalysis. In the field of
lomefloxacin hydrochloride adsorption, the highest degradation efficiency of the C60 / CNT
composite material with the mC60 / mCNT ratio of 0.2% reaches 87%; in the field of
photocatalytic degradation of
lomefloxacin hydrochloride, mC60 / mCNT is 5% of the C60 / CNT
composite material, and the
photocatalytic degradation efficiency is highest.