Method for improving plasticity of amorphous alloy through supersonic particle bombarding (SPB) technique
A technology of amorphous alloy and particle bombardment, which is applied in the field of amorphous materials, can solve the problems of complex process, high cost, and difficulty in effectively improving the plasticity of amorphous alloys, and achieve the effects of good repeatability, low cost, and less time-consuming
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Embodiment 1
[0025] (1) Preparation of Ti 32.8 Zr 30.2 Ni 5.3 Cu 9 be 22.7 Amorphous alloy plate: five kinds of metal blocks with a purity of ≥99.95% Ti, Zr, Ni, Cu, and Be are mixed according to the atomic percentage of 32.8:30.2:5.3:9:22.7, and then under the protection of a high-purity argon atmosphere , use an electric arc melting furnace to melt, repeat the melting 4 times, and form an alloy ingot. The alloy ingot is melted and poured into a copper mold by a reverse casting method to prepare a Ti-based amorphous alloy plate.
[0026] (2) Preliminary treatment: wire-cut the amorphous alloy plate prepared in step (1) into a size of 22×5×1.8mm 3 block samples.
[0027] (3) Fix the amorphous alloy block sample on the supersonic power spraying equipment.
[0028] (4) Using supersonic power spraying equipment, the compressed gas is N 2 , under the gas pressure of 620KPa, the temperature is selected at 100°C, and Al with an average particle size of 30μm is used 2 o 3 The particles ...
Embodiment 2
[0035] (1) Preliminary treatment: wire-cut the entire amorphous alloy plate prepared in Example 1 into a size of 22×5×1.8mm 3 block samples.
[0036] (3) Fix the amorphous alloy block sample on the supersonic power spraying equipment.
[0037] (4) Using supersonic power spraying equipment, the compressed gas is He, under the gas pressure of 620KPa, the temperature is selected at 150°C, and Al with an average particle size of 40μm is used. 2 o 3 The particles bombard the surface of the amorphous alloy bulk sample for 2.5s.
[0038] (5) After the supersonic particle bombardment is completed, the amorphous alloy block sample is ultrasonically cleaned with acetone.
[0039] Through the analysis of the surface X-ray diffraction pattern of the amorphous alloy bulk sample after bombardment, it can be found that there are sharp crystal peaks distributed in the amorphous diffuse scattering peaks, and the phase retrieval is carried out using the MDI jade software, and the chemical el...
Embodiment 3
[0044] (1) Preliminary treatment: wire-cut the entire amorphous alloy plate prepared in Example 1 into a size of 22×5×1.8mm 3 block samples.
[0045] (3) Fix the amorphous alloy block sample on the supersonic power spraying equipment.
[0046] (4) Using supersonic power spraying equipment, the compressed gas is He, under the gas pressure of 620KPa, the temperature is selected at 200°C, and Al with an average particle size of 50μm is used. 2 o 3 The particles bombard the surface of the amorphous alloy bulk sample for 3s.
[0047] (5) After the supersonic particle bombardment is completed, the amorphous alloy block sample is ultrasonically cleaned with acetone.
[0048] Through the analysis of the surface X-ray diffraction pattern of the amorphous alloy bulk sample after bombardment, it can be found that there are sharp crystal peaks distributed in the amorphous diffuse scattering peaks, and the phase retrieval is carried out using the MDI jade software, and the chemical elem...
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