Monochamus alternatus adult attractant
A technology of pine brown longhorn beetle and attractant, which is applied in the directions of attracting harmful substances, biocides, animal repellents, etc. Set the target specificity is not strong and other problems, to achieve the effect of less effective dosage, low production cost, high efficiency of attracting insects
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Embodiment 1
[0015] 1. Preparation of artificially synthesized complexes
[0016] Add 5 ml of undecanol to the flask, then slowly drop in 10 ml of thionyl chloride, stir, and after standing for 2 hours, add 15 ml of semi-saturated saline, mix, separate the layers, collect the organic layer, and use anhydrous Dry over sodium sulfate, and then remove the solvent with a rotary evaporator to obtain liquid A. Add 10 ml of ethylene glycol to another flask, then slowly add 6 grams of sodium metal, continue heating at 60 °C for 6 hours, cool to room temperature, add 6 ml of A solution to the flask, stir for 2 hours, and heat to 60 °C Stirring was continued for 6 hours, and then a mixed solution of 80 ml semi-saturated saline, 80 ml petroleum ether and 30 ml diethyl ether was added, shaken, separated, and the organic layer was collected. The organic layer was dried over anhydrous sodium sulfate and concentrated to obtain the synthetic compound. The prepared compound was used to carry out the ante...
Embodiment 2
[0036] A kind of synthetic compound of the present invention, its preparation method is as follows:
[0037] Add 50 ml of undecyl alcohol in the flask, then slowly drop into 150 ml of thionyl chloride, stir, and after standing for 3 hours, add 300 ml of semi-saturated saline, mix, separate, collect the organic layer, and use Dry over anhydrous sodium sulfate, remove the solvent to obtain liquid A; add 30 ml of ethylene glycol to another flask, then add 12 grams of sodium metal, continue heating at 70 °C for 2 hours, cool to room temperature, and add dropwise to the flask 24 ml of liquid A, stirred for 5 hours, heated to 50 °C, stirred for 2 hours, then added 200 ml of semi-saturated saline, 200 ml of petroleum ether and 120 ml of diethyl ether, shaken, separated, collected the organic layer, and used anhydrous After drying over sodium sulfate and concentrating, synthetic compound 1 was obtained.
Embodiment 3
[0039] A kind of synthetic compound of the present invention, its preparation method is as follows:
[0040] Add 20 ml of undecanol to the flask, then slowly drop into 40 ml of thionyl chloride, stir, and after standing for 6 hours, add 200 ml of semi-saturated saline, mix, separate, collect the organic layer, and use Dry over sodium sulfate, remove the solvent to obtain liquid A; add 20 ml of ethylene glycol to another flask, then slowly add 8 grams of sodium metal, continue heating at 50 ° C for 6 hours, cool to room temperature, and drop 6 1 ml of liquid A, stirred for 2 hours, heated to 60 °C, stirred for 8 hours, then added 150 ml of semi-saturated saline, 100 ml of petroleum ether and 80 ml of diethyl ether, oscillated, separated, collected the organic layer, the organic layer After drying with anhydrous sodium sulfate and concentrating, synthetic compound 2 was obtained.
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