A wastewater treatment device for phosphorus flame retardant processing
By designing a wastewater treatment device for phosphorus-based flame retardant processing, the problem of poor wastewater treatment quality is solved and efficient wastewater treatment is achieved and efficient treatment of wastewater and Improve environmental protection and improve the safety of the device.
Patent Information
- Application Number
- CN202011163866.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2020-10-27
- Publication Date
- 2024-12-13
- Estimated Expiration
- 2040-10-27
AI Technical Summary
The wastewater generated during the processing of existing phosphorus-based flame retardants has poor quality of treatment, and contains non-toxic liquid and wastewater to treat it uniformly, which affects environmental protection.
A wastewater treatment device including a main body, feed pipe, first water tank, functional box, agitating rod, filter mesh, water pump, heating tube and condenser tube is designed, and the filter mesh separation, evaporation heating and activity are carried out through neutralization, stirring, filter mesh separation, evaporation heating and activity. Coke adsorption and other steps, treat wastewater multiple times, separate non-toxic liquids, and improve treatment quality and environmental protection.
Through multiple treatments, the quality of wastewater treatment is improved, and the non-toxic liquid is separated, which avoids the unified treatment of non-toxic liquid and wastewater, which improves environmental protection, and avoids the risk of misoperation of staff and toxic waste gas leakage through safe design.
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Figure CN112209556B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field related to phosphorus-based flame retardant processing equipment, and in particular to a wastewater treatment device used for phosphorus-based flame retardant processing. Background Art
[0002] As synthetic materials are increasingly used in people's daily lives and national economic construction, the flame retardant treatment of their polymers has attracted more and more attention. Although halogen flame retardants have unparalleled high efficiency compared to other flame retardants, their harm to the environment and people cannot be ignored. In recent years, the research on alkyl phosphinate flame retardants as green and environmentally friendly flame retardants has become one of the hot spots in the development and research of the phosphorus flame retardant industry. The wastewater generated in the production process of phosphorus flame retardants is still harmful to the environment. It is necessary to treat the wastewater before discharging it in a centralized manner. However, the current conventional wastewater treatment equipment simply neutralizes its acidity, collects it in a centralized manner, and then treats it in a unified manner. Due to the poor quality of the pre-treatment of wastewater, the subsequent unified treatment of wastewater is inconvenient, and the wastewater still contains non-toxic liquids. If it is treated as wastewater for unified treatment, it becomes less environmentally friendly. Summary of the invention
[0003] The purpose of the present invention is to solve the shortcomings of the prior art and to propose a wastewater treatment device for phosphorus-based flame retardant processing.
[0004] In order to achieve the above object, the present invention adopts the following technical solutions:
[0005] A wastewater treatment device for phosphorus flame retardant processing, comprising a main body, a feed pipe is fixedly connected to the top of the main body, a first water tank is fixedly connected in the main body, the first water tank is located below the feed pipe, a function box is fixedly connected in the main body, a motor is fixedly connected in the function box, a plurality of stirring rods are rotatably connected in the first water tank, the stirring rods are connected together through a pulley sleeve, the output shaft end of the motor is fixedly connected to one of the plurality of stirring rods, a fixed rod is fixedly connected in the main body, a storage rod is fixedly connected in the fixed rod, the outer wall of the storage rod is hollowed out and the storage rod is located in the first water tank, a first discharge pipe is connected to the bottom of the first water tank, and a fixed rod is fixedly connected in the main body. A second water tank is fixedly connected thereto, the second water tank is located below the first discharge pipe, a filter is fixedly connected therein, a second water tank is connected to a second discharge pipe on one side of the second water tank, a water pump is fixedly connected therein, the second discharge pipe is connected to an output end of the water pump, a third water tank is fixedly connected therein, the second discharge pipe is connected to the second water tank and the third water tank respectively, a partition is fixedly connected therein, a plurality of heating pipes are provided below the partition, a condenser is connected to the top of the third water tank, a second grid plate is fixedly connected therein, activated coke is placed in the second grid plate, a fan is provided at one end of the condenser, and a drain pipe is connected to a section of the condenser close to the fan.
[0006] Preferably, a section of the condenser tube outside the main body is sheathed with a heat-insulating layer, and the drain pipe is located between the heat-insulating layer and the fan.
[0007] Preferably, the stirring rod is made of acid-resistant material.
[0008] Preferably, a first baffle is rotatably connected to the main body, and the first baffle is located at the function box.
[0009] Preferably, the first water tank, the second water tank and the third water tank are all connected to an exhaust pipe, the exhaust pipe is fixedly connected to a first grid plate at the pipe opening outside the main body, active coke is placed in the first grid plate, and a one-way valve is fixedly connected in the exhaust pipe.
[0010] Preferably, the first water trough, the second water trough and the third water trough are all connected with sampling tubes, the sampling tubes are slidably connected to the main body, the sampling tubes are fixedly connected to a connecting plate, the main body is fixedly connected to a fixing plate, the fixing plate is located above the connecting plate, and the fixing plate and the connecting plate are both provided with limiting holes, the limiting holes are slidably connected to a limiting rod, the limiting rod is provided with a limiting groove, the limiting groove is slidably connected to a limiting plate, the sampling tubes are slidably connected to a piston plate, the piston plate is fixedly connected to a connecting rod on one side close to the connecting plate, an opening is provided below the sampling tube, and the outer wall of the main body is provided with three sampling boxes, the three sampling boxes are respectively located below the three sampling tubes.
[0011] Preferably, the fixing rod extends out of the main body, and a knob is rotatably connected to the top of the fixing rod, the storage rod is threadedly connected to the knob, and the storage rod is slidably connected to the fixing rod, a second baffle is provided at the bottom end of the storage rod, and two telescopic rods are fixedly connected between the second baffle and the fixing rod.
[0012] The beneficial effects of the present invention are:
[0013] 1. A wastewater treatment device for phosphorus flame retardant processing proposed by the present invention is provided with a main body. When in use, a soluble trivalent iron salt is placed in the storage rod. The wastewater is now neutralized in the first water tank, and the first step of treatment is performed by stirring and the like, and then the wastewater is discharged into the second water tank. The sediment in the wastewater treated for the first time is separated from the wastewater by a filter screen, and the wastewater is then sent to the third water tank for evaporation and heating by a water pump. The partition is used to collect the concentrated wastewater obtained after heating, and the evaporated gas is discharged through the condenser. The toxic substances are adsorbed by the activated coke in the second grid plate, and the non-toxic condensed water finally formed is discharged from the drain pipe. By treating the wastewater multiple times, the quality of wastewater treatment is improved, and the non-toxic liquid therein is separated and not treated uniformly with the wastewater, thereby improving environmental protection.
[0014] 2. The present invention proposes a wastewater treatment device for the processing of phosphorus-based flame retardants. A sampling tube is provided. When in use, the limit plate and the limit rod are pulled out in turn to release the limit of the sampling tube. The pre-step can avoid accidental operation of the staff. The connecting rod is pulled to press the wastewater into the sampling tube, and then the sampling tube is pulled out to collect the wastewater in a collection box. This makes it convenient for the staff to sample and monitor the wastewater and can avoid safety accidents caused by accidental operation of the staff.
[0015] 3. The present invention proposes a wastewater treatment device for phosphorus-based flame retardant processing. A fixed rod is set and the placement rod is taken out by turning a knob. An elastic member is fixedly connected between the telescopic rod and the fixed rod. During the process of taking out the placement rod, the telescopic rod drives the second baffle to rise, and finally closes the opening under the fixed rod, ensuring that toxic waste gas will not leak when replacing the placement rod filler, thereby improving the safety of the device. BRIEF DESCRIPTION OF THE DRAWINGS
[0016] Figure 1 This is a schematic structural diagram of a wastewater treatment device for phosphorus-based flame retardant processing proposed in Example 1;
[0017] Figure 2 This is a schematic diagram of the structure of a sampling tube of a wastewater treatment device for phosphorus-based flame retardant processing proposed in Example 1;
[0018] Figure 3This is a schematic structural diagram of a limit rod of a wastewater treatment device for phosphorus-based flame retardant processing proposed in Example 1;
[0019] Figure 4 This is a schematic structural diagram of a fixing rod of a wastewater treatment device for processing phosphorus-based flame retardants proposed in Example 2.
[0020] In the figure: 1, main body 2, feed pipe 3, fixing rod 4, storage rod 5, first water tank 6, water pump 7, first grid plate 8, exhaust pipe 9, one-way valve 10, condenser 11, second grid plate 12, insulation layer 13, fan 14, sampling tube 15, third water tank 16, partition 17, heating tube 18, second water tank 19, filter 20, motor 21, first baffle 22, stirring rod 24, piston plate 25, connecting rod 26, connecting plate 27, sampling box 28, limit rod 29, limit plate 30, telescopic rod 31, second baffle 32, knob. DETAILED DESCRIPTION
[0021] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.
[0022] Example 1
[0023] Reference Figure 1-3A wastewater treatment device for phosphorus flame retardant processing, comprising a main body 1, a feed pipe 2 is fixedly connected to the top of the main body 1, a first water tank 5 is fixedly connected to the main body 1, the first water tank 5 is located below the feed pipe 2, a function box is fixedly connected to the main body 1, a motor 20 is fixedly connected to the function box, a plurality of stirring rods 22 are rotatably connected to the first water tank 5, the stirring rods 22 are connected together by a pulley sleeve, the output shaft end of the motor 20 is fixedly connected to one of the plurality of stirring rods 22, a fixed rod 3 is fixedly connected to the main body 1, a storage rod 4 is fixedly connected to the fixed rod 3, the outer wall of the storage rod 4 is a hollow design and the storage rod 4 is located in the first water tank 5, the bottom of the first water tank 5 is connected to a first discharge pipe, and a second water tank is fixedly connected to the main body 1 18, the second water tank 18 is located below the first discharge pipe, a filter screen 19 is fixedly connected in the second water tank 18, a second discharge pipe is connected to one side of the second water tank 18, a water pump 6 is fixedly connected in the main body 1, the second discharge pipe is connected to the output end of the water pump 6, a third water tank 15 is fixedly connected in the main body 1, the second discharge pipe is connected to the second water tank 18 and the third water tank 15 respectively, a partition 16 is fixedly connected in the third water tank 15, a plurality of heating pipes 17 are arranged below the partition 16, a condenser 10 is connected above the third water tank 15, a second grid plate 11 is fixedly connected in the condenser 10, activated coke is placed in the second grid plate 11, a fan 13 is arranged at one end of the condenser 10, and a section of the condenser 10 close to the fan 13 is connected to a drain pipe.
[0024] In the present invention, a section of the condenser tube 10 disposed outside the main body 1 is sheathed with a heat-insulating layer 12 , and the drain pipe is located between the heat-insulating layer 12 and the fan 13 .
[0025] Wherein, the stirring rod 22 is made of acid-resistant material.
[0026] Wherein, a first baffle 21 is rotatably connected to the main body 1, and the first baffle 21 is located at the function box.
[0027] Among them, the first water tank 5, the second water tank 18 and the third water tank 15 are all connected to the exhaust pipe 8, and the exhaust pipe 8 is fixedly connected to the first grid plate 7 at the pipe mouth located on the outside of the main body 1. Active coke is placed in the first grid plate 7, and a one-way valve 8 is fixedly connected to the exhaust pipe 8.
[0028] Among them, the first water tank 5, the second water tank 18 and the third water tank 15 are all connected with the sampling tube 14, the sampling tube 14 is slidably connected to the main body 1, the sampling tube 14 is fixedly connected with a connecting plate 26, the main body 1 is fixedly connected with a fixing plate, the fixing plate is located above the connecting plate 26, and the fixing plate and the connecting plate 26 are both provided with limiting holes, the limiting hole is slidably connected with a limiting rod 28, the limiting rod 28 is provided with a limiting groove, the limiting groove is slidably connected with a limiting plate 29, the sampling tube 14 is slidably connected with a piston plate 24, the piston plate 24 is fixedly connected with a connecting rod 25 on one side close to the connecting plate 26, an opening is provided below the sampling tube 14, and three sampling boxes 27 are provided on the outer wall of the main body 1, and the three sampling boxes 27 are respectively located below the three sampling tubes 14.
[0029] Working principle: When in use, soluble trivalent iron salt is placed in the placing rod 4, the wastewater is now neutralized in the first water tank 5, and the first step of treatment is performed by stirring and other operations, and then discharged into the second water tank 18, the sediment in the first treated wastewater is separated from the wastewater by the filter 19, and then the wastewater is sent to the third water tank 15 for evaporation and heating by the water pump 6, the partition 16 is used to collect the concentrated wastewater obtained after heating, the evaporated gas is discharged through the condenser 10, the toxic substances are adsorbed by the active coke in the second grid plate 11, and the non-toxic condensed water finally formed is discharged from the drain pipe, and the By treating the wastewater multiple times, the quality of wastewater treatment is improved, and the non-toxic liquid therein is separated and not treated uniformly with the wastewater, thereby improving environmental protection. When in use, during the processing of phosphorus-based flame retardants, wastewater is continuously discharged, and the limit plate 28 and the limit rod 28 are pulled out in succession to release the limit of the sampling tube 14. The pre-step is set to avoid misoperation by the staff, and the connecting rod 25 is pulled to press the wastewater into the sampling tube 14, and then the sampling tube 14 is pulled out to collect the wastewater in the collection box 27. While facilitating the staff to sample and monitor the wastewater, it can also avoid safety accidents caused by misoperation of the staff.
[0030] Example 2
[0031] Reference Figure 4 , a wastewater treatment device for processing phosphorus-based flame retardants. Compared with Example 1, in this embodiment, the fixing rod 3 extends outside the main body 1, and the top of the fixing rod 3 is rotatably connected to a knob 32, the placement rod 4 is connected to the knob 32 by threads, and the placement rod 4 is slidably connected to the fixing rod 3, and a second baffle 31 is provided at the bottom end of the placement rod 4, and two telescopic rods 30 are fixedly connected between the second baffle 31 and the fixing rod 3.
[0032] Working principle: When in use, since the material in the storage rod 4 is a consumable and needs to be replaced and filled many times, the storage rod 4 is taken out by turning the knob 32. An elastic member is fixedly connected between the telescopic rod 30 and the fixed rod 3. In the process of taking out the storage rod 4, the telescopic rod 30 drives the second baffle 31 to rise, and finally closes the opening below the fixed rod 3, ensuring that toxic waste gas will not leak when replacing the filling material of the storage rod 4, thereby improving the safety of the device.
[0033] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.
Claims
1. A wastewater treatment device for phosphorus flame retardant processing, comprising a main body (1), characterized in that: A feed pipe (2) is fixedly connected to the top of the main body (1), a first water tank (5) is fixedly connected to the inside of the main body (1), the first water tank (5) is located below the feed pipe (2), a function box is fixedly connected to the inside of the main body (1), a motor (20) is fixedly connected to the inside of the function box, a plurality of stirring rods (22) are rotatably connected to the inside of the first water tank (5), the stirring rods (22) are connected together via a pulley sleeve, an output shaft end of the motor (20) is fixedly connected to one of the plurality of stirring rods (22), a fixing rod (3) is fixedly connected to the inside of the main body (1), a storage rod (4) is fixedly connected to the inside of the fixing rod (3), the outer wall of the storage rod (4) is hollow and the storage rod (4) is located in the first water tank (5), a first discharge pipe is connected to the bottom of the first water tank (5), a second water tank (18) is fixedly connected to the inside of the main body (1), the second water tank (18) is located Below the first discharge pipe, a filter screen (19) is fixedly connected in the second water tank (18), one side of the second water tank (18) is connected to the second discharge pipe, a water pump (6) is fixedly connected in the main body (1), the second discharge pipe is connected to the output end of the water pump (6), a third water tank (15) is fixedly connected in the main body (1), the second discharge pipe is connected to the second water tank (18) and the third water tank (15) respectively, a partition (16) is fixedly connected in the third water tank (15), a plurality of heating pipes (17) are arranged below the partition (16), a condenser (10) is connected above the third water tank (15), a second grid plate (11) is fixedly connected in the condenser (10), activated coke is placed in the second grid plate (11), a fan (13) is arranged at one end of the condenser (10), and a section of the condenser (10) close to the fan (13) is connected to a drain pipe; The condenser tube (10) is disposed outside the main body (1) and is covered with a heat-insulating layer (12), and the drain pipe is located between the heat-insulating layer (12) and the fan (13); The stirring rod (22) is made of acid-resistant material; A first baffle (21) is rotatably connected to the main body (1), and the first baffle (21) is located at the function box; The first water tank (5), the second water tank (18) and the third water tank (15) are all connected to an exhaust pipe (8); a first mesh plate (7) is fixedly connected to the exhaust pipe (8) at a pipe opening located outside the main body (1); activated coke is placed inside the first mesh plate (7); and a one-way valve (9) is fixedly connected inside the exhaust pipe (8); The first water trough (5), the second water trough (18) and the third water trough (15) are all connected to a sampling tube (14), the sampling tube (14) is slidably connected to the main body (1), a connecting plate (26) is fixedly connected to the sampling tube (14), a fixing plate is fixedly connected to the main body (1), the fixing plate is located above the connecting plate (26), and both the fixing plate and the connecting plate (26) are provided with a limiting hole, a limiting rod (28) is slidably connected in the limiting hole, a limiting groove is provided on the limiting rod (28), a limiting plate (29) is slidably connected in the limiting groove, a piston plate (24) is slidably connected in the sampling tube (14), a connecting rod (25) is fixedly connected to a side of the piston plate (24) close to the connecting plate (26), an opening is provided below the sampling tube (14), and three sampling boxes (27) are provided on the outer wall of the main body (1), and the three sampling boxes (27) are respectively located below the three sampling tubes (14); The fixing rod (3) extends outside the main body (1), and a knob (32) is rotatably connected to the top of the fixing rod (3), the storage rod (4) is connected to the knob (32) by a thread, and the storage rod (4) is slidably connected to the fixing rod (3), a second baffle (31) is provided at the bottom end of the storage rod (4), two telescopic rods (30) are fixedly connected between the second baffle (31) and the fixing rod (3), and an elastic member is fixedly connected between the telescopic rod (30) and the fixing rod (3).
