A freezing concentration device
By designing a freezing and concentration device composed of cooling panels and heating panels, the solution can be received in segments and refrigerated and concentrated, solving the problems of complex equipment, high cost and low efficiency in the prior art, and improving solution concentration and separation The efficiency of purification is suitable for multiple fields.
Patent Information
- Application Number
- CN202411098566.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-08-12
- Publication Date
- 2024-12-10
- Estimated Expiration
- 2044-08-12
AI Technical Summary
The equipment of the existing frozen and concentration method has complex structure, high cost and low efficiency, making it difficult to achieve efficient solution concentration and separation and purification.
A freezing and concentration device is designed, including a tank grid composed of parallel cooling panels and heating panels. The solution is received in segments through the freezing and dissolution process, so as to achieve solution separation and refrigeration concentration of different concentrations to increase the solution concentration.
It improves the efficiency of frozen concentration and separation and purification, simplifies equipment and operations, and is suitable for food, cosmetics, biomedicine and environmentally friendly treatment fields.
Smart Images

Figure CN118615744B_ABST
Abstract
Description
Technical Field
[0001] The invention belongs to the technical field of freeze concentration, and in particular relates to a freeze concentration device. Background Art
[0002] The freeze concentration method in the prior art is a concentration technology that utilizes the solid-liquid phase relationship between a dilute solution and ice below the freezing point. There are two main methods: suspended crystallization freeze concentration and progressive freeze concentration. The principle of the suspended crystallization freeze concentration method is that when a dilute solution is frozen, the free small ice crystals suspended in the liquid are continuously removed to increase the liquid concentration. The principle of the progressive freeze concentration method is that when a dilute solution is frozen, as the ice layer is generated and grows on the cooling surface, the solute near the solid-liquid interface is removed to the liquid phase side, resulting in a concentration method in which the mass concentration of the solute in the liquid phase gradually increases. The existing freeze concentration method has a complex equipment structure, high equipment cost and production cost, and low efficiency. Summary of the invention
[0003] In order to solve the problems existing in the prior art, the main purpose of the present invention is to provide a freezing concentration device.
[0004] To solve the above technical problems, according to one aspect of the present invention, the present invention provides the following technical solutions:
[0005] A freeze concentration device, comprising: a freeze-thaw component;
[0006] The freeze-thaw component is a tank container group: the tank container group is composed of a tank grid group formed by parallel cooling panels and heating panels, an upper cover plate, a lower cover plate, and a common side panel; wherein, in each tank grid, there are two parallel panels: one is a cooling panel through which the refrigerant passes, and the other is a heating panel with a heat source inside; when the dilute solution is frozen into a solid or a solid-liquid mixture in the freeze-thaw component, the solution is received in sections when it is dissolved by heat to obtain solutions of different concentrations; the solution that meets the target concentration is retained for use; the solution that does not meet the target concentration is continuously frozen and dissolved by the freeze concentration device to increase the solution concentration.
[0007] As a preferred solution of the freezing concentration device described in the present invention, each heating panel of the tank container group is located between two cooling panels.
[0008] As a preferred embodiment of the freezing concentration device described in the present invention, each heating panel and cooling panel of the tank container group has a gap at the lower end thereof for connecting adjacent tank cells. When the lower cover plate of the tank container group is sealed and combined with its lower end, each tank cell of the tank container group is a connecting (container).
[0009] As a preferred embodiment of the freezing concentration device described in the present invention, the lower cover plate of the tank container group is moved up and down by a screw rod, a motor, and a control system to achieve sealing combination or separation with the lower end of the tank container group.
[0010] As a preferred embodiment of the freezing concentration device described in the present invention, an ice support rack is arranged at the lower end of the trough grid of the trough container group, and the ice support rack is locked together with the lower end of the trough grid of the trough container group through an ice support rack lock, and the switch of the ice support rack lock is arranged outside the insulation layer, and a protective cover is arranged outside the switch of the ice support rack lock.
[0011] As a preferred embodiment of the freeze concentration device described in the present invention, the refrigerant required by the freeze concentration device is provided by a refrigeration device, and the refrigerant provided by the refrigeration device enters the freeze-thaw component through a refrigerant pipeline connected to the freeze-thaw component and passes through each cooling panel of the tank container group.
[0012] As a preferred embodiment of the freeze concentration device described in the present invention, the heat source of the heating panel is a heating element (such as an electric heating element, etc.), or a heat source medium (such as a fluid, etc.) is used as the heat source.
[0013] As a preferred embodiment of the freeze concentration device described in the present invention, when injecting the dilute solution into the tank container group of the freeze-thaw component, first open the upper cover plate, inject the dilute solution from the dilute solution tank into the tank container group through the liquid pump, and then close the upper cover plate; or pre-set a dilute solution inlet on the upper cover plate of the freeze concentration component, and pump the dilute solution from the dilute solution tank into the tank container group through the dilute solution inlet through the liquid pump.
[0014] As a preferred solution of the freezing concentration device described in the present invention, a supporting panel vertically connecting the cooling panel and the heating panel is provided between the cooling panel and the heating panel in the tank container group.
[0015] As a preferred solution of the freezing concentration device described in the present invention, the freezing and thawing assembly is fixed on a bracket, and a control system is also arranged on the bracket.
[0016] To solve the above technical problem, according to another aspect of the present invention, the present invention provides the following technical solution:
[0017] The above-mentioned freezing concentration device can be used in the fields of food, cosmetics, biomedicine, environmental protection treatment, etc.
[0018] The above-mentioned freezing concentration device can be used in the fields of milk, wine, juice, coffee, tea, beverages, soy milk, chemical liquid, Chinese herbal medicine liquid, plant extract, seawater purification, wastewater treatment, etc.
[0019] The above-mentioned freeze concentration device can be used in the field of freeze concentration and separation and purification of heat-sensitive raw materials.
[0020] The above-mentioned freezing concentration device can be used in the fields of freezing concentration and separation and purification of milk, wine, juice, coffee, tea, beverages, soybean milk, soy milk, chemical liquid, Chinese herbal liquid, plant extract, seawater purification, wastewater treatment, etc.
[0021] The beneficial effects of the present invention are as follows:
[0022] The present invention proposes a freeze concentration device, including a freeze-thaw component; the freeze-thaw component is a tank container group: a tank grid group formed by parallel cooling panels and heating panels, an upper cover plate, a lower cover plate, and a common side panel form the tank container group; wherein, in each tank grid, there are two panels parallel to each other: one is a cooling panel through which a refrigerant passes, and the other is a heating panel with a heat source inside; when a dilute solution is frozen into a solid or a solid-liquid mixture in the freeze-thaw component, the solution is received in sections when it is dissolved by heat to obtain solutions of different concentrations; solutions that meet the target concentration are retained for standby use; solutions that do not meet the target concentration are continuously frozen and dissolved by the freeze concentration device to increase the solution concentration. The present invention improves the efficiency of freeze concentration and separation and purification, and the equipment and operation are simple, which is convenient for application in the fields of food, cosmetics, biomedicine, environmental protection treatment, etc. BRIEF DESCRIPTION OF THE DRAWINGS
[0023] In order to more clearly illustrate the technical solutions in the present invention, the following is a brief introduction to the drawings required for the prior art description. The drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on the structures shown in these drawings without creative work.
[0024] Figure 1 It is a schematic cross-sectional view of the freeze concentration device of the present invention.
[0025] Figure 2 Schematic diagram of the freeze-thaw assembly.
[0026] Figure 3 A schematic diagram of the structure of a freeze-thaw assembly including a support panel.
[0027] In the figure, 1,3,5,7,9-cooling panel, 2,4,6,8-heating panel, 10-insulation layer, 12-ice support rack, 13-solution outlet, 14-refrigerant inlet pipe, 15-refrigerant outlet pipe, 16-bracket, 17-ice support rack lock, 18-protective cover, 20-solid or solid-liquid mixture, 21-control system, 22-motor, 23-screw rod, 24-edge of solution collecting tank, 25-support panel, A-upper cover plate, C-lower cover plate.
[0028] The realization of the purpose, functional features and advantages of the present invention will be further explained in conjunction with embodiments and with reference to the accompanying drawings. DETAILED DESCRIPTION
[0029] The following will be described clearly and completely in conjunction with the technical solutions in the embodiments. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0030] The present invention proposes a freeze concentration device, which breaks the traditional freeze concentration thinking, improves the efficiency of freeze concentration and separation and purification, has simple equipment and operation, and is convenient for application in the fields of food, cosmetics, biomedicine, environmental protection treatment, etc.
[0031] like Figure 1-3 As shown, a specific embodiment of the present invention provides a freeze concentration device, including: a freeze-thaw component;
[0032] The freeze-thaw assembly is a tank container group: a tank container group consisting of a tank grid group formed by mutually parallel cooling panels 1, 3, 5, 7, 9 and heating panels 2, 4, 6, 8, an upper cover A, a lower cover C, and a common side panel; wherein, in each tank grid, there are two mutually parallel panels: one is the cooling panel 1, 3, 5, 7, 9 through which the refrigerant passes, and the other is the heating panel 2, 4, 6, 8 with a heat source inside; when the dilute solution is frozen into a solid or a solid-liquid mixture 20 in the freeze-thaw assembly, the solution is received in sections through the solution collecting tank and the solution outlet 13 arranged on the lower cover C when it is dissolved by heat, and solutions of different concentrations are obtained; solutions that meet the target concentration are retained for standby use; solutions that do not meet the target concentration are further freeze-concentrated by the freeze concentration device to increase the solution concentration.
[0033] In one embodiment of the present invention, each heating panel of the tank container group is located between two cooling panels, for example, the heating panel 2 is located between the cooling panels 1 and 3 .
[0034] In one embodiment of the present invention, each heating panel and cooling panel of the tank container group has a gap at the lower end thereof for connecting adjacent tank cells. When the lower cover plate C of the tank container group is sealed and combined with its lower end, each tank cell of the tank container group is a connecting (container).
[0035] In one embodiment of the present invention, the lower cover plate of the tank container group is moved up and down by a screw rod 23, a motor 22, and a control system 21 to achieve sealing combination or separation with the lower end of the tank container group.
[0036] In one embodiment of the present invention, an ice support rack 12 is provided at the lower end of the trough grid of the trough container group, and the ice support rack 12 is locked together with the lower end of the trough grid of the trough container group through an ice support rack lock 17. The switch of the ice support rack lock 17 is arranged outside the insulation layer 10 (the insulation layer 10 is arranged outside the side panel, or the insulation layer 10 is used as the side panel), and a protective cover 18 is arranged outside the switch of the ice support rack lock 17.
[0037] In one embodiment of the present invention, the refrigerant required by the freeze concentration device is provided by a refrigeration device. The refrigerant provided by the refrigeration equipment enters the freeze-thaw component through a refrigerant pipeline (including a refrigerant inlet pipe 14 and a refrigerant outlet pipe 15) connected to the freeze-thaw component and passes through each cooling panel of the tank container group.
[0038] In one embodiment of the present invention, the heat source of each heating panel may be a heating element (such as an electric heating element, etc.), or a heat source medium (such as a fluid, etc.) may be used as the heat source.
[0039] In one embodiment of the present invention, when injecting the dilute solution into the tank container group of the freeze-thaw component, first open the upper cover A, inject the dilute solution from the dilute solution tank into the tank container group through a liquid pump, and then cover the upper cover A tightly; or pre-set a dilute solution inlet on the upper cover A of the freeze-concentration component, and pump the dilute solution from the dilute solution tank into the tank container group through the dilute solution inlet through a liquid pump.
[0040] In one embodiment of the present invention, a support panel 25 (such as a support panel 25) vertically connecting the cooling panel and the heating panel is provided between the cooling panel and the heating panel in the tank container group. Figure 3 as shown).
[0041] In one embodiment of the present invention, the cryo-thawing assembly is fixed on the bracket 16 , and the control system 21 is disposed on the bracket 16 .
[0042] When using the device of the present invention for freeze concentration operation, first seal the lower cover plate C with the lower end of the tank container group through the screw rod 23, the motor 22, and the control system 21, then inject the dilute solution into the tank container group, cover the upper cover plate A, start the refrigeration equipment, and the refrigerant freezes and dissolves the components through the refrigerant pipeline and passes through the various cooling panels of the tank container group. According to needs, the dilute solution is frozen into a solid or a solid-liquid mixture, and the refrigeration equipment is turned off. Then, after starting the heating switch in the control system 21 (the heating element provides the heat source or the heat source medium such as runny nose provides the heat source), the control switch of the motor 22 is started again, and the lower cover plate C moves downward a short distance: the edge 24 of the solution collection tank on the lower cover plate C is not separated from the protective cover 18, so that a narrow sealed space is formed between the lower cover plate C, the edge 24 of the solution collection tank, the protective cover 18, and the lower end of the tank grid group. The solution falls into the solution collection tank through the ice support rack 12, and flows out from the solution outlet 13, and the solution is received in sections to obtain solutions of different concentrations. The solution that meets the target concentration is transferred to the next stage for storage (or direct use); the solution that does not meet the target concentration can be frozen and dissolved again by the freezing concentration device to further increase the concentration of the solution.
[0043] The above description is only a preferred embodiment of the present invention, and does not limit the patent scope of the present invention. All equivalent structural changes made by using the contents of the present invention specification under the inventive concept of the present invention, or directly / indirectly applied in other related technical fields are included in the patent protection scope of the present invention.
Claims
1. A freeze concentration device, characterized in that: include: Freeze-thaw components; The freezing and thawing assembly is a tank container group: the tank container group is composed of a tank grid group formed by parallel cooling panels and heating panels, an upper cover plate, a lower cover plate, and a common side panel; wherein, in each tank grid, there are two parallel panels: one is a cooling panel through which the refrigerant passes, and the other is a heating panel with a heat source inside; each heating panel of the tank container group is located between the two cooling panels; each heating panel and cooling panel of the tank container group has a gap at the lower end to connect the adjacent tank grids, and when the lower cover plate of the tank container group is sealed and combined with its lower end, each tank grid of the tank container group is a communicating vessel; the lower cover plate of the tank container group is moved up and down by a screw rod, a motor, and a control system to be sealed and combined or separated with the lower end of the tank container group; an ice support rack is provided at the lower end of the tank grid of the tank container group; When the dilute solution is frozen into a solid or a solid-liquid mixture in the freezing and dissolving component, the solution is received in sections through the solution collecting tank and the solution outlet arranged on the lower cover plate when it is heated and dissolved, so as to obtain solutions of different concentrations; the solution that meets the target concentration is retained for standby use; the solution that does not meet the target concentration is further frozen and dissolved by the freezing and concentrating device to increase the solution concentration.
2. The freeze concentration device according to claim 1, characterized in that: The ice support rack is locked together with the lower end of the slot grid of the slot container group through an ice support rack lock. The switch of the ice support rack lock is arranged outside the insulation layer, and a protective cover is arranged outside the switch of the ice support rack lock.
3. The freeze concentration device according to claim 1, characterized in that: The refrigerant required by the freeze concentration device is provided by the refrigeration equipment. The refrigerant provided by the refrigeration equipment enters the freeze-thaw component through the refrigerant pipeline connected to the freeze-thaw component and passes through the various cooling panels of the tank container group; the heat source of the heating panel is the heating element, or a heat source medium is used as the heat source.
4. The freeze concentration device according to claim 1, characterized in that: When injecting the dilute solution into the tank container group of the freeze-thaw component, first open the upper cover plate, inject the dilute solution from the dilute solution tank into the tank container group through the liquid pump, and then close the upper cover plate; or pre-set a dilute solution inlet on the upper cover plate of the freeze-concentration component, and pump the dilute solution from the dilute solution tank into the tank container group through the dilute solution inlet through the liquid pump.
5. The freeze concentration device according to claim 1, characterized in that: Between the cooling panel and the heating panel in the tank container group, a supporting panel is arranged to vertically connect the cooling panel and the heating panel.
6. Application of the freezing concentration device according to any one of claims 1 to 5 in the fields of food, cosmetics, biomedicine, and environmental protection treatment.
