Improved stirring rod for purifying praseodymium neodymium oxide mixed acid

By using the fixed connection between the positioning rod and the adapter of PTFE material, the stirring leaves of the T-shaped slot and the sealant in the praseodymium-norch-oxide mixed acid purified stirrer, the separation, breaking and sealing of the existing stirrer in an acidic environment is solved. The problem of insufficient sexuality achieves higher sealing, stability and service life.

CN222489649UActive Publication Date: 2025-02-18CHINALCO RARE EARTH (CHANGZHOU) CO LTD
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Patent Information

Application Number
CN202420547863.X
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-03-20
Publication Date
2025-02-18
Estimated Expiration
2034-03-20

AI Technical Summary

Technical Problem

The existing praseodymium-oxide-neodymium mixed acid purified stirring rods are prone to separation between the adapter rod and the adapter barrel, breakage of the stirring leaf and insufficient sealing properties in an acidic environment, resulting in low service life and cumbersome installation.

Method used

An improved stirring rod is designed, using the insertion assembly structure between the positioning rod and the adapter barrel, and the adapter barrel is used to adjust the adapter barrel with PTFE material and the stirring blade of the T-shaped slot to improve sealing and stability through the fixed connection of the sealant. sex.

Benefits of technology

Through the application of positioning rods and PTFE materials, the sealing and stability of the stirring rods are improved, the stirring leaves are avoided, the service life is extended, and the installation process is simplified.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses an improved stirring rod for praseodymium and neodymium oxide mixed acid purification, which comprises an adapter lock, the adapter lock is fixedly connected to the driving end of a rotating device through a positioning pin, an adapter rod is welded to the bottom of the adapter lock, a positioning rod is arranged at the bottom of the adapter rod, an adapter cylinder is fixedly assembled on the outer side of the adapter rod, and the adapter cylinder is fixedly connected with the positioning rod. A gluing groove is formed in the top of the transfer cylinder, sealant is filled through the gluing groove, the transfer rod and the transfer cylinder are fixedly connected, a rotating head is assembled and fastened at the bottom of the transfer cylinder, the joint of the transfer cylinder and the rotating head is sealed and fixed through the sealant, symmetrical clamping grooves are formed in the rotating head, and the clamping grooves are clamped in the clamping grooves. The stirring device has the advantages that the whole structure is good in sealing performance, high in rotation synchronism, convenient to disassemble and assemble and good in stirring stability, the stirring blades are more stable to install, larger resistance can be borne, and the service life is prolonged.
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Description

Technical Field

[0001] The utility model belongs to the technical field of purifying and stirring praseodymium-neodymium oxide mixed acid, and more specifically, particularly relates to an improved stirring rod for purifying praseodymium-neodymium oxide mixed acid. Background Art

[0002] At present, in the existing workshop praseodymium-neodymium oxide mixed acid purification operation, the commonly used stirring rod structure is as follows Figure 5 As shown, the adapter lock is connected to the driving end of the rotating device through a locating pin, and a transfer rod is arranged at the bottom of the adapter lock. Both the adapter lock and the transfer rod are made of metal, so they cannot directly contact the acid solution. A polytetrafluoroethylene adapter cylinder is installed on the outside of the adapter rod to isolate the metal adapter rod from contact with the acid solution. The adapter rod and the adapter cylinder are connected and fixed by multiple pins, and the hole is sealed by sealant. A rotating head is arranged at the bottom of the adapter cylinder, and symmetrical stirring blades are arranged on the outer circumference of the rotating head to stir and mix the acid solution.

[0003] However, although the adapter tube and the adapter rod fixed by multiple pins have good connectivity, the sockets on the sides of the adapter tube need to be sealed. Acid can easily enter during the praseodymium-neodymium mixed acid oxidation process, causing corrosion reaction of the pins, resulting in separation of the adapter rod and the adapter tube, affecting the stirring operation. Since the rotating head has stirring blades fixed on both sides, stirring can be performed, but the force is uneven. During high-speed rotation, the stirring blades are easily broken, the stability is poor, the service life is short, and the overall structure is cumbersome to install. Utility Model Content

[0004] In view of the deficiencies in the prior art, the utility model provides an improved stirring rod for purifying praseodymium-neodymium oxide mixed acid to solve the problems raised in the above-mentioned background technology.

[0005] To achieve the above objectives, the utility model is implemented through the following technical solutions: an improved stirring rod for purifying praseodymium-neodymium oxide mixed acid, comprising an adapter lock, which is connected and fixed to the driving end of a rotating device through a locating pin, a transfer rod is welded to the bottom of the transfer lock, a locating rod is arranged at the bottom of the transfer rod, a transfer cylinder is assembled and fixed on the outside of the transfer rod, a glue coating groove is arranged on the top of the transfer cylinder, sealant is filled into the glue coating groove, the transfer rod is fixedly connected to the transfer cylinder, a rotating head is assembled and fastened at the bottom of the transfer cylinder, the connection between the transfer cylinder and the rotating head is sealed and fixed by sealant, symmetrical slots are arranged on the rotating head, and stirring blades are fixed in the slots.

[0006] As an optional solution of the present invention, the positioning rod is a rectangular parallelepiped as a whole, and its cross section is a square.

[0007] As an optional solution of the present invention, the adapter tube is made of PTFE material, that is, polytetrafluoroethylene.

[0008] As an optional solution of the present invention, the card slot is T-shaped.

[0009] As an optional solution of the utility model, the cross-section of the stirring blade is T-shaped, and the upper left corner of one stirring blade is chamfered, and the lower right corner of the other stirring blade is chamfered.

[0010] As an optional solution of the utility model, a positioning pressure plate is provided on the top of the rotating head. The positioning pressure plate is annular as a whole. The positioning pressure plate is fitted on the top of the rotating head. The rotating head and the positioning pressure plate are sealed and fixed by sealant. The connection between the positioning pressure plate and the adapter tube is also sealed and fixed by sealant.

[0011] The utility model provides an improved stirring rod for purifying praseodymium-neodymium oxide mixed acid, which has the following beneficial effects:

[0012] By setting a positioning rod, the positioning rod adopts a rectangular structure design, which can be plugged and assembled with the adapter tube, and while ensuring the stability of rotation, it can also ensure the rotation synchronization of the positioning plate and the adapter tube. There is no need for a positioning pin, which reduces the sealing surface and improves the overall sealing. A glue coating groove is provided on the top of the adapter tube, and a special sealant can be filled into the glue coating groove to fix the adapter rod and the adapter tube. Compared with the previous positioning pin fixed with the sealant sealing method, the sealing is stronger and leakage is avoided. By providing a symmetrical T-slot on the rotating head, a T-shaped stirring blade with a corresponding structure can be installed, so that the connection between the stirring blade and the rotating head is more stable and the force is stronger, which avoids the stirring blade from breaking due to lack of force and improves the service life. BRIEF DESCRIPTION OF THE DRAWINGS

[0013] Figure 1 It is a schematic diagram of the structure of the utility model;

[0014] Figure 2 It is the structural explosion diagram of the utility model;

[0015] Figure 3 It is a front view of the utility model;

[0016] Figure 4 It is a cross-sectional view of the utility model;

[0017] Figure 5 This is a schematic diagram of the structure of the existing stirring rod before improvement.

[0018] In the figure: 1. Adapter lock; 101. Positioning pin; 2. Adapter rod; 201. Positioning rod; 3. Adapter cylinder; 301. Glue coating groove; 4. Positioning pin; 5. Rotating head; 501. Stirring blade; 5011. Chamfer; 6. Positioning pressure plate. DETAILED DESCRIPTION

[0019] The following is a further detailed description of the implementation of the present invention in conjunction with the accompanying drawings and examples. The following examples are used to illustrate the present invention, but cannot be used to limit the scope of the present invention.

[0020] In the description of the present invention, unless otherwise specified, "multiple" means two or more; the terms "upper", "lower", "left", "right", "inner", "outer", "front end", "rear end", "head", "tail" and the like indicate the orientation or positional relationship based on the orientation or positional relationship shown in the drawings, which is only for the convenience of describing the present invention and simplifying the description, and does not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operate in a specific orientation, and therefore cannot be understood as limiting the present invention. In addition, the terms "first", "second", "third" and the like are only used for descriptive purposes and cannot be understood as indicating or implying relative importance.

[0021] In the description of the present invention, it should be noted that, unless otherwise clearly specified and limited, the terms "connected" and "connection" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.

[0022] See also Figures 1 to 5The utility model provides a technical solution: an improved stirring rod for purifying praseodymium-neodymium oxide mixed acid, comprising an adapter lock 1, which is connected and fixed to the driving end of a rotating device through a positioning pin 101, and a transfer rod 2 is welded at the bottom of the transfer lock 1. The transfer rod 2 and the transfer lock 1 are both made of metal. A positioning rod 201 is arranged at the bottom of the transfer rod 2. The positioning rod 201 is a rectangular parallelepiped as a whole, and has a square cross-section. A transfer tube 3 is fixedly assembled on the outer side of the transfer rod 2. The positioning rod 201 adopts a rectangular parallelepiped structure design, which can be plugged and assembled with the transfer tube 3, and the rotation stability and the rotation synchronization of the positioning plate and the transfer tube 3 are ensured. No positioning pin is required, the sealing surface is reduced, and the overall sealing is improved. The transfer tube 3 adopts PTFE material, also known as polytetrafluoroethylene: it has the advantages of being resistant to acid and alkali, and various organic solvents, and is almost insoluble in all solvents. At the same time, polytetrafluoroethylene is resistant to high temperatures and can protect the internal metal transfer rod 2 during the stirring process, thereby preventing the metal transfer rod 2 from being corroded by the mixed acid.

[0023] A glue coating groove 301 is provided on the top of the adapter tube 3, and a special sealant can be filled into the glue coating groove 301 to fix the adapter rod 2 and the adapter tube 3. Compared with the previous positioning pin fixing and sealant sealing method, the sealing is stronger, leakage is avoided, and the service life of the stirring rod is increased. The bottom of the adapter tube 3 is fastened with a rotating head 5, and the connection between the adapter tube 3 and the rotating head 5 is sealed and fixed by a special sealant.

[0024] A symmetrical slot is provided on the rotating head 5, and the slot is T-shaped. A stirring blade 501 is fixed in the slot. The cross-section of the stirring blade 501 is T-shaped, and the upper left corner of one of the stirring blades 501 is a chamfered angle 5011, and the lower right corner of the other stirring blade 501 is a chamfered angle 5011, thereby reducing the stirring resistance and increasing the stirring speed. By installing and fixing the stirring blade 501 inside the rotating head 5, the overall stability is improved, and the phenomenon of the stirring blade 501 breaking during rotation is avoided, and the service life is longer. A positioning plate 6 is provided on the top of the rotating head 5. The positioning plate 6 is annular as a whole and fits on the top of the rotating head 5. The rotating head 5 and the positioning plate 6 are sealed and fixed by sealant. The connection between the positioning plate 6 and the adapter tube 3 is also sealed and fixed by sealant, so that the overall connection is tighter.

[0025] The specific usage and function of this embodiment are as follows: first, the positioning rod 201 is quickly inserted into the adapter tube 3 and sealed and fixed, and then the rotating head 5 is sealed and fixed to the bottom of the adapter tube 3, and the T-shaped stirring blade 501 is symmetrically installed in the slot, so that the stirring blade 501 is set in the rotating head 5 to avoid being set on the outside without being subjected to force, and the stirring blade 501 is further sealed by the positioning pressure plate 6, and is further sealed and fixed with the rotating head 5 and the adapter tube 3 by the positioning pressure plate 6, which greatly improves the overall sealing performance and avoids the leakage of mixed acid and the contact reaction with the internal adapter rod 2, and finally the rotating lock is connected to the driving end of the rotating equipment at the top through the positioning pin 101 to stir the mixed acid.

[0026] The device embodiments described above are merely illustrative, wherein the units described as separate components may or may not be physically separated, and the components displayed as units may or may not be physical units, that is, they may be located in one place, or they may be distributed on multiple network units. Some or all of the modules may be selected according to actual needs to achieve the purpose of the scheme of this embodiment. Ordinary technicians in this field can understand and implement it without paying creative labor.

[0027] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the utility model, rather than to limit it. Although the utility model has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that they can still modify the technical solutions described in the aforementioned embodiments, or make equivalent replacements for some of the technical features therein. However, these modifications or replacements do not deviate the essence of the corresponding technical solutions from the spirit and scope of the technical solutions of the various embodiments of the utility model.

Claims

1. An improved stirring rod for purifying praseodymium-neodymium oxide mixed acid, characterized in that: The invention comprises an adapter lock (1), wherein the adapter lock (1) is connected and fixed to the driving end of the rotating device through a positioning pin (101), a adapter rod (2) is welded at the bottom of the adapter lock (1), a positioning rod (201) is arranged at the bottom of the adapter rod (2), an adapter cylinder (3) is assembled and fixed on the outer side of the adapter rod (2), a glue coating groove (301) is arranged at the top of the adapter cylinder (3), a sealant is filled through the glue coating groove (301), and the adapter rod (2) and the adapter cylinder (3) are fixedly connected, a rotating head (5) is assembled and fastened at the bottom of the adapter cylinder (3), and the connection between the adapter cylinder (3) and the rotating head (5) is sealed and fixed by the sealant, and a symmetrical clamping groove is arranged on the rotating head (5), and a stirring blade (501) is fixed in the clamping groove.

2. The improved stirring rod for purifying praseodymium-neodymium oxide mixed acid according to claim 1, characterized in that: The positioning rod (201) is in the shape of a rectangular parallelepiped as a whole, and has a square cross section.

3. The improved stirring rod for purifying praseodymium-neodymium oxide mixed acid according to claim 1, characterized in that: The adapter tube (3) is made of PTFE material, namely polytetrafluoroethylene.

4. The improved stirring rod for purifying praseodymium-neodymium oxide mixed acid according to claim 1, characterized in that: The card slot is T-shaped.

5. The improved stirring rod for purifying praseodymium-neodymium oxide mixed acid according to claim 1, characterized in that: The cross section of the stirring blade (501) is T-shaped, and the upper left corner of one stirring blade (501) is a chamfered angle (5011), and the lower right corner of the other stirring blade (501) is a chamfered angle (5011).

6. The improved stirring rod for purifying praseodymium-neodymium oxide mixed acid according to claim 1, characterized in that: A positioning pressure plate (6) is arranged on the top of the rotating head (5). The positioning pressure plate (6) is annular in shape as a whole. The positioning pressure plate (6) is fitted on the top of the rotating head (5). The rotating head (5) and the positioning pressure plate (6) are sealed and fixed by means of sealant. The connection between the positioning pressure plate (6) and the adapter tube (3) is also sealed and fixed by means of sealant.