Efficient epoxiconazole synthesis reaction device

Abstract

The utility model belongs to the technical field of synthesis reaction equipment, in particular relates to an epoxiconazole efficient synthesis reaction device, and aims to solve the problems that when an epoxiconazole suspending agent is prepared, a stirring device is generally used for accelerating the synthesis reaction, but residues on the inner wall of a stirring tank are inconvenient to clean, and the internal temperature of the stirring tank is fixed, so that the reaction rate is not favorably improved. According to the scheme, the device comprises a tank body, stirring rods are rotationally installed at the two ends of the inner wall of the tank body, a plurality of stirring blades are fixedly arranged on the stirring rods, a driving motor used for driving the stirring rods to rotate is fixedly installed in the center of the top of the outer wall of the tank body, and the top and the bottom of the tank body are communicated with a feeding pipe and a discharging pipe respectively. When the reaction kettle is used, by optimizing the structure and configuration, the efficient mixing of raw materials, the uniform reaction and the rapid discharge of products are realized, the waste of the raw materials and the blockage of the reaction kettle are avoided, and the production efficiency and the product quality are improved.

Description

Technical Field

[0001] The utility model relates to the technical field of synthesis reaction equipment, in particular to a high-efficiency synthesis reaction device of epoxiconazole. Background Art

[0002] Fluoxepiconazole is a broad-spectrum fungicide widely used in agricultural planting. Among them, the more commonly used is the fluoxepiconazole suspension, which is mainly composed of the following raw materials: fluoxepiconazole (generally accounting for 10-15%), surfactant (8-14%), sodium alginate (0.2-0.5%), urea (0.2-1%), sodium acetate (0.5-1%), saponin powder (0.2-0.6%), polyoxyethylene glycerol ether (0.02-0.05%), and the balance is water. Among them, the surfactant is composed of sucrose fatty acid esters and sodium ditridecyl sulfosuccinate.

[0003] When preparing the epoxiconazole suspension concentrate, a stirring device is usually used to accelerate the synthesis reaction, but the residue on the inner wall of the stirring tank is inconvenient to clean, and the internal temperature of the stirring tank is fixed, which is not conducive to increasing the reaction rate.

[0004] In view of the above problems, the utility model document proposes a highly efficient synthesis reaction device for epoxiconazole. Utility Model Content

[0005] The utility model provides a fluopicolide efficient synthesis reaction device, which solves the shortcomings in the prior art that, when preparing fluopicolide suspension, a stirring device is usually used to accelerate the synthesis reaction, but the residue on the inner wall of the stirring tank is inconvenient to clean, and the internal temperature of the stirring tank is fixed, which is not conducive to improving the reaction rate.

[0006] The utility model provides the following technical solutions:

[0007] A highly efficient synthesis reaction device of epoxiconazole, comprising:

[0008] A tank body, wherein stirring rods are rotatably mounted at both ends of the inner wall of the tank body, a plurality of stirring blades are fixedly mounted on the stirring rods, a driving motor for driving the stirring rods to rotate is fixedly mounted at the center of the top of the outer wall of the tank body, and a feeding pipe and a discharging pipe are respectively connected to the top and bottom of the tank body;

[0009] The cleaning component is installed on the stirring rod to prevent the residue from being deposited on the inner wall of the tank and to facilitate the mixed solution to be discharged to the discharge pipe;

[0010] The heating component is arranged on the tank body and is used to increase the internal temperature of the tank body, thereby accelerating the synthesis reaction.

[0011] In a possible design, the cleaning assembly includes a U-shaped scraper fixedly mounted on the stirring rod, and the outer wall of the U-shaped scraper is arranged to fit the inner wall of the tank body.

[0012] In one possible design, the heating assembly includes a heating seat arranged outside the tank body, the tank body is clamped in the heating seat, and three anti-slip legs are fixedly arranged in a circular array at the bottom of the heating seat. The bottom of the heating seat is provided with a through hole for the discharge pipe to pass through.

[0013] In a possible design, a temperature controller for adjusting the heating temperature is fixedly disposed on the outer wall of the heating seat.

[0014] In a possible design, the feeding tube is provided with a first solenoid valve and a scale line set based on a valve plate of the first solenoid valve so as to measure the amount of raw material added.

[0015] In a possible design, the discharge pipe is provided with a second solenoid valve for conveniently controlling the discharge.

[0016] It should be understood that the above general description and the following detailed description are merely exemplary and do not limit the present invention.

[0017] In this application, the specific workflow is as follows:

[0018] Raw material adding stage: add the raw materials into the tank one by one through the feeding pipe. During the process of adding raw materials, the operator can accurately measure and add the required amount of raw materials by controlling the switch of the first solenoid valve according to the indication of the scale line. When all the raw materials are added, close the first solenoid valve to ensure the sealing of the tank;

[0019] Stirring and heating stage: start the drive motor to drive the stirring rod and stirring blade to rotate in the tank body to evenly mix and stir the raw materials. At the same time, turn on the temperature controller of the heating component, set the appropriate heating temperature, and the heating seat starts to heat the tank body to increase the temperature inside the tank body, thereby accelerating the synthesis reaction. During the stirring and heating process, the U-shaped scraper continuously scrapes the inner wall of the tank body as the stirring rod rotates to prevent the raw materials from depositing on the tank wall to form residues;

[0020] Discharge stage: when the synthesis reaction is completed, turn off the temperature controller to stop heating, open the second solenoid valve on the discharge pipe, so that the synthesized fluopicolide suspension solution can be discharged smoothly from the discharge pipe. The opening of the second solenoid valve can be adjusted as needed to control the speed and amount of discharge. As the stirring rod continues to rotate, the U-shaped scraper is driven to push the mixed solution to the discharge pipe to promote the discharge of the solution. After the discharge is completed, the cleaning water source can be connected from the feeding pipe to assist the U-shaped scraper to clean the inner wall of the tank, which is convenient to use.

[0021] The utility model has the following beneficial effects:

[0022] The utility model realizes efficient mixing of raw materials, uniform reaction and rapid discharge of products by optimizing structure and configuration, and at the same time avoids waste of raw materials and blockage of the device, thereby improving production efficiency and product quality. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] Figure 1 A schematic diagram of the three-dimensional structure of a highly efficient synthesis reaction device of epoxiconazole provided in an embodiment of the utility model;

[0024] Figure 2 A schematic diagram of the separation structure of the tank body and the heating seat of a fluopicolide efficient synthesis reaction device provided by an embodiment of the utility model;

[0025] Figure 3 A schematic diagram of the internal structure of a tank of a highly efficient epoxiconazole synthesis reaction device provided by an embodiment of the utility model;

[0026] Figure 4 A schematic diagram of the connection structure of a U-shaped scraper and a stirring rod of a fluphenazine efficient synthesis reaction device provided in an embodiment of the utility model.

[0027] Figure numerals: 1. tank body; 2. stirring rod; 3. stirring blade; 4. driving motor; 5. feeding tube; 6. scale line; 7. first solenoid valve; 8. discharge tube; 9. second solenoid valve; 10. U-shaped scraper; 11. heating seat; 12. temperature controller; 13. through hole; 14. anti-slip support leg. DETAILED DESCRIPTION

[0028] The technical solutions in the embodiments of the utility model will be clearly and completely described below in conjunction with the drawings in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, rather than all of the embodiments. Based on the embodiments of the utility model, all other embodiments obtained by ordinary technicians in this field without making creative work are within the scope of protection of the utility model.

[0029] In the description of the present invention, it should be understood that the terms "opening", "upper", "middle", "length", "inside" and the like indicating orientation or positional relationship are only for the convenience of describing the present invention and simplifying the description, and do not indicate or imply that the components or elements referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore should not be understood as a limitation on the present invention.

[0030] In order to keep the following description of the embodiments of the present invention clear and concise, the present invention omits detailed descriptions of known functions and known components.

[0031] Example 1

[0032] Please refer to Figure 1-4 , the present application provides a synthesis reaction device, comprising:

[0033] The tank body 1 has stirring rods 2 rotatably mounted at both ends of its inner wall, and a plurality of stirring blades 3 are fixedly mounted on the stirring rods 2. These stirring blades 3 can effectively stir the raw materials in the tank body 1 when the stirring rod 2 rotates, so as to promote the uniform reaction. A driving motor 4 is fixedly mounted at the center of the top of the outer wall of the tank body 1. The driving motor 4 is connected to an external power supply through an external controller and powered. The driving motor 4 provides power for the stirring rod 2 to ensure its stable and efficient rotation.

[0034] In addition, the top and bottom of the tank body 1 are respectively connected with a feeding pipe 5 and a discharging pipe 8, the feeding pipe 5 is used to add raw materials into the tank body 1, and the discharging pipe 8 is used to discharge the synthesized fluopicolide suspension solution, this design makes the addition of raw materials and the discharge of products simple and convenient, and a second solenoid valve 9 is provided on the discharging pipe 8, which is convenient for the operator to control the discharge timing and discharge amount. When the synthesis reaction is completed, the second solenoid valve 9 is opened to discharge the fluopicolide suspension solution from the device;

[0035] In order to improve the practicality and efficiency of the device, the device is also equipped with a cleaning component, which includes a U-shaped scraper 10 fixedly arranged on the stirring rod 2. The outer wall of the U-shaped scraper 10 is closely attached to the inner wall of the tank body 1. During the rotation of the stirring rod 2, the U-shaped scraper 10 can scrape off the residue on the inner wall of the tank body 1 to avoid the waste of raw materials and the blockage of the device. At the same time, the U-shaped scraper 10 can also push the mixed solution to the discharge pipe 8 to promote the discharge of the solution.

[0036] In order to speed up the synthesis reaction, the device is also provided with a heating component, which includes a heating seat 11 arranged outside the tank body 1, and the tank body 1 is clamped in the heating seat 11. A through hole 13 is provided at the bottom of the heating seat 11 to facilitate the passage of the discharge pipe 8. The bottom of the heating seat 11 is also fixedly provided with three anti-slip legs 14 in a circular array to ensure the stability of the device during the heating process. In addition, a temperature controller 12 is fixedly provided on the outer wall of the heating seat 11 for adjusting the heating temperature to meet the needs of different synthesis reactions.

[0037] Example 2

[0038] Improved on the basis of Example 1: A highly efficient synthesis reaction device of epoxiconazole, which aims to achieve highly efficient synthesis of epoxiconazole suspension agent through optimized structure and configuration, while improving production efficiency and product quality. It is used in the field of epoxiconazole suspension agent processing, please refer to Figure 1 and Figure 3In order to more accurately control the amount of raw material added, the feeding tube 5 is provided with a first solenoid valve 7 and a scale line 6 set based on the valve plate of the first solenoid valve 7. The operator can accurately measure and add the required amount of raw material by controlling the switch of the first solenoid valve 7 according to the indication of the scale line 6.

[0039] However, as is well known to those skilled in the art, the working principles and wiring methods of the drive motor 4, the first solenoid valve 7, the second solenoid valve 9 and the heating seat 11 are commonplace, and are conventional means or common knowledge, and will not be elaborated here. Those skilled in the art can make any optional selections according to their needs or convenience.

[0040] The above are only specific implementation methods of the present invention, but the protection scope of the present invention is not limited to this. Any technician familiar with the technical field can easily think of changes or substitutions within the technical scope disclosed by the present invention, which should be included in the protection scope of the present invention. In the absence of conflict, the embodiments of the present invention and the features in the embodiments can be combined with each other. Therefore, the protection scope of the present invention should be based on the protection scope of the claims.

Claims

1. A highly efficient synthesis reaction device for epoxiconazole, characterized in that: include: A tank body (1), wherein stirring rods (2) are rotatably mounted at both ends of the inner wall of the tank body (1), and a plurality of stirring blades (3) are fixedly mounted on the stirring rods (2); a driving motor (4) for driving the stirring rods (2) to rotate is fixedly mounted at the center of the top of the outer wall of the tank body (1); and a feeding pipe (5) and a discharging pipe (8) are respectively connected to the top and bottom of the tank body (1); A cleaning component is provided on the stirring rod (2) and is used to prevent residue from being deposited on the inner wall of the tank (1) and to facilitate the mixed solution to be pushed to the discharge pipe (8) for discharge; The heating component is arranged on the tank body (1) and is used to increase the internal temperature of the tank body (1), thereby accelerating the synthesis reaction.

2. A highly efficient synthesis reaction device of epoxiconazole according to claim 1, characterized in that: The cleaning assembly comprises a U-shaped scraper (10) fixedly arranged on the stirring rod (2), and the outer wall of the U-shaped scraper (10) is arranged to fit the inner wall of the tank body (1).

3. A highly efficient synthesis reaction device of epoxiconazole according to claim 1, characterized in that: The heating assembly comprises a heating seat (11) arranged outside the tank body (1), the tank body (1) being snap-fitted into the heating seat (11), three anti-slip legs (14) being fixedly arranged in a circular array at the bottom of the heating seat (11), and a through hole (13) for a discharge pipe (8) to pass through being provided at the bottom of the heating seat (11).

4. A highly efficient synthesis reaction device of epoxiconazole according to claim 3, characterized in that: A temperature controller (12) for adjusting the heating temperature is fixedly arranged on the outer wall of the heating seat (11).

5. A highly efficient synthesis reaction device of epoxiconazole according to claim 1, characterized in that: The feeding pipe (5) is provided with a first electromagnetic valve (7) and a scale line (6) arranged with the valve plate of the first electromagnetic valve (7) as a reference, so as to measure the amount of raw material added.

6. A highly efficient synthesis reaction device of epoxiconazole according to claim 1, characterized in that: The discharge pipe (8) is provided with a second solenoid valve (9) for conveniently controlling the discharge of material.

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