Relating to the technical field of
hydrogen energy application, the invention discloses a preparation method of a
nickel phosphide / foamed
nickel electrochemical functional
hydrogen evolution material.The method includes: pretreatment of a foamed
nickel current collector, preparation of a chemical nickel-
phosphorus plating solution, loading of a chemical nickel-
phosphorus plating
coating on the surface of a foamed nickel sheet, preparation of a nickel
hydroxide / foamed nickel precursor containing a nickel-
phosphorus coating, and preparation of a nickel
phosphide / foamed nickel self-supporting
electrode. The nickel
phosphide / foamed nickel self-supporting
electrode prepared by the method provided by the invention has excellent electrochemical catalytic
hydrogen evolution performance, efficientand stable properties, and wide application range, the required materials have wide sources, the preparation process is convenient, the requirement for the pH value condition is wide, the preparationprocess is green and
pollution-free, the technical implementation process is concise, easy to operate, and low in cost, and is easy for industrial popularization.