The invention relates to a
sodium vanadium fluorophosphate positive
electrode material, a preparation method and a
sodium ion battery, and belongs to the technical field of
sodium ion batteries. Mixing a
vanadium source, a sodium source, a
phosphate radical source, a
fluorine source and deionized water to obtain a
mixed solution; and adding a complexing precipitator into the
mixed solution at a
constant speed within 0.5-2 hours, then adding an anti-
solvent at a
constant speed within 10-90 minutes, and after the addition is finished, carrying out
solid-liquid separation, washing and
drying to obtain the sodium
vanadium fluorophosphate positive
electrode material. By optimizing the proportion and adding time of the complexing precipitant and the anti-
solvent,
nucleation and growth
kinetics in the synthesis process are continuously improved, and finally the high-
crystallinity vanadium sodium fluorophosphate material is successfully prepared under the conditions of
room temperature and normal pressure. The preparation method has the advantages that the high conversion rate of the product is guaranteed, the preparation
time efficiency is obviously improved, the
energy consumption is reduced, the production and preparation cost is greatly reduced, and the method is suitable for industrial production.