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A kind of extraction method of selenium cordyceps essence

An extraction method and selenium cordyceps technology are applied in the directions of pharmaceutical formulations, medical preparations containing active ingredients, plant raw materials, etc., to achieve the effects of optimizing extraction time, shortening extraction time, and sufficient extraction

Active Publication Date: 2017-08-04
湖北圣峰药业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Embodiment 1

[0031] A method for extracting selenium cordyceps essence, characterized in that, by the following extraction steps:

[0032] a. Drying treatment of Cordyceps selenium: drying the secondary Cordyceps selenium and its turf so that the water content is less than 6%;

[0033] b. Pulverization: Use a pulverizer to pulverize to 40-50 mesh, so as to increase the extraction surface area and extract more nutrients from Selenium Cordyceps;

[0034] c. Reflux extraction: add deionized water to make "glycine-HCl buffer solution" with pH = 3.2-4.5, assisted ultrasonic reflux extraction at 60°C for 90 minutes, centrifuged in a tubular centrifuge, and then used 30%-40% ethanol to assist ultrasonic 50 Reflux and extract at ℃ for 60 minutes, centrifuge; combine the two filtrates, concentrate under reduced pressure at 60℃ to 60%;

[0035]d. Spray drying: spray drying conditions are inlet temperature 136°C, outlet temperature 67°C, wind speed 44.18 rpm, electric spray head speed 4000 rpm, and ...

Embodiment 2

[0040] A method for extracting selenium cordyceps essence, characterized in that, by the following extraction steps:

[0041] a. Drying treatment of Selenium Cordyceps: Dry the secondary Selenium Cordyceps and its fungus turf at 60-80°C to make the

[0042] The amount of water is less than 6%;

[0043] b. Pulverization: use Shanghai Ruiyuan Machinery Equipment Co., Ltd., model RY-NSG-100L-C pulverizer to pulverize and sieve 3000g of selenium cordyceps powder to 50 mesh, and put it into an ultrasonic extraction tank;

[0044] c. Reflux extraction: Add 45 liters of glycine-HCl buffer solution 0.05mol / L with pH 4.2, ultrasonically extract at 20K for 90 minutes at 55°C, filter with a 100-mesh sieve, add 30L of 40% ethanol to the filter residue, and conduct 20K at 55°C Ultrasonic extraction for 60 minutes, filtered with a 100-mesh sieve, combined the above two filtrates, and concentrated with Shanghai Ruiyuan Machinery Equipment Co., Ltd., model RY-NSG-100L-C concentration tank, t...

Embodiment 3

[0048] A method for extracting selenium cordyceps essence, characterized in that, by the following extraction steps:

[0049] a. Drying treatment of Cordyceps selenium: drying the secondary Cordyceps selenium and its fungus turf at 70°C to make the water content less than 6%;

[0050] b. Pulverization: use a pulverizer to pulverize to 40 meshes, so as to increase the extraction surface area and extract more nutritional components of Selenium Cordyceps;

[0051] c. Reflux extraction: Add deionized water to make "glycine-HCl buffer solution" with pH = 3.2, assisted ultrasonic reflux extraction at 60°C for 90 minutes, centrifuged in a tubular centrifuge, and 30% ethanol assisted ultrasonic reflux extraction at 50°C for 60 minutes , centrifuged; the two filtrates were combined, concentrated under reduced pressure at 60°C to 60%;

[0052] d. Spray drying: spray drying conditions are inlet temperature 136°C, outlet temperature 67°C, wind speed 44.18 rpm, electric spray head speed 4...

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Abstract

The invention provides a method for extracting selenium cordyceps essence. The method is characterized by comprising the following extracting steps: (a) drying and processing selenium cordyceps; (b) crushing the dried and processed selenium cordyceps; (c) extracting the crushed selenium cordyceps in a regurgitation manner; (d) spray drying the selenium cordyceps which is extracted in the regurgitation manner; (e) vacuum packing the dried selenium cordyceps. According to the method for extracting the selenium cordyceps essence, a solvent auxiliary ultrasound two-step hot reflux extraction method is used, so that effective components in the selenium cordyceps are more sufficiently extracted, and the extraction rate of selenium reaches more than 90%; the solvent auxiliary ultrasound two-step hot reflux extraction method optimizes the extraction time, so that the extraction time is greatly shortened by more than 2 / 3 when compared with that of the traditional method; the extraction temperature is below 60 DEG C, so that the method has a protection effect on effective components in medicinal materials which are unstable when being heated and are easy to hydrolyze or oxidize, and the energy consumption is greatly reduced.

Description

technical field [0001] The invention relates to a method for extracting selenium cordyceps essence. Background technique [0002] Cordyceps contains cordycepin, cordycepic acid, polysaccharides, more than 10 kinds of amino acids and various trace elements. Modern medical and nutritional studies have shown that Cordyceps can regulate the immune system and blood system, protect and prevent kidney, liver, and heart damage, and have anti-aging, anti-stress, and anti-tumor effects. However, due to strict parasitism and special growth geographical environment restrictions, drug sources are in short supply and expensive, which is far from meeting the market demand. Selenium is an essential trace element for the human body. Modern medical research shows that selenium deficiency is related to the occurrence of more than 40 diseases such as Keshan disease, Kaschin-Beck disease, cardiovascular and cerebrovascular diseases, and cancer. Selenium supplementation can effectively reduce t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/068
CPCA61K36/068A61K2236/15A61K2236/331A61K2236/333A61K2236/51
Inventor 郭明南苏宏灿
Owner 湖北圣峰药业有限公司
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