Hydrogen sulfide gas generating device
By designing a hydrogen sulfide gas generator including hydrogen cylinders, sulfur tanks, heaters and collection tanks, the problems of hydrogen sulfide leakage and low purity in the prior art are solved, and the production of hydrogen sulfide gas without leakage and high purity is achieved.
Patent Information
- Application Number
- CN202420370967.8
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-02-28
- Publication Date
- 2025-03-11
- Estimated Expiration
- 2034-02-28
AI Technical Summary
In the prior art, it is difficult to achieve complete sealing of the hydrogen sulfide gas generator, resulting in leakage of hydrogen sulfide, and the prepared hydrogen sulfide gas often contains hydrogen chloride gas, and the purity is insufficient.
A hydrogen sulfide gas generator including a hydrogen cylinder, a sulfur tank, a heater and a collection tank is designed. The hydrogen sulfide gas is generated in the reactor by reacting hydrogen with the heated sulfur, and entering the collection tank through a second transfer tube.
The production of hydrogen sulfide gas is achieved without leakage. The prepared hydrogen sulfide gas is high in purity, few impurities, safe and environmentally friendly, and has industrial practical value.
Smart Images
Figure CN222586519U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of hydrogen sulfide gas generation, in particular to a hydrogen sulfide gas generation device. Background Art
[0002] The principle of hydrogen sulfide preparation commonly used in laboratories in the chemical industry is to generate hydrogen sulfide gas by reacting ferrous sulfide with hydrochloric acid at room temperature. However, this preparation method generally requires a Kipp generator made of glass, and the Kipp generator has many connection points and is difficult to be completely sealed. Therefore, a certain amount of hydrogen sulfide often leaks out during the generation of hydrogen sulfide. Since hydrogen sulfide is a highly toxic gas, the leaked hydrogen sulfide will not only have a huge impact on the surrounding environment, but also greatly damage the health of the experimental operators. At the same time, since hydrochloric acid is a volatile acid, a certain amount of hydrogen chloride gas is inevitably mixed into the hydrogen sulfide gas prepared by the method of reacting ferrous sulfide with hydrochloric acid, resulting in insufficient purity of the prepared hydrogen sulfide and a large impurity content. In summary, the disadvantages of the existing method for preparing hydrogen sulfide gas are: ① The experimental device is difficult to be completely sealed, resulting in hydrogen sulfide leakage, which affects the surrounding environment and the personal health of the experimenter; ② The prepared hydrogen sulfide gas often contains hydrogen chloride gas, which is not pure enough. Utility Model Content
[0003] The purpose of the utility model is to provide a hydrogen sulfide gas generating device to solve the problems raised in the above background technology.
[0004] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a hydrogen sulfide gas generating device, comprising a hydrogen cylinder, the hydrogen cylinder, a sulfur tank, a heater and a collecting tank, the top of the hydrogen cylinder is fixedly connected to one end of a first transmission pipe, the other end of the first transmission pipe is connected to the sulfur tank, a reactor is provided on the top of the sulfur tank, the heater is arranged on the right side of the sulfur tank, and the heating end of the heater is located inside the sulfur tank, a flow meter and a first valve are fixedly connected to the outer wall of the first transmission pipe, one end of a second transmission pipe is fixedly connected to the top of the reactor, the other end of the second transmission pipe is fixedly connected to the collecting tank, and a second valve is fixedly connected to the outer wall of the second transmission pipe.
[0005] Compared with the prior art, the utility model has the following beneficial effects: the hydrogen sulfide gas generating device heats the sulfur tank heater to a certain temperature, adjusts the temperature of the reactor to the temperature required for the reaction, opens the first valve of the hydrogen cylinder, introduces hydrogen into the sulfur tank, sulfur enters the reactor under the agitation of hydrogen to start the reaction, and the prepared hydrogen sulfide gas enters the collecting tank through the second transmission pipe. The utility model has a simple and reasonable structure, good sealing performance, no hydrogen sulfide gas leakage, safety and environmental protection, and the prepared hydrogen sulfide gas does not contain hydrogen chloride, has high purity, and has few impurities, and has strong industrial practical value. BRIEF DESCRIPTION OF THE DRAWINGS
[0006] Figure 1 This is an axonometric drawing of the main structure of the utility model.
[0007] In the figure: 1-hydrogen cylinder, 2-first transmission pipe, 3-first valve, 4-sulfur tank, 5-reactor, 6-heater, 7-second transmission pipe, 8-second valve, 9-collecting tank, 10-flow meter. DETAILED DESCRIPTION
[0008] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.
[0009] See also Figure 1 The utility model provides a hydrogen sulfide gas generating device, comprising a hydrogen cylinder 1, a hydrogen cylinder 1, a sulfur tank 4, a heater 6 and a collecting tank 9, one end of a first transmission pipe 2 is fixedly connected to the top of the hydrogen cylinder 1, the first transmission pipe 2 and the second transmission pipe 7 are used for gas transmission, the other end of the first transmission pipe 2 is connected to the sulfur tank 4, a reactor 5 is provided on the top of the sulfur tank 4, a heater 6 is provided on the right side of the sulfur tank 4, and the heating end of the heater 6 is located inside the sulfur tank 4, a flow meter 10 and a first valve 3 are fixedly connected to the outer wall of the first transmission pipe 2, one end of a second transmission pipe 7 is fixedly connected to the top of the reactor 5, the other end of the second transmission pipe 7 is fixedly connected to the collecting tank 9, and a second valve 8 is fixedly connected to the outer wall of the second transmission pipe 7, the function of the hydrogen cylinder 1 is to store a certain amount of hydrogen so as to react with sulfur to produce hydrogen sulfide; the function of the first valve 3 is to control the start and stop of hydrogen, and to control the start and stop of hydrogen in the production of hydrogen sulfide The first valve 3 is opened to allow hydrogen to flow out, and the first valve 3 is closed after the reaction is completed to prevent hydrogen leakage; the temperature in the reactor 5 is adjusted to a suitable temperature for the reaction of sulfur and hydrogen; the temperature of the sulfur tank 4 is controlled so that the sulfur is heated to facilitate the reaction; the function of the sulfur tank 4 is to store a certain amount of sulfur so that it can react with hydrogen to prepare hydrogen sulfide; the function of the heater 6 is to heat the sulfur to liquefy the solid sulfur and further gasify it to facilitate the reaction with hydrogen; the reactor 5 is equipped with a synthetic hydrogen sulfide catalyst, and its function is to enable sulfur and hydrogen to react at a specific temperature; the function of the second valve 8 is to control the opening and closing of the hydrogen sulfide gas branch, which is opened when testing the hydrogen sulfide concentration and kept closed when collecting hydrogen sulfide gas; the function of the collecting tank 9 is to store the prepared hydrogen sulfide for easy use; the function of the mass flowmeter 10 is to control the flow of hydrogen so that hydrogen and sulfur can react fully.
[0010] Working principle: first, a certain amount of sulfur is loaded into the sulfur tank 4, and then a certain amount of synthetic hydrogen sulfide catalyst is loaded into the reactor 5, the sulfur tank 4 is opened and heated to a certain temperature by the heater 6, and at the same time, the temperature of the reactor 5 is adjusted to the temperature required for the reaction, the first valve 3 of the hydrogen cylinder 1 is opened, and hydrogen is introduced into the sulfur tank 4. Sulfur enters the reactor 5 under the agitation of hydrogen to start the reaction, and the prepared hydrogen sulfide gas enters the collection tank 9 through the second transmission pipe 7.
[0011] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.
Claims
1. A hydrogen sulfide gas generating device, characterized in that: The invention comprises a hydrogen cylinder (1), the hydrogen cylinder (1), a sulfur tank (4), a heater (6) and a collecting tank (9), wherein one end of a first transmission pipe (2) is fixedly connected to the top of the hydrogen cylinder (1), the other end of the first transmission pipe (2) is connected to the sulfur tank (4), a reaction kettle (5) is provided on the top of the sulfur tank (4), the heater (6) is arranged on the right side of the sulfur tank (4), and the heating end of the heater (6) is located inside the sulfur tank (4), a flow meter (10) and a first valve (3) are fixedly connected to the outer wall of the first transmission pipe (2), one end of a second transmission pipe (7) is fixedly connected to the top of the reaction kettle (5), the other end of the second transmission pipe (7) is fixedly connected to the collecting tank (9), and a second valve (8) is fixedly connected to the outer wall of the second transmission pipe (7).